CN114217016A - Device and method for testing cockroach prevention performance of ceramic tile - Google Patents

Device and method for testing cockroach prevention performance of ceramic tile Download PDF

Info

Publication number
CN114217016A
CN114217016A CN202111446025.0A CN202111446025A CN114217016A CN 114217016 A CN114217016 A CN 114217016A CN 202111446025 A CN202111446025 A CN 202111446025A CN 114217016 A CN114217016 A CN 114217016A
Authority
CN
China
Prior art keywords
ceramic tile
test
cockroach
testing
box
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202111446025.0A
Other languages
Chinese (zh)
Inventor
孙飞野
柯善军
田维
马超
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Foshan Oceano Ceramics Co Ltd
Original Assignee
Foshan Oceano Ceramics Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Foshan Oceano Ceramics Co Ltd filed Critical Foshan Oceano Ceramics Co Ltd
Priority to CN202111446025.0A priority Critical patent/CN114217016A/en
Publication of CN114217016A publication Critical patent/CN114217016A/en
Pending legal-status Critical Current

Links

Images

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/0001Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00 by organoleptic means
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/15Medicinal preparations ; Physical properties thereof, e.g. dissolubility

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Biophysics (AREA)
  • Molecular Biology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Catching Or Destruction (AREA)

Abstract

The invention belongs to the technical field of ceramic tile performance testing, and particularly discloses a device and a method for testing cockroach prevention performance of a ceramic tile. The test device comprises: the test box comprises a buffer box with an opening at the upper end and a plurality of test boxes, wherein the plurality of test boxes are arranged on the periphery of the buffer box at equal intervals; the buffer box is communicated with the test box through a channel; the top covers of the buffer box and the test box are provided with a first top cover and a second top cover, so that the test device forms a closed space. The test method comprises the following steps: placing a ceramic tile to be tested or a control ceramic tile in the center of each test box, and placing cockroach feed with the same weight on the surface of the ceramic tile to be tested and the control ceramic tile, wherein the number of the ceramic tile to be tested and the number of the control ceramic tile are equal; placing a plurality of cockroach test insects in the buffer box, and covering a first top cover and a second top cover; respectively counting the number of cockroach and insect test in the test box corresponding to the to-be-tested ceramic tile and the control ceramic tile, and recording as S1 and S2; and calculating the barrier prevention index K according to the formula K which is S2/S1, and evaluating the barrier prevention efficacy of the to-be-tested ceramic tile.

