CN113712856A - Daily chemical product with anti-radiation water replenishing oil and preparation method thereof - Google Patents
Daily chemical product with anti-radiation water replenishing oil and preparation method thereof Download PDFInfo
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- CN113712856A CN113712856A CN202111048169.0A CN202111048169A CN113712856A CN 113712856 A CN113712856 A CN 113712856A CN 202111048169 A CN202111048169 A CN 202111048169A CN 113712856 A CN113712856 A CN 113712856A
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- daily chemical
- oil
- essential oil
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/49—Solubiliser, Solubilising system
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/522—Antioxidants; Radical scavengers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
The invention discloses a daily chemical product with anti-radiation moisturizing oil and a preparation method thereof, wherein the daily chemical product comprises the following raw materials in parts by weight: 60-80 parts of mango seed essential oil, 40-50 parts of ginseng total saponin extract, 30-40 parts of papaya extract, 10-15 parts of rose essential oil, 15-20 parts of resveratrol, 10-15 parts of UV-filtering agent, 10-15 parts of procyanidine, 3-5 parts of olive oil, 8-15 parts of oat beta-glucan and a proper amount of preservative and purified water. The invention has scientific and reasonable raw material formula and is prepared according to reasonable proportion, so that the active ingredients of different raw materials are fully fused and complemented, the invention has higher economic benefit, social benefit and popularization value, belongs to a pure natural skin care product, does not contain essence, pigment, hormone, whitening agent and fluorescent agent, has obvious effects of whitening, moisturizing and locking water on skin, and also has the effects of resisting radiation, moistening and moisturizing, and preventing sun and isolating.
Description
Technical Field
The invention relates to the technical field of daily necessities, in particular to a daily chemical article with anti-radiation moisturizing oil and a preparation method thereof.
Background
Computers, mobile phones, microwave ovens and the like which cannot be felt by skins of office workers at ordinary times are subjected to electromagnetic wave radiation, the functions of cells in a dermis layer can be changed, the skins are greatly damaged, and daily chemical articles are not only used by female people, but also used by most male people. Therefore, daily chemical articles in the market are divided into daily articles for men and women according to the difference of gender, skin quality and the like of men and women. However, the daily necessities are classified according to the degree of water replenishing and the moisture content, and although many women who use the daily necessities in the market add components such as anti-wrinkle, the effect is only retained in the water replenishing effect at the end, and the effect does not have the anti-radiation effect.
Disclosure of Invention
The invention aims to provide a daily chemical product with anti-radiation moisturizing oil and a preparation method thereof, and aims to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme:
a daily chemical product with anti-radiation moisturizing oil and a preparation method thereof comprise the following raw materials in parts by weight: 60-80 parts of mango seed essential oil, 40-50 parts of ginseng total saponin extract, 30-40 parts of pawpaw extract, 10-15 parts of rose essential oil, 15-20 parts of resveratrol, 10-15 parts of UV-filtering agent, 10-15 parts of procyanidine, 3-5 parts of olive oil, 8-15 parts of oat beta-glucan and a proper amount of preservative and purified water;
the preparation method of the radiation-resistant moisturizing oil daily chemical product comprises the following steps:
s1: weighing the raw materials in parts by weight;
s2: soaking mango seed essential oil, ginseng total saponin extract and pawpaw extract in purified water for 10-15h, wherein the ratio of the amount of the added purified water to the amount of the extract is 1-1.5: 1, boiling for 3-4h, and keeping the boiling state for 6-8h with slow fire to obtain a mixed solution;
s3: filtering the mixed solution, sequentially adding rose essential oil, resveratrol, UV-filtering agent, procyanidine, olive oil, oat beta-glucan and preservative into the filtrate, and uniformly mixing;
s4: cooling to room temperature, cooling the filtrate, and filtering again to obtain filtrate, namely the anti-radiation moisturizing oil daily chemical product;
s5: sterilizing, packaging, and bottling.
