CN114180935A - Fried alabaster for washing jeans garments and preparation method thereof - Google Patents

Fried alabaster for washing jeans garments and preparation method thereof Download PDF

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Publication number
CN114180935A
CN114180935A CN202111448242.3A CN202111448242A CN114180935A CN 114180935 A CN114180935 A CN 114180935A CN 202111448242 A CN202111448242 A CN 202111448242A CN 114180935 A CN114180935 A CN 114180935A
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parts
fried
grinding
dolomite
stone
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林柄楠
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Fujian Dehua Shuochang Technology Co ltd
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Fujian Dehua Shuochang Technology Co ltd
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Priority to CN202111448242.3A priority Critical patent/CN114180935A/en
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/02Preparing or treating the raw materials individually or as batches
    • C04B33/04Clay; Kaolin
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/02Preparing or treating the raw materials individually or as batches
    • C04B33/13Compounding ingredients
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06BTREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B3/00Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
    • D06B3/10Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427Silicates other than clay, e.g. water glass
    • C04B2235/3463Alumino-silicates other than clay, e.g. mullite
    • C04B2235/3472Alkali metal alumino-silicates other than clay, e.g. spodumene, alkali feldspars such as albite or orthoclase, micas such as muscovite, zeolites such as natrolite
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/44Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
    • C04B2235/442Carbonates

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Dispersion Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Textile Engineering (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention relates to fried snow stone for washing jeans wear and a preparation method thereof, belonging to the technical field of artificial pumice, wherein the fried snow stone comprises the following components in parts by weight: 40-50 parts of kaolin, 20-30 parts of potassium feldspar, 15-25 parts of dolomite, 10-20 parts of pyrophyllite and 80-100 parts of tap water; the preparation method of the fried snow stone comprises the following steps: step 1, preparing mixed particles of potassium feldspar and dolomite; step 2, grinding the mixed particles of the potassium feldspar and the dolomite and the kaolin to prepare fine particle powder; step 3, adding tap water into the fine particle powder, stirring, drying and grinding; step 4, grinding the powder ground in the step 3 and pyrophyllite into powder and roasting to obtain the fried snowflake; the fried snow stone solves the problems of more waste residues, poor environmental protection, high cost and the like generated after the traditional fried snowflake washing process.

Description

Fried alabaster for washing jeans garments and preparation method thereof
Technical Field
The invention belongs to the technical field of artificial pumice, and particularly relates to fried snow stone for washing jeans garments and a preparation method thereof.
Background
The cloth needs to be washed after dyeing, so that the dyed cloth is not easy to fade, and meanwhile, the process also needs to use a stone, namely washing stone. The effect of the clothes washed by the water stone with different types is different, and especially the effect of the jeans clothes is more obvious.
The traditional snowflake frying and washing process comprises the following steps: soaking the dried pumice with a potassium permanganate solution, airing the soaked pumice, polishing the pumice loaded with potassium permanganate and the fabric, oxidizing the dye at the friction point by the potassium permanganate to ensure that the fabric surface is irregularly faded to form a white effect similar to flying snowflakes, fishing out the finished fabric, and then putting the fabric into a washing machine for cleaning and drying; however, the traditional snowflake frying and water washing method has the following problems:
(1) before cleaning and drying, the pumice stones in the fabric pocket need to be completely removed, and the labor time is much;
(2) the residue of pumice stone abrasion is present in the gaps of the fabric;
(3) the metal in the pumice stone is difficult to detect by a metal needle checking machine.
The existing textile such as jeans wear or cloth is generally subjected to water washing treatment, and the textile subjected to the water washing treatment is bright in color, soft in texture and comfortable. The existing textile washing needs to consume a large amount of natural pumice, the textile contains a large amount of broken stones and slurry after the natural pumice washing, the broken stones and the slurry can be removed through rinsing for many times, the discharged slurry water causes great pressure on the treatment of later-stage water and environmental pollution, and meanwhile, manpower and material resources are increased.
Disclosure of Invention
The invention provides a fried snow stone for washing jeans, aiming at the problems of more waste residues, poor environmental protection, high cost and the like generated after washing jeans in the prior art, and the fried snow stone comprises the following components in parts by weight: 40-50 parts of kaolin, 20-30 parts of potassium feldspar, 15-25 parts of dolomite, 10-20 parts of pyrophyllite and 80-100 parts of tap water.
Further, the components of the fried snow stone are respectively as follows according to the parts by weight: 45 parts of kaolin, 25 parts of potassium feldspar, 20 parts of dolomite, 15 parts of pyrophyllite and 90 parts of tap water.
The invention also provides a preparation method of the fried snow stone for washing jeans wear, which comprises the following steps:
step 1, preparing mixed particles of potassium feldspar and dolomite:
step 1.1, conveying 25 parts of potassium feldspar and 20 parts of dolomite into a rotary kiln through a conveying belt, and rotating the rotary kiln to obtain a raw material mixture;
step 1.2, carrying out initial preheating on the raw material mixture obtained by the rotary kiln at the temperature of 400 ℃ for 5 hours;
step 1.3, introducing high-temperature gas of 1000 ℃ into a rotary kiln to calcine the raw material mixture obtained in the step 1.2 for 2 hours;
step 1.4, discharging the calcined raw material mixture and naturally cooling to obtain a first grinding material;
step 1.5, putting a first grinding material into the vertical ball mill, wherein the weight ratio of the first grinding material to the ball-milled particles is 5: 15, carrying out dry ball milling to obtain mixed particles of potassium feldspar and dolomite with the diameter of 1-10 mu m;
step 2, grinding the mixed particles of the potassium feldspar and the dolomite and preparing fine particle powder from the kaolin:
step 2.1, weighing 20 parts of mixed particles of potassium feldspar and dolomite and 45 parts of kaolin, putting the mixture into a planetary ball mill, and carrying out mechanical ball milling for 3 hours to obtain coarse particle powder;
step 2.2, screening out coarse particle powder of 180 meshes, and drying the coarse particle powder in a dryer for 1.5 hours;
step 2.3, placing the dried coarse particle powder into a high-temperature furnace for heat treatment at 750 ℃ for 2.5 hours;
step 2.4, continuously putting the coarse particle powder after heat treatment into a planetary ball mill for ball milling for 3 hours, and screening out fine particle powder of 400 meshes;
step 3, adding tap water into the fine particle powder, stirring, drying and grinding:
step 3.1, putting the fine particle powder of 400 meshes into a stirrer, adding 90 parts of tap water into the stirrer, and stirring for 30min to obtain slurry;
step 3.2, drying the slurry in an oven at the temperature of 60 ℃ for 3.5 h;
step 3.3, raising the temperature of the oven to 90 ℃, continuously drying, and taking out the materials in the oven after drying for 1 h;
step 3.4, cooling the material in a cooling device until the cooling temperature is 20 ℃;
step 3.5, putting the cooled material into a grinder for grinding, and screening 600-mesh powder;
step 4, grinding the powder ground in the step 3 and pyrophyllite into powder and roasting to obtain the fried snowflake:
step 4.1, putting 600-mesh powder and 15 parts of pyrophyllite into a Raymond pulverizer for pulverizing;
step 4.2, performing magnetic separation on the ground mineral ores to remove iron impurities;
step 4.3, adding 2L of purified water into the magnetically-separated mineral materials, stirring until 8-10% of water is absorbed, and stopping stirring;
4.4, roasting the stirred mineral materials at the low temperature of 400-600 ℃ for 30-60 min;
and 4.5, roasting the mineral material subjected to low-temperature roasting at the high temperature of 950-1050 ℃ for 30-60 min to obtain the fried alabaster.
Further, in the step 2.1, the rotating speed of the ball mill is 350-400 r/min, the diameter of the ball mill is 2-10 mm, and the ball mill is switched to rotate once every 10-15 min.
Further, in step 3.4, the cooling device is a cooler, and the cooling rate of the cooling device is 30-35 ℃/min.
Further, in the step 4.5, the mass ratio of the fried snow stone to the jeans wear is 150-200 g: 600-800 g, and the time for frying the cedarwood is 30-45 min.
Compared with the prior art, the invention has the beneficial effects that:
1. the fried snowflake stones are not easy to be stained on jeans garments, residual components are removed without rinsing with clear water for multiple times, the number of times of rinsing is reduced, and water resources are saved.
2. The method for frying the snowflake without frequently cleaning the ditch and the sewage sedimentation tank saves the cost of manpower and material resources.
3. The washing time of the fried snowflake stones is 30-45 min, so that the washing quality of the jeans wear is improved.
4. The weight of the fried snow stone is 3-15 g, and the color is at least one of gray, white, off-white and beige.
Drawings
FIG. 1 is a schematic view of the structure of the fried snowflake according to the present invention.
Detailed Description
The stir-fried snowflake according to the present invention and the preparation method thereof will be further explained with reference to the drawings of the specification.
The invention provides a fried snow stone for washing jeans wear, which comprises the following components in parts by weight: 40-50 parts of kaolin, 20-30 parts of potassium feldspar, 15-25 parts of dolomite, 10-20 parts of pyrophyllite and 80-100 parts of tap water.
Further, the components of the fried snow stone are respectively as follows according to the parts by weight: 45 parts of kaolin, 25 parts of potassium feldspar, 20 parts of dolomite, 15 parts of pyrophyllite and 90 parts of tap water.
The invention also provides a preparation method of the fried snow stone for washing jeans wear, which comprises the following steps as shown in figure 1:
step 1, preparing mixed particles of potassium feldspar and dolomite:
step 1.1, conveying 25 parts of potassium feldspar and 20 parts of dolomite into a rotary kiln through a feeding conveyor belt, and rotating the rotary kiln to obtain a raw material mixture;
step 1.2, carrying out initial preheating on the raw material mixture obtained by the rotary kiln at the temperature of 400 ℃ for 5 hours;
step 1.3, introducing high-temperature gas of 1000 ℃ into a rotary kiln to calcine the raw material mixture obtained in the step 1.2 for 2 hours;
step 1.4, discharging the calcined raw material mixture and naturally cooling to obtain a first grinding material;
step 1.5, putting a first grinding material into the vertical ball mill, wherein the weight ratio of the first grinding material to the ball-milled particles is 5: 15, carrying out dry ball milling to obtain mixed particles of potassium feldspar and dolomite with the diameter of 1-10 mu m;
step 2, grinding the mixed particles of the potassium feldspar and the dolomite and preparing fine particle powder from the kaolin:
step 2.1, weighing 20 parts of mixed particles of potassium feldspar and dolomite and 45 parts of kaolin, putting the mixture into a planetary ball mill, and carrying out mechanical ball milling for 3 hours to obtain coarse particle powder;
step 2.2, screening out coarse particle powder of 180 meshes, and drying the coarse particle powder in a dryer for 1.5 hours;
step 2.3, placing the dried coarse particle powder into a high-temperature furnace for heat treatment at 750 ℃ for 2.5 hours;
step 2.4, continuously putting the coarse particle powder after heat treatment into a planetary ball mill for ball milling for 3 hours, and screening out fine particle powder of 400 meshes;
step 3, adding tap water into the fine particle powder, stirring, drying and grinding:
step 3.1, putting the fine particle powder of 400 meshes into a stirrer, adding 90 parts of tap water into the stirrer, and stirring for 30min to obtain slurry;
step 3.2, drying the slurry in an oven at the temperature of 60 ℃ for 3.5 h;
step 3.3, raising the temperature of the oven to 90 ℃, continuously drying, and taking out the materials in the oven after drying for 1 h;
step 3.4, cooling the material in a cooling device until the cooling temperature is 20 ℃;
step 3.5, grinding the cooled material in a grinder, and screening 600-mesh powder;
step 4, grinding the powder ground in the step 3 and pyrophyllite into powder and roasting to obtain the fried snowflake:
step 4.1, putting 600-mesh powder and 15 parts of pyrophyllite into a Raymond pulverizer for pulverizing;
step 4.2, carrying out magnetic separation on the ground mineral ores to remove iron impurities;
step 4.3, adding 2L of purified water into the magnetically-separated mineral materials, stirring until 8-10% of water is absorbed, and stopping stirring;
4.4, roasting the stirred mineral materials at the low temperature of 400-600 ℃ for 30-60 min;
and 4.5, roasting the mineral material roasted at the low temperature at 950-1050 ℃ for 30-60 min to obtain the fried alabaster.
Further, in the step 2.1, the rotating speed of the ball mill is 350-400 r/min, the diameter of the ball mill is 2-10 mm, and the ball mill is switched to rotate once every 10-15 min.
Further, in step 3.4, the cooling device is a cooler, and the cooling rate of the cooling device is 30-35 ℃/min.
Further, in the step 4.5, the mass ratio of the fried snow stone to the jeans wear is 150-200 g: 600-800 g, and the time for frying the cedarwood is 30-45 min.
Finally, it should be understood that the above-mentioned embodiments are merely preferred embodiments of the present invention, and not intended to limit the present invention, and any modifications, equivalents and improvements made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (10)

1. The fried snow stone for washing jeans wear is characterized by comprising the following components in parts by weight: 40-50 parts of kaolin, 20-30 parts of potassium feldspar, 15-25 parts of dolomite, 10-20 parts of pyrophyllite and 80-100 parts of tap water.
2. The fried snowflake stone for washing jeans wear according to claim 1, which is characterized by comprising the following components in parts by weight: 45 parts of kaolin, 25 parts of potassium feldspar, 20 parts of dolomite, 15 parts of pyrophyllite and 90 parts of tap water.
3. A method for preparing the fried snowflake stone for washing the jeans wear as claimed in claim 1, comprising the following steps:
step 1, preparing mixed particles of potassium feldspar and dolomite;
step 2, grinding the mixed particles of the potassium feldspar and the dolomite and the kaolin to prepare fine particle powder;
step 3, adding tap water into the fine particle powder, stirring, drying and grinding;
and 4, grinding the powder ground in the step 3 and the pyrophyllite into powder and roasting to obtain the fried snowflake.
4. The method for preparing fried snow stone for washing jeans wear according to claim 3, wherein the step 1 of preparing the mixed particles of potassium feldspar and dolomite comprises the following steps:
step 1.1, conveying 25 parts of potassium feldspar and 20 parts of dolomite into a rotary kiln through a feeding conveyor belt, and rotating the rotary kiln to obtain a raw material mixture;
step 1.2, carrying out initial preheating on the raw material mixture obtained by the rotary kiln at the temperature of 400 ℃ for 5 hours;
step 1.3, introducing high-temperature gas of 1000 ℃ into a rotary kiln to calcine the raw material mixture obtained in the step 1.2 for 2 hours;
step 1.4, discharging the calcined raw material mixture and naturally cooling to obtain a first grinding material;
step 1.5, putting a first grinding material into the vertical ball mill, wherein the weight ratio of the first grinding material to the ball-milled particles is 5: 15, carrying out dry ball milling to obtain mixed particles of the potassium feldspar and the dolomite with the diameter of 1-10 mu m.
5. The method for preparing fried snow stone for washing jeans wear according to claim 3, wherein the step 2 of grinding the mixed particles of potassium feldspar and dolomite and kaolin to prepare fine particle powder comprises the following steps:
step 2.1, weighing 20 parts of mixed particles of potassium feldspar and dolomite and 45 parts of kaolin, putting the mixture into a planetary ball mill, and carrying out mechanical ball milling for 3 hours to obtain coarse particle powder;
step 2.2, screening out coarse particle powder of 180 meshes, and drying the coarse particle powder in a dryer for 1.5 hours;
step 2.3, placing the dried coarse particle powder into a high-temperature furnace for heat treatment at 750 ℃ for 2.5 hours;
and 2.4, continuously putting the coarse particle powder after heat treatment into a planetary ball mill for ball milling for 3 hours, and screening out fine particle powder of 400 meshes.
6. The method for preparing fried snowflake stone for washing jeans wear according to claim 3, wherein the step 3 of adding tap water into the fine particle powder, stirring, drying and grinding comprises the following steps:
step 3.1, putting the fine particle powder of 400 meshes into a stirrer, adding 90 parts of tap water into the stirrer, and stirring for 30min to obtain slurry;
step 3.2, drying the slurry in an oven at the temperature of 60 ℃ for 3.5 h;
step 3.3, raising the temperature of the oven to 90 ℃, continuously drying, and taking out the materials in the oven after drying for 1 h;
step 3.4, cooling the material in a cooling device until the cooling temperature is 20 ℃;
and 3.5, grinding the cooled material in a grinder, and screening out 600-mesh powder.
7. The method for preparing fried snow stone for washing jeans wear according to claim 3, wherein the step 4 of grinding the powder ground in the step 3 and pyrophyllite into powder and roasting comprises the following steps:
step 4.1, putting 600-mesh powder and 15 parts of pyrophyllite into a Raymond pulverizer for pulverizing;
step 4.2, carrying out magnetic separation on the ground mineral ores to remove iron impurities;
step 4.3, adding 2L of purified water into the magnetically-separated mineral materials, stirring until 8-10% of water is absorbed, and stopping stirring;
4.4, roasting the stirred mineral materials at the low temperature of 400-600 ℃ for 30-60 min;
and 4.5, roasting the mineral material roasted at the low temperature at 950-1050 ℃ for 30-60 min to obtain the fried alabaster.
8. The preparation method of the fried snowflake stone for washing jeans wear is characterized in that in the step 2.1, the rotating speed of the ball mill is 350-400 r/min, the diameter of the ball mill is 2-10 mm, and the ball mill is switched to rotate once every 10-15 min.
9. The method for preparing fried snowflake stone for washing jeans wear according to claim 6, wherein in the step 3.4, the cooling device is a cooler, and the cooling rate of the cooling device is 30-35 ℃/min.
10. The preparation method of the fried snow stone for washing jeans wear according to claim 7, wherein in the step 4.5, the mass ratio of the fried snow stone to the jeans wear is 150-200 g: 600-800 g, and the time for frying the cedarwood is 30-45 min.
CN202111448242.3A 2021-11-30 2021-11-30 Fried alabaster for washing jeans garments and preparation method thereof Pending CN114180935A (en)

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CN202111448242.3A CN114180935A (en) 2021-11-30 2021-11-30 Fried alabaster for washing jeans garments and preparation method thereof

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Application Number Priority Date Filing Date Title
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2730875Y (en) * 2004-06-04 2005-10-05 林柄楠 Ceramic washed-granolithic
CN1762910A (en) * 2005-09-02 2006-04-26 何晓洪 Lightweight environment-friendly type pumice for ceramic ware and its production method and usage
CN201074209Y (en) * 2007-02-12 2008-06-18 林柄楠 Washing float stone for ceramic products
CN101880608A (en) * 2010-06-28 2010-11-10 深圳市成为生物科技有限公司 Natural solid cleaning agent
CN105153861A (en) * 2015-09-12 2015-12-16 宁波申泰干粉建材有限公司 Self-cleaning water-resistant paint and preparation method thereof
CN110787184A (en) * 2019-12-03 2020-02-14 平措绕吉 Method for processing alabaster
CN113402296A (en) * 2021-06-11 2021-09-17 福建省德化硕昌科技有限公司 Artificial ceramic pumice and preparation method thereof

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2730875Y (en) * 2004-06-04 2005-10-05 林柄楠 Ceramic washed-granolithic
CN1762910A (en) * 2005-09-02 2006-04-26 何晓洪 Lightweight environment-friendly type pumice for ceramic ware and its production method and usage
CN201074209Y (en) * 2007-02-12 2008-06-18 林柄楠 Washing float stone for ceramic products
CN101880608A (en) * 2010-06-28 2010-11-10 深圳市成为生物科技有限公司 Natural solid cleaning agent
CN105153861A (en) * 2015-09-12 2015-12-16 宁波申泰干粉建材有限公司 Self-cleaning water-resistant paint and preparation method thereof
CN110787184A (en) * 2019-12-03 2020-02-14 平措绕吉 Method for processing alabaster
CN113402296A (en) * 2021-06-11 2021-09-17 福建省德化硕昌科技有限公司 Artificial ceramic pumice and preparation method thereof

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