CN102733176A - Nano-anion far infrared after-treatment method for silk wadding quilt - Google Patents

Nano-anion far infrared after-treatment method for silk wadding quilt Download PDF

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CN102733176A
CN102733176A CN2012102389369A CN201210238936A CN102733176A CN 102733176 A CN102733176 A CN 102733176A CN 2012102389369 A CN2012102389369 A CN 2012102389369A CN 201210238936 A CN201210238936 A CN 201210238936A CN 102733176 A CN102733176 A CN 102733176A
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silk floss
nano
far infrared
negative ion
quilt
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CN102733176B (en
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潘世俊
石继均
梅德祥
盛家镛
丁桂莲
胡小明
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Jiangsu Xinyuan Silk Science and Technology Co., Ltd.
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NAFUER GARMENT ORNAMENT CO LD NANTONG
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Abstract

The invention discloses a nano-anion far infrared after-treatment method for a silk wadding quilt, and the method comprises the following steps: (a) preparing treatment impregnation liquid containing 2%-6% of nano-anion far infrared radiators, 0.3%-1% of additives and 0.2%-1.5% of a silk wadding softening agent by weight, and the balance of water, wherein the nano-anion far infrared radiators are nanoscale powder made through mixing opal and far infrared ceramic powder; (b) heating the treatment impregnation liquid to 40-45 DEG C, and adding dry silk wadding, wherein the bath ratio ranges from 1:30 to 1:40, and the impregnation time ranges from 30 minutes to 40 minutes; and (c) dehydrating and drying the impregnated silk wadding, and manufacturing the silk wadding quilt by use of a conventional method. According to the method, one-time impregnation is enough to realize after-treatment, the production technology is greatly simplified, the processing cost is lowered, the production efficiency is improved, and the manpower is saved.

Description

The nano-negative ion far infrared after-finishing method of silk floss quilt
Technical field
The present invention relates to a kind of nano-negative ion far infrared after-finishing method of silk floss quilt.
Background technology
The Along with people's growth in the living standard, People more and more is advocated back to nature, and the consumption of silk floss quilt increases severely, and the consumption market enlarges year by year.Simultaneously, the Along with people's health care consciousness strengthens, and increasing consumer favors use and integrates warming and articles for use health care.Chinese invention patent application CN1782169A discloses a kind of anion far infrared post finishing method of silk floss quilt; Adopt tourmaline and far-infrared ceramic powder to be mixed into the nano-negative ion far-infrared radiator and carry out the back arrangement; Can make product obtain the health care function, improve air quality and promote the microcirculatory effect of blood of human body thereby reach.
Yet; There is following problem in above-mentioned afterfinish method: (1) is attached on the silk floss in order to make nano-negative ion far infrared radiation physical efficiency well, prevents that it from coming off, and this method need dispose two kinds of arrangement maceration extracts; Promptly put maceration extract A and arrangement maceration extract B in order; Obviously, this has increased processing step, has improved complicated operation degree and production cost; Can know by embodiment that (2) anion concentration that this method makes in the silk floss quilt is 570/cm 3About, the needs of further lifting are arranged.
Summary of the invention
The object of the invention provides a kind of nano-negative ion far infrared after-finishing method of silk floss quilt.
For achieving the above object, the technical scheme that the present invention adopts is: a kind of nano-negative ion far infrared after-finishing method of silk floss quilt comprises the steps:
(a) configuration arrangement maceration extract, said arrangement maceration extract comprise that percentage by weight is 2 ~ 6% nano-negative ion far-infrared radiator, 0.3 ~ 1% auxiliary agent and 0.2 ~ 1.5% silk floss softener, and surplus is a water;
Said nano-negative ion far-infrared radiator is a nanometer grade powder, is mixed by opal and far-infrared ceramic powder; Said auxiliary agent is made up of Sodium Polyacrylate dispersant and silane coupler;
(b) above-mentioned arrangement maceration extract is heated to 40 ~ 45 ℃, puts into the shredded dried bean curd silk floss, bath raio is 1:30 ~ 1:40, and dip time is 30 ~ 40 min;
(c) after the dehydration of the silk floss after will flooding, the oven dry, be made into silk floss quilt with conventional method.
In the technique scheme, said silane coupler is selected from vinyl silanes, amino silane, methacryloxy silane, hydrosulphonyl silane or urea groups silane.
In the technique scheme, said silk floss softener is an amido organosilicon.
In the technique scheme, dehydration is centrifugal dehydration in the said step (c), and bake out temperature is 95 ~ 98 ℃.
In the technique scheme, in the said step (b), put the shredded dried bean curd silk floss of putting into 40 ~ 80 g in the maceration extract in order for every liter.
The present invention asks for protection the silk floss quilt that is obtained by above-mentioned preparation method simultaneously.
Because the technique scheme utilization, the present invention compared with prior art has advantage:
1. the present invention has developed a kind of nano-negative ion far infrared after-finishing method of silk floss quilt, and single-steeping can be realized the back arrangement, has simplified production technology greatly, has reduced processing cost, has improved production efficiency, has practiced thrift manpower.
2. adopting opal and far-infrared ceramic powder to be mixed and made into the nano-negative ion far-infrared radiator in the present invention is nanometer grade powder, and evidence: by the anion concentration in its silk floss quilt that makes is 3750/cm 3About, improved health-care effect greatly, obtained beyond thought technique effect.
3. experiment showed, the above inherent quality requirement of (GB/T 24252-2009) primes that can be up to state standards " cocoon silk quilt " of silk floss quilt that the present invention makes, be suitable for applying.
4. preparation method of the present invention is simple, easy operating, has a good application prospect.
The specific embodiment
Below in conjunction with embodiment the present invention is further described:
Embodiment one
A kind of nano-negative ion far infrared after-finishing method of silk floss quilt comprises the steps:
(a) configuration arrangement maceration extract, said arrangement maceration extract comprise that percentage by weight is 3% nano-negative ion far-infrared radiator, 1% auxiliary agent and 0.8% silk floss softener, and surplus is a water;
Said nano-negative ion far-infrared radiator is a nanometer grade powder, is mixed by opal and far-infrared ceramic powder; Said auxiliary agent is made up of Sodium Polyacrylate dispersant and silane coupler;
(b) above-mentioned arrangement maceration extract is heated to 45 ℃, puts into the shredded dried bean curd silk floss, bath raio is 1:30, and dip time is 35 min;
(c) after the dehydration of the silk floss after will flooding, the oven dry, be made into silk floss quilt with conventional method.
In the technique scheme, said silane coupler is an amino silane.Said silk floss softener is an amido organosilicon.
Dehydration is centrifugal dehydration in the said step (c), and bake out temperature is 96 ℃.In the said step (b), put the shredded dried bean curd silk floss of putting into 70 g in the maceration extract in order for every liter.
 
The silk floss quilt that the foregoing description one is made is made into the sample of 1cm, carries out anion and detects, and the result is following:
Figure 2012102389369100002DEST_PATH_IMAGE001
Then, the silk floss quilt that the foregoing description one is made is incubated the mensuration of rate, and does comparison with Chinese invention patent application CN1782169A, and the result is following:
Figure 336941DEST_PATH_IMAGE002
Can know by above-mentioned test; Anion far infrared post finishing method (Chinese invention patent application CN1782169A) with respect to existing silk floss quilt; Afterfinish method of the present invention not only promotes on the insulation rate to some extent, and the anion concentration in the silk floss quilt is 3750/cm 3About, improved 6.58 times, obtained beyond thought technique effect.

Claims (6)

1. the nano-negative ion far infrared after-finishing method of a silk floss quilt is characterized in that, comprises the steps:
(a) configuration arrangement maceration extract, said arrangement maceration extract comprise that percentage by weight is 2 ~ 6% nano-negative ion far-infrared radiator, 0.3 ~ 1% auxiliary agent and 0.2 ~ 1.5% silk floss softener, and surplus is a water;
Said nano-negative ion far-infrared radiator is a nanometer grade powder, is mixed by opal and far-infrared ceramic powder; Said auxiliary agent is made up of Sodium Polyacrylate dispersant and silane coupler;
(b) above-mentioned arrangement maceration extract is heated to 40 ~ 45 ℃, puts into the shredded dried bean curd silk floss, bath raio is 1:30 ~ 1:40, and dip time is 30 ~ 40 min;
(c) after the dehydration of the silk floss after will flooding, the oven dry, be made into silk floss quilt with conventional method.
2. the nano-negative ion far infrared after-finishing method of silk floss quilt according to claim 1, it is characterized in that: said silane coupler is selected from vinyl silanes, amino silane, methacryloxy silane, hydrosulphonyl silane or urea groups silane.
3. the nano-negative ion far infrared after-finishing method of silk floss quilt according to claim 1, it is characterized in that: said silk floss softener is an amido organosilicon.
4. the nano-negative ion far infrared after-finishing method of silk floss quilt according to claim 1 is characterized in that: dehydration is centrifugal dehydration in the said step (c), and bake out temperature is 95 ~ 98 ℃.
5. the nano-negative ion far infrared after-finishing method of silk floss quilt according to claim 1 is characterized in that: in the said step (b), put the shredded dried bean curd silk floss of putting into 40 ~ 80 g in the maceration extract in order for every liter.
6. the silk floss quilt that preparation method according to claim 1 obtains.
CN201210238936.9A 2012-07-11 2012-07-11 Nano-anion far infrared after-treatment method for silk wadding quilt Active CN102733176B (en)

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104746349A (en) * 2013-12-31 2015-07-01 上海水星家用纺织品股份有限公司 Preparation method of negative-ion down feather material and negative-ion down feather quilt
WO2017000420A1 (en) * 2015-06-30 2017-01-05 紫罗兰家纺科技股份有限公司 Antibacterial anti-mite far-infrared massage magnetic therapy back cushion and manufacturing method therefor
CN106351005A (en) * 2016-08-27 2017-01-25 新马(安徽)制衣有限公司 Fouling-resistant fabric with high air permeability and processing technology thereof
CN107435241A (en) * 2017-09-04 2017-12-05 西南大学 Far infrared silk fabric is prepared with the NMMO aqueous solution
CN107541951A (en) * 2017-09-04 2018-01-05 西南大学 Far infrared wool fabric is prepared with the NMMO aqueous solution
CN114108315A (en) * 2021-12-20 2022-03-01 江苏鑫缘丝绸科技有限公司 Finishing silk floss sheet and silk floss quilt prepared from same
CN114158892A (en) * 2021-12-26 2022-03-11 江苏鑫缘丝绸科技有限公司 Health-care silkworm excrement pillow and preparation method thereof
CN114224113A (en) * 2021-12-23 2022-03-25 江苏鑫缘丝绸科技有限公司 Silk moxa back cushion and preparation method thereof

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KR20040094209A (en) * 2003-05-02 2004-11-09 크리원 월드(주) Far-infrared-and-anion-radiating fextile and manufacturing method for the same
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CN101215778A (en) * 2008-01-09 2008-07-09 南通那芙尔服饰有限公司 Anion far infrared post finishing method for silk wadding quilt
CN101349006A (en) * 2008-09-03 2009-01-21 苏州大学 Method for preparing nanometer negative ion automobile inner decoration facing
CN101481872A (en) * 2008-12-17 2009-07-15 盛虹集团有限公司 Heat storing heat preserving finishing method

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CN101215778A (en) * 2008-01-09 2008-07-09 南通那芙尔服饰有限公司 Anion far infrared post finishing method for silk wadding quilt
CN101349006A (en) * 2008-09-03 2009-01-21 苏州大学 Method for preparing nanometer negative ion automobile inner decoration facing
CN101481872A (en) * 2008-12-17 2009-07-15 盛虹集团有限公司 Heat storing heat preserving finishing method

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104746349A (en) * 2013-12-31 2015-07-01 上海水星家用纺织品股份有限公司 Preparation method of negative-ion down feather material and negative-ion down feather quilt
WO2017000420A1 (en) * 2015-06-30 2017-01-05 紫罗兰家纺科技股份有限公司 Antibacterial anti-mite far-infrared massage magnetic therapy back cushion and manufacturing method therefor
CN106351005A (en) * 2016-08-27 2017-01-25 新马(安徽)制衣有限公司 Fouling-resistant fabric with high air permeability and processing technology thereof
CN107435241A (en) * 2017-09-04 2017-12-05 西南大学 Far infrared silk fabric is prepared with the NMMO aqueous solution
CN107541951A (en) * 2017-09-04 2018-01-05 西南大学 Far infrared wool fabric is prepared with the NMMO aqueous solution
CN114108315A (en) * 2021-12-20 2022-03-01 江苏鑫缘丝绸科技有限公司 Finishing silk floss sheet and silk floss quilt prepared from same
CN114108315B (en) * 2021-12-20 2024-03-08 江苏鑫缘丝绸科技有限公司 Finishing silk floss sheet and silk floss quilt prepared from same
CN114224113A (en) * 2021-12-23 2022-03-25 江苏鑫缘丝绸科技有限公司 Silk moxa back cushion and preparation method thereof
CN114158892A (en) * 2021-12-26 2022-03-11 江苏鑫缘丝绸科技有限公司 Health-care silkworm excrement pillow and preparation method thereof

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Address after: 226600 Haian Jiangsu Development Zone, East Lake Road, No. 1 silk industrial park

Patentee after: Jiangsu Xinyuan Silk Science and Technology Co., Ltd.

Address before: 226600, silk industrial park, No. 1, East Lake Road, Haian Economic Development Zone, Haian County, Nantong, Jiangsu, China G

Patentee before: Nafuer Garment Ornament Co., Ld., Nantong

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