Preferably, the feed comprises the following raw materials in parts by weight: 70 parts of mango seed essential oil, 45 parts of ginseng total saponin extract, 35 parts of pawpaw extract, 12 parts of rose essential oil, 17 parts of resveratrol, 12 parts of UV-filtering agent, 15 parts of procyanidine, 4 parts of olive oil, 10 parts of oat beta-glucan and a proper amount of preservative and purified water.
Preferably, the feed comprises the following raw materials in parts by weight: 80 parts of mango seed essential oil, 50 parts of ginseng total saponin extract, 40 parts of pawpaw extract, 15 parts of rose essential oil, 20 parts of resveratrol, 15 parts of UV-filtering agent, 15 parts of procyanidine, 5 parts of olive oil, 15 parts of oat beta-glucan and a proper amount of preservative and purified water.
Preferably, the feed comprises the following raw materials in parts by weight: 60 parts of mango seed essential oil, 40 parts of ginseng total saponin extract, 30 parts of pawpaw extract, 10 parts of rose essential oil, 15 parts of resveratrol, 10 parts of UV-filtering agent, 10 parts of procyanidine, 3 parts of olive oil, 8 parts of oat beta-glucan and a proper amount of preservative and purified water.
Preferably, the UV-filter is free titanium dioxide, zinc oxide or a mixture of both.
Preferably, the preservative consists of the following substances in percentage by weight: 15-20% of chlorphenesin, 45-60% of 2-bromo-2-nitro-1, 3-propylene glycol, 15-30% of solubilizer and 0.1-0.5% of iminodisuccinic acid.
Preferably, the solubilizer is polyoxyethylene ether or polyoxypropylene ether.
Preferably, the sterilization and disinfection in step S5 is performed at 85-95 deg.C for 30-45 min.
Preferably, the extraction method of the mango seed essential oil comprises the following steps:
s21: drying mango seeds, and crushing the mango seeds through 40-60 meshes to prepare mango seed powder for later use;
s22: spraying a small amount of water into the mango seed powder until the water content of the mango seed powder is 15-20%; refrigerating the mango seed powder at 0-4 ℃ for 20-30h, performing microwave treatment on the mango seed powder, and cooling to room temperature for later use;
s23: placing the mango seed powder subjected to microwave pretreatment in supercritical CO2Supercritical CO is carried out in an extraction kettle of an extraction device2Extracting, separating the extract in a separating tank to obtain coarse essential oil of mango seed from the bottom of the separating tank and CO from the top of the separating tank2，CO2After gasification, the mixture enters an extraction device for recycling; the supercritical CO2The extraction conditions were: under supercritical conditions, CO2The flow rate of the extraction is 10-35L/min, the extraction pressure is 20-40MPa, the extraction temperature is 30-50 ℃, the resolution temperature is 30-40 ℃, and the extraction time is 1-3 h; in the separation tank, the extract is subjected to reduced pressure separation and extraction, the pressure of the separation tank is 10-15MPa, and the temperature is 25-55 ℃;
s24: and placing the obtained mango kernel crude essential oil in a molecular distillation reaction kettle for molecular distillation to obtain the mango kernel essential oil.
Preferably, in step S22, the microwave frequency is 200-450MHz, and the power is 600-800W; the microwave is treated by interval microwave; the interval microwave treatment mode is as follows: stopping the microwave for 1min after the microwave treatment is carried out for 30-45s, and then continuing the microwave treatment for 30-45s, wherein the total time of the interval microwave treatment is 120-150 s.
Compared with the prior art, the invention has the beneficial effects that:
1. the daily chemical product with the anti-radiation moisturizing oil and the preparation method thereof have the advantages that the raw material formula is scientific and reasonable, the raw materials are blended according to a reasonable proportion, the active ingredients of different raw materials are fully fused and complemented, the economic benefit, the social benefit and the popularization value are higher, the daily chemical product belongs to a pure natural skin care product, the daily chemical product does not contain essence, pigment, hormone, whitening agent and fluorescent agent, has obvious effects of whitening, moisturizing and locking water on skin, also has the effects of resisting radiation, moistening and moisturizing and sun-blocking, is natural and safe in components, has no toxic or side effect, has no stimulation, and is suitable for people with various skin qualities.
