CN114344157A - Effective component extraction method based on water decoction method - Google Patents
Effective component extraction method based on water decoction method Download PDFInfo
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- CN114344157A CN114344157A CN202210029810.4A CN202210029810A CN114344157A CN 114344157 A CN114344157 A CN 114344157A CN 202210029810 A CN202210029810 A CN 202210029810A CN 114344157 A CN114344157 A CN 114344157A
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- ring
- splicing
- reaction kettle
- liquid medicine
- medicinal materials
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61J—CONTAINERS SPECIALLY ADAPTED FOR MEDICAL OR PHARMACEUTICAL PURPOSES; DEVICES OR METHODS SPECIALLY ADAPTED FOR BRINGING PHARMACEUTICAL PRODUCTS INTO PARTICULAR PHYSICAL OR ADMINISTERING FORMS; DEVICES FOR ADMINISTERING FOOD OR MEDICINES ORALLY; BABY COMFORTERS; DEVICES FOR RECEIVING SPITTLE
- A61J3/00—Devices or methods specially adapted for bringing pharmaceutical products into particular physical or administering forms
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0269—Solid material in other moving receptacles
- B01D11/0273—Solid material in other moving receptacles in rotating drums
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/028—Flow sheets
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/028—Flow sheets
- B01D11/0284—Multistage extraction
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0292—Treatment of the solvent
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D33/00—Filters with filtering elements which move during the filtering operation
- B01D33/06—Filters with filtering elements which move during the filtering operation with rotary cylindrical filtering surfaces, e.g. hollow drums
- B01D33/11—Filters with filtering elements which move during the filtering operation with rotary cylindrical filtering surfaces, e.g. hollow drums arranged for outward flow filtration
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D33/00—Filters with filtering elements which move during the filtering operation
- B01D33/80—Accessories
- B01D33/801—Driving means, shaft packing systems or the like
Abstract
The invention discloses an effective component extraction method based on a water decoction method, which comprises the following steps of S1: after selecting suitable medicinal materials, cut into suitable size through cutting device with the medicinal material to collect the medicinal material that will cut well and concentrate together, S2, wash and soak: the medical material that cuts is washed fast to the medicinal material after will washing is mixed and is deposited in soaking the bucket, in order that subsequent medicinal material active ingredient decocte, the invention forms an independent cavity through keeping apart intranet, keeping apart extranet and concatenation orifice plate in the reation kettle main part, thereby make the medicinal material be restricted in a less scope all the time in the decocte in-process in the reation kettle main part, avoided the impurity that the medicinal material outside dropped and the tiny tissue that drops to enter into the liquid medicine, and then improved the purity of liquid medicine, impurity in the reduction liquid medicine, the effectual processing pressure who reduces the subsequent filtration equipment of liquid medicine.
Description
Technical Field
The invention relates to the technical field of extraction of active ingredients of medicinal materials, in particular to an active ingredient extraction method based on a water decoction method.
Background
The reaction kettle is widely understood as a container with physical or chemical reaction, realizes the heating, evaporation, cooling and low-speed mixing functions of process requirements through the structural design and parameter configuration of the container, is widely applied to the fields of petroleum, chemical engineering, rubber, pesticides, dyes, medicines, food and the like, is a pressure container for completing the technological processes of vulcanization, nitration, hydrogenation, polymerization, condensation and the like, and generally consists of a kettle body, a kettle cover, a jacket, a stirrer, a transmission device, a shaft seal device, a support and the like;
but the impurity that its outside absorption drops and the tiny tissue separation of medicinal material skin enters into the liquid medicine in the medicinal material decocting process at present, leads to the inside solid impurity content of liquid medicine to rise, increases filtration equipment's processing burden, simultaneously because the medicinal material inner structure is inseparable, so lead to effective component in the medicinal material to separate out efficiency slowly, for effectively extracting the effective component in the medicinal material, need carry out a lot of decocte to the dregs of a decoction to the extraction cost of medicinal material effective component has been increased.
Disclosure of Invention
The invention provides an effective component extraction method based on a water decoction method, which can effectively solve the problems that in the decocting process of medicinal materials, impurities adsorbed outside the medicinal materials fall off and fine tissues on the outer layers of the medicinal materials are separated and enter the medicinal liquid, so that the content of solid impurities in the medicinal liquid rises, and the processing burden of filtering equipment is increased.
In order to achieve the purpose, the invention provides the following technical scheme: a method for extracting effective components based on a water decoction method comprises the following steps:
s1, cutting medicinal materials: after selecting proper medicinal materials, cutting the medicinal materials into proper sizes through a cutting device, and collecting and gathering the cut medicinal materials together;
s2, cleaning and soaking: quickly cleaning the cut medicinal materials, mixing the cleaned medicinal materials and storing the mixture in a soaking barrel for subsequent decoction of the effective components of the medicinal materials;
s3, decocting the medicinal materials: the medicinal materials and water are added into the reaction kettle main body through the soaking barrel, and the effective components in the medicinal materials are quickly and efficiently extracted through the matching of all components in the reaction kettle main body;
s4, separating liquid medicine: after the extraction of the active ingredients in the medicinal materials in the reaction kettle main body is finished, opening a liquid medicine discharge pipe, and driving all components in the reaction kettle main body to rotate in a reciprocating manner by rotating a motor so as to quickly separate liquid medicine and medicine residues in the reaction kettle main body;
s5, filtering the liquid medicine: collect the inside exhaust liquid medicine of reation kettle main part through collection device to filter the purification to the liquid medicine through filter equipment, and collect the back liquid medicine that filters, in order to accomplish the extraction of medicinal material active ingredient.
