CN113845877A - Preparation method and use method of adhesive with far infrared, antibacterial and antioxidant functions - Google Patents
Preparation method and use method of adhesive with far infrared, antibacterial and antioxidant functions Download PDFInfo
- Publication number
- CN113845877A CN113845877A CN202111112655.4A CN202111112655A CN113845877A CN 113845877 A CN113845877 A CN 113845877A CN 202111112655 A CN202111112655 A CN 202111112655A CN 113845877 A CN113845877 A CN 113845877A
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- CN
- China
- Prior art keywords
- antibacterial
- far infrared
- adhesive
- antioxidant
- steps
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J189/00—Adhesives based on proteins; Adhesives based on derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J201/00—Adhesives based on unspecified macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2296—Oxides; Hydroxides of metals of zinc
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
Abstract
The invention relates to the field of food stickers, in particular to a preparation method and a use method of an adhesive with far infrared, antibacterial and antioxidant functions, which is prepared by allowing water vapor to penetrate through a substrate material by a gas phase method, condensing and taking out water with nano particles, mixing the water with liquid nano zinc and other materials according to a proper proportion, and mixing the mixture with an adhesive material prepared from a natural high molecular compound.
Description
Technical Field
The invention relates to the field of food stickers, in particular to a preparation method and a use method of an adhesive with far infrared, antibacterial and antioxidant functions.
Background
The food label is the most common maintenance label in the market and is used for displaying corresponding information, the most common food label is a self-adhesive sticker, and the paper base material of the self-adhesive label is as follows: the adhesive paper, the coated paper, the glass paperboard, the laser paper, the kraft paper, the fluorescent paper, the gold-plated paper, the aluminum foil paper, the fragile (anti-counterfeiting) paper, the silver-plated paper, the textured paper, the cloth label (tavy/nylon) paper, the pearlescent paper, the sandwich coated paper, the variable information paper and the like are coated on the back of the adhesive paper, and in the process of storing and displaying foods such as vegetables and fruits, because the propagation of microorganisms on the surfaces of the foods is avoided, if certain refrigeration conditions are not provided to inhibit the propagation of the microorganisms, the shelf life of the foods is shortened, the flavor of the foods is influenced, however, the vegetables and fruits do not have refrigeration conditions in the process of displaying actually, or the sales cost is greatly improved due to the refrigeration conditions, so that the packaging sticker or the sticker which is convenient to operate, low in cost and has good antibacterial and antioxidant functions is developed, has wide market prospect and good market prospect, the scheme is generated.
Disclosure of Invention
An object of the present invention is to solve at least the above problems by a method for preparing an adhesive having far infrared ray, antibacterial and antioxidant functions and a method for using the same.
In order to solve the technical problems, the technical scheme adopted by the invention is as follows: the preparation method of the adhesive with far infrared, antibacterial and antioxidant functions is characterized by comprising the following steps:
step one, water vapor permeates a substrate material by a vapor phase method, and a nano particle water solution additive is obtained after condensation;
step two, mixing the nano particle aqueous solution additive obtained in the step one with a liquid nano zinc material in proportion;
and step three, uniformly mixing the aqueous solution obtained by mixing the step two and the step three with a hydrophilic adhesive to obtain the adhesive with far infrared, antibacterial and antioxidant functions.
Preferably, in the second step, the aqueous nanoparticle solution additive obtained in the first step and the liquid nano zinc material are mixed according to the proportion of 80-120: 1.
Preferably, in the second step, the aqueous nanoparticle solution additive obtained in the first step is mixed with the liquid nano zinc material according to the ratio of 100: 1.
Preferably, in the third step, the aqueous solution obtained by mixing the second step and the third step is uniformly mixed with the hydrophilic adhesive according to the proportion of 10-20: 1, so as to obtain the adhesive with far infrared, antibacterial and antioxidant functions.
Preferably, in the third step, the aqueous solution obtained by mixing the second step and the third step is uniformly mixed with the hydrophilic adhesive according to the proportion of 15:1 to obtain the adhesive with far infrared, antibacterial and antioxidant functions.
Preferably, the concentration of the liquid nano zinc material is 50000 ppm.
Preferably, the liquid nano zinc material is nano zinc oxide dispersion liquid, and the solvent is isooctyl palmitate.
Preferably, the substrate material is a 30nm nanoporous particulate material.
Preferably, the raw materials of the granular material comprise SiO2, TiO2, Al2O3, Fe2O3, FeO, MnO, MgO, CaO, Na2O, K2O, P2O5, Ca CO3, P2O5, ZrO2, SiC and TiC, and the weight ratio is as follows: 1.2-1.5:0.4-0.65:0.78-0.85:1.35-1.56:0.12-0.16: 1.15-1.52:0.45-0.68:0.79-0.88:1.36-1.58:0.18-0.19:2.2-2.5:1.4-1.65:1.78-1.85:0.35-0.56:0.12-0.16: 1.15-1.52.
The application method of the adhesive with far infrared, antibacterial and antioxidant functions is characterized by comprising the following steps: the prepared adhesive with far infrared, antibacterial and antioxidant functions is applied to packing materials such as stickers, and the packing materials are adhered to fruits such as vegetables or fruits.
From the above description, the preparation method and the using method of the adhesive with far infrared, antibacterial and antioxidant functions provided by the invention have the following beneficial effects: the water solution technology that the nano particles are extracted by utilizing the 30nm nano-pore particle material through a gas phase method is mixed with the liquid nano zinc material according to a proper proportion and then is fused with the hydrophilic adhesive material, the paster coated on the paper is coated to ensure that the paster prepared on the paper has the characteristic functions of far infrared ray, antibiosis and antioxidation, the preparation cost is low, the preparation process is simple, the operation is convenient, the paster can be directly adhered on food to prolong the preservation period and the antibacterial performance of the food and the vegetables and fruits, the high-efficiency antibacterial power of the liquid nano zinc is added, and the storage period and the flavor can be effectively prolonged.
Detailed Description
The invention is further described below by means of specific embodiments.
In order to make the technical means, the creation characteristics, the achievement purposes and the effects of the invention easy to understand, the invention is further described with the specific embodiments.
The preparation method of the adhesive with far infrared, antibacterial and antioxidant functions is characterized by comprising the following steps:
step one, water vapor permeates a substrate material by a vapor phase method, and a nano particle water solution additive is obtained after condensation;
step two, mixing the nano particle aqueous solution additive obtained in the step one with a liquid nano zinc material in proportion;
and step three, uniformly mixing the aqueous solution obtained by mixing the step two and the step three with a hydrophilic adhesive (such as hydrophilic gelatin) to obtain the adhesive with far infrared, antibacterial and antioxidant functions.
In the second step, the nano particle aqueous solution additive obtained in the first step and the liquid nano zinc material are mixed according to the proportion of 80-120: 1.
As a preferred embodiment, in the second step, the aqueous nanoparticle solution additive obtained in the first step is mixed with the liquid nano zinc material in a ratio of 100: 1.
In the third step, the aqueous solution obtained by mixing the second step and the third step is uniformly mixed with the hydrophilic adhesive according to the proportion of 10-20: 1 to obtain the adhesive with far infrared, antibacterial and antioxidant functions.
In a preferred embodiment, in the third step, the aqueous solution obtained by mixing the second step and the third step is uniformly mixed with the hydrophilic adhesive according to a ratio of 15:1 to obtain the adhesive with far infrared, antibacterial and antioxidant functions.
The concentration of the liquid nano zinc material is 50000 ppm.
The liquid nano zinc material is nano zinc oxide dispersion liquid, and the solvent is isooctyl palmitate.
The substrate material is a 30nm nanoporous particle material.
The raw materials of the particle material comprise SiO2, TiO2, Al2O3, Fe2O3, FeO, MnO, MgO, CaO, Na2O, K2O, P2O5, Ca CO3, P2O5, ZrO2, SiC and TiC, and the weight ratio is as follows: 1.2-1.5:0.4-0.65:0.78-0.85:1.35-1.56:0.12-0.16: 1.15-1.52:0.45-0.68:0.79-0.88:1.36-1.58:0.18-0.19:2.2-2.5:1.4-1.65:1.78-1.85:0.35-0.56:0.12-0.16: 1.15-1.52.
Preferably, the raw materials of the granular material comprise SiO2, TiO2, Al2O3, Fe2O3, FeO, MnO, MgO, CaO, Na2O, K2O, P2O5, Ca CO3, P2O5, ZrO2, SiC and TiC, and the weight ratio is as follows: 1.3:0.5:0.8:1.4:0.13: 1.23:0.52:0.8:1.41:0.18:2.3:1.5:1.82:0.42:0.13: 1.23.
the application method of the adhesive with the far infrared ray, antibacterial function and antioxidant function is characterized in that the prepared adhesive with the far infrared ray, antibacterial function and antioxidant function is applied to packaging materials such as stickers, and the packaging materials are adhered to fruits such as vegetables or fruits.
The water solution technology that the nano particles are extracted by utilizing the 30nm nano-pore particle material through a gas phase method is mixed with the liquid nano zinc material according to a proper proportion and then is fused with the hydrophilic adhesive material, the paster coated on the paper is coated to ensure that the paster prepared on the paper has the characteristic functions of far infrared ray, antibiosis and antioxidation, the preparation cost is low, the preparation process is simple, the operation is convenient, the paster can be directly adhered on food to prolong the preservation period and the antibacterial performance of the food and the vegetables and fruits, the high-efficiency antibacterial power of the liquid nano zinc is added, and the storage period and the flavor can be effectively prolonged.
The above description is only a few specific embodiments of the present invention, but the design concept of the present invention is not limited thereto, and any insubstantial modifications made by the design concept should fall within the scope of the present invention.
Claims (10)
1. The preparation method of the adhesive with far infrared, antibacterial and antioxidant functions is characterized by comprising the following steps:
step one, water vapor permeates a substrate material by a vapor phase method, and a nano particle water solution additive is obtained after condensation;
step two, mixing the nano particle aqueous solution additive obtained in the step one with a liquid nano zinc material in proportion;
and step three, uniformly mixing the aqueous solution obtained by mixing the step two and the step three with a hydrophilic adhesive to obtain the adhesive with far infrared, antibacterial and antioxidant functions.
2. The method for preparing far infrared, antibacterial and antioxidant adhesive according to claim 1, wherein the method comprises the following steps: in the second step, the nano particle aqueous solution additive obtained in the first step and the liquid nano zinc material are mixed according to the proportion of 80-120: 1.
3. The method for preparing far infrared, antibacterial and antioxidant adhesive according to claim 1, wherein the method comprises the following steps: in the second step, the nano particle aqueous solution additive obtained in the first step and the liquid nano zinc material are mixed according to the proportion of 100: 1.
4. The method for preparing far infrared, antibacterial and antioxidant adhesive according to claim 1, wherein the method comprises the following steps: in the third step, the aqueous solution obtained by mixing the second step and the third step is uniformly mixed with the hydrophilic adhesive according to the proportion of 10-20: 1 to obtain the adhesive with far infrared, antibacterial and antioxidant functions.
5. The method for preparing far infrared, antibacterial and antioxidant adhesive according to claim 1, wherein the method comprises the following steps: in the third step, the aqueous solution obtained by mixing the second step and the third step is uniformly mixed with the hydrophilic adhesive according to the proportion of 15:1 to obtain the adhesive with far infrared, antibacterial and antioxidant functions.
6. The method for preparing far infrared, antibacterial and antioxidant adhesive according to claim 1, wherein the method comprises the following steps: the concentration of the liquid nano zinc material is 50000 ppm.
7. The method for preparing far infrared, antibacterial and antioxidant adhesive according to claim 1, wherein the method comprises the following steps: the liquid nano zinc material is nano zinc oxide dispersion liquid, and the solvent is isooctyl palmitate.
8. The method for preparing far infrared, antibacterial and antioxidant adhesive according to claim 1 is characterized in that: the substrate material is a 30nm nanoporous particle material.
9. The method for preparing far infrared, antibacterial and antioxidant adhesive according to claim 1, wherein the method comprises the following steps: the raw materials of the particle material comprise SiO2, TiO2, Al2O3, Fe2O3, FeO, MnO, MgO, CaO, Na2O, K2O, P2O5, Ca CO3, P2O5, ZrO2, SiC and TiC, and the weight ratio is as follows: 1.2-1.5:0.4-0.65:0.78-0.85:1.35-1.56:0.12-0.16: 1.15-1.52:0.45-0.68:0.79-0.88:1.36-1.58:0.18-0.19:2.2-2.5:1.4-1.65:1.78-1.85:0.35-0.56:0.12-0.16: 1.15-1.52.
10. The method for using the adhesive with far infrared, antibacterial and antioxidant functions according to any one of claims 1 to 9, wherein the adhesive comprises: the prepared adhesive with far infrared, antibacterial and antioxidant functions is applied to packing materials such as stickers, and the packing materials are adhered to fruits such as vegetables or fruits.
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CN202111112655.4A CN113845877A (en) | 2021-09-23 | 2021-09-23 | Preparation method and use method of adhesive with far infrared, antibacterial and antioxidant functions |
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CN202111112655.4A CN113845877A (en) | 2021-09-23 | 2021-09-23 | Preparation method and use method of adhesive with far infrared, antibacterial and antioxidant functions |
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Citations (6)
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JP2007039392A (en) * | 2005-08-04 | 2007-02-15 | Trendon Touch Technology Corp | Contact-controlling screen having antibacterial layer, and method for producing the same |
CN103951467A (en) * | 2014-05-12 | 2014-07-30 | 福建省博创生化有限责任公司 | Preparation and usage methods of ceramic glaze nano-pore aqueous solution additive |
CN104017410A (en) * | 2014-06-19 | 2014-09-03 | 江苏凯尚节能科技有限公司 | Antibacterial composite floor based on nano zinc particles |
CN111439943A (en) * | 2019-11-27 | 2020-07-24 | 谢文富 | Environment-friendly building material and preparation method of nano pore water solution additive |
CN112063021A (en) * | 2020-09-14 | 2020-12-11 | 谢文富 | Preparation and use method of three-in-one oily solvent additive with antibacterial zinc ions |
CN113337247A (en) * | 2021-06-18 | 2021-09-03 | 陕西科技大学 | Formaldehyde-free gelatin-based adhesive with water resistance and antibacterial property for artificial board and preparation method thereof |
-
2021
- 2021-09-23 CN CN202111112655.4A patent/CN113845877A/en active Pending
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2007039392A (en) * | 2005-08-04 | 2007-02-15 | Trendon Touch Technology Corp | Contact-controlling screen having antibacterial layer, and method for producing the same |
CN103951467A (en) * | 2014-05-12 | 2014-07-30 | 福建省博创生化有限责任公司 | Preparation and usage methods of ceramic glaze nano-pore aqueous solution additive |
CN104017410A (en) * | 2014-06-19 | 2014-09-03 | 江苏凯尚节能科技有限公司 | Antibacterial composite floor based on nano zinc particles |
CN111439943A (en) * | 2019-11-27 | 2020-07-24 | 谢文富 | Environment-friendly building material and preparation method of nano pore water solution additive |
CN112063021A (en) * | 2020-09-14 | 2020-12-11 | 谢文富 | Preparation and use method of three-in-one oily solvent additive with antibacterial zinc ions |
CN113337247A (en) * | 2021-06-18 | 2021-09-03 | 陕西科技大学 | Formaldehyde-free gelatin-based adhesive with water resistance and antibacterial property for artificial board and preparation method thereof |
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