CN114224780A - 一种具有杀菌功能的免水去污洗手液 - Google Patents

一种具有杀菌功能的免水去污洗手液 Download PDF

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CN114224780A
CN114224780A CN202210051445.7A CN202210051445A CN114224780A CN 114224780 A CN114224780 A CN 114224780A CN 202210051445 A CN202210051445 A CN 202210051445A CN 114224780 A CN114224780 A CN 114224780A
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hand sanitizer
polyvinyl alcohol
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胡帅
徐健康
吕飞
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Jinhua Hongmi Precision Instrument Co ltd
Yongkang Institute Of Quality And Technology Monitoring
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Yongkang Institute Of Quality And Technology Monitoring
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Abstract

本发明公开了一种具有杀菌功能的免水去污洗手液。其特征在于按重量份数计,包括以下组分:无机粉料30~40份、DP300为5~10份、表面活性剂1~5份、聚乙烯醇20~40份、甘油40~60份、水50~70份、戊二醛2份和柠檬酸10~20份。该洗手液再无水的环境下,通过双手不断搓洗,污垢脱落,杀菌、去污效果好。

Description

一种具有杀菌功能的免水去污洗手液
技术领域
本发明涉及洗手液领域,具体为一种具有杀菌功能的免水去污洗手液。
背景技术
免水洗手液具有不需要不受水源限制,使用极其方便。但现有技术所公开的免水洗手液去污效果较差,将洗手液喷涂于手上后,自然挥发,不能完全去除手上的油污、灰尘等,基本只能起到清凉、保湿、杀菌的效果,手上原先的污渍、油污并不能除去。
发明内容
为了解决以上技术问题,本发明公开了一种具有杀菌功能的免水洗去污洗手液。
本发明的上述技术目的是通过以下技术方案得以实现的:一种具有杀菌功能的免水去污洗手液,按重量份数计,包括以下组分:无机粉料30~40份、DP300为5~10份、表面活性剂1~5份、聚乙烯醇20~40份、甘油40~60份、水50~70份、乙醇10~20份、戊二醛2份和柠檬酸10~20份。
在其中一个实施例中,还包括质量为所述无机粉料质量的2~10%的碳酸钠或碳酸氢钠。
在其中一个实施例中,所述无机粉料选自天然黏土、高岭土、气相二氧化硅、钠基膨润土、竹炭粉中的至少一种。
在其中一个实施例中,所述表面活性剂选自十二烷基苯磺酸钠、OP-10、十二烷基硫酸钠、二辛基琥珀酸磺酸钠中的一种或几种,所述表面活性剂配合碳酸钠或碳酸氢钠使用。
在其中一个实施例中,还包括清凉油。
在其中一个实施例中,所述无机粉料选自天然黏土、高岭土、二氧化硅、膨润土、竹炭粉中的至少一种。
一种具有杀菌功能的免水去污洗手液,包括如下步骤:
步骤一,按重量分数比,称取聚乙烯醇和水,将水加热至90℃,使聚乙烯醇充分溶解;
步骤二,按比例向步骤一得到的聚乙烯醇水溶液中添加甘油,继续加温至120~130℃,使聚乙烯醇和甘油混溶;
步骤三,按比例向步骤二得到的聚乙烯醇-甘油水溶液中添加柠檬酸、表面活性剂、碳酸氢钠或碳酸钠、DP300、无机粉料,常温静置24-48小时,得到具有杀菌功能的免水去污洗手液。
本发明采用聚乙烯醇交联成膜性,结合戊二醛、柠檬酸等高效无毒杀菌消毒剂,以及表面活性剂,制备了一种杀菌功能的免水去污洗手液,与现有技术相比,本发明的优势在于:使用者在手上喷上少量的杀菌功能的免水去污洗手液,通过反复的揉搓10~30秒,手上的油污、灰尘等就会随聚乙烯醇交联膜脱落,解决乐现有技术中,免水洗手液喷涂手上后,油污、灰尘不能脱落的缺点,同时,本发明所述洗手液还能达到杀菌、消毒、抑菌、润肤的效果,解决了户外无水、无肥皂等环境下,无法洗手的难题。
一种具有杀菌功能的免水去污洗手液制造原理:本发明主要利用了聚乙烯醇和戊二醛在酸性环境中容易交联成膜的原理。在无水搓洗过程中无机粉料能增加摩擦力同时,加速污渍脱落。DP300的化学名称为2.4.4’-三氯-2’-羟基二苯醚,具有对引起感染或病原性革兰氏阳性及阴性菌、真菌、酵母及病毒(如甲、乙肝、狂犬病毒、艾滋病IHV)等都具有广泛的杀灭及抑制作用。表面活性剂能增强去油污的功效。甘油起保湿和润滑到的作用。乙醇除了杀菌的作用外,还起到加速水分挥发,促进聚乙烯醇-戊二醛成膜。柠檬酸起到酸性的作用,促进聚乙烯醇和戊二醛反应成膜。与聚乙烯醇反应后多余的戊二醛起到杀菌的作用。
有益效果:本发明的具有杀菌功能的免水去污洗手液,使用时,将少量的洗手液放置手心,通过不断搓洗,随着水分挥发的同时,聚乙烯醇和戊二醛反应成膜,反应所生成的成膜物夹杂着污垢、油污、细菌等脱落,与此同时,洗手液中的杀菌物质起到了杀菌和抑制的作用。该发明使用方便,去污、杀菌一体完成,随着成膜物的脱落,明显发现手上污垢去除。
具体实施方式
为使本发明的目的、技术方案和优点更加清楚,下面对本发明的技术方案做进一步说明。本发明所述的技术方案并不仅限于以下所述的实施方式。提供这些实施方式的目的是使本领域技术人员对本发明的公开内容理解更加透彻全面。
实施例1:一种具有杀菌功能的免水去污洗手液,原料各组分如表1所示。
一种具有杀菌功能的免水去污洗手液的制备方法如下:
步骤一,按重量分数比,称取聚乙烯醇和水,将水加热至90℃,使聚乙烯醇充分溶解;
步骤二,按比例向步骤一得到的聚乙烯醇水溶液中添加甘油,继续加温至120~130℃,使聚乙烯醇和甘油混溶;
步骤三,按比例向步骤二得到的聚乙烯醇-甘油水溶液中添加柠檬酸、op-10、DP300、二氧化硅、膨润土、乙醇、竹炭粉,常温静置24-48小时,得到具有杀菌功能的免水去污洗手液。
实施例2:一种具有杀菌功能的免水去污洗手液,原料各组分如表1所示。
一种具有杀菌功能的免水去污洗手液的制备方法如下:
步骤一,按重量分数比,称取聚乙烯醇和水,将水加热至90℃,使聚乙烯醇充分溶解;
步骤二,按比例向步骤一得到的聚乙烯醇水溶液中添加甘油,继续加温至120~130℃,使聚乙烯醇和甘油混溶;
步骤三,按比例向步骤二得到的聚乙烯醇-甘油水溶液中添加柠檬酸、戊二醛、乙醇、碳酸氢钠、op-10、DP300、二氧化硅,搅拌均匀后,常温静置24-48小时,得到具有杀菌功能的免水去污洗手液。
实施例3:一种具有杀菌功能的免水去污洗手液,原料各组分如表1所示。
一种具有杀菌功能的免水去污洗手液的制备方法如下:
步骤一,按重量分数比,称取聚乙烯醇和水,将水加热至90℃,使聚乙烯醇充分溶解;
步骤二,按比例向步骤一得到的聚乙烯醇水溶液中添加甘油,继续加温至120~130℃,使聚乙烯醇和甘油混溶;
步骤三,按比例向步骤二得到的聚乙烯醇-甘油水溶液中添加柠檬酸、戊二醛、碳乙醇、酸氢钠、op-10、DP300、二氧化硅、膨润土、竹炭粉,工业淀粉、聚丙烯酰胺,搅拌均匀后,常温静置24-48小时,得到具有杀菌功能的免水去污洗手液。
对比例:按照常规洗手方法进行清洗双手,具体步骤如下:
步骤一,先在水龙头下把手淋湿;
步骤二,在手掌上抹市面上购置的普通肥皂或洗手液,均匀涂抹,搓出泡沫,让手掌、手背、手指、指缝等都沾满肥皂泡沫,然后反复搓揉双手1分钟;
步骤三,在水龙头下,将手冲洗干净。
表1 单位:Kg
Figure DEST_PATH_IMAGE001
本发明所述的一种具有杀菌功能的免水去污洗手液,与现有技术相比,其主要功能主要体现在三方面:1、杀菌功能。该功能由戊二醛、柠檬酸、DP30三个组分实现,其中,戊二醛广谱、高效消毒剂,可以杀灭一切微生物;具有刺激性小、腐蚀性低、安全低毒等优点,但其存在短期杀菌率不高的缺点,因此,需配合柠檬酸、DP30使用,其中DP30的化学名称为2,4,4’-三氯-2’-羟基-二苯醚【三氯生】;2、免水功能。该功能主要由聚乙烯醇交联柠檬酸制成的溶液实现,该交联溶液涂覆手上后,反复揉搓,水分挥发后,聚乙烯醇交联柠檬酸在手上逐渐成膜脱落;3、去污功能。该功能主要有表面活性剂配合膨润土等无机粉料得以实现。
杀菌率检测方法
步骤一,五指并拢,用浸有无菌生理盐水的棉拭子一支,在双手指曲面从指根到指端来回涂覆各2次,手接触部分剪去,然后将棉拭子放入盛有10ml无菌生理盐水中的试管中,立即送检。
步骤二,将样品试管永振荡器震荡1min,取1ml加入无菌平皿中,加入普通营养琼脂,置36℃温箱中培养48小时进行菌落计数。
步骤三,采用平板菌落计数法,统计菌落数。
采用以上所述的杀菌率检测方法,分别检测本发明所述杀菌功能的免水去污洗手液使用前后的杀菌数,并计算出杀菌率。杀菌率(100%)=免水去污洗手液使用后菌落总数(个)/免水去污洗手液使用后菌落总数(个)。
本发明所述各实施例的杀菌率如表1所示:
表1
Figure DEST_PATH_IMAGE003
最后说明的是:以上所述仅为本发明的优选实施例而已,并不用于限制本发明,尽管参照前述实施例对本发明进行了详细说明,对于本领域的技术人员来说,其依然可以对前述个实施例所记载的技术方案进行修改,或者对其中部分技术特征进行等同替换。上述实施例和说明书中描述的知识说明本发明的原理,在不脱离本发明精神和范围的前提下,本发明还会有各种变化和改进,这些变化和改进都落入要求保护的本发明范围内。

Claims (7)

1.一种具有杀菌功能的免水去污洗手液,其特征在于,按重量份数计,包括无机粉料30~40份、DP300为5~10份、表面活性剂1~5份、聚乙烯醇20~40份、甘油40~60份、水50~70份、乙醇10~20份、戊二醛2份和柠檬酸10~20份。
2.根据权利要求1所述的具有杀菌功能的免水去污洗手液,其特征在于:还包括质量为所述无机粉料质量的10~20%的碳酸钠或碳酸氢钠。
3.根据权利要求1所述的具有杀菌功能的免水去污洗手液,其特征在于:还包括质量为所述聚乙烯醇质量的10~20%工业淀粉。
4.根据权利要求3所述的具有杀菌功能的免水去污洗手液,其特征在于:还包括质量为所述工业淀粉质量的5~10%聚丙烯酰胺。
5.根据权利要求1所述的具有杀菌功能的免水去污洗手液,其特征在于:所述无机粉料选自天然黏土、高岭土、二氧化硅、膨润土、石墨粉、竹炭粉中的至少一种。
6.根据权利要求1所述的具有杀菌功能的免水去污洗手液,其特征在于:所述表面活性剂选自十二烷基苯磺酸钠、OP-10、十二烷基硫酸钠、二辛基琥珀酸磺酸钠中的一种或几种。
7.一种具有杀菌功能的免水去污洗手液的制备方法,其特征在于,包括如下步骤:
步骤一,按重量分数比,称取聚乙烯醇和甘油,将水加热至90℃,使聚乙烯醇充分溶解;
步骤二,按比例向步骤一得到的聚乙烯醇水溶液中添加甘油,继续加温至120~130℃,使聚乙烯醇和甘油混溶;
步骤三,按比例向步骤二得到的聚乙烯醇-甘油水溶液中添加柠檬酸、戊二醛、碳酸氢钠、op-10、DP300、二氧化硅、膨润土、竹炭粉,工业淀粉、聚丙烯酰胺,搅拌均匀后,常温静置24-48小时,得到具有杀菌功能的免水去污洗手液。
CN202210051445.7A 2022-01-18 2022-01-18 一种具有杀菌功能的免水去污洗手液 Pending CN114224780A (zh)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107837210A (zh) * 2017-11-15 2018-03-27 济宁锦祥科技发展有限公司 一种绿色食品级杀菌洗手液
CN109288727A (zh) * 2018-11-19 2019-02-01 巩义市宏盛稀有金属有限公司 一种用于工业去重油污的磨砂型洗手液及其制备方法
CN110960444A (zh) * 2020-01-06 2020-04-07 浙江神英科技股份有限公司 一种缓释持久抑菌性洗手液及制备方法
CN112237554A (zh) * 2020-10-16 2021-01-19 临沂京瑞新材料科技有限公司 一种免水洗手消毒液

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107837210A (zh) * 2017-11-15 2018-03-27 济宁锦祥科技发展有限公司 一种绿色食品级杀菌洗手液
CN109288727A (zh) * 2018-11-19 2019-02-01 巩义市宏盛稀有金属有限公司 一种用于工业去重油污的磨砂型洗手液及其制备方法
CN110960444A (zh) * 2020-01-06 2020-04-07 浙江神英科技股份有限公司 一种缓释持久抑菌性洗手液及制备方法
CN112237554A (zh) * 2020-10-16 2021-01-19 临沂京瑞新材料科技有限公司 一种免水洗手消毒液

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