Preferably, the middle part of the outer side surface of the reaction kettle main body is uniformly welded with mounting side lugs at equal intervals along the circumferential direction, the middle parts of two mounting side lugs positioned at two sides of the reaction kettle main body are fixedly provided with electric telescopic links, the input end of each electric telescopic link is electrically connected with the output end of an external power supply, the middle part of the top end of each electric telescopic link is fixedly connected with a connecting circular plate, and the top end of each connecting circular plate is fixedly connected with a connecting transverse plate;
a sealing cover plate is fixedly connected between the two connecting transverse plates corresponding to the opening at the top end of the reaction kettle main body, and a mounting seat, a rotating motor, a connecting disc, a transmission rotating shaft, a connecting chuck, a connecting upper disc, a contact backing ring and a connecting conical block are arranged on the outer side of the sealing cover plate;
the middle part of the bottom end of the inner side of the reaction kettle main body is fixedly provided with an installation lower column, and the outer side of the installation lower column is provided with a limiting annular plate, a buffer backing ring, a guide lower tube, a rotary upper column, a guide upper tube, a connecting rotary block, a positioning conical groove, a rotary concave ring and a rotary convex ring;
a clamping round cover is placed at the top end of the connecting rotating block, and a splicing round groove, an upper connecting column, a connecting conical groove, a positioning conical block, a splicing inner curved ring, a clamping upper ring, a splicing lower ring, a clamping lower ring, a guiding rectangular groove and an isolating inner net are arranged on the outer side of the clamping round cover;
the top of fitting with a contraceptive ring of centre gripping has the concatenation lantern ring through bolted connection, concatenation lantern ring bottom limit portion has fixed fitting with a contraceptive ring through bolted connection, fixed fitting with a contraceptive ring bottom is provided with the outer looper of concatenation, concatenation outer ring, fixed lower ring and keeps apart the outer net.
Preferably, the middle part of the top of the sealing cover plate is connected with a mounting seat, the middle part of the top of the mounting seat is fixedly provided with a rotating motor, the input end of the rotating motor is electrically connected with the output end of an external power supply, the bottom end of an output shaft of the rotating motor corresponds to the fixedly connected with connecting disc at the inner side position of the mounting seat, the middle part of the bottom end of the connecting disc is fixedly connected with a transmission rotating shaft, the bottom end of the transmission rotating shaft is provided with a connecting upper disc through a connecting chuck, the bottom end edge part of the connecting upper disc is bonded with a contact pad ring, and the middle part of the bottom end of the connecting upper disc corresponds to the inner side position of the contact pad ring and is fixedly provided with a connecting conical block.
Preferably, the transmission rotating shaft penetrates through the middle of the sealing cover plate and is in rotating connection with the sealing cover plate, and the bottom of the sealing cover plate is matched with the top of the reaction kettle main body.
Preferably, the bottom end of the outer side of the lower mounting column is fixedly sleeved with a limiting annular plate, the edge part of the top end of the limiting annular plate is bonded with a cushion ring, and the position, corresponding to the top part of the limiting annular plate, of the outer side of the lower mounting column is fixedly sleeved with a lower guide tube;
the middle part of the top end of the lower mounting column is rotatably connected with an upper rotating column through a rotating disc, and a guide upper tube is fixedly sleeved on the outer side of the upper rotating column;
rotate upper column top position department and be provided with the connection commentaries on classics piece, connect commentaries on classics piece top limit portion and evenly seted up four location taper grooves along the circumferencial direction equidistance, rotate upper column top middle part and install through the bolt and rotate the concave ring, connect commentaries on classics piece bottom middle part and install through the bolt and rotate the bulge loop, and rotate between concave ring and the rotation bulge loop for sliding connection.
Preferably, the direction lower tube limit portion circumferencial direction evenly is provided with the direction draw runner, direction upper tube limit portion circumferencial direction evenly is provided with the direction draw runner, rotate and agree with each other between concave ring and the rotation bulge loop, the frictional force between installation lower prop and the rotation upper prop is greater than the frictional force between rotation concave ring and the rotation bulge loop.
Preferably, the middle part of the bottom end of the clamping circular cover is provided with a splicing circular groove, the middle part of the top end of the clamping circular cover is fixedly connected with an upper column, the middle part of the top end of the upper column is provided with a connecting conical groove, and the top surface of the inner side of the splicing circular groove is uniformly and fixedly connected with four positioning conical blocks in the circumferential direction;
the joint dome outside bottom has a concatenation inner loop through bolt fixed mounting, the concatenation inner loop top is fitted with a contraceptive ring through bolt fixedly connected with centre gripping, the corresponding cushion collar top position department in the direction low tube outside is provided with the concatenation lower ring, there is the centre gripping lower ring at concatenation lower ring top through bolted connection, the inboard circumferencial direction of concatenation lower ring has evenly seted up the direction rectangular channel, keep apart intranet top centre gripping in the concatenation between the inner loop of curved ring and the centre gripping upper ring, keep apart intranet bottom centre gripping between concatenation lower ring and centre gripping lower ring.
Preferably, the sectional dimension of the splicing circular groove is the same as the dimension of the top surface of the connecting rotating block, the connecting conical groove corresponds to the connecting conical block in position, the connecting conical block is matched with the connecting conical groove, the positioning conical block corresponds to the positioning conical groove in position, and the positioning conical block is matched with the positioning conical groove;
the direction rectangular channel corresponds each other between the direction draw runner in direction low tube and the direction top tube outside, and is sliding connection between direction rectangular channel inner wall and the direction draw runner outside, closely slide the laminating between the inboard arcwall face of direction rectangular channel and the cambered surface of direction draw runner one side, the width in direction rectangular channel is greater than the width of direction draw runner.