Description

Device and method for testing cockroach prevention performance of ceramic tile
Technical Field
The invention belongs to the technical field of ceramic tile performance testing, and particularly relates to a testing device and a testing method for cockroach prevention performance of a ceramic tile.
Background
Cockroaches are common sanitary pests, and their abuse has brought about a great influence on the normal lives of people. Because the cockroaches have strong viability and reproductive capacity, the common killing means can hardly remove the cockroaches completely. Cockroaches are characterized by omnivorous nature and are often moved in places such as garbage dumps, toilets, and the like. Through detection, cockroaches caught in hospitals and families of residents almost carry pathogenic bacteria. Consequently, the activity of cockroaches presents a potentially serious health hazard to residents. The ceramic tile is a building material which is most widely adopted in modern home and commercial decoration, and the ceramic tile with the cockroach-repelling function is prepared by taking the ceramic tile as a carrier of the cockroach-repelling and cockroach-preventing functional agent, so that the cockroach-repelling effect can be improved to the greatest extent, the ceramic tile has a positive effect on cockroach-repelling and cockroach-preventing, and the ceramic tile is beneficial to improving the sanitation of home and office environments and reducing disease spread.
The invention patent of China (CN 112525756A) discloses a method for testing the cockroach prevention effect of a ceramic tile, which is characterized in that two ceramic tile samples with cockroach feed on the surfaces are placed in a national standard square box, the reduction condition of the cockroach feed on the surface of the ceramic tile to be tested in a certain time period is tested, and the more the feed is left, the better the pesticide effect is. However, this method generally takes 7 days or more to obtain the test result, and is not sufficient for rapid detection.
At present, a quick testing device and a corresponding testing method for the cockroach prevention performance of the ceramic tile are not available. The existing cockroach-preventing drug effect test method is long in time consumption, and the drug effect test result fluctuates, so that the method is not beneficial to quickly and accurately evaluating the cockroach-preventing drug effect of the ceramic tile.
Disclosure of Invention
The invention provides a device and a method for testing cockroach prevention performance of a ceramic tile, which are used for solving one or more technical problems in the prior art and at least providing a beneficial choice or creation condition.
The invention has the following inventive concept: lure the cockroach test worm through the cockroach fodder and get to eat, it volatilizes or contacts and produces to repel the cockroach test worm and keep away the effect to utilize in the ceramic tile that awaits measuring (prevent the cockroach ceramic tile), reduces the cockroach test worm and gets the food activity on the ceramic tile that awaits measuring, forces the cockroach test worm to get to eat on the control ceramic tile (the ordinary ceramic tile of no obstacle-preventing effect), through statistics and calculate the ratio of the cockroach test worm total number in control ceramic tile test box and the ceramic tile test box that awaits measuring, the obstacle-preventing performance of preventing the cockroach ceramic tile is evaluated.
In order to overcome the technical problems, the first technical scheme of the invention is to provide a device for testing the cockroach prevention performance of a ceramic tile.
Specifically, a pottery brick prevents testing arrangement of cockroach performance, testing arrangement includes:
the upper end of the buffer box is opened;
the upper end of the test box is opened, and the test boxes are arranged on the periphery of the buffer box at equal intervals;
the channel is arranged between the buffer box and the test box and communicated with the buffer box and the test box;
the first top cover and the second top cover are respectively covered on the top of the buffer box and the top of the test box, so that the test device forms a closed space.
As a further improvement of the scheme, the central position of each test box is equal to the central position of the buffer box, so that the test error is reduced.
Preferably, the number of the test boxes is even; further preferably, the number of test cases is 4.
As the further improvement of above-mentioned scheme, the material of device is transparent material to the activity condition of observing the cockroach examination worm and the statistics test incasement cockroach examination worm's quantity.
Preferably, the transparent material is transparent glass or transparent acrylic.
Preferably, the inside wall of baffle-box with the test box all is scribbled emollient to restrict the climbing of cockroach test worm at the inner wall of box, in order to further reduce the test error.
Preferably, the lubricant is petrolatum.
Preferably, the lubricant is applied at a height of 20 cm from the bottom of the buffer tank and the test tank.
Preferably, the buffer box is a cubic box body with the length, width and height of 50 centimeters.
Preferably, the test box is a cylindrical box body with the diameter of 15 cm and the height of 50 cm.
Preferably, the channel is communicated with the bottom ends of the outer sides of the buffer box and the test box.
Preferably, the channel is a square channel with the length, width and height of 10 centimeters, and the cockroach test insects can freely crawl between the buffer box and the test area through the channel.
The second technical scheme of the invention is to provide a method for testing the cockroach prevention performance of the ceramic tile.
Specifically, the test method utilizes the test device for the cockroach prevention performance of the ceramic tile to test.
As a further improvement of the scheme, the method for testing the cockroach prevention performance of the ceramic tile comprises the following steps:
(1) placing a ceramic tile to be tested or a control ceramic tile in the center of each test box, and placing cockroach feed with the same weight on the surface of each ceramic tile to be tested and the surface of each control ceramic tile, wherein the number of the ceramic tiles to be tested is equal to that of the control ceramic tiles;
(2) placing a plurality of cockroach test insects in the buffer box, and covering a first top cover and a second top cover;
(3) counting the number of cockroach test insects in the test box corresponding to the to-be-tested ceramic tile, and recording as S1; counting the number of cockroach and insect test in the test box corresponding to the control ceramic tile, and recording as S2;
(4) and calculating an obstacle prevention index K according to the formula K which is S2/S1, and evaluating the obstacle prevention drug effect of the to-be-detected ceramic tile.
Specifically, the ceramic tile that awaits measuring is the ceramic tile that has the function of preventing obstacles, the contrast ceramic tile is the ordinary ceramic tile that does not possess the function of preventing cockroaches, and the numerical value of preventing obstacles index K is the bigger then shows that the effect of preventing cockroaches is better, and the effect of preventing cockroaches can adopt different grades to express, wherein: the zero order indicates no cockroach prevention effect, the third order indicates weak effect, the second order indicates good effect, and the first order indicates excellent effect.
When the cockroach prevention index K is less than or equal to 1, the cockroach prevention effect of the to-be-detected ceramic tile is zero order, and no cockroach prevention effect is achieved; when K is more than 1 and less than or equal to 1.5, the cockroach prevention effect of the to-be-tested ceramic tile is three-level, and the evaluation result is weak; when K is more than 1.5 and less than 3, the cockroach prevention effect of the ceramic tile to be tested is of the second level, and the evaluation result is good; and when K is more than or equal to 3, the cockroach prevention effect of the to-be-detected ceramic tile is first grade, and the evaluation result is excellent.
