CN1141943C - Production process and product of instant osteocalcium composition - Google Patents
Production process and product of instant osteocalcium composition Download PDFInfo
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- CN1141943C CN1141943C CNB011421061A CN01142106A CN1141943C CN 1141943 C CN1141943 C CN 1141943C CN B011421061 A CNB011421061 A CN B011421061A CN 01142106 A CN01142106 A CN 01142106A CN 1141943 C CN1141943 C CN 1141943C
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- monopteri albi
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Abstract
The present invention belongs to a health care product and the field of special dietary foods, which relates to a production method and a technology for compositions of instant pearl powder, snake bone powder and ell bone powder. Snake bone powder and ell bone powder can not be dissolved in water, full components extracted from snake bone powder and ell bone powder in a modern biochemical method (dual dissolution method) are synthesized into 'instant bone calcium powder' with instant pearl powder, complementary action is performed by containing calcium, protein, etc., and single dietary foods are converted into composite multifunctional solid products. The 'instant bone calcium powder' which can be instantly dissolved in water has the advantages of rich nutrition and convenient eating, and the key point is that the present invention has the advantages of selected product formula, appropriate dosage and simple production method and technology. Eel bone used in raw materials can replace snake bone powder.
Description
(1) technical field
The present invention relates to a kind of health food and preparation method thereof, particularly a kind of instant bone calcium powder composition and method of making the same that contains Margarita (powder), Monopteri albi bone meal and snake bone powder.
(2) background technology
Chinese patent CN1154855A discloses a kind of tonic " Margarita Jin Serpentis essence ", primary raw material is 6 kinds of valuable medicinals such as Margarita, Jin Serpentis, Radix Polygoni Multiflori, and therefrom effective component extracting is a kind of liquid preparation, its raw material and equipment all compare expensive, and canned transportation is inconvenient.CN1056280C discloses a kind of " the preparation of compositions method of snake powder, Testudinis powder ", is the capsule that the powder below 80 orders of Ophidia black snake powder, Agkistrodon halys powder, mountain Testudinis powder composition is filled, and major defect is water insoluble, can not be absorbed fully after taking.CN1262932A discloses " a kind of snake bone product and production method thereof ", is with the cold drying of snake bone process, makes capsule with flavoring agent after the superfine grinding, and calcium wherein is the nonionic state, is difficult for being absorbed, and needs jet mill, and cost is higher.
(3) summary of the invention
The objective of the invention is that prior art products is water insoluble in order to solve, bioavailability is low shortcoming such as is difficult to absorb fully, prepare instant bone calcium powder product and the method for forming by instant Margarita powder, Chinese yellow eel bone meal and snake bone powder and provide a kind of with lactic acid and acid protease associating Hydrolyze method, said composition nutritional labeling water soluble is absorbed easily.
Instant bone calcium powder compositions of the present invention, by weight content is that 60～70% instant Margarita powder, weight content are that 15～20% snake bone powder and weight content are that 15～20% Monopteri albi bone meal is formed, described snake bone powder and Monopteri albi bone meal mix with described instant Margarita powder after lactic acid, acid protease associating hydrolysis, concentrate drying, pulverize the soluble solids preparation.
The preferred version of above-mentioned instant bone calcium powder compositions is: by weight content is that 70% instant Margarita powder, weight content are that 15% snake bone powder and weight content are that 15% Monopteri albi bone meal is formed.
Described instant bone calcium powder preparation of compositions method may further comprise the steps: the preparation of (one) snake bone and Os Monopteri albi aqueous solution
1) powder process: raw material Serpentis, Monopteri albi are put to death, remove internal organs, the peeling fleshing, wash clean in 80-90 ℃ of condition (the best remains on 90 ℃) baking 18 hours down, is snake bone powder and Monopteri albi bone meal with the snake bone and the Os Monopteri albi pulverize separately of described oven dry, it is standby to cross 100 mesh sieves;
2) acidolysis: get described snake bone powder and Monopteri albi bone meal and put reaction pot into, add deionized water with bone meal equivalent, adding concentration is 15% lactic acid hydrolysis when being heated to 70-80 ℃, pH value remains on 3.5-4.5, do not shut down when to reaction pot, bubble not occurring, its bubble is a carbon dioxide, cooling;
3) sour enzyme associating hydrolysis: when the reaction kettle temperature drops to 40-45 ℃, transfer pH to 4.0-4.5, add the acid protease that accounts for raw material weight 1-2%, stir hydrolysis 5 hours, begin to take a morsel " lamp inspection " behind the material filtering, it is qualified that hydrolysis continues to " lamp inspection ", and its qualified standard does not have microgranule or precipitate and transparent at the bottom of for test tube;
4) enzyme denaturing: rising reaction pot temperature continues 0.5-1 hour to 60-65 ℃, removes upper foam impurity and fishy smell, gets the material filtering slagging-off, and filterable material returns reaction pot, and transfers pH to 6.0-6.8, and product at this moment claims " first material "; (2) instant bone calcium powder compositions is synthetic
5) by the prescription required amount instant Margarita powder is slowly added in described " first material ", stir in the time of reinforced, regulate pH to 6.0-6.8;
6) concentrate, discharging, cooling is frozen into crystallization afterwards, stripping and slicing, oven dry is pulverized and is obtained instant bone calcium powder compositions, packing, sterilization, check finished product.
Described instant Margarita powder also can prepare temporarily, directly makes instant Margarita hydrolyzed solution by Margarita powder and adds in the compositions, and the preparation method of instant Margarita hydrolyzed solution is:
A) get a certain amount of Margarita powder and pack in the autoclave, add the water that is four times in Margarita powder weight, mixing, heating kept cooling 1-2 hour under 9-12Mpa and 106-110 ℃ of condition;
B) take autoclave apart, add lactic acid therein, regulate pH to 3.0-4.0, boil under the normal pressure, kept 1-2 hour, stir, remove supernatant foam and fishy smell thereof, filter while boiling.
The beneficial effect of instant bone calcium powder preparation of compositions method of the present invention and products thereof: with lactic acid hydrolysis Monopteri albi bone meal or snake bone powder, can displace 20 various trace elements such as inorganic calcium in the bone meal, zinc, soluble in water; Can obtain multiple polypeptides, aminoacid with acid protease hydrolysis angle glutelin, absorb soon the bioavailability height; Bone meal hydrolysate and Margarita hydrolysate scientific combination play complementary action, have multiple nutritional components; The technology equipment needed thereby is simple, and technical difficulty is little.
(4) description of drawings
Accompanying drawing 1 is the process chart of the instant bone calcium powder of the present invention preparation method of composition
(5) specific embodiment
The prescription of the instant bone calcium powder compositions of the embodiment of the invention is: instant Margarita powder 14Kg, and Monopteri albi bone meal 3Kg, snake bone powder 3Kg adopts commercially available instant Margarita powder.
With reference to accompanying drawing, the technological process of the instant bone calcium powder of the present invention compositions embodiment is as follows:
1) powder process: raw material Serpentis, Monopteri albi are put to death, remove internal organs, the peeling fleshing, whole vertebraes (comprising bone marrow) wash clean is drained, and in air dry oven, baking is 18 hours under 90 ℃ of conditions, the snake bone and the Os Monopteri albi of described oven dry are pulverized in high speed disintegrator respectively, and it is standby to cross 100 mesh sieves;
2) acidolysis: get described snake bone powder and each 3Kg of Monopteri albi bone meal puts reaction pot into, add the 6Kg deionized water, splash into 15% lactic acid hydrolysis when being heated to 80 ℃, pH value remains on 4.5, do not shut down when bubble not occurring to reaction pot, its bubble is a carbon dioxide, cooling;
3) sour enzyme associating hydrolysis: when the reaction kettle temperature drops to 45 ℃, transfer pH to 4.5; add the acid protease that is equivalent to raw material 2%; stir hydrolysis 5 hours; begin to take a morsel " lamp inspection " behind the material filtering; it is qualified that hydrolysis continues to " lamp inspection ", and its qualified standard does not have microgranule or precipitate and transparent at the bottom of for test tube).
4) enzyme denaturing: rising reaction pot temperature to 65 ℃, continue 1 hour, remove upper foam impurity and fishy smell, get the material filtering slagging-off, filterable material returns reaction pot, and transfers pH to 6.0, and material is called " first material " in this moment reaction pot;
5) getting described instant Margarita powder 14Kg adds in the reaction pot and mixes adding sodium bicarbonate, accent pH to 6.0 with " first material ", temperature keeps 60 ℃, and puddle is through concentrating, discharging, cooling is frozen into crystallization, stripping and slicing, oven dry obtains instant bone calcium powder compositions after the pulverizing, packing, the sterilization, the check, put in storage finished product.
The comparison sheet of calcium and protein content in instant bone calcium powder compositions that makes with said method and the instant Margarita powder of raw material, Monopteri albi bone meal, the snake bone powder:
" dragon is precious " instant bone calcium powder of " power good fortune " instant bone calcium powder
Instant Margarita powder Monopteri albi bone meal
Snake bone powder snake bone powder 12 calcium
6.2 6.0 3.2 11.3 15.4 17.2 (g) % protein
1.8 48.1 52.1 53.3 7.8 8.2(g)％
Annotate: " dragon is precious " described in the table, " power good fortune " are manufacturer's titles of described snake bone powder.
As above table as seen: instant bone calcium powder compositions has higher calcium and protein content, calcium in the described instant bone calcium powder compositions is ionic state, protein has been hydrolyzed to polypeptide, amino acid form, absorb easily, be a kind of valuable health product, and the calcium content of other snake bone powder is low, and described calcium and protein are all water insoluble, and nutritional labeling is difficult for being absorbed; The calcium and the protein content that are also shown in Monopteri albi bone meal and snake bone powder are basic identical, so the effect of Monopteri albi bone meal is analogous to the snake bone powder.
Claims (2)
1, a kind of instant bone calcium powder compositions, it is characterized in that: described instant bone calcium powder compositions is that 70% instant Margarita powder, weight content are that 15% snake bone powder and weight content are that 15% Monopteri albi bone meal is formed by weight content, described snake bone powder and Monopteri albi bone meal mix with described instant Margarita powder after lactic acid, acid protease associating hydrolysis, concentrate drying, pulverize the soluble solids preparation.
2, the instant according to claim 1 bone calcium powder of a kind of preparation method for compositions, it is characterized in that described instant bone calcium powder compositions is that 70% instant Margarita powder, weight content are that 15% snake bone powder and weight content are that 15% Monopteri albi bone meal is formed by weight content, and may further comprise the steps: the preparation of (one) snake bone and Os Monopteri albi aqueous solution
1) powder process: raw material Serpentis, Monopteri albi are put to death, remove internal organs, the peeling fleshing, wash clean, baking is 18 hours under 80-90 ℃ of condition, is snake bone powder and Monopteri albi bone meal with the snake bone and the Os Monopteri albi pulverize separately of described oven dry, and it is standby to cross 100 mesh sieves;
2) acidolysis: get described snake bone powder and Monopteri albi bone meal and put reaction pot into, add and the deionized water that mixes bone meal equivalent, splash into concentration when being heated to 70-80 ℃ and be 15% lactic acid hydrolysis, pH value remains on 3.5-4.5, do not shut down when to reaction pot, bubble not occurring, its steam bubble is a carbon dioxide, cooling;
3) sour enzyme associating hydrolysis: transfer pH to 4.0-4.5 when the reaction kettle temperature drops to 40-45 ℃, add the acid protease that accounts for raw material weight 1-2%, stir hydrolysis 5 hours, behind the material filtering that begins to take a morsel " lamp inspection ", it is qualified that hydrolysis continues to " lamp inspection ";
4) enzyme denaturing: rising reaction pot temperature continues 0.5-1 hour to 60-65 ℃, removes upper foam impurity and fishy smell, gets the material filtering slagging-off, and filterable material returns reaction pot, and transfers pH to 6.0-6.8; (2) instant bone calcium powder compositions is synthetic
5) by the prescription required amount instant Margarita powder is slowly added in the described reaction pot, stir in the time of reinforced, regulate pH to 6.0-6.8;
6) concentrate, discharging, cooling is frozen into crystallization, stripping and slicing, oven dry obtains instant bone calcium powder after the pulverizing, packing, sterilization, check finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB011421061A CN1141943C (en) | 2001-09-12 | 2001-09-12 | Production process and product of instant osteocalcium composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB011421061A CN1141943C (en) | 2001-09-12 | 2001-09-12 | Production process and product of instant osteocalcium composition |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1344542A CN1344542A (en) | 2002-04-17 |
| CN1141943C true CN1141943C (en) | 2004-03-17 |
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| Application Number | Title | Priority Date | Filing Date |
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| CNB011421061A Expired - Fee Related CN1141943C (en) | 2001-09-12 | 2001-09-12 | Production process and product of instant osteocalcium composition |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101773249B (en) * | 2010-03-01 | 2012-05-23 | 宋艳 | Method for preparing active peptide calcium from loach and eel bone and sheep placenta |
| CN107893094A (en) * | 2017-11-21 | 2018-04-10 | 常州市阿曼特化工有限公司 | A kind of preparation method of active snake gelatine polypeptide chelate calcium |
| CN108902793A (en) * | 2018-08-26 | 2018-11-30 | 卓小玲 | A kind of preparation method of snakehead enzymolysis liquid |
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2001
- 2001-09-12 CN CNB011421061A patent/CN1141943C/en not_active Expired - Fee Related
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| CN1344542A (en) | 2002-04-17 |
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Granted publication date: 20040317 Termination date: 20100912 |