Preferably, the bottom end of the fixed upper ring is connected with a spliced outer curved ring through a bolt, the bottom of the inner side of the reaction kettle main body is provided with a spliced outer ring at the same height corresponding to the outer side of the spliced lower ring, the top end of the spliced outer ring is connected with the fixed lower ring through a bolt, the top end of the isolation outer net is clamped between the fixed upper ring and the spliced outer curved ring, and the bottom end of the isolation outer net is clamped between the spliced outer ring and the fixed lower ring;
reinforcing cables are uniformly and fixedly connected between the splicing inner bent ring and the clamping lower ring as well as between the splicing outer bent ring and the fixed lower ring, extrusion balls are uniformly and fixedly connected to the outer sides of the reinforcing cables at equal intervals, and a splicing pore plate is fixedly connected between the splicing lower ring and the splicing outer ring;
the device comprises a reaction kettle body and is characterized in that a liquid medicine discharge pipe is fixedly installed on one side of the bottom of the reaction kettle body, a cleaning discharge pipe is fixedly connected to the other side of the bottom of the reaction kettle body, and the liquid medicine discharge pipe and the cleaning discharge pipe are both sealed through a sealing valve.
Preferably, the concatenation lantern ring comprises inner ring and outer loop jointly, and passes through spliced pole interconnect between inner ring and the outer loop, the concatenation orifice plate top surface flushes each other with the concatenation between lower ring of concatenation and the concatenation outer loop top surface.
Compared with the prior art, the invention has the beneficial effects that: the invention has scientific and reasonable structure and safe and convenient use:
1. through keeping apart the intranet, keeping apart outer net and concatenation orifice plate at the inside independent cavity that forms of reation kettle main part to make the medicinal material be restricted at a less within range all the time at the inside decocte in-process of reation kettle main part, avoided the impurity that the medicinal material outside dropped and the tiny tissue that drops to enter into the liquid medicine, and then improved the purity of liquid medicine, reduce the impurity in the liquid medicine, the effectual subsequent filtration equipment's of liquid medicine treatment pressure that has reduced.
2. Utilize the rotation in turn of rotating the motor, carry out periodic cycle extrusion through strengthening cable and extrusion ball to keeping apart the intranet and keeping apart the inside medicinal material of outer net, and then accelerate the inside liquid exchange of medicinal material, make the inside active ingredient of medicinal material can be quick appear in the exchange process of liquid, the inner structure becomes loose under strengthening cable and extrusion ball's the repeated extrusion of medicinal material simultaneously, has further accelerated the discharge efficiency of active ingredient in the medicinal material.
3. In the discharge process of liquid medicine, drive the medicinal material through keeping apart the intranet and keeping apart the outer net and carry out synchronous rotation, make the medicinal material discharge fast under the effect of centrifugal force to after the liquid medicine is whole to be discharged, through keeping apart the intranet and keeping apart the outer net with the dregs of a decoction from the inside taking out of reation kettle main part, thereby the effectual clean convenience that has improved the reation kettle main part.
4. Through mutually supporting between each subassembly, the effectual efficiency that has improved the medicinal material active ingredient and draw, simultaneously through concentrating on reation kettle with the medicinal material active ingredient extraction process, and then reduced the work burden of other relevant equipment of extraction in-process, thereby the ageing speed of enterprise's equipment has been reduced, simultaneously through the extrusion in turn to the medicinal material make the medicinal material through once decocte alright with draw, and then shortened single batch medicinal material active ingredient and draw the expense, thereby the energy consumption of enterprise has been reduced indirectly, the economic benefits of enterprise has been improved.
Drawings
The accompanying drawings, which are included to provide a further understanding of the invention and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention and together with the description serve to explain the principles of the invention and not to limit the invention.
In the drawings:
FIG. 1 is a flow chart of the steps of the present invention;
FIG. 2 is a schematic view of the overall structure of the present invention;
FIG. 3 is a schematic view of the structure inside the main body of the reaction vessel of the present invention;
FIG. 4 is a schematic view of the structure of the cleaning drain pipe installation of the present invention;
FIG. 5 is a schematic structural view of the installation of the connecting cone block of the present invention;
FIG. 6 is a schematic view of the guide down tube mounting configuration of the present invention;
FIG. 7 is a schematic view of the installation structure of the stop collar plate of the present invention;
FIG. 8 is a schematic view of the construction of the present invention for the installation of a spliced orifice plate;
FIG. 9 is a schematic view of the configuration of the rotating female ring mount of the present invention;
FIG. 10 is a schematic view of the construction of the squeeze bulb mounting of the present invention;
FIG. 11 is a schematic view of the construction of the isolated outer net installation of the present invention;
reference numbers in the figures: 1. a reaction kettle main body; 2. mounting a side lug; 3. an electric telescopic rod; 4. connecting the circular plate; 5. connecting the transverse plates;
6. sealing the cover plate; 601. a mounting seat; 602. rotating the motor; 603. a connecting disc; 604. a transmission rotating shaft; 605. connecting the chuck; 606. connecting the upper disc; 607. a contact backing ring; 608. connecting the conical blocks;
7. installing a lower column; 701. a limiting annular plate; 702. a cushion ring; 703. guiding the lower pipe; 704. rotating the upper column; 705. guiding the upper pipe; 706. connecting the rotary block; 707. positioning the conical groove; 708. rotating the concave ring; 709. rotating the convex ring;
8. clamping the round cover; 801. splicing the circular grooves; 802. connecting the upper column; 803. connecting the conical grooves; 804. positioning a conical block; 805. splicing the inner curved ring; 806. clamping the upper ring; 807. splicing a lower ring; 808. clamping the lower ring; 809. a guide rectangular groove; 810. isolating the inner net; 9. splicing lantern rings;
10. fixing the upper ring; 1001. splicing the outer curved ring; 1002. splicing the outer ring; 1003. fixing the lower ring; 1004. isolating the outer net;
11. a reinforcing cable; 12. extruding the ball; 13. splicing the pore plates; 14. a liquid medicine discharge pipe; 15. and cleaning the discharge pipe.