As the further improvement of the scheme, a water source is placed at the central position of the buffer box, so that the path from the cockroach test insects to the water source and the path from the cockroach test insects to the cockroach feed are equal in the test process, the influence of the water source on the cockroach test insects is under the same condition, and the test accuracy is guaranteed.
Preferably, the cockroach test insect is adult periplaneta americana or german cockroach; further preferably, the cockroach test insect is a standard sensitive line product raised in a laboratory.
Preferably, in the step (2), the number of the cockroach test insects is not less than 50 so as to ensure a certain number of statistical probabilities.
As a further improvement of the above scheme, the statistical method comprises: counting the number of the cockroach test insects in the test box every 15-60 minutes for 4-16 times, wherein S1 and S2 are the sum of the counted number of each time.
Preferably, the test is repeated for three times each time, and the average value of the three calculated obstacle prevention indexes K is taken as the final evaluation value of the cockroach prevention performance of the to-be-tested ceramic tile.
As a further improvement of the scheme, the applicable environment temperature of the testing method is 24-26 ℃, the environment relative humidity is 70-80%, and the optimal activity of the cockroaches can be ensured under the conditions of the appropriate environment temperature and humidity, so that the evaluation accuracy is further improved.
As a further improvement of the above scheme, before each test, the test device needs to be fully cleaned by using a sodium dodecyl sulfate aqueous solution with the content of 5%, the test device is washed by deionized water for 3 times, and the test is carried out after full drying.
The technical scheme provided by the embodiment of the application at least has the following technical effects or advantages:
the device for testing the cockroach prevention performance of the ceramic tile and the method for testing the cockroach prevention performance of the ceramic tile by using the device have the advantages of rapidness and high efficiency, and can complete the drug effect test within 2 hours. Compared with the existing method for determining the cockroach-preventing drug effect by comparing the amount of the feed eaten by cockroaches, the result of the method is greatly influenced by the feeding of the cockroaches and other environments, most importantly, the test period of the prior art scheme needs more than 7 days, and the drug effect detection work of the cockroach-preventing ceramic tile is severely limited.
Drawings
FIG. 1 is a front view of a device for testing cockroach prevention performance of ceramic tiles;
FIG. 2 is a top view of a device for testing cockroach-preventing performance of ceramic tiles;
FIG. 3 is a distribution diagram of test areas.
In the figure: 100 denotes a buffer tank; 200 denotes a test box; 300 denotes a channel; 400 denotes a first top cover; and 500 denotes a second cap.
Detailed Description
The present invention is described in detail below by way of examples to facilitate understanding of the present invention by those skilled in the art, and it is to be specifically noted that the examples are provided only for the purpose of further illustrating the present invention and are not to be construed as limiting the scope of the present invention.
As shown in fig. 1 and 2, a testing apparatus for cockroach prevention performance of ceramic tiles includes a buffer box 100, a plurality of test boxes 200, a channel 300, a first top cover 400 and a second top cover 500.
The upper end of the buffer box 100 is provided with an opening, so that a water source, cockroach and insect test can be conveniently placed, and a lubricant can be conveniently coated on the inner wall of the buffer box; the first top cover 400 is covered on the top of the buffer box 100 to prevent the cockroach and insect from escaping through the upper opening of the buffer box 100. After the first top cover 400 and the second top cover 500 are closed, the testing device forms a closed space.
The upper end of the test box 200 is opened, so that the lubricant can be conveniently coated on the inner wall of the test box; the plurality of test boxes are arranged on the periphery of the buffer box 100 at equal intervals, and the central position of each test box 200 is equal to the central position of the buffer box 100, so that the distance from the cockroach and insect test to each test box is the same, and the test errors are reduced; the second top cap 500 is fitted over the top of the test box 200 to prevent the cockroach and insect from escaping through the upper opening of the test box 200.
The passage 300 is provided between the buffer box 100 and the test box 200 and communicates the buffer box 100 and the test box 200, and the cockroach test insects can freely crawl between the buffer box 100 and the test area 200 through the passage 300.
In a preferred embodiment, the material of the testing device is transparent material, so that the activity of the cockroach test insects can be observed conveniently, and the number of the cockroach test insects in the testing box can be counted conveniently.
In a preferred embodiment, the inner walls of the buffer box 100 and the test box 200 are coated with a lubricant to limit the cockroach and insect from climbing on the inner wall of the box body, thereby reducing test errors.
As a preferred embodiment, as shown in fig. 1, the buffer box 100 is a cubic box with length, width and height of 50 cm; the test boxes 200 are 4 cylindrical box bodies with the diameter of 15 cm and the height of 50 cm, and the 4 test boxes 200 are respectively arranged in the middle of the four peripheries of the buffer box 100; the side surfaces of the bottoms of the buffer box 100 and the test box are respectively provided with a square hole of 10cm and are communicated through a channel 300; the top of the buffer box 100 is covered with a first top cover 400, the top of the test box 200 is covered with a second top cover 500, and after the first top cover 400 and the second top cover 500 are covered, the whole test device forms a closed space; the inner side walls of the buffer box 100 and the test box 200 are coated with vaseline; the testing device is made of transparent acrylic.
The control tiles adopted in the following examples are the same, and are polished tiles which are normally produced on a production line and are not added with the cockroach-repelling and cockroach-preventing functional agent, and the polished tiles are cut into squares with the size of 10 multiplied by 10cm, and the tiles to be detected are squares with the size of 10 multiplied by 10 cm. In the following embodiments, the test device is not covered by black cloth and can be carried out in a dark room.
Example 1
The ceramic tile that awaits measuring that this embodiment adopted does: carrying out cockroach prevention treatment on the same polished ceramic tile as a control ceramic tile, wherein the used cockroach prevention reagent is benzyl benzoate solution (the solvent is ethyl acetate), 2 g of benzyl benzoate is loaded on each square meter of the polished ceramic tile, standing for 1 day, and testing after the solvent on the surface of the ceramic tile is fully volatilized; the test temperature was 25 degrees and the test humidity was 78%.
The placing positions of the reference ceramic tile and the ceramic tile to be tested are shown in figure 3, the reference ceramic tile is placed in a testing area 1 and a testing area 3, the ceramic tile to be tested is placed in a testing area 2 and a testing area 4, 5 g of cockroach feed is placed on the reference ceramic tile and the ceramic tile to be tested respectively, the feed is framed by a ring with the height of 3 mm, and the ring is located at the center of the ceramic tile; and a water source is placed in the center of the buffer box and is positioned on the central axis of the central connecting line of the ceramic tile to be detected and the control ceramic tile, so that the distance between the water source and the ceramic tile to be detected and the distance between the water source and the control ceramic tile are equal.
