CN114134003A - Preparation method of fruit wine containing ultra-trace elements - Google Patents
Preparation method of fruit wine containing ultra-trace elements Download PDFInfo
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- CN114134003A CN114134003A CN202111609164.0A CN202111609164A CN114134003A CN 114134003 A CN114134003 A CN 114134003A CN 202111609164 A CN202111609164 A CN 202111609164A CN 114134003 A CN114134003 A CN 114134003A
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/04—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
- C12G3/05—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with health-improving ingredients, e.g. flavonoids, flavones, polyphenols or polysaccharides
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D9/00—Other inorganic fertilisers
- C05D9/02—Other inorganic fertilisers containing trace elements
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Abstract
The invention discloses a method for preparing fruit wine containing ultra-trace elements, which comprises the steps of taking 100 parts of raw material ores containing more than 50 ultra-trace elements and marine biomass in equal mass, crushing, heating, drying, carrying out acidolysis, filtering to prepare ultra-trace element stock solution, and blending the ultra-trace element stock solution with prepared fruit distilled wine according to the proportion of 1: 320; or packaging 1.6mL of the ultramicro element stock solution separately for every 500mL of fruit wine; when the fruit wine is mixed or mixed with fruit wine, dozens of ultra-micro mineral elements can be supplemented for human body, and the corresponding ultra-micro elements can be absorbed by human body, and simultaneously, various diseases caused by lack of mineral elements and chronic diseases caused by overnutrition or unbalanced nutrition can be inhibited, prevented and alleviated for people, so that the fruit wine has the positive effects of safety, health, blood circulation promotion and the like.
Description
Technical Field
The invention relates to the technical field of brewing of fruit wine, in particular to a preparation method of fruit wine containing ultra-trace elements.
Background
The mineral substance is a general name of various elements which form human tissues and are necessary for maintaining normal physiological functions, is one of seven essential nutrients for human bodies, participates in various enzyme activities, balance body fluid, energy supply and other biochemical reactions of the human bodies, does not contain vitamins, can react independently, but lacks the participation of the mineral substance, and does not have the effect when being eaten by more vitamins, so the mineral substance is regarded as the first of the five essential nutrients;
although the total amount of minerals in a human body is less than 5 percent of the body weight, the minerals can not provide energy, can not be synthesized in the body by self, are supplied by the external environment, play an important role in the physiological action of human tissues, are important raw materials for forming body tissues, such as calcium, phosphorus and magnesium, which are main raw materials for forming bones and teeth and are necessary conditions for maintaining acid-base balance and normal osmotic pressure of the body, and some special physiological substances in the human body, such as hemoglobin, thyroxine and the like in blood, can be synthesized only by the participation of iron and iodine; part of minerals are in small need, the range of physiological need and toxic dose is narrow, and poisoning is easily caused by excessive intake; during the metabolism process of a human body, a certain amount of mineral substances are discharged out of the body through feces, urine, sweat, hair and the like every day, so that the mineral substances must be supplemented through diet;
the fourth national nutrition survey shows that protein, fat and carbohydrate in the diet of residents in China can meet the requirements of human bodies, but the residents in China generally lack vitamins and trace elements, the seriously deficient crowds are youngsters, women (pregnant women) and old people, chronic diseases caused by overnutrition or unbalanced nutrition are increased, and mineral supplements or products which are beneficial to health are urgently needed in order to meet the daily needs of the human bodies for energy and nutrient substances.
Disclosure of Invention
The invention provides a preparation method of fruit wine containing ultra-trace elements, which aims to solve the technical problems in the prior art.
The technical scheme of the invention is realized as follows: a method for preparing fruit wine containing ultra-trace elements; the method is characterized in that: the method comprises the following steps:
selecting materials, namely selecting marine ore, marine biomass and land ore raw materials, and weighing 100 parts of the marine ore, the marine biomass and the land ore raw materials with the same mass;
step two, heating and expanding, namely putting 100 parts of weighed marine ore and land ore raw materials into a crusher together to be crushed and sieved to 60-200 meshes, then moving the crushed marine ore and land ore raw materials into a high-temperature high-pressure furnace to be heated to 120 ℃ and pressurized to 1-2MP, and after heating for 1-2 hours, opening the furnace instantly to expand the volume of the crushed ore raw materials;
step three, soaking 100 parts of the weighed marine biomass in 20% KOH solution for 1 hour, washing with clear water to remove residual alkali, drying, and crushing and sieving to 200 meshes in a crusher;
step four, mixing 30-80 parts of the expanded ore and the soaked and crushed marine biomass according to the same mass;
fifthly, heating the reaction kettle, and keeping the interlayer outside the reaction kettle at a constant temperature of 70-80 ℃;
step six, adding the mixed substances in the step four, water and concentrated sulfuric acid into a reaction kettle according to a proportion, firstly stirring and mixing the mixed substances with the water, then slowly adding the concentrated sulfuric acid, continuously stirring to carry out acidolysis, and keeping the temperature of the reaction kettle at 110-120 ℃ in the process of adding the concentrated sulfuric acid, and carrying out acidolysis for 2-5 hours;
seventhly, obtaining stock solution, after the acidolysis is finished, extracting acidolysis matters in the reaction kettle in the sixth step under the condition of continuous stirring to a filtering device, and performing vacuum filtration to obtain finished product ultra-trace element stock solution and slag;
and step eight, blending the ultra-trace element fruit wine, namely taking the brewed fruit wine and the finished product stock solution prepared in the step seven, mixing the fruit wine and the ultra-trace element stock solution according to the proportion of 320:1, and uniformly stirring to obtain the ultra-trace element fruit wine.
The trace element ingredients of the marine ore, the marine biomass and the land ore raw materials in the step one are more than 50, no radioactive element is contained, and the heavy metal elements do not exceed the standard. The preferable land ore can be selected from vermiculite, mica rock, and Muntang mica group ore (Muntang mica group) of Tokyo county of Tokyo city of south-Yang of Henan province.
In the sixth step, the mixed substances are: water: concentrated sulfuric acid =25% -30%, 40% -50% and 20% -25%.
The fruit wine is fruit distilled wine, which is prepared by taking one or more of pomegranate, apricot, plum, pear, peach, kiwi fruit, apple, pawpaw and mulberry as main raw materials, pretreating, adding white granulated sugar and yeast for fermentation, distilling, storing, blending, filtering, encapsulating and packaging.
Step eight, separately packaging the ultra-trace element stock solution and fruit wine, wherein 1.6mL of the ultra-trace element stock solution can be separately packaged in every 500mL of the fruit wine; mixing and shaking before drinking fruit wine to obtain fruit wine containing ultra-trace elements.
The raw material ore adopted by the invention is 100 parts by mass with the same mass of more than 50 ultramicro elements and marine biomass, and is prepared by crushing, heating, drying, carrying out acidolysis, filtering to prepare an ultramicro element stock solution, and blending the ultramicro element stock solution with prepared fruit distilled liquor according to the proportion of 1: 320; or packaging 1.6mL of the ultramicro element stock solution separately for every 500mL of fruit wine; when in use, 1.6mL of independently packaged ultra-trace element stock solution is poured into 500mL of fruit wine to be mixed and shaken evenly, and the fruit wine containing ultra-trace elements is obtained.
The invention can produce slag and unfiltered trace elements while preparing the ultramicro-trace element stock solution, and can be used as fertilizers.
The invention has the beneficial effects that the invention provides the preparation method of the fruit wine containing the ultra-trace elements, which extracts the ultra-trace element stock solution which is easy to be absorbed by human bodies by extracting, acidolyzing and filtering the existing marine ore, marine biomass and land ore raw materials, can supplement dozens of ultra-trace mineral elements for the human bodies in the mixing or mixed loading and mixing use of the fruit wine, can inhibit, prevent and alleviate various diseases caused by lack of mineral elements and chronic diseases caused by over-nutrition or unbalanced nutrition while the corresponding ultra-trace elements are absorbed by the human bodies, and has the positive effects of safety, health, blood circulation promotion and the like.
Detailed Description
The present invention will be further described with reference to the following examples for facilitating understanding of those skilled in the art, and the description of the embodiments is not intended to limit the present invention.
[ example 1 ]
Selecting marine ore, marine biomass and land ore containing more than 50 element components, and weighing 100 parts of marine ore, marine biomass and land ore raw materials with the same mass; soaking marine biomass in 20% KOH solution for 1 hour, removing organic impurities of the marine biomass, washing with clear water to remove residual alkali, drying, and pulverizing in a pulverizer to 200 mesh; put into rubbing crusher after will weighing jointly and smash and sieve to 60 meshes after to the marine ore of 100 parts and land ore raw materials, move into high temperature high-pressure furnace and heat to 100 ℃, pressurize to 2MP, after heating 2 hours, the blow-in makes the ore raw materials volume after smashing popped in the twinkling of an eye, make the outer intermediate layer keep 70 ℃ constant temperature with reation kettle heating, get the popped ore of equal quality and soak each 30 parts of the kibbling marine biomass of back and mix and get the material after mixing, the material after mixing: water: stirring and acidolyzing concentrated sulfuric acid =25% and 40% and 20%, stirring and mixing the mixed substances with water, slowly adding concentrated sulfuric acid, continuously stirring to acidolyze the mixed substances, and keeping the temperature of a reaction kettle at 110 ℃ for acidolysis for 5 hours in the process of adding concentrated sulfuric acid; after the acidolysis is finished, extracting acidolysis matters in the reaction kettle under the condition of continuous stirring to a filtering device, and performing vacuum filtration to obtain finished product ultra-trace element stock solution and slag; adding the slag into a fertilizer to obtain a compound fertilizer;
the obtained finished product stock solution of the ultra-trace elements and brewed fruit wine are separately packaged, and 1.6mL of the stock solution of the ultra-trace elements can be separately packaged in every 500mL of fruit wine; mixing and shaking before drinking fruit wine to obtain fruit wine containing ultra-trace elements.
[ example 2 ]
Similar to example 1, the difference is that 100 parts of the weighed marine ore and land ore raw materials are put into a pulverizer together to be pulverized and sieved to 200 meshes, then the raw materials are moved into a high-temperature high-pressure furnace to be heated to 120 ℃, pressurized to 1MP, after being heated for 1 hour, the furnace is opened instantly to expand the volume of the pulverized ore raw materials, a reaction kettle is heated to ensure that an outer interlayer keeps a constant temperature of 80 ℃, 80 parts of the expanded ore with the same mass and 80 parts of the pulverized marine biomass after being soaked are taken to be mixed to obtain mixed substances, and the mixed substances are: water: stirring and acidolyzing concentrated sulfuric acid =30% and 50% and 25%, stirring and mixing the mixed substances with water, slowly adding concentrated sulfuric acid, continuously stirring to acidolyze the mixed substances, and keeping the temperature of a reaction kettle at 120 ℃ in the process of adding concentrated sulfuric acid for acidolysis for 2 hours; after the acidolysis is finished, extracting acidolysis matters in the reaction kettle under the condition of continuous stirring to a filtering device, and performing vacuum filtration to obtain finished product ultra-trace element stock solution and slag; adding the slag into a fertilizer to obtain a compound fertilizer;
mixing the obtained stock solution with brewed fruit wine at a ratio of 320:1, stirring, and packaging to obtain fruit wine containing ultra-trace elements.
[ example 3 ]
Similar to example 1, the difference is that 100 parts of the weighed marine ore and land ore raw materials are put into a pulverizer together to be pulverized and sieved to 150 meshes, then the raw materials are moved into a high-temperature high-pressure furnace to be heated to 110 ℃, pressurized to 1.5MP, after being heated for 1.5 hours, the furnace is opened instantly to expand the volume of the pulverized ore raw materials, a reaction kettle is heated to ensure that an outer interlayer keeps a constant temperature of 75 ℃, 60 parts of each of the expanded ore with the same mass and the pulverized marine biomass after being soaked are taken to be mixed to obtain mixed substances, and the mixed substances are: water: stirring and acidolyzing concentrated sulfuric acid =26% and 42% and 21%, stirring and mixing the mixed substances with water, slowly adding concentrated sulfuric acid, continuously stirring to acidolyze the mixed substances, and keeping the temperature of a reaction kettle at 110 ℃ for acidolysis for 1.5 hours in the process of adding concentrated sulfuric acid; after the acidolysis is finished, extracting acidolysis matters in the reaction kettle under the condition of continuous stirring to a filtering device, and performing vacuum filtration to obtain finished product ultra-trace element stock solution and slag; adding the slag into a fertilizer to obtain a compound fertilizer;
mixing the obtained stock solution with brewed fruit wine at a ratio of 320:1, stirring, and packaging to obtain fruit wine containing ultra-trace elements; or packaging the finished product of the stock solution of the ultra-trace elements and brewed fruit wine separately, wherein 1.6mL of the stock solution of the ultra-trace elements can be packaged separately for every 500mL of the fruit wine; mixing and shaking before drinking fruit wine to obtain fruit wine containing ultra-trace elements.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (5)
1. A method for preparing fruit wine containing ultra-trace elements; the method is characterized in that: the method comprises the following steps:
selecting materials, namely selecting marine ore, marine biomass and land ore raw materials, and weighing 100 parts of the marine ore, the marine biomass and the land ore raw materials with the same mass;
step two, heating and expanding, namely putting 100 parts of weighed marine ore and land ore raw materials into a crusher together to be crushed and sieved to 60-200 meshes, then moving the crushed marine ore and land ore raw materials into a high-temperature high-pressure furnace to be heated to 120 ℃ and pressurized to 1-2MP, and after heating for 1-2 hours, opening the furnace instantly to expand the volume of the crushed ore raw materials;
step three, soaking 100 parts of the weighed marine biomass in 20% KOH solution for 1 hour, washing with clear water to remove residual alkali, drying, and crushing and sieving to 200 meshes in a crusher;
step four, mixing 30-80 parts of the expanded ore and the soaked and crushed marine biomass according to the same mass;
fifthly, heating the reaction kettle, and keeping the interlayer outside the reaction kettle at a constant temperature of 70-80 ℃;
step six, adding the mixed substances in the step four, water and concentrated sulfuric acid into a reaction kettle according to a proportion, firstly stirring and mixing the mixed substances with the water, then slowly adding the concentrated sulfuric acid, continuously stirring to carry out acidolysis, and keeping the temperature of the reaction kettle at 110-120 ℃ in the process of adding the concentrated sulfuric acid, and carrying out acidolysis for 2-5 hours;
seventhly, obtaining stock solution, after the acidolysis is finished, extracting acidolysis matters in the reaction kettle in the sixth step under the condition of continuous stirring to a filtering device, and performing vacuum filtration to obtain finished product ultra-trace element stock solution and slag;
and step eight, blending the ultra-trace element fruit wine, namely taking the brewed fruit wine and the stock solution prepared in the step seven, wherein the fruit wine and the ultra-trace element stock solution are blended according to the ratio of 320:1, mixing and shaking uniformly to obtain the ultra-trace element containing fruit wine.
2. The method for producing ultra-trace element-containing fruit wine according to claim 1, wherein: the trace element ingredients of the raw materials of the marine ore, the marine biomass and the land ore in the step one are more than 50, no radioactive element is contained, and the heavy metal elements do not exceed the standard.
3. The method for producing ultra-trace element-containing fruit wine according to claim 1, wherein: in the sixth step, the mixed substances are: water: concentrated sulfuric acid =25% -30%, 40% -50% and 20% -25%.
4. The method for producing ultra-trace element-containing fruit wine according to claim 1, wherein: the fruit wine is fruit distilled wine, which is prepared by taking one or more of pomegranate, apricot, plum, pear, peach, kiwi fruit, apple, pawpaw and mulberry as main raw materials, pretreating, adding white granulated sugar and yeast for fermentation, distilling, storing, blending, filtering, encapsulating and packaging.
5. The method for producing ultra-trace element-containing fruit wine according to claim 1, wherein: and step eight, separately packaging the ultra-trace element stock solution and the fruit wine, namely packaging 1.6mL of the ultra-trace element stock solution for every 500mL of the fruit wine.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202111609164.0A CN114134003A (en) | 2021-12-27 | 2021-12-27 | Preparation method of fruit wine containing ultra-trace elements |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1686855A (en) * | 2005-04-20 | 2005-10-26 | 黄玉霖 | Concentrated water of natural mineral matter and method of preparation |
| CN112645773A (en) * | 2021-01-08 | 2021-04-13 | 河南炜炎肥业有限责任公司 | Mineral supplement preparation, fertilizer comprising mineral supplement preparation, preparation method and application |
| CN113046208A (en) * | 2021-03-19 | 2021-06-29 | 罗苏 | A beverage containing 68 minerals |
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2021
- 2021-12-27 CN CN202111609164.0A patent/CN114134003A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1686855A (en) * | 2005-04-20 | 2005-10-26 | 黄玉霖 | Concentrated water of natural mineral matter and method of preparation |
| CN112645773A (en) * | 2021-01-08 | 2021-04-13 | 河南炜炎肥业有限责任公司 | Mineral supplement preparation, fertilizer comprising mineral supplement preparation, preparation method and application |
| CN113046208A (en) * | 2021-03-19 | 2021-06-29 | 罗苏 | A beverage containing 68 minerals |
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