Detailed Description
The preferred embodiments of the present invention will be described in conjunction with the accompanying drawings, and it will be understood that they are described herein for the purpose of illustration and explanation and not limitation.
Example (b): as shown in fig. 1 to 11, the present invention provides a technical solution, a method for extracting active ingredients based on a water decoction method, comprising the steps of:
s1, cutting medicinal materials: after selecting proper medicinal materials, cutting the medicinal materials into proper sizes through a cutting device, and collecting and gathering the cut medicinal materials together;
s2, cleaning and soaking: quickly cleaning the cut medicinal materials, mixing the cleaned medicinal materials and storing the mixture in a soaking barrel for subsequent decoction of the effective components of the medicinal materials;
s3, decocting the medicinal materials: the medicinal materials and water are added into the reaction kettle main body 1 through the soaking barrel, and the effective components in the medicinal materials are quickly and efficiently extracted through the matching of all components in the reaction kettle main body 1;
s4, separating liquid medicine: after the extraction of the active ingredients in the medicinal materials in the reaction kettle main body 1 is completed, the liquid medicine discharge pipe 14 is opened, and the rotating motor 602 drives each component in the reaction kettle main body 1 to rotate in a reciprocating manner, so that the liquid medicine and the medicine residues in the reaction kettle main body 1 are quickly separated;
s5, filtering the liquid medicine: collecting the liquid medicine discharged from the interior of the reaction kettle main body 1 through a collecting device, filtering and purifying the liquid medicine through a filtering device, and collecting the filtered liquid medicine to finish extracting the active ingredients of the medicinal materials;
the middle part of the outer side surface of the reaction kettle main body 1 is uniformly welded with mounting side lugs 2 at equal intervals along the circumferential direction, the middle parts of two mounting side lugs 2 positioned at two sides of the reaction kettle main body 1 are fixedly provided with electric telescopic rods 3, the input end of each electric telescopic rod 3 is electrically connected with the output end of an external power supply, the middle part of the top end of each electric telescopic rod 3 is fixedly connected with a connecting circular plate 4, and the top end of each connecting circular plate 4 is fixedly connected with a connecting transverse plate 5;
a sealing cover plate 6 is fixedly connected between the two connecting transverse plates 5 corresponding to the opening at the top end of the reaction kettle main body 1, the top of the reaction kettle main body 1 is sealed through the sealing cover plate 6, and a mounting seat 601, a rotating motor 602, a connecting disc 603, a transmission rotating shaft 604, a connecting chuck 605, a connecting upper disc 606, a contact backing ring 607 and a connecting conical block 608 are arranged on the outer side of the sealing cover plate 6;
the middle part of the bottom end of the inner side of the reaction kettle main body 1 is fixedly provided with a lower mounting column 7, and the outer side of the lower mounting column 7 is provided with a limiting annular plate 701, a cushion ring 702, a lower guide pipe 703, an upper rotating column 704, an upper guide pipe 705, a connecting rotating block 706, a positioning conical groove 707, a concave rotating ring 708 and a convex rotating ring 709;
a clamping round cover 8 is arranged at the top end of the connecting rotary block 706, and a splicing round groove 801, an upper connecting column 802, a connecting cone groove 803, a positioning cone block 804, a splicing inner curved ring 805, an upper clamping ring 806, a lower splicing ring 807, a lower clamping ring 808, a rectangular guide groove 809 and an internal isolation net 810 are arranged on the outer side of the clamping round cover 8;
the top end of the clamping upper ring 806 is connected with a splicing lantern ring 9 through a bolt, the edge part of the bottom of the splicing lantern ring 9 is connected with a fixed upper ring 10 through a bolt, and the bottom of the fixed upper ring 10 is provided with a splicing outer bent ring 1001, a splicing outer ring 1002, a fixed lower ring 1003 and an isolation outer net 1004;
the middle part of the top end of the sealing cover plate 6 is connected with a mounting seat 601, the middle part of the top end of the mounting seat 601 is fixedly provided with a rotating motor 602, the input end of the rotating motor 602 is electrically connected with the output end of an external power supply, the bottom end of the output shaft of the rotating motor 602 is fixedly connected with a connecting disc 603 corresponding to the inner side position of the mounting seat 601, the middle part of the bottom end of the connecting disc 603 is fixedly connected with a transmission rotating shaft 604, the bottom end of the transmission rotating shaft 604 is provided with a connecting upper disc 606 through a connecting chuck 605, the edge part of the bottom end of the connecting upper disc 606 is adhered with a contact backing ring 607, the contact backing ring 607 provides buffer memory in the contact process of the connecting upper disc 606 and an upper column 802 to prevent the connecting upper disc 606 and the upper column 802 from being damaged in the collision process, the middle part of the bottom end of the connecting upper disc 606 is fixedly provided with a connecting conical block 608 corresponding to the inner side position of the contact backing ring 607, the transmission rotating shaft 604 penetrates through the middle part of the sealing cover plate 6 and is rotatably connected with the sealing cover plate 6, the bottom of the sealing cover plate 6 is matched with the top of the reaction kettle main body 1;
the bottom end of the outer side of the lower mounting column 7 is fixedly sleeved with a limiting ring-shaped plate 701, the edge part of the top end of the limiting ring-shaped plate 701 is bonded with a cushion ring 702, and the position, corresponding to the top part of the limiting ring-shaped plate 701, of the outer side of the lower mounting column 7 is fixedly sleeved with a lower guide pipe 703;