50 adult periplaneta americana test insects are placed into a buffer box, vaseline is coated on the inner walls of the buffer box and the test box, timing is started after a first top cover and a second top cover are covered, data for the first time are counted after 15 minutes, the number of the test insects in each test area is recorded, the number of the test insects is recorded for the second time at intervals of 15 minutes, the number of the test insects for 8 times is continuously recorded, and the whole process consumes 120 minutes.
After the test is finished, adding the test insect numbers of the to-be-tested ceramic tile test area and the comparison ceramic tile test area recorded each time, wherein the sum of the test insect numbers of the to-be-tested ceramic tile test area is S1, the sum of the test insect numbers of the comparison ceramic tile test area is S2, and calculating the cockroach prevention index K which is S2/S1.
And repeating the test for three times, and calculating the average value of the cockroach-preventing index K values calculated in each test to obtain the average K value of the cockroach-preventing index of the ceramic tile to be tested.
Example 2
The ceramic tile that awaits measuring that this embodiment adopted does: carrying out cockroach prevention treatment on the same polished ceramic tile as a control ceramic tile, wherein the used cockroach prevention reagent is benzyl benzoate solution (the solvent is ethyl acetate), 50 g of benzyl benzoate is loaded on each square meter of the polished ceramic tile, standing for 1 day, and testing after the solvent on the surface of the ceramic tile is fully volatilized; the test temperature was 25 degrees and the test humidity was 78%.
The placing positions of the reference ceramic tile and the ceramic tile to be tested are shown in figure 3, the reference ceramic tile is placed in a testing area 1 and a testing area 3, the ceramic tile to be tested is placed in a testing area 2 and a testing area 4, 5 g of cockroach feed is placed on the reference ceramic tile and the ceramic tile to be tested respectively, the feed is framed by a ring with the height of 3 mm, and the ring is located at the center of the ceramic tile; and a water source is placed in the center of the buffer box and is positioned on the central axis of the central connecting line of the ceramic tile to be detected and the control ceramic tile, so that the distance between the water source and the ceramic tile to be detected and the distance between the water source and the control ceramic tile are equal.
50 adult periplaneta americana test insects are placed into a buffer box, vaseline is coated on the inner walls of the buffer box and the test box, timing is started after a first top cover and a second top cover are covered, data for the first time are counted after 15 minutes, the number of the test insects in each test area is recorded, the number of the test insects is recorded for the second time at intervals of 15 minutes, the number of the test insects for 8 times is continuously recorded, and the whole process consumes 120 minutes.
After the test is finished, adding the test insect numbers of the to-be-tested ceramic tile test area and the comparison ceramic tile test area recorded each time, wherein the sum of the test insect numbers of the to-be-tested ceramic tile test area is S1, the sum of the test insect numbers of the comparison ceramic tile test area is S2, and calculating the cockroach prevention index K which is S2/S1.
And repeating the test for three times, and calculating the average value of the cockroach-preventing index K values calculated in each test to obtain the average K value of the cockroach-preventing index of the ceramic tile to be tested.
Example 3
The ceramic tile that awaits measuring that this embodiment adopted does: carrying out cockroach prevention treatment on the same polished ceramic tile as a control ceramic tile, wherein the used cockroach prevention reagent is benzyl benzoate solution (the solvent is ethyl acetate), 50 g of benzyl benzoate is loaded on each square meter of the polished ceramic tile, standing for 1 day, after the solvent on the surface of the ceramic tile is fully volatilized, standing for 1 month in a shady and cool environment at 29 ℃, and then testing; the test temperature was 25 degrees and the test humidity was 79%.
The placing positions of the reference ceramic tile and the ceramic tile to be tested are shown in figure 3, the reference ceramic tile is placed in a testing area 1 and a testing area 3, the ceramic tile to be tested is placed in a testing area 2 and a testing area 4, 5 g of cockroach feed is placed on the reference ceramic tile and the ceramic tile to be tested respectively, the feed is framed by a ring with the height of 3 mm, and the ring is located at the center of the ceramic tile; and a water source is placed in the center of the buffer box and is positioned on the central axis of the central connecting line of the ceramic tile to be detected and the control ceramic tile, so that the distance between the water source and the ceramic tile to be detected and the distance between the water source and the control ceramic tile are equal.
50 adult periplaneta americana test insects are placed into a buffer box, vaseline is coated on the inner walls of the buffer box and the test box, timing is started after a first top cover and a second top cover are covered, data for the first time are counted after 15 minutes, the number of the test insects in each test area is recorded, the number of the test insects is recorded for the second time at intervals of 15 minutes, the number of the test insects for 8 times is continuously recorded, and the whole process consumes 120 minutes.
After the test is finished, adding the test insect numbers of the to-be-tested ceramic tile test area and the comparison ceramic tile test area recorded each time, wherein the sum of the test insect numbers of the to-be-tested ceramic tile test area is S1, the sum of the test insect numbers of the comparison ceramic tile test area is S2, and calculating the cockroach prevention index K which is S2/S1.
And repeating the test for three times, and calculating the average value of the cockroach-preventing index K values calculated in each test to obtain the average K value of the cockroach-preventing index of the ceramic tile to be tested.
Example 4
The ceramic tile that awaits measuring that this embodiment adopted does: carrying out cockroach prevention treatment on the same polished ceramic tile as a control ceramic tile, wherein the used cockroach prevention reagent is benzyl benzoate solution (the solvent is ethyl acetate), 2 g of benzyl benzoate is loaded on each square meter of the polished ceramic tile, standing for 1 day, and testing after the solvent on the surface of the ceramic tile is fully volatilized; the test temperature was 25 degrees and the test humidity was 78%.
The placing positions of the reference ceramic tile and the ceramic tile to be tested are shown in figure 3, the reference ceramic tile is placed in a testing area 1 and a testing area 2, the ceramic tile to be tested is placed in a testing area 3 and a testing area 4, 5 g of cockroach feed is placed on the reference ceramic tile and the ceramic tile to be tested respectively, the feed is framed by a ring with the height of 3 mm, and the ring is located at the center of the ceramic tile; and a water source is placed in the center of the buffer box and is positioned on the central axis of the central connecting line of the ceramic tile to be detected and the control ceramic tile, so that the distance between the water source and the ceramic tile to be detected and the distance between the water source and the control ceramic tile are equal.
50 adult periplaneta americana test insects are placed into a buffer box, vaseline is coated on the inner walls of the buffer box and the test box, timing is started after a first top cover and a second top cover are covered, data for the first time are counted after 15 minutes, the number of the test insects in each test area is recorded, the number of the test insects is recorded for the second time at intervals of 15 minutes, the number of the test insects for 8 times is continuously recorded, and the whole process consumes 120 minutes.
After the test is finished, adding the test insect numbers of the to-be-tested ceramic tile test area and the comparison ceramic tile test area recorded each time, wherein the sum of the test insect numbers of the to-be-tested ceramic tile test area is S1, the sum of the test insect numbers of the comparison ceramic tile test area is S2, and calculating the cockroach prevention index K which is S2/S1.
And repeating the test for three times, and calculating the average value of the cockroach-preventing index K values calculated in each test to obtain the average K value of the cockroach-preventing index of the ceramic tile to be tested.
Example 5
The ceramic tile that awaits measuring that this embodiment adopted does: carrying out cockroach prevention treatment on the same polished ceramic tile as a control ceramic tile, wherein the used cockroach prevention reagent is benzyl benzoate solution (the solvent is ethyl acetate), 10 g of benzyl benzoate is loaded on each square meter of the polished ceramic tile, standing for 1 day, after the solvent on the surface of the ceramic tile is fully volatilized, standing for 1 month in a shady and cool environment at 29 ℃, and then testing; the test temperature was 25 degrees and the test humidity was 75%.
The placing positions of the reference ceramic tile and the ceramic tile to be tested are shown in figure 3, the reference ceramic tile is placed in a testing area 1 and a testing area 3, the ceramic tile to be tested is placed in a testing area 2 and a testing area 4, 5 g of cockroach feed is placed on the reference ceramic tile and the ceramic tile to be tested respectively, the feed is framed by a ring with the height of 3 mm, and the ring is located at the center of the ceramic tile; and a water source is placed in the center of the buffer box and is positioned on the central axis of the central connecting line of the ceramic tile to be detected and the control ceramic tile, so that the distance between the water source and the ceramic tile to be detected and the distance between the water source and the control ceramic tile are equal.
50 adult periplaneta americana test insects are placed into a buffer box, vaseline is coated on the inner walls of the buffer box and the test box, timing is started after a first top cover and a second top cover are covered, data for the first time are counted after 15 minutes, the number of the test insects in each test area is recorded, the number of the test insects is recorded for the second time at intervals of 15 minutes, the number of the test insects for 8 times is continuously recorded, and the whole process consumes 120 minutes.
After the test is finished, adding the test insect numbers of the to-be-tested ceramic tile test area and the comparison ceramic tile test area recorded each time, wherein the sum of the test insect numbers of the to-be-tested ceramic tile test area is S1, the sum of the test insect numbers of the comparison ceramic tile test area is S2, and calculating the cockroach prevention index K which is S2/S1.
And repeating the test for three times, and calculating the average value of the cockroach-preventing index K values calculated in each test to obtain the average K value of the cockroach-preventing index of the ceramic tile to be tested.
Example 6
The ceramic tile that awaits measuring that this embodiment adopted does: carrying out cockroach prevention treatment on the same polished ceramic tile as a control ceramic tile, wherein the used cockroach prevention reagent is benzyl benzoate solution (the solvent is ethyl acetate), 50 g of benzyl benzoate is loaded on each square meter of the polished ceramic tile, standing for 1 day, and testing after the solvent on the surface of the ceramic tile is fully volatilized; the test temperature was 25 degrees and the test humidity was 75%.
The placing positions of the reference ceramic tile and the ceramic tile to be tested are shown in figure 3, the reference ceramic tile is placed in a testing area 1 and a testing area 2, the ceramic tile to be tested is placed in a testing area 3 and a testing area 4, 5 g of cockroach feed is placed on the reference ceramic tile and the ceramic tile to be tested respectively, the feed is framed by a ring with the height of 3 mm, and the ring is located at the center of the ceramic tile; and a water source is placed in the center of the buffer box and is positioned on the central axis of the central connecting line of the ceramic tile to be detected and the control ceramic tile, so that the distance between the water source and the ceramic tile to be detected and the distance between the water source and the control ceramic tile are equal.
50 adult periplaneta americana test insects are placed into a buffer box, vaseline is coated on the inner walls of the buffer box and the test box, timing is started after a first top cover and a second top cover are covered, data for the first time are counted after 15 minutes, the number of the test insects in each test area is recorded, the number of the test insects is recorded for the second time at an interval of 5 minutes, the number of the test insects for 8 times is continuously recorded, and the whole process consumes 40 minutes.
After the test is finished, adding the test insect numbers of the to-be-tested ceramic tile test area and the comparison ceramic tile test area recorded each time, wherein the sum of the test insect numbers of the to-be-tested ceramic tile test area is S1, the sum of the test insect numbers of the comparison ceramic tile test area is S2, and calculating the cockroach prevention index K which is S2/S1.
And repeating the test for three times, and calculating the average value of the cockroach-preventing index K values calculated in each test to obtain the average K value of the cockroach-preventing index of the ceramic tile to be tested.
Example 7
The ceramic tile that awaits measuring that this embodiment adopted does: carrying out cockroach prevention treatment on the same polished ceramic tile as a control ceramic tile, wherein the used cockroach prevention reagent is benzyl benzoate solution (the solvent is ethyl acetate), 50 g of benzyl benzoate is loaded on each square meter of the polished ceramic tile, standing for 1 day, and testing after the solvent on the surface of the ceramic tile is fully volatilized; the test temperature was 25 degrees and the test humidity was 75%.
The placing positions of the reference ceramic tile and the ceramic tile to be tested are shown in figure 3, the reference ceramic tile is placed in a testing area 1 and a testing area 2, the ceramic tile to be tested is placed in a testing area 3 and a testing area 4, 5 g of cockroach feed is placed on the reference ceramic tile and the ceramic tile to be tested respectively, the feed is framed by a ring with the height of 3 mm, and the ring is located at the center of the ceramic tile; and a water source is placed in the center of the buffer box and is positioned on the central axis of the central connecting line of the ceramic tile to be detected and the control ceramic tile, so that the distance between the water source and the ceramic tile to be detected and the distance between the water source and the control ceramic tile are equal.
50 adult periplaneta americana test insects are placed into a buffer box, vaseline is coated on the inner walls of the buffer box and the test box, timing is started after a first top cover and a second top cover are covered, data for the first time are counted after 15 minutes, the number of the test insects in each test area is recorded, the number of the test insects is recorded for the second time at intervals of 60 minutes, the number of the test insects for 8 times is continuously recorded, and the time consumed in the whole process is 480 minutes.