2. In the invention, the added mango seed essential oil contains plant polyphenol which has an antioxidant effect; has strong inhibiting and killing effects on bacteria and fungi.
3. The ginseng extract can make skin smooth, soft and elastic, delay senility and inhibit the generation of melanin, and the ginseng total saponin extract can be slowly absorbed by skin without any harmful stimulation to skin, can expand skin capillary vessels, promote skin blood circulation, increase skin nutrition, regulate skin water-oil balance, prevent skin dehydration, hardening and wrinkling, and can enhance skin elasticity and make cells regenerate after long-term use of the product containing ginseng. Meanwhile, the ginseng active substance also has the function of inhibiting the reduction of melanin, so that the skin is white and smooth. Its beauty effect is not good, and it is an excellent product for skin care and beauty.
4. In the invention, the added pawpaw extract contains rich papain, vitamin C, vitamin B, calcium, phosphorus and mineral substances, and is also rich in beta carotene, protein, calcium salt, protease, citrate enzyme and the like. Papain has the function of decomposing and removing aged horny layer on the surface of skin, and is a natural antioxidant capable of effectively resisting oxidation of systemic cells and destroying oxygen free radicals which can accelerate aging of human body.
5. In the invention, the added rose essential oil is an extract of rose, is widely applied to cosmetics, health products and foods, has the effects of resisting bacteria, calming, regulating endocrine, promoting metabolism and the like, and is called 'liquid gold'. However, in the process of producing the rose essential oil, most of the byproduct rose dregs can only be treated as waste, which wastes resources and pollutes the environment. Studies have proved that the rose dregs contain comprehensive amino acid components, vitamin C, anthocyanin components and flavonoid compounds, and have good capacities of resisting oxidation and removing free radicals. Therefore, the mask mud takes the rose dregs as the main component, has the effects of whitening, replenishing water, locking water and the like, reduces the cost, avoids resource waste and improves the economic benefit.
6. In the invention, the resveratrol and the UV-filtering agent are added to be polyphenol compounds, and the main sources are plants such as giant knotweed rhizome, grape, peanut and the like. Resveratrol is a very strong antioxidant, and can remove or inhibit the generation of free radicals, thereby playing the role of antioxidation and simultaneously having the function of water replenishing. And reports prove that the resveratrol which is a plant hormone can reduce melanin synthesis, thereby achieving the whitening effect. Although resveratrol has the above advantages, it is poorly soluble in water, but is dissolved in a polyhydric alcohol (e.g., glycerin), and is sensitive to UV, which induces decomposition of resveratrol, and the like, and thus its use in cosmetics is greatly limited. However, many years of research by scientists have demonstrated that the combination of resveratrol with UV-filters and polyols also has: preventing or reducing UV-induced breakdown of resveratrol; enhances dermal permeability and thus improves bioavailability; recrystallization of the resveratrol is avoided, and the solubility is improved; enhancing the stability of the cosmetic formulation.
7. In the invention, the added procyanidin is a bioflavonoid with a special molecular structure, and the polyhydroxy structure in the structure ensures that the bioflavonoid has special antioxidant activity and free radical scavenging capability, is widely applied in the field of cosmetics and enjoys the reputation of skin vitamins and oral cosmetics. The combined use of procyanidin and hydroxytyrosol has been reported to have a synergistic effect, reduce the synthesis of melanin, maintain the synthesis of collagen, and improve the skin elasticity, so as to achieve the effects of whitening and moisturizing.
8. In the invention, the added oat beta-glucan can regulate blood sugar, improve immunity, resist tumors, resist aging and the like, and the excellent effect of the oat beta-glucan in radiation resistance is discovered by scientists in recent years, thus gradually drawing wide attention all over the world. The results of numerous animal and plant experiments show that the radiation-resistant effect of the beta-1, 3-D-glucan derived from the oat is the strongest, so the beta-1, 3-D-glucan of the oat is also called as the immune polysaccharide. The biological activity of the beta-1, 3-D-glucan of the oat mainly embodies the following aspects: regulating immunity of human body; anti-tumor; radiation resistance; anti-inflammatory effects; promoting the repair of the organism and healing the wound; and (5) moisturizing.
9. According to the invention, the added preservative has good synergistic effect, small usage amount, strong bactericidal power and strong lasting effect, can provide comprehensive preservative protection for daily chemical products, effectively prevents microorganisms from generating drug resistance to the preservative, and has high preservative safety and comprehensive guarantee.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention provides the following technical scheme:
example 1
A daily chemical product with anti-radiation moisturizing oil and a preparation method thereof comprise the following raw materials in parts by weight: 70 parts of mango seed essential oil, 45 parts of ginseng total saponin extract, 35 parts of pawpaw extract, 12 parts of rose essential oil, 17 parts of resveratrol, 12 parts of UV-filtering agent, 15 parts of procyanidine, 4 parts of olive oil, 10 parts of oat beta-glucan and a proper amount of preservative and purified water.
The preparation method of the daily chemical product with the anti-radiation moisturizing oil in the embodiment comprises the following steps:
s1: weighing the raw materials in parts by weight;
s2: putting mango seed essential oil, ginseng total saponin extract liquor and pawpaw extract liquor into purified water for soaking for 12 hours, wherein the ratio of the amount of the added purified water to the amount of the extract liquor is 1: 1, boiling for 3 hours, and then continuously keeping the boiling state for 7 hours by using slow fire to obtain a mixed solution;
s3: filtering the mixed solution, sequentially adding rose essential oil, resveratrol, UV-filtering agent, procyanidine, olive oil, oat beta-glucan and preservative into the filtrate, and uniformly mixing;
s4: cooling to room temperature, cooling the filtrate, and filtering again to obtain filtrate, namely the anti-radiation moisturizing oil daily chemical product;
s5: sterilizing, packaging, and bottling.
The UV-filter in this example is a mixture of free titanium dioxide and zinc oxide.
Specifically, the preservative comprises the following substances in percentage by weight: 20 percent of chlorphenesin, 50 percent of 2-bromo-2-nitro-1, 3-propylene glycol, 29.7 percent of solubilizer and 0.3 percent of iminodisuccinic acid.
Furthermore, the solubilizer adopts polyoxyethylene ether.
Further, the sterilization in step S5 is performed at 90 ℃ for 40 min.
In this embodiment, the method for extracting mango seed essential oil includes the following steps:
s21: drying mango seeds, and crushing and sieving by a 50-mesh sieve to prepare mango seed powder for later use;
s22: spraying a small amount of water into the mango seed powder until the water content of the mango seed powder is 18%; placing the mango seed powder at 0 ℃ for cold storage for 25h, performing microwave treatment on the mango seed powder, and cooling to room temperature for later use;
s23: placing the mango seed powder subjected to microwave pretreatment in supercritical CO2Supercritical CO is carried out in an extraction kettle of an extraction device2Extracting, separating the extract in a separating tank to obtain coarse essential oil of mango seed from the bottom of the separating tank and CO from the top of the separating tank2，CO2After gasification, the mixture enters an extraction device for recycling; the supercritical CO2The extraction conditions were: under supercritical conditions, CO2The flow rate of (A) is 20L/min, the extraction pressure is 30MPa, the extraction temperature is 45 ℃, the resolution temperature is 35 ℃, and the extraction time isIs 2 h; in the separation tank, the extract is subjected to reduced pressure separation and extraction, the pressure of the separation tank is 12MPa, and the temperature is 40 ℃;
s24: and placing the obtained mango kernel crude essential oil in a molecular distillation reaction kettle for molecular distillation to obtain the mango kernel essential oil.
It should be noted that, in step S22, the microwave frequency is 30MHz, and the power is 750W; the microwave is treated by interval microwave; the interval microwave treatment mode is as follows: stopping the microwave for 1min after the microwave lasts for 45s, and continuing the microwave for 45s, wherein the total time of the interval microwave treatment is 150 s.
Example 2
A daily chemical product with anti-radiation moisturizing oil and a preparation method thereof comprise the following raw materials in parts by weight: 80 parts of mango seed essential oil, 50 parts of ginseng total saponin extract, 40 parts of pawpaw extract, 15 parts of rose essential oil, 20 parts of resveratrol, 15 parts of UV-filtering agent, 15 parts of procyanidine, 5 parts of olive oil, 15 parts of oat beta-glucan and a proper amount of preservative and purified water.
The preparation method of the daily chemical product with the anti-radiation moisturizing oil in the embodiment comprises the following steps:
s1: weighing the raw materials in parts by weight;
s2: putting the mango seed essential oil, the ginseng total saponin extract and the pawpaw extract into purified water for soaking for 15 hours, wherein the ratio of the amount of the added purified water to the amount of the extract is 1.5: 1, boiling for 4 hours, and then continuously keeping the boiling state for 7 hours by using slow fire to obtain a mixed solution;
s3: filtering the mixed solution, sequentially adding rose essential oil, resveratrol, UV-filtering agent, procyanidine, olive oil, oat beta-glucan and preservative into the filtrate, and uniformly mixing;
s4: cooling to room temperature, cooling the filtrate, and filtering again to obtain filtrate, namely the anti-radiation moisturizing oil daily chemical product;
s5: sterilizing, packaging, and bottling.
The UV-filter in this example is free titanium dioxide.
Specifically, the preservative comprises the following substances in percentage by weight: 15 percent of chlorphenesin, 60 percent of 2-bromo-2-nitro-1, 3-propylene glycol, 24.5 percent of solubilizer and 0.5 percent of iminodisuccinic acid.
Furthermore, the solubilizer adopts polyoxypropylene ether.
Further, the sterilization in step S5 is performed at 95 ℃ for 30 min.
In this embodiment, the method for extracting mango seed essential oil includes the following steps:
s21: drying mango seeds, and crushing and sieving by a 50-mesh sieve to prepare mango seed powder for later use;
s22: spraying a small amount of water into the mango seed powder until the water content of the mango seed powder is 18%; placing the mango seed powder at 0 ℃ for cold storage for 25h, performing microwave treatment on the mango seed powder, and cooling to room temperature for later use;
s23: placing the mango seed powder subjected to microwave pretreatment in supercritical CO2Supercritical CO is carried out in an extraction kettle of an extraction device2Extracting, separating the extract in a separating tank to obtain coarse essential oil of mango seed from the bottom of the separating tank and CO from the top of the separating tank2，CO2After gasification, the mixture enters an extraction device for recycling; the supercritical CO2The extraction conditions were: under supercritical conditions, CO2The flow rate of the extraction is 20L/min, the extraction pressure is 30MPa, the extraction temperature is 45 ℃, the resolution temperature is 35 ℃, and the extraction time is 2 h; in the separation tank, the extract is subjected to reduced pressure separation and extraction, the pressure of the separation tank is 12MPa, and the temperature is 40 ℃;
s24: and placing the obtained mango kernel crude essential oil in a molecular distillation reaction kettle for molecular distillation to obtain the mango kernel essential oil.
It should be noted that, in step S22, the microwave frequency is 30MHz, and the power is 750W; the microwave is treated by interval microwave; the interval microwave treatment mode is as follows: stopping the microwave for 1min after the microwave lasts for 45s, and continuing the microwave for 45s, wherein the total time of the interval microwave treatment is 150 s.
Example 3
A daily chemical product with anti-radiation moisturizing oil and a preparation method thereof comprise the following raw materials in parts by weight: 60 parts of mango seed essential oil, 40 parts of ginseng total saponin extract, 30 parts of pawpaw extract, 10 parts of rose essential oil, 15 parts of resveratrol, 10 parts of UV-filtering agent, 10 parts of procyanidine, 3 parts of olive oil, 8 parts of oat beta-glucan and a proper amount of preservative and purified water.
The preparation method of the daily chemical product with the anti-radiation moisturizing oil in the embodiment comprises the following steps:
s1: weighing the raw materials in parts by weight;
s2: putting mango seed essential oil, ginseng total saponin extract liquor and pawpaw extract liquor into purified water for soaking for 10 hours, wherein the ratio of the amount of the added purified water to the amount of the extract liquor is 1.3: 1, boiling for 4 hours, and then continuously keeping the boiling state for 6 hours by using slow fire to obtain a mixed solution;
s3: filtering the mixed solution, sequentially adding rose essential oil, resveratrol, UV-filtering agent, procyanidine, olive oil, oat beta-glucan and preservative into the filtrate, and uniformly mixing;
s4: cooling to room temperature, cooling the filtrate, and filtering again to obtain filtrate, namely the anti-radiation moisturizing oil daily chemical product;
s5: sterilizing, packaging, and bottling.
The UV-filter in this example is zinc oxide.
Specifically, the preservative comprises the following substances in percentage by weight: 20 percent of chlorphenesin, 60 percent of 2-bromo-2-nitro-1, 3-propylene glycol, 19.9 percent of solubilizer and 0.1 percent of iminodisuccinic acid.
Furthermore, the solubilizer adopts polyoxypropylene ether.
Further, the sterilization in step S5 is performed at 85 ℃ for 45 min.
In this embodiment, the method for extracting mango seed essential oil includes the following steps:
s21: drying mango seeds, and crushing and sieving by a 50-mesh sieve to prepare mango seed powder for later use;
s22: spraying a small amount of water into the mango seed powder until the water content of the mango seed powder is 18%; placing the mango seed powder at 0 ℃ for cold storage for 25h, performing microwave treatment on the mango seed powder, and cooling to room temperature for later use;
s23: placing the mango seed powder subjected to microwave pretreatment in supercritical CO2Supercritical CO is carried out in an extraction kettle of an extraction device2Extracting, separating the extract in a separating tank to obtain coarse essential oil of mango seed from the bottom of the separating tank and CO from the top of the separating tank2，CO2After gasification, the mixture enters an extraction device for recycling; the supercritical CO2The extraction conditions were: under supercritical conditions, CO2The flow rate of the extraction is 20L/min, the extraction pressure is 30MPa, the extraction temperature is 45 ℃, the resolution temperature is 35 ℃, and the extraction time is 2 h; in the separation tank, the extract is subjected to reduced pressure separation and extraction, the pressure of the separation tank is 12MPa, and the temperature is 40 ℃;
s24: and placing the obtained mango kernel crude essential oil in a molecular distillation reaction kettle for molecular distillation to obtain the mango kernel essential oil.
It should be noted that, in step S22, the microwave frequency is 30MHz, and the power is 750W; the microwave is treated by interval microwave; the interval microwave treatment mode is as follows: stopping the microwave for 1min after the microwave lasts for 45s, and continuing the microwave for 45s, wherein the total time of the interval microwave treatment is 150 s.
(1) In the invention, the added plant polyphenol contained in the mango seed essential oil has an antioxidant effect; has strong inhibiting and killing effects on bacteria and fungi.
(2) The ginseng extract can make skin smooth, soft and elastic, delay senility and inhibit the generation of melanin, and the ginseng total saponin extract can be slowly absorbed by skin without any harmful stimulation to skin, can expand skin capillary vessels, promote skin blood circulation, increase skin nutrition, regulate skin water-oil balance, prevent skin dehydration, hardening and wrinkling, and can enhance skin elasticity and make cells regenerate after long-term use of the product containing ginseng. Meanwhile, the ginseng active substance also has the function of inhibiting the reduction of melanin, so that the skin is white and smooth. Its beauty effect is not good, and it is an excellent product for skin care and beauty.
(3) In the invention, the added pawpaw extract contains rich papain, vitamin C, vitamin B, calcium, phosphorus and mineral substances, and is also rich in beta carotene, protein, calcium salt, protease, citrate enzyme and the like. Papain has the function of decomposing and removing aged horny layer on the surface of skin, and is a natural antioxidant capable of effectively resisