CN114317125A - Natural essential oil soap and preparation method thereof - Google Patents
Natural essential oil soap and preparation method thereof Download PDFInfo
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- CN114317125A CN114317125A CN202111388948.5A CN202111388948A CN114317125A CN 114317125 A CN114317125 A CN 114317125A CN 202111388948 A CN202111388948 A CN 202111388948A CN 114317125 A CN114317125 A CN 114317125A
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Abstract
The invention provides a natural essential oil soap and a preparation method thereof, the natural essential oil soap adopts a soap-free base system, only gels, surfactants, natural essential oil, base oil, humectants and the like in a specific ratio are compounded and formed, and the whole product has weak acid pH, a structure Q elasticity, moisturizing and sterilizing effects, has no irritation, and is suitable for long-term use by human bodies. The natural essential oil soap product disclosed by the invention is strong in fragrance, rich in foam and good in cleaning effect, the raw materials are all green and natural substances, the safety is high, the product structure Q is elastic, the strength is proper, the production process is simple, and the industrial production can be realized.
Description
Technical Field
The invention relates to the technical field of perfumed soaps, in particular to a natural essential oil soap and a preparation method thereof.
Background
Soaps are generally solid block-shaped products, but also pasty and liquid products. Both conventional cold soaps and hot soaps are fatty acid soaps with fatty acid salts as the primary surfactant. The pH value of the fatty acid soap is alkaline, the degreasing force is strong, the skin after washing is tight and strong in feeling, the horny layer can be thinned after long-term use, and the fatty acid soap has great irritation and damage to the skin.
The essential oil soap is a kind of toilet soap with gradually increasing demand at present. The essential oil soap mainly contains plant essential oil which is extracted from flowers, leaves, stems, roots or fruits of plants by a steam distillation method, an extrusion method, a cold soaking method or a solvent extraction method, and has the advantages of strong permeability, most safety, no side effect, sterilization effect and the like.
The essential oil soap in the market is prepared by adding plant essential oil after soap base is dissolved thermally or alkali liquor is subjected to saponification reaction. Thus, existing essential oil soap products are substantially more alkaline. Although some essential oil soaps have the advantages of strong fragrance, high moisturizing effect, lasting fragrance, good sterilizing effect and the like, the alkaline essential oil soaps are still not suitable for long-term use by human bodies because the skin of the human bodies is weakly acidic.
Disclosure of Invention
Based on the above, there is a need for a weakly acidic natural essential oil soap and a preparation method thereof, which are non-irritating to human skin and suitable for long-term use.
The invention adopts the following technical scheme:
the invention provides a natural essential oil soap which is mainly prepared from the following raw materials in percentage by weight: 1-8% of gel, 5-25% of surfactant, 1-15% of natural essential oil, 0-5% of base oil, 2-25% of humectant and the balance of water; wherein the gelling agent is at least selected from a mixture of tamarind seed polysaccharide gum and konjac gum.
In some embodiments, the natural essential oil soap is mainly prepared from the following raw materials in percentage by weight: 3-8% of gel, 15-20% of surfactant, 3-12% of natural essential oil, 1-5% of base oil, 15-25% of humectant and the balance of water.
In some of these embodiments, the weight ratio of the konjac gum to the tamarind polysaccharide gum is 1 (3-4).
In some of these embodiments, the konjac gum is konjac glucomannan with a molecular weight of 5000-.
In some of these embodiments, the gelling agent is further selected from the group consisting of at least one of guar gum, locust bean gum, xanthan gum, gellan gum, gum arabic, pectin, carrageenan.
In some of these embodiments, the surfactant is selected from at least one of sodium lauroyl glutamate, sodium lauroyl sarcosinate, sodium cocoyl glutamate, sodium cocoyl amido propionate, sodium cocoyl methyl taurate, sodium cocoyl glycinate.
In some of these embodiments, the surfactant is further selected from at least one of alkyl glycoside surfactants, glucose amide surfactants, alcohol ether carboxylate surfactants, amide ether carboxylate surfactants, and monoalkyl phosphate ester surfactants.
In some of these embodiments, the natural essential oil is selected from at least one of lavender essential oil, sandalwood essential oil, ylang essential oil, lemon essential oil, rose essential oil, tea tree essential oil, rosemary essential oil, calendula essential oil, chamomile essential oil, mint essential oil, sage essential oil, and myrrh essential oil.
In some of these embodiments, the base oil is selected from at least one of coconut oil, olive oil, shea butter, crabapple oil, meadowfoam seed oil, wheat germ oil.
In some of these embodiments, the humectant is selected from at least one of glycerin, propylene glycol, butylene glycol, sorbitol, mannitol, pentylene glycol, hexylene glycol.
The invention provides a preparation method of natural essential oil soap, which comprises the following steps:
s1, adding the gel into the humectant, and uniformly stirring and dispersing to obtain a mixed solution a; s2, adding pure water into the mixed solution a under the stirring state, keeping the temperature at 80-95 ℃, and stirring until the mixed solution a is completely swelled to obtain mixed glue solution b; s3, sequentially adding a surfactant and base oil into the mixed glue solution b under the stirring state, and keeping the temperature of 80-95 ℃ to stir uniformly to obtain a mixed material body c; s4, reducing the temperature in the stirring container to 40-60 ℃ under the stirring state, adding natural essential oil into the mixture body c, and continuously stirring until the mixture body c is uniform to obtain a mixed base material d; s5, transferring the mixed base material d into a hopper of a filling machine, filling into a mold, and standing for forming to obtain the composite material.
In some embodiments, in the step S3, homogeneous stirring may be selected for better mixing effect.
In some embodiments, the process parameters of the standing forming are as follows: standing at normal temperature for 6-24 h.
The invention has the beneficial effects that:
compared with the prior art, the natural essential oil soap is formed by compounding and forming the gel, the surfactant, the natural essential oil, the base oil, the humectant and water in a specific ratio, integrally forms an essential oil soap product without a soap base system, is weakly acidic, and is suitable for long-term use by a human body. The natural essential oil soap disclosed by the invention is good in cleaning effect, has the effects of moisturizing, inhibiting bacteria and killing bacteria, is in a product structure Q-elasticity, and can be industrially produced.
Drawings
FIG. 1 is a photograph of essential oil soaps prepared by different examples; wherein (a) is the essential oil soap prepared in example 1, (b) is the essential oil soap prepared in example 4, and (c) is the essential oil soap prepared in example 5.
Detailed Description
The present invention is further described in detail below with reference to specific examples so that those skilled in the art can more clearly understand the present invention.
The following examples are provided only for illustrating the present invention and are not intended to limit the scope of the present invention. All other embodiments obtained by a person skilled in the art based on the specific embodiments of the present invention without any inventive step are within the scope of the present invention.
In the examples of the present invention, all the raw material components are commercially available products well known to those skilled in the art, unless otherwise specified; in the examples of the present invention, unless otherwise specified, all technical means used are conventional means well known to those skilled in the art.
Key material source manufacturers and their physicochemical properties:
example 1
This example provides a natural essential oil soap, which is composed of the following raw materials as shown in the following table:
the preparation method of the essential oil soap comprises the following steps:
(1) adding gel (mixture of tamarind polysaccharide gum, konjac gum and guar gum) into humectant (mixture of glycerol, propylene glycol and pentanediol), stirring, and dispersing to obtain mixed solution a.
(2) And adding pure water into the mixed solution a under the stirring state, keeping the temperature at 80 ℃, and stirring until the mixed solution is completely swelled to obtain a mixed glue solution b.
(3) And sequentially adding a surfactant (mixed by sodium lauroyl glutamate and sodium lauroyl sarcosinate) and base oil (mixed by coconut oil and shea butter) into the mixed glue solution b under stirring, and continuously keeping the temperature of 80 ℃ and stirring uniformly to obtain a mixed material body c.
(4) And (3) reducing the temperature in the stirring container to 40 ℃ under the stirring state, adding natural essential oil (the lavender essential oil, the sandalwood essential oil and the myrrh essential oil are mixed) into the mixture body c, and continuously stirring until the mixture is uniform to obtain a mixed base material d.
(5) And transferring the mixed base material d into a hopper of a filling machine, filling into a mold, and standing for forming.
Example 2
This example provides an essential oil soap, which is composed of the following raw materials as shown in the following table:
the preparation method of the essential oil soap comprises the following steps:
(1) adding the gel into 80 parts of humectant, and stirring to disperse uniformly to obtain a mixed solution a.
(2) And adding pure water into the mixed solution a under the stirring state, keeping the temperature at 90 ℃ and stirring until the mixed solution is completely swelled to obtain a mixed glue solution b.
(3) And (3) sequentially adding a surfactant and base oil into the mixed glue solution b under the stirring state, and keeping the temperature at 90 ℃ to be uniform and stirring to obtain a mixed material body c.
(4) And (3) reducing the temperature in the stirring container to 50 ℃ under the stirring state, adding the natural essential oil into the mixture body c, and continuously stirring until the mixture is uniform to obtain a mixed base material d.
(5) And (3) transferring the mixed base material d into a hopper of a filling machine, filling into a half mold, standing for 6-24 hours at normal temperature (0-25 ℃), and standing for forming to obtain the composite material.
Example 3
This example provides an essential oil soap, which is composed of the following raw materials as shown in the following table:
the preparation method of the essential oil soap comprises the following steps:
(1) adding the gel into the humectant, and uniformly stirring and dispersing to obtain a mixed solution a.
(2) And adding pure water into the mixed solution a under the stirring state, keeping the temperature at 95 ℃, and stirring until the mixed solution is completely swelled to obtain a mixed glue solution b.
(3) And (3) sequentially adding a surfactant and base oil into the mixed glue solution b under the stirring state, and keeping the temperature of 95 ℃ to be kept, homogenizing and stirring until the mixture is uniform to obtain a mixed material body c.
(4) And (3) reducing the temperature in the stirring container to 60 ℃ under the stirring state, adding the natural essential oil into the mixture body c, and continuously stirring until the mixture is uniform to obtain a mixed base material d.
(5) And transferring the mixed base material d into a hopper of a filling machine, filling into a hemispherical mold, standing for 6-24h at normal temperature (0-25 ℃), and standing for forming.
Example 4
This example provides an essential oil soap, which is composed of the following raw materials as shown in the following table:
the preparation method of the essential oil soap comprises the following steps:
(1) adding the gel into the humectant, and uniformly stirring and dispersing to obtain a mixed solution a.
(2) And adding pure water into the mixed solution a under the stirring state, keeping the temperature at 90 ℃ and stirring until the mixed solution is completely swelled to obtain a mixed glue solution b.
(3) And (3) sequentially adding a surfactant and base oil into the mixed glue solution b under the stirring state, and keeping the temperature at 90 ℃ to be uniform and stirring to obtain a mixed material body c.
(4) And (3) reducing the temperature in the stirring container to 50 ℃ under the stirring state, adding the natural essential oil into the mixture body c, and continuously stirring until the mixture is uniform to obtain a mixed base material d.
(5) And transferring the mixed base material d into a hopper of a filling machine, filling into a mold, standing for 6-24 hours at normal temperature (0-25 ℃), and standing for forming.
Example 5
This example provides an essential oil soap having substantially the same raw material composition as in example 4, except that: the surfactant sodium cocoyl glycinate is replaced by sodium fatty alcohol polyoxyethylene ether carboxylate, and the surfactant does not contain base oil.
Comparative example 1
This comparative example provides a feedstock for an essential oil soap having substantially the same composition as example 4, except that: the gel is only konjac gum. Tests show that the essential oil soap cannot be formed only by adopting the konjac gum.
Comparative example 2
This comparative example provides an essential oil soap having substantially the same raw material composition as in example 4, except that: the gel agent only adopts tamarind polysaccharide gum.
Comparative example 3
This comparative example provides an essential oil soap having substantially the same raw material composition as in example 4, except that: the gel agent only adopts Arabic gum.
And (3) performance detection:
taking the essential oil soap products prepared in the examples 1 to 5 and the comparative examples 1 to 3 respectively, and detecting various physical and chemical indexes, wherein the hardness is detected according to GB/T10807-2006 standard, the elasticity is detected according to GB/T6670-2008 standard, and the foaming force is detected according to QB/T2486-2008 standard, and the results are as follows:
as can be seen from the table above, the konjac gum and the tamarind seed polysaccharide gum are compounded, and the product has better gel strength and Q elastic property.
The cleaning and sterilizing effects of the essential oil soap samples of examples 1 to 5 and comparative examples 1 to 3 were respectively tested according to the GB15979-2002 standard, and the results are shown in the following table:
as can be seen from the table above, the essential oil soap has good bactericidal effects on staphylococcus aureus (ATCC 6538), escherichia coli (8099) and candida albicans (ATCC 10231).
It should be noted that the above examples are only for further illustration and description of the technical solution of the present invention, and are not intended to further limit the technical solution of the present invention, and the method of the present invention is only a preferred embodiment, and is not intended to limit the protection scope of the present invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (10)
1. The natural essential oil soap is characterized by being mainly prepared from the following raw materials in percentage by weight:
wherein the gelling agent is at least selected from a mixture of tamarind seed polysaccharide gum and konjac gum.
2. The natural essential oil soap according to claim 1, which is prepared from the following raw materials in percentage by weight:
3. the natural essential oil soap according to claim 1 or 2, wherein the weight ratio of the konjac gum to the tamarind polysaccharide gum is 1 (3-4).
4. The natural essential oil soap of claim 1 or 2, wherein the gelling agent is further selected from at least one of guar gum, locust bean gum, xanthan gum, gellan gum, gum arabic, pectin, carrageenan.
5. The natural essential oil soap of claim 1 or 2, wherein the surfactant is selected from at least one of sodium lauroyl glutamate, sodium lauroyl sarcosinate, sodium cocoyl glutamate, sodium cocoyl amido propionate, sodium cocoyl methyl taurate, sodium cocoyl glycinate; and/or
The surfactant is at least one selected from alkyl glycoside surfactants, glucose amide surfactants, alcohol ether carboxylate surfactants, amide ether carboxylate surfactants and monoalkyl phosphate surfactants.
6. The natural essential oil soap according to claim 1 or 2, wherein the natural essential oil is at least one selected from lavender essential oil, sandalwood essential oil, ylang essential oil, lemon essential oil, rose essential oil, tea tree essential oil, rosemary essential oil, calendula essential oil, chamomile essential oil, mint essential oil, sage essential oil, and myrrh essential oil.
7. The natural essential oil soap according to claim 1 or 2, wherein the base oil is at least one selected from coconut oil, olive oil, shea butter, crabapple oil, meadowfoam seed oil, wheat germ oil.
8. The natural essential oil soap according to claim 1 or 2, wherein the humectant is at least one selected from glycerin, propylene glycol, butylene glycol, sorbitol, mannitol, pentylene glycol, hexylene glycol.
9. The method for preparing a natural essential oil soap according to any one of claims 1 to 8, comprising the steps of:
s1, adding the gel into the humectant, and uniformly stirring and dispersing to obtain a mixed solution a;
s2, adding pure water into the mixed solution a under the stirring state, keeping the temperature at 80-95 ℃, and stirring until the mixed solution a is completely swelled to obtain mixed glue solution b;
s3, sequentially adding a surfactant and base oil into the mixed glue solution b under the stirring state, and keeping the temperature of 80-95 ℃ to stir uniformly to obtain a mixed material body c;
s4, reducing the temperature in the stirring container to 40-60 ℃ under the stirring state, adding natural essential oil into the mixture body c, and continuously stirring until the mixture body c is uniform to obtain a mixed base material d;
s5, transferring the mixed base material d into a hopper of a filling machine, filling into a mold, and standing for forming to obtain the composite material.
10. The method for preparing natural essential oil soap according to claim 9, wherein in the step S3, homogeneous stirring is selected for better mixing effect; in the step S5, the process parameters of the standing molding are as follows: standing at normal temperature for 6-24 h.
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| CN102617249A (en) * | 2012-03-31 | 2012-08-01 | 山东喜丰田生态肥业有限公司 | Novel polysaccharide gel water retaining and slow release fertilizer |
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