After the test is finished, adding the test insect numbers of the to-be-tested ceramic tile test area and the comparison ceramic tile test area recorded each time, wherein the sum of the test insect numbers of the to-be-tested ceramic tile test area is S1, the sum of the test insect numbers of the comparison ceramic tile test area is S2, and calculating the cockroach prevention index K which is S2/S1.
And repeating the test for three times, and calculating the average value of the cockroach-preventing index K values calculated in each test to obtain the average K value of the cockroach-preventing index of the ceramic tile to be tested.
Example 8
The ceramic tile that awaits measuring that this embodiment adopted does: carrying out cockroach prevention treatment on the same polished ceramic tile as a control ceramic tile, wherein the used cockroach prevention reagent is benzyl benzoate solution (the solvent is ethyl acetate), 50 g of benzyl benzoate is loaded on each square meter of the polished ceramic tile, standing for 1 day, and testing after the solvent on the surface of the ceramic tile is fully volatilized; the test temperature was 25 degrees and the test humidity was 75%.
The placing positions of the reference ceramic tile and the ceramic tile to be tested are shown in figure 3, the reference ceramic tile is placed in a testing area 1 and a testing area 2, the ceramic tile to be tested is placed in a testing area 3 and a testing area 4, 5 g of cockroach feed is placed on the reference ceramic tile and the ceramic tile to be tested respectively, the feed is framed by a ring with the height of 3 mm, and the ring is located at the center of the ceramic tile; and a water source is placed in the center of the buffer box and is positioned on the central axis of the central connecting line of the ceramic tile to be detected and the control ceramic tile, so that the distance between the water source and the ceramic tile to be detected and the distance between the water source and the control ceramic tile are equal.
50 adult periplaneta americana test insects are placed into a buffer box, vaseline is coated on the inner walls of the buffer box and the test box, timing is started after a first top cover and a second top cover are covered, data for the first time are counted after 15 minutes, the number of the test insects in each test area is recorded, the number of the test insects is recorded for the second time at intervals of 15 minutes, the number of the test insects for 16 times is continuously recorded, and the whole process takes 240 minutes.
After the test is finished, adding the test insect numbers of the to-be-tested ceramic tile test area and the comparison ceramic tile test area recorded each time, wherein the sum of the test insect numbers of the to-be-tested ceramic tile test area is S1, the sum of the test insect numbers of the comparison ceramic tile test area is S2, and calculating the cockroach prevention index K which is S2/S1.
And repeating the test for three times, and calculating the average value of the cockroach-preventing index K values calculated in each test to obtain the average K value of the cockroach-preventing index of the ceramic tile to be tested.
Example 9
The ceramic tile that awaits measuring that this embodiment adopted does: carrying out cockroach prevention treatment on the same polished ceramic tile as a control ceramic tile, wherein the used cockroach prevention reagent is benzyl benzoate solution (the solvent is ethyl acetate), 50 g of benzyl benzoate is loaded on each square meter of the polished ceramic tile, standing for 1 day, and testing after the solvent on the surface of the ceramic tile is fully volatilized; the test temperature was 25 degrees and the test humidity was 75%.
The placing positions of the reference ceramic tile and the ceramic tile to be tested are shown in figure 3, the reference ceramic tile is placed in a testing area 1 and a testing area 2, the ceramic tile to be tested is placed in a testing area 3 and a testing area 4, 5 g of cockroach feed is placed on the reference ceramic tile and the ceramic tile to be tested respectively, the feed is framed by a ring with the height of 3 mm, and the ring is located at the center of the ceramic tile; and a water source is placed in the center of the buffer box and is positioned on the central axis of the central connecting line of the ceramic tile to be detected and the control ceramic tile, so that the distance between the water source and the ceramic tile to be detected and the distance between the water source and the control ceramic tile are equal.
50 adult periplaneta americana test insects are placed into a buffer box, vaseline is coated on the inner walls of the buffer box and the test box, timing is started after a first top cover and a second top cover are covered, data for the first time are counted after 15 minutes, the number of the test insects in each test area is recorded, the number of the test insects is recorded for the second time at intervals of 15 minutes, the number of the test insects for 4 times is continuously recorded, and the whole process consumes 60 minutes.
After the test is finished, adding the test insect numbers of the to-be-tested ceramic tile test area and the comparison ceramic tile test area recorded each time, wherein the sum of the test insect numbers of the to-be-tested ceramic tile test area is S1, the sum of the test insect numbers of the comparison ceramic tile test area is S2, and calculating the cockroach prevention index K which is S2/S1.
And repeating the test for three times, and calculating the average value of the cockroach-preventing index K values calculated in each test to obtain the average K value of the cockroach-preventing index of the ceramic tile to be tested.
Comparative example 1
The comparative example was tested by the method disclosed in the patent publication (CN 112525756a), and the test procedure and evaluation method were performed according to the disclosure of the patent, and the test time was 7 days.
Evaluation of test results
The results of cockroach-proof index of the tested tiles obtained in examples 1 to 9 are shown in table 1.
Table 1: comparative table of test results of examples 1 to 9
Figure BDA0003381706190000131
As can be seen from table 1, in examples 1 to 9, analysis and study were performed from different angles of the amount of the cockroach-preventing agent loaded on the cockroach-preventing ceramic tile, the sustained-release time of the agent, and the placement position of the ceramic tile, respectively, and the differences of the test results exhibited by the ceramic tile were small, the data fluctuation of the three-time parallel test was also small, the measured values of the cockroach-preventing index K were within the normal test error range, and the reliability was high, and the ceramic tile cockroach-preventing effect evaluation method was suitable for rapid evaluation of the cockroach-preventing effect of the ceramic tile.
Compared with the testing method for the ceramic tile cockroach prevention effect of the comparative example 1, the testing method for the obstacle prevention performance can ensure that the cockroach prevention index K value is stable and the deviation among groups is small, and simultaneously, the testing time is shortened from 7 days (10080 minutes) to 120 minutes, so that the testing time is greatly shortened, the rapid testing of the pesticide effect of the cockroach prevention ceramic tile in a ceramic enterprise can be more satisfied, and even the instant on-line detection of the pesticide effect of the cockroach prevention ceramic tile product is realized.
It should be understood that the above examples are only for clarity of illustration and are not intended to limit the embodiments. Other variations and modifications will be apparent to persons skilled in the art in light of the above description. And are neither required nor exhaustive of all embodiments. And obvious variations or modifications therefrom are intended to be within the scope of the invention.

Claims (10)

1. The utility model provides a testing arrangement of pottery brick cockroach prevention performance which characterized in that, testing arrangement includes:
the upper end of the buffer box is opened;
the upper end of the test box is opened, and the test boxes are arranged on the periphery of the buffer box at equal intervals;
the channel is arranged between the buffer box and the test box and communicated with the buffer box and the test box;
the first top cover and the second top cover are respectively covered on the top of the buffer box and the top of the test box, so that the test device forms a closed space.
2. The apparatus for testing cockroach prevention performance of ceramic tiles according to claim 1, wherein the distance between the center position of each test box and the center position of the buffer box is equal.
3. The ceramic tile cockroach prevention performance test device as claimed in claim 1, wherein the material of the test device is a transparent material.
4. A method for testing the cockroach prevention performance of a ceramic tile, which is characterized by using the device for testing the cockroach prevention performance of the ceramic tile according to any one of claims 1 to 3.
5. The method for testing the cockroach prevention performance of the ceramic tile according to claim 4, characterized by comprising the following steps:
(1) placing a ceramic tile to be tested or a control ceramic tile in the center of each test box, and placing cockroach feed with the same weight on the surface of each ceramic tile to be tested and the surface of each control ceramic tile, wherein the number of the ceramic tiles to be tested is equal to that of the control ceramic tiles;
(2) placing a plurality of cockroach test insects in the buffer box, and covering a first top cover and a second top cover;
(3) counting the number of cockroach test insects in the test box corresponding to the to-be-tested ceramic tile, and recording as S1; counting the number of cockroach and insect test in the test box corresponding to the control ceramic tile, and recording as S2;
(4) and calculating an obstacle prevention index K according to the formula K which is S2/S1, and evaluating the obstacle prevention drug effect of the to-be-detected ceramic tile.
6. The method for testing the cockroach prevention performance of the ceramic tile according to claim 5, wherein a water source is placed at the central position of the buffer box.
7. The method for testing the cockroach prevention performance of the ceramic tile according to claim 5, wherein the cockroach test insect is selected from adult periplaneta americana or german cockroach.
8. The method for testing the cockroach-preventing performance of the ceramic tile according to claim 5, wherein in the step (2), the number of the cockroach test insects is not less than 50.
9. The method for testing the cockroach prevention performance of the ceramic tile according to claim 5, wherein in the step (3), the statistical method comprises the following steps: counting the number of the cockroach test insects in the test box every 15-60 minutes for 4-16 times, wherein S1 and S2 are the sum of the counted number of each time.
10. The method for testing the cockroach prevention performance of the ceramic tile according to claim 5, wherein the testing method is applicable to an environment temperature of 24-26 ℃ and an environment relative humidity of 70-80%.
CN202111446025.0A 2021-11-29 2021-11-29 Device and method for testing cockroach prevention performance of ceramic tile Pending CN114217016A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202111446025.0A CN114217016A (en) 2021-11-29 2021-11-29 Device and method for testing cockroach prevention performance of ceramic tile

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202111446025.0A CN114217016A (en) 2021-11-29 2021-11-29 Device and method for testing cockroach prevention performance of ceramic tile

Publications (1)

Publication Number Publication Date
CN114217016A true CN114217016A (en) 2022-03-22

Family

ID=80699086

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202111446025.0A Pending CN114217016A (en) 2021-11-29 2021-11-29 Device and method for testing cockroach prevention performance of ceramic tile

Country Status (1)

Country Link
CN (1) CN114217016A (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107182949A (en) * 2017-06-14 2017-09-22 福建师范大学 A kind of test device and its method of testing of insect repellent behavior
CN107247121A (en) * 2017-08-14 2017-10-13 无限极(中国)有限公司 The test device of repellent worm effect
CN112525872A (en) * 2020-11-09 2021-03-19 佛山欧神诺陶瓷有限公司 Ceramic tile anti-mite effect testing method
CN112525756A (en) * 2020-11-11 2021-03-19 佛山欧神诺陶瓷有限公司 Method for testing cockroach prevention effect of ceramic tile

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107182949A (en) * 2017-06-14 2017-09-22 福建师范大学 A kind of test device and its method of testing of insect repellent behavior
CN107247121A (en) * 2017-08-14 2017-10-13 无限极(中国)有限公司 The test device of repellent worm effect
CN112525872A (en) * 2020-11-09 2021-03-19 佛山欧神诺陶瓷有限公司 Ceramic tile anti-mite effect testing method
CN112525756A (en) * 2020-11-11 2021-03-19 佛山欧神诺陶瓷有限公司 Method for testing cockroach prevention effect of ceramic tile

Similar Documents

Publication Publication Date Title
Russo et al. Aggregated seed dispersal by spider monkeys limits recruitment to clumped patterns in Virola calophylla
US10219505B2 (en) Methods and apparatus for surveillance and control of insect vectors
Swisher et al. Fluorescein diacetate hydrolysis as an estimator of microbial biomass on coniferous needle surfaces
Crofton et al. Interlaboratory comparison of motor activity experiments: implications for neurotoxicological assessments
Brown et al. The relationship of habitat quality to group size in Hall's babbler (Pomatostomus halli)
Edwards et al. Avian communities and habitat relationships in South Carolina Piedmont beaver ponds
CN108967437A (en) A kind of pair of the third ring worm ester and Acetamiprid compound synergic insecticide and its application
Mahmoud Ecological investigation, density, infestation rate and control strategy of German cockroach, Blattella germanica (L.) in two hospitals in Ismailia, Egypt
CN108902052A (en) A kind of method of cotten aphid indoor bioassay
Jacas et al. Analysis of a laboratory method to test the effects of pesticides on adult females of Opius concolor (Hym., Braconidae), a parasitoid of the olive fruit fly, Bactrocera oleae (Dip., Tephritidae)
CN114217016A (en) Device and method for testing cockroach prevention performance of ceramic tile
RU2570637C1 (en) Method to detect toxicity of medium by extent of suppression of growth of microorganism test cultures
CN104407125B (en) A kind of method and test kit being suitable for the responsive cotten aphid detection and identification of land for growing field crops cotton planting
CN109221190A (en) A kind of compounded pesticides effectively preventing cotten aphid
Sokolowski et al. Genetic analyses of pupation distance in Drosophila melanogaster
CN112525756A (en) Method for testing cockroach prevention effect of ceramic tile
CN111066734B (en) Red imported fire ant bait field evaluation method
Clements et al. Comparison between defined-area slug traps and other methods of trapping slugs in cereal fields
CN108738950A (en) The biological control method of random tarsonemid
Faucette et al. A three-year study of viable airborne fungi in the North Carolina Zoological Park RJR Nabisco Rocky Coast Alcid Exhibit
Sandhu et al. Evaluation of 10 chemicals for aneuploidy induction in the hexaploid wheat assay
CN201195724Y (en) Tumour cell drug sensitive test compound checker board
Asea et al. Development of greenhouse inoculation procedures for evaluation of partial resistance to Cercospora zeae‐maydis in maize inbreds
CN109142635A (en) A kind of cockroach attractant simulation field efficacy test method
Hebrard Habitat selection in two species of Spizella: a concurrent laboratory and field study

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination