CN114158892A - Health-care silkworm excrement pillow and preparation method thereof - Google Patents

Health-care silkworm excrement pillow and preparation method thereof Download PDF

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Publication number
CN114158892A
CN114158892A CN202111606736.XA CN202111606736A CN114158892A CN 114158892 A CN114158892 A CN 114158892A CN 202111606736 A CN202111606736 A CN 202111606736A CN 114158892 A CN114158892 A CN 114158892A
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China
Prior art keywords
silkworm excrement
pillow
health
silk fabric
care
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CN202111606736.XA
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Chinese (zh)
Inventor
朱昱霖
张立新
潘世俊
梅德祥
石继均
胡小明
盛家镛
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Jiangsu Xinyuan Silk Technology Co ltd
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Jiangsu Xinyuan Silk Technology Co ltd
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Priority to CN202111606736.XA priority Critical patent/CN114158892A/en
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    • AHUMAN NECESSITIES
    • A47FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
    • A47GHOUSEHOLD OR TABLE EQUIPMENT
    • A47G9/00Bed-covers; Counterpanes; Travelling rugs; Sleeping rugs; Sleeping bags; Pillows
    • A47G9/10Pillows

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  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Otolaryngology (AREA)
  • Pulmonology (AREA)
  • Bedding Items (AREA)

Abstract

The invention discloses a health-care silkworm excrement pillow and a preparation method thereof. Mixing opal, a dispersing agent, silane and water to obtain a finishing liquid, then soaking the real silk fabric in the finishing liquid, heating and oscillating, taking out, washing and drying to obtain a finished real silk fabric; filling silkworm excrement into the finished silk fabric, sewing to obtain silkworm excrement bags, filling the silkworm excrement bags and the fillers into the pillowcase, and sewing to obtain the health-care silkworm excrement pillow. The invention adopts the existing pillow structure and has the health care function.

Description

Health-care silkworm excrement pillow and preparation method thereof
Technical Field
The invention belongs to the technology of health-care household articles, and particularly relates to a health-care silkworm excrement pillow and a preparation method thereof.
Background
Silkworm excrement, namely silkworm excrement, granular chlorophyll crystals, are sweet in taste, warm in nature and non-toxic, the medicinal value of the silkworm excrement is highly evaluated in compendium of materia medica, and the silkworm excrement and the granular chlorophyll crystals are widely used in modern Chinese medicine for treating diseases such as borborygmus, anemogenous arthritis and urticaria. In the prior art, silkworm excrement is cleaned and dried in the sun, and then is sewn into a pillow case to form the silkworm excrement pillow, and Chinese herbal medicines and buckwheat are adopted to assist filling at most. The prior art discloses a medicinal composition for a health-care pillow and a silk traditional Chinese medicine cervical vertebra health-care pillow, wherein silk, silkworm excrement, wild chrysanthemum flower, notopterygium root, calcined magnetite, borneol, albizia flower, tuber fleeceflower stem, grassleaf sweelflag rhizome, flos caryophyllata, sandalwood, dragon bone, oyster shell, ricepaperplant pith, radix angelicae, safflower, chicken bone essence, ligusticum wallichii, cassia twig, magnolia obavata, rhizoma atractylodis and kudzu root powder are used in the health-care pillow, and when the health-care pillow is used, the effective ingredients of the medicines in the pillow are slowly diffused by the head temperature and the pressure of the head, and the medicines breathe into the lung, enter the blood circulation and are distributed to the whole body. The prior art discloses a radiation-proof double-sided health care pillow, which consists of a pillowcase and a pillow core; the pillow core is divided into four parts, the middle part of the pillow core is divided into an upper layer and a lower layer, the surface layers on the two sides of the pillow core are made of radiation-proof materials, and the upper layer and the lower layer are isolated and protected; the upper layer and the lower layer of the pillow core are respectively provided with two medicine bag pockets, and a connecting isolation layer is arranged between the two medicine bag pockets. The prior art discloses a light awakening health care pillow, which comprises: the novel pillow comprises a pillow support, a pillow outer cover, a control circuit, a flexible protective shell, a light-emitting assembly, a vibration motor, a filler and a medicine bag, wherein the pillow outer cover is sleeved on the pillow support, the control circuit is connected with the light-emitting assembly and the vibration motor, the control circuit is arranged in the flexible protective shell, the light-emitting assembly and the vibration motor are arranged in the pillow support, and the filler and the medicine bag are further arranged in the pillow support. The applicant previously discloses an expanded silk floss pillow and a preparation method thereof, wherein a mixed solution of turmeric extract, acetic acid and carboxymethyl cellulose is added into a degummed silk fibroin fiber solution for ultrasonic treatment, and then polyurea formaldehyde and selenocysteine hydrochloride are added for ultrasonic treatment; then dehydrating and drying in the sun to obtain the treated silk; heating the treated silk to obtain silk with holes; preparing silk with holes into a silk floss sheet, and then soaking the silk floss sheet in an amino polyethylene glycol aqueous solution to obtain a treated silk floss sheet; placing the treated silk floss sheet into a rotary closed container with a rupture membrane for swelling to obtain a wet swelling silk floss sheet; dehydrating the expanded wet silk floss sheet, manually loosening and drying to obtain an expanded dry silk floss sheet; combining the dry silk floss sheet with cotton cloth bag wrapped with faeces Bombycis, and sewing to obtain the expanded silk floss pillow with silk floss as main material. The concept of negative ions and the effect thereof have been disclosed for a long time, and besides the natural oxygen bar, some inorganic materials capable of generating negative ions are also applied to daily life, so that the report of matching the silkworm excrement pillow with the negative ions is not seen so far.
Disclosure of Invention
The invention adopts the prior silkworm excrement pillow structure, depends on mature silk products and commercially available opals, realizes the effect of improving the attachment of the opals by a dipping finishing method, has the function of releasing anions, and has the health-care function.
The invention adopts the following technical scheme:
a health pillow containing faeces Bombycis comprises faeces Bombycis bag, filler and pillowcase, wherein the faeces Bombycis bag and filler are located in the pillowcase to form health pillow containing faeces Bombycis; the silkworm excrement bag is composed of a finished silk fabric and silkworm excrement wrapped by the same; the finished silk fabric is finished by opal.
According to the invention, opal, a dispersing agent, silane and water are mixed to obtain a finishing liquid, then the real silk fabric is soaked in the finishing liquid, heated and oscillated, then taken out, washed and dried to obtain the finished real silk fabric. Preferably, the dispersant is an ethoxylated nonionic Fluorocarbon Surfactant (FSO); the silane is KH 792; the mass ratio of the opal to the dispersant to the silane to the water is (1.5-2) to (0.5-0.8) to (0.3-0.5) to 100.
In the invention, the real silk fabric is soaked in finishing liquor, and the bath ratio is 1: 30-50; the heating and oscillating temperature is 40-60 ℃, and the time is 30-90 minutes.
In the present invention, the filler is the existing filling fiber, such as high-elasticity PET; the volume ratio of the silkworm excrement bag and the filler is not particularly limited and is determined according to the designed silkworm excrement pillow structure; the pillow cover is made of conventional material, such as cotton cloth.
The applicant specializes in the research, development, production and sale of improved silkworm breeding, silk production, silk spinning, silk dress home textile, silk culture originality, comprehensive utilization of silkworm cocoon silk resources and the like, and the silkworm excrement pillow is widely known as a silkworm breeding industry byproduct, and has an improved physical therapy effect according to the reports of the existing documents. According to the invention, the silkworm excrement is used as the core, the silkworm excrement pillow is prepared by combining the filler, and the silkworm excrement is wrapped by the real silk fabric finished by the opal, so that the negative ion effect can be introduced, the effect exertion capability of the silkworm excrement is improved, and the health care effect can be achieved by combining the negative ion.
Detailed Description
The raw materials of the invention are commercial products, and the specific experimental operation and the testing method are the existing methods. Most suitable for preparing silkworm excrement health care pillow of 3-4 years old, when collecting silkworm excrement, lift the silkworm net, sieve the mulberry leaf branch and stem, leafstalk and silkworm excrement that the silkworm eats and separate, the silkworm excrement of sunning, until the silkworm excrement is pinched by hand and indeformable, then the winnowing, remove impurity such as ash powder in the silkworm excrement tentatively, then rinse, dry in the sun again, obtain the silkworm excrement for pillow, specifically the conventional technology.
Opals are existing products, are found in great Khingan and Yangtze river basin of Heilongjiang province in China, are used as negative ion additives for preparing rubber and plastic materials, fiber fabrics and paint coatings releasing negative ions, the prior art directly uses micron-sized opals, and the invention is also a commercially available product and is directly used for finishing silk fabrics; the silk fabric is mulberry silk fabric without after-treatment. The pillow structure of silkworm excrement in the following examples is consistent, and the volume ratio of silkworm excrement bag to high-elasticity PET is about 2: 3; stitching is a conventional technique.
Example one
Mixing opal, a dispersing agent FSO-100, silane KH792 and water to obtain a finishing liquid, then soaking 1Kg of real silk fabric in the finishing liquid at a bath ratio of 1: 40, heating and oscillating at 50 ℃ for 1 hour (80 rpm), taking out and washing, soaking in the finishing liquid, heating and oscillating at 50 ℃ for 1 hour (120 rpm), taking out, washing and drying to obtain the finished real silk fabric; the mass ratio of the opal to the dispersant to the silane to the water is 2: 0.6: 0.5: 100; the chemical structural formula of KH792 is as follows:
Figure 191597DEST_PATH_IMAGE001
filling silkworm excrement into a finished silk fabric, sewing to obtain silkworm excrement bags, filling the three silkworm excrement bags and high-elasticity PET into a pillowcase, and sewing to obtain the health silkworm excrement pillow. The negative ion tester is adopted to test the edges (six)Point position) of the ion source, and the quantity of the negative ions reaches 1380-1420/cm3
Comparative example
Mixing opal, a dispersing agent FSO-100, silane KH792 and water to obtain a finishing liquid, then soaking 1Kg of cotton fabric (not finished) in the finishing liquid at a bath ratio of 1: 40, heating and oscillating at 50 ℃ for 1 hour (80 rpm), taking out for washing, soaking in the finishing liquid again, heating and oscillating at 50 ℃ for 1 hour (120 rpm), taking out for washing and drying to obtain a finished cotton fabric; the mass ratio of the opal to the dispersant to the silane to the water is 2: 0.6: 0.5: 100. Filling silkworm excrement into a finished cotton fabric, sewing to obtain silkworm excrement bags, filling the three silkworm excrement bags and high-elasticity PET into a pillowcase, and sewing to obtain a health silkworm excrement pillow; the anion tester is adopted to test the anion amount of the edge (six point positions) of the back cushion, and the anion amount reaches 940-990/cm3
Example two
Mixing opal, a dispersant Tween 80, silane KH792 and water to obtain a finishing liquid, then soaking 1Kg of real silk fabric in the finishing liquid at a bath ratio of 1: 40, heating and oscillating at 50 ℃ for 1 hour (80 rpm), taking out and washing, soaking in the finishing liquid, heating and oscillating at 50 ℃ for 1 hour (120 rpm), taking out and washing, and drying to obtain a finished real silk fabric; the mass ratio of the opal to the dispersant to the silane to the water is 2: 0.6: 0.5: 100. And (3) filling silkworm excrement into the finished silk fabric, sewing to obtain silkworm excrement bags, filling the three silkworm excrement bags and high-elasticity PET into the pillow case, and sewing to obtain the health-care silkworm excrement pillow, wherein the anion amount is lower than that in the first embodiment.
EXAMPLE III
Mixing opal, a dispersing agent FSO-100, silane KH792 and water to obtain a finishing liquid, then soaking 1Kg of real silk fabric in the finishing liquid at a bath ratio of 1: 35, heating and oscillating at 40 ℃ for 1 hour (90 rpm), taking out and washing, soaking in the finishing liquid, heating and oscillating at 50 ℃ for 1 hour (100 rpm), taking out, washing and drying to obtain the finished real silk fabric; the mass ratio of the opal to the dispersant to the silane to the water is 1.8: 0.6: 0.4: 100; filling silkworm excrement into a finished silk fabric, sewing to obtain silkworm excrement bags, filling the three silkworm excrement bags and high-elasticity PET into a pillowcase, and sewing to obtain the health silkworm excrement pillow.
In practical use, silkworm excrement rubs the fabric, opal falls off or gathers, negative ions of the silkworm excrement can be influenced, the silkworm excrement pillow in the embodiment I and the silkworm excrement pillow in the embodiment II are placed on a vibration table, slightly vibrate, simulate small actions such as turning over and the like, after 100 hours, a negative ion tester is used for testing the quantity of the negative ions at the edge (six points), and according to the average value, the silkworm excrement pillow retention rate in the embodiment I is 99.87% and the silkworm excrement pillow retention rate in the embodiment II is 98.61% on the basis of the value before vibration testing. The simulation test shows that the product of the first embodiment is better and can be used for a long time in practical application, and the silkworm excrement pillow does not detect harmful substances, so that the silkworm excrement pillow is simple to process and excellent in performance.

Claims (10)

1. A health pillow containing faeces Bombycis comprises faeces Bombycis bag, filler and pillowcase, wherein the faeces Bombycis bag and filler are located in the pillowcase, and is characterized in that the faeces Bombycis bag is composed of finished silk fabric and faeces Bombycis wrapped by the fabric; the finished silk fabric is finished by opal.
2. The pillow of claim 1, wherein the pillow comprises faeces Bombycis bag, filler and pillowcase.
3. The health-care silkworm excrement pillow as claimed in claim 1, wherein the opal, the dispersing agent, the silane and the water are mixed to obtain a finishing liquid, then the real silk fabric is soaked in the finishing liquid, heated and oscillated, taken out, washed and dried to obtain the finished real silk fabric.
4. The pillow of claim 3, wherein the dispersant is an ethoxylated nonionic fluorocarbon surfactant.
5. A health pillow containing faeces Bombycis as claimed in claim 3, wherein the silane is KH 792.
6. The health-care silkworm excrement pillow as claimed in claim 3, wherein the mass ratio of the opal to the dispersing agent to the silane to the water is (1.5-2) to (0.5-0.8) to (0.3-0.5) to 100.
7. The preparation method of the health-care silkworm excrement pillow as claimed in claim 1, wherein opal, dispersing agent, silane and water are mixed to obtain finishing liquid, then the real silk fabric is soaked in the finishing liquid, heated and oscillated, taken out, washed and dried to obtain the finished real silk fabric; filling silkworm excrement into the finished silk fabric, sewing to obtain silkworm excrement bags, filling the silkworm excrement bags and the fillers into the pillowcase, and sewing to obtain the health-care silkworm excrement pillow.
8. The preparation method of the health-care silkworm excrement pillow according to claim 7, wherein the real silk fabric is soaked in the finishing liquid in a bath ratio of 1: 30-50; the heating and oscillating temperature is 40-60 ℃, and the time is 30-90 minutes.
9. Use of a finished silk fabric in the preparation of the health-care silkworm excrement pillow of claim 1.
10. Use of the health-care silkworm excrement pillow as set forth in claim 1 as a household product.
CN202111606736.XA 2021-12-26 2021-12-26 Health-care silkworm excrement pillow and preparation method thereof Pending CN114158892A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101349006A (en) * 2008-09-03 2009-01-21 苏州大学 Method for preparing nanometer negative ion automobile inner decoration facing
CN102733176A (en) * 2012-07-11 2012-10-17 南通那芙尔服饰有限公司 Nano-anion far infrared after-treatment method for silk wadding quilt
CN203391652U (en) * 2013-08-16 2014-01-15 辽宁易兴丝绵有限责任公司 Vehicle-mounted negative oxygen ion combination back cushion
CN205390919U (en) * 2015-12-31 2016-07-27 郑州德惠纺织科技有限公司 Rib anion pillow
CN105962709A (en) * 2016-06-20 2016-09-28 南通茧缘丝绸纺织有限公司 Silk health-care pillow and preparation method of magnetic therapy silk thereof
CN206534448U (en) * 2016-12-01 2017-10-03 成都科创智远信息技术有限公司 One kind purification air health pillow

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101349006A (en) * 2008-09-03 2009-01-21 苏州大学 Method for preparing nanometer negative ion automobile inner decoration facing
CN102733176A (en) * 2012-07-11 2012-10-17 南通那芙尔服饰有限公司 Nano-anion far infrared after-treatment method for silk wadding quilt
CN203391652U (en) * 2013-08-16 2014-01-15 辽宁易兴丝绵有限责任公司 Vehicle-mounted negative oxygen ion combination back cushion
CN205390919U (en) * 2015-12-31 2016-07-27 郑州德惠纺织科技有限公司 Rib anion pillow
CN105962709A (en) * 2016-06-20 2016-09-28 南通茧缘丝绸纺织有限公司 Silk health-care pillow and preparation method of magnetic therapy silk thereof
CN206534448U (en) * 2016-12-01 2017-10-03 成都科创智远信息技术有限公司 One kind purification air health pillow

Non-Patent Citations (2)

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Title
卢欣旸等: "自修复疏水蚕丝植物的制备及性能", 现代丝绸科学与技术, vol. 31, no. 4, pages 128 - 130 *
洪剑寒等: "甲基丙烯酸十八烷基酯疏水整理真丝植物的自修复性能", 印染, pages 7 - 11 *

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Application publication date: 20220311

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