the middle part of the top end of the lower column 7 is rotatably connected with a rotating upper column 704 through a rotating disc, and the outer side of the rotating upper column 704 is fixedly sleeved with a guide upper tube 705;
a connecting rotating block 706 is arranged at the top end of the upper rotating column 704, four positioning conical grooves 707 are uniformly arranged at the top end of the connecting rotating block 706 at equal intervals along the circumferential direction, a rotating concave ring 708 is arranged in the middle of the top of the upper rotating column 704 through a bolt, a rotating convex ring 709 is arranged in the middle of the bottom end of the connecting rotating block 706 through a bolt, the rotating concave ring 708 and the rotating convex ring 709 are in sliding connection, guide sliding strips are uniformly arranged in the circumferential direction of the edge of the lower guide pipe 703, guide sliding strips are uniformly arranged in the circumferential direction of the edge of the upper guide pipe 705, the rotating concave ring 708 and the rotating convex ring 709 are mutually matched, the friction force between the lower mounting column 7 and the upper rotating column 704 is larger than the friction force between the rotating concave ring 708 and the rotating convex ring 709, and the rotating concave ring 708 and the rotating convex ring 709 can rotate in preference to the mounting between the lower column 7 and the upper rotating column 704 through the difference of resistance;
the middle of the bottom end of the clamping circular cover 8 is provided with a splicing circular groove 801, the middle of the top end of the clamping circular cover 8 is fixedly connected with an upper column 802, the middle of the top end of the upper column 802 is provided with a connecting conical groove 803, and the top surface of the inner side of the splicing circular groove 801 is uniformly and fixedly connected with four positioning conical blocks 804 along the circumferential direction;
the bottom of the outer side of the clamping circular cover 8 is fixedly provided with a splicing inner curved ring 805 through bolts, the top end of the splicing inner curved ring 805 is fixedly connected with a clamping upper ring 806 through bolts, the outer side of the guide lower pipe 703 is provided with a splicing lower ring 807 at the position corresponding to the top of the buffer backing ring 702, the top of the splicing lower ring 807 is connected with a clamping lower ring 808 through bolts, the inner side of the splicing lower ring 807 is uniformly provided with a guide rectangular groove 809 along the circumferential direction, the top end of an isolation inner net 810 is clamped between the splicing inner curved ring 805 and the clamping upper ring 806, the bottom end of the isolation inner net 810 is clamped between the splicing lower ring 807 and the clamping lower ring 808, the cross-sectional dimension of the splicing circular groove 801 is the same as the top dimension of the connecting rotating block 706, the connecting conical groove 803 and the connecting conical block 608 correspond to each other in position, and the connecting conical block 608 and the connecting conical block are mutually engaged, so that the rotation of the transmission rotating shaft 604 is downwards transmitted to the clamping circular cover 8 through the connecting conical groove 803 and the connecting conical block 608, the positioning conical block 804 corresponds to the positioning conical groove 707 in position, and the positioning conical block 804 fits with the positioning conical groove 707, so that the rotation of the clamping dome 8 is transmitted downwards to the connecting rotary block 706 through the positioning conical block 804 and the positioning conical groove 707;
the guide rectangular groove 809 corresponds to the guide sliding strips on the outer sides of the lower guide pipe 703 and the upper guide pipe 705, the inner wall of the guide rectangular groove 809 is in sliding connection with the outer sides of the guide sliding strips, so that the splicing lower ring 807 is ensured to slide upwards preferentially along the axial direction of the lower mounting column 7 after receiving external force, the arc-shaped surface on the inner side of the guide rectangular groove 809 is in close sliding fit with the arc-shaped surface on one side of the guide sliding strips, and the width of the guide rectangular groove 809 is greater than that of the guide sliding strips;
the bottom end of the fixed upper ring 10 is connected with a splicing outer bent ring 1001 through a bolt, the bottom of the inner side of the reaction kettle main body 1 is provided with a splicing outer ring 1002 at the same height corresponding to the outer side of the splicing lower ring 807, the top end of the splicing outer ring 1002 is connected with a fixed lower ring 1003 through a bolt, the top end of the isolation outer net 1004 is clamped between the fixed upper ring 10 and the splicing outer bent ring 1001, and the bottom end of the isolation outer net 1004 is clamped between the splicing outer ring 1002 and the fixed lower ring 1003;
reinforcing cables 11 are uniformly and fixedly connected between the splicing inner curved ring 805 and the clamping lower ring 808 and between the splicing outer curved ring 1001 and the fixed lower ring 1003, extrusion balls 12 are uniformly and fixedly connected to the outer sides of the reinforcing cables 11 at equal intervals, and a splicing pore plate 13 is fixedly connected between the splicing lower ring 807 and the splicing outer ring 1002;
a liquid medicine discharge pipe 14 is fixedly installed on one side of the bottom of the reaction kettle body 1, a cleaning discharge pipe 15 is fixedly connected to the other side of the bottom of the reaction kettle body 1, the liquid medicine discharge pipe 14 and the cleaning discharge pipe 15 are both sealed through a sealing valve, the splicing sleeve ring 9 is composed of an inner ring and an outer ring together, the inner ring and the outer ring are connected with each other through a connecting column, and the top surface of the splicing pore plate 13 and the top surfaces of the splicing lower ring 807 and the splicing outer ring 1002 are flush with each other.
The working principle and the using process of the invention are as follows: in the practical application process of the invention, in the process of adding the soaked medicinal materials and water into the reaction kettle main body 1, the extension of the electric telescopic rod 3 drives the connecting circular plate 4 and the connecting transverse plate 5 to synchronously move upwards, and further drives the sealing cover plate 6 to move upwards synchronously through the connecting transverse plate 5, and drives the mounting seat 601, the rotating motor 602, the connecting disc 603, the transmission rotating shaft 604, the connecting chuck 605, the connecting upper disc 606, the contact backing ring 607 and the connecting cone block 608 to move upwards synchronously through the movement of the sealing cover plate 6, so that the top of the reaction kettle main body 1 is opened normally, then the medicinal materials in the container for soaking the medicinal materials and water are added together between the inner isolation net 810 and the outer isolation net 1004 in the reaction kettle main body 1, and water is added into the reaction kettle main body 1 through a water pipe, so that the water in the reaction kettle main body 1 reaches the target water level, and the addition of the raw materials in the decoction process of the medicinal materials is completed.
After the raw material addition in the reaction kettle main body 1 is completed, the sealing cover plate 6 is driven to move downwards and seal the top of the reaction kettle main body 1 by the contraction of the electric telescopic rod 3, the connecting cone block 608 is embedded into the connecting cone groove 803 while the sealing cover plate 6 and the top of the reaction kettle main body 1 are closed, water and medicinal materials in the reaction kettle main body 1 are heated, after the reaction kettle main body 1 is heated for a period of time, the rotating motor 602 is started, the connecting disc 603, the transmission rotating shaft 604, the connecting chuck 605, the connecting upper disc 606 and the connecting cone block 608 are driven to synchronously rotate by the rotating motor 602, the clamping circular cover 8 and the connecting cone 802 are driven to synchronously rotate by the mutual matching between the connecting cone block 608 and the connecting cone groove 803, and the clamping circular cover 8 rotates by the mutual matching between the positioning cone block 804 and the positioning cone groove 707, the connecting rotating block 706 is driven to rotate synchronously.
In the rotation process of the clamping round cover 8 and the connecting rotation block 706, the splicing inner curved ring 805, the clamping upper ring 806, the fixed upper ring 10, the splicing outer curved ring 1001, the isolating inner net 810, the top of the isolating outer net 1004 and the top of the reinforcing cable 11 are driven to rotate by the splicing lantern ring 9, in the rotation process of the isolating inner net 810, the top of the isolating outer net 1004 and the top of the reinforcing cable 11, because the common limit of the splicing lower ring 807, the clamping lower ring 808, the splicing outer ring 1002 and the fixed lower ring 1003 are received by the top of the isolating inner net 810, the isolating outer net 1004 and the bottom of the reinforcing cable 11 and cannot synchronously rotate, the top of the isolating outer net 1002 and the bottom of the reinforcing cable 11 are gradually spirally wound on the outer side of the mounting lower column 7, and the splicing lower ring 807, the clamping lower ring 808 and the splicing outer ring 1002 are driven to gradually wind along with the top of the isolating inner net 810, the isolating outer net 1004 and the reinforcing cable 11 and the top of the isolating outer net 1002 and the reinforcing cable 11, The fixed lower ring 1003 and the splicing pore plate 13 move upwards along the axial direction of the lower installation column 7, and after the splicing lower ring 807 slides to the outer side of the upper guide pipe 705, the upper guide pipe 705 is driven by the splicing lower ring 807 to synchronously rotate together with the connecting rotating block 706 and the clamping circular cover 8.
In the process of continuously winding the isolation inner net 810, the isolation outer net 1004 and the reinforcing cable 11, the space inside the isolation inner net 810 and the isolation outer net 1004 is contracted, the medicinal materials between the isolation inner net 810 and the isolation outer net 1004 are extruded through the reinforcing cable 11 and the extrusion balls 12, water absorbed in the medicinal materials and the effective components inside the medicinal materials are extruded together, so that the separation of the effective components in the medicinal materials is accelerated, the medicinal materials are isolated through the isolation inner net 810 and the isolation outer net 1004, the medicinal materials, the impurities falling on the medicinal materials and the falling fine tissues are limited in a cavity formed by the isolation inner net 810, the isolation outer net 1004 and the splicing pore plate 13, the reinforcing cable 11 and the extrusion balls 12 can repeatedly extrude the medicinal materials through the periodic forward and reverse rotation of the rotating motor 602, the structure inside the medicinal materials gradually becomes loose through the periodic extrusion of the medicinal materials for a plurality of times, further, the effective components in the medicinal materials can be separated out more quickly.
After a certain time of decoction, the effective components in the medicinal materials are fully separated out by water in the reaction kettle main body 1, the liquid medicine in the reaction kettle main body 1 is discharged by opening the liquid medicine discharge pipe 14 and is stored in a collection container transported by a pipeline for subsequent continuous processing, in the liquid discharging process, the splicing lower ring 807, the clamping lower ring 808, the splicing outer ring 1002, the fixed lower ring 1003, the isolation inner net 810 and the isolation outer net 1004 which are lifted to the outer side of the guide upper pipe 705 are driven by a motor to synchronously rotate, so that the residual liquid in the medicinal materials is thrown out under the action of centrifugal force, after the liquid medicine is completely discharged, the rotating motor 602 is closed, the electric telescopic rod 3 is extended to drive the sealing cover plate 6 to be separated from the top of the reaction kettle main body 1, the top of the reaction kettle main body 1 is opened, and then an operator carries the isolation inner net 810, the isolation outer net 1004 and all components connected with the isolation outer net 1004 out of the reaction kettle main body 1 together, so that the residual medicine dregs after decoction are taken away from the interior of the reaction kettle main body 1 together, thereby completing the whole extraction process of the effective components of the medicinal materials.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (10)
1. An effective component extraction method based on a water decoction method is characterized by comprising the following steps:
s1, cutting medicinal materials: after selecting proper medicinal materials, cutting the medicinal materials into proper sizes through a cutting device, and collecting and gathering the cut medicinal materials together;
s2, cleaning and soaking: quickly cleaning the cut medicinal materials, mixing the cleaned medicinal materials and storing the mixture in a soaking barrel for subsequent decoction of the effective components of the medicinal materials;
s3, decocting the medicinal materials: the medicinal materials and water are added into the reaction kettle main body (1) through the soaking barrel, and the effective components in the medicinal materials are quickly and efficiently extracted through the matching of all components in the reaction kettle main body (1);
s4, separating liquid medicine: after the extraction of the active ingredients in the medicinal materials in the reaction kettle main body (1) is finished, the liquid medicine discharge pipe (14) is opened, and then the rotating motor (602) drives each component in the reaction kettle main body (1) to rotate in a reciprocating manner, so that the liquid medicine and the medicine residues in the reaction kettle main body (1) are quickly separated;
s5, filtering the liquid medicine: collect the inside exhaust liquid medicine of reation kettle main part (1) through collection device to filter the purification to the liquid medicine through filter equipment, and collect the back liquid medicine that filters, in order to accomplish the extraction of medicinal material active ingredient.
2. The effective component extraction method based on the water decoction method according to claim 1, wherein the mounting side lugs (2) are uniformly welded in the middle of the outer side surface of the reaction kettle body (1) at equal intervals along the circumferential direction, the electric telescopic rods (3) are fixedly mounted in the middle of the two mounting side lugs (2) positioned on both sides of the reaction kettle body (1), the input end of each electric telescopic rod (3) is electrically connected with the output end of an external power supply, the middle of the top end of each electric telescopic rod (3) is fixedly connected with a connecting circular plate (4), and the top end of each connecting circular plate (4) is fixedly connected with a connecting transverse plate (5);
a sealing cover plate (6) is fixedly connected between the two connecting transverse plates (5) corresponding to the opening at the top end of the reaction kettle main body (1), and a mounting seat (601), a rotating motor (602), a connecting disc (603), a transmission rotating shaft (604), a connecting chuck (605), a connecting upper disc (606), a contact backing ring (607) and a connecting conical block (608) are arranged on the outer side of the sealing cover plate (6);
the middle part of the bottom end of the inner side of the reaction kettle main body (1) is fixedly provided with a mounting lower column (7), and the outer side of the mounting lower column (7) is provided with a limiting annular plate (701), a cushion ring (702), a guide lower pipe (703), a rotary upper column (704), a guide upper pipe (705), a connecting rotary block (706), a positioning conical groove (707), a rotary concave ring (708) and a rotary convex ring (709);
a clamping round cover (8) is placed at the top end of the connecting rotary block (706), a splicing round groove (801), an upper connecting column (802), a connecting conical groove (803), a positioning conical block (804), a splicing inner curved ring (805), an upper clamping ring (806), a lower splicing ring (807), a lower clamping ring (808), a guide rectangular groove (809) and an isolation inner net (810) are arranged on the outer side of the clamping round cover (8);
the clamp is fitted with a ring (806) top and is connected with a splicing lantern ring (9) through bolts, the edge of the bottom of the splicing lantern ring (9) is connected with a fixed upper ring (10) through bolts, and the bottom of the fixed upper ring (10) is provided with a splicing outer curved ring (1001), a splicing outer ring (1002), a fixed lower ring (1003) and an isolation outer net (1004).
3. The method for extracting active ingredients based on water decoction method according to claim 2, the middle part of the top end of the sealing cover plate (6) is connected with an installation seat (601), the middle part of the top end of the installation seat (601) is fixedly provided with a rotating motor (602), the input end of the rotating motor (602) is electrically connected with the output end of an external power supply, the bottom end of the output shaft of the rotating motor (602) is fixedly connected with a connecting disc (603) corresponding to the inner side of the mounting seat (601), the middle part of the bottom end of the connecting disc (603) is fixedly connected with a transmission rotating shaft (604), the bottom end of the transmission rotating shaft (604) is provided with a connecting upper disc (606) through a connecting chuck (605), the edge of the bottom end of the upper connecting disc (606) is bonded with a contact backing ring (607), and the middle of the bottom end of the upper connecting disc (606) is fixedly provided with a connecting conical block (608) corresponding to the inner side of the contact backing ring (607).
4. The method for extracting active ingredients based on the water decoction method, according to the claim 3, characterized in that the transmission rotating shaft (604) penetrates through the middle part of the sealing cover plate (6) and is rotatably connected with the sealing cover plate (6), and the bottom of the sealing cover plate (6) is mutually matched with the top of the reaction kettle main body (1).
5. The method for extracting active ingredients based on the decoction method according to claim 2, wherein a limiting annular plate (701) is fixedly sleeved at the bottom end of the outer side of the lower mounting column (7), a cushion ring (702) is bonded at the edge of the top end of the limiting annular plate (701), and a lower guide tube (703) is fixedly sleeved at the position, corresponding to the top of the limiting annular plate (701), of the outer side of the lower mounting column (7);
the middle part of the top end of the lower mounting column (7) is rotatably connected with an upper rotating column (704) through a rotating disc, and the outer side of the upper rotating column (704) is fixedly sleeved with an upper guide tube (705);
rotate upper prop (704) top position department and be provided with and connect commentaries on classics piece (706), connect and change piece (706) top limit portion and evenly seted up four location taper grooves (707) along the circumferencial direction equidistance, rotate upper prop (704) top middle part and install through the bolt and rotate concave ring (708), connect and change piece (706) bottom middle part and install through the bolt and rotate convex ring (709), and rotate between concave ring (708) and the rotation convex ring (709) be sliding connection.
6. The method for extracting active ingredients by decoction method according to claim 5, wherein the lower guide tube (703) is uniformly provided with guide sliding strips along the circumferential direction of the edge, the upper guide tube (705) is uniformly provided with guide sliding strips along the circumferential direction of the edge, the rotating concave ring (708) and the rotating convex ring (709) are engaged with each other, and the friction force between the lower mounting pillar (7) and the upper rotating pillar (704) is greater than the friction force between the rotating concave ring (708) and the rotating convex ring (709).
7. The active ingredient extraction method based on the decoction method according to claim 2, wherein a splicing circular groove (801) is formed in the middle of the bottom end of the clamping circular cover (8), an upper column (802) is fixedly connected to the middle of the top end of the clamping circular cover (8), a connecting conical groove (803) is formed in the middle of the top end of the upper column (802), and four positioning conical blocks (804) are uniformly and fixedly connected to the top surface of the inner side of the splicing circular groove (801) in the circumferential direction;
joint dome (8) outside bottom has concatenation inner loop (805) through bolt fixed mounting, there is ring (806) in the concatenation inner loop (805) top through bolt fixedly connected with centre gripping, direction low tube (703) outside corresponds cushion ring (702) top position department and is provided with concatenation lower ring (807), there is ring (808) down the centre gripping at concatenation lower ring (807) top through bolted connection, direction rectangular channel (809) have evenly been seted up to the inboard circumferencial direction of concatenation lower ring (807), keep apart between intranet (810) top centre gripping in the concatenation inner loop (805) and centre gripping upper ring (806), keep apart intranet (810) bottom centre gripping under the concatenation between ring (807) and centre gripping lower ring (808).
8. The method for extracting active ingredients based on the decoction method according to claim 7, wherein the sectional dimension of the splicing circular groove (801) is the same as the dimension of the top surface of the connecting rotating block (706), the connecting conical groove (803) and the connecting conical block (608) are positioned correspondingly, the connecting conical block (608) is engaged with the connecting conical groove (803), the positioning conical block (804) is positioned correspondingly with the positioning conical groove (707), and the positioning conical block (804) is engaged with the positioning conical groove (707);
the guide rectangular groove (809) corresponds to the guide sliding strips on the outer sides of the guide lower pipe (703) and the guide upper pipe (705), the inner wall of the guide rectangular groove (809) is in sliding connection with the outer sides of the guide sliding strips, the arc-shaped surface on the inner side of the guide rectangular groove (809) is tightly attached to the arc surface on one side of the guide sliding strips in a sliding mode, and the width of the guide rectangular groove (809) is larger than that of the guide sliding strips.
9. The decoction-based active ingredient extraction method according to claim 2, wherein the bottom end of the fixed upper ring (10) is connected with a spliced outer curved ring (1001) through a bolt, the bottom of the inner side of the reaction kettle body (1) is provided with a spliced outer ring (1002) at the same height as the outer side of the spliced lower ring (807), the top end of the spliced outer ring (1002) is connected with a fixed lower ring (1003) through a bolt, the top end of the isolation outer net (1004) is clamped between the fixed upper ring (10) and the spliced outer curved ring (1001), and the bottom end of the isolation outer net (1004) is clamped between the spliced outer ring (1002) and the fixed lower ring (1003);
reinforcing cables (11) are uniformly and fixedly connected between the splicing inner curved ring (805) and the clamping lower ring (808) and between the splicing outer curved ring (1001) and the fixed lower ring (1003), extrusion balls (12) are uniformly and fixedly connected to the outer side of each reinforcing cable (11) at equal intervals, and a splicing pore plate (13) is fixedly connected between the splicing lower ring (807) and the splicing outer ring (1002);
the device is characterized in that a liquid medicine discharge pipe (14) is fixedly mounted on one side of the bottom of the reaction kettle main body (1), a cleaning discharge pipe (15) is fixedly connected to the other side of the bottom of the reaction kettle main body (1), and the liquid medicine discharge pipe (14) and the cleaning discharge pipe (15) are both sealed through a sealing valve.
10. The method for extracting active ingredients based on the decoction method according to claim 9, wherein the spliced lantern ring (9) is composed of an inner ring and an outer ring, the inner ring and the outer ring are connected with each other through a connecting column, and the top surface of the spliced orifice plate (13) and the top surfaces of the spliced lower ring (807) and the spliced outer ring (1002) are flush with each other.
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| Publication number | Publication date |
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| CN114344157B (en) | 2023-09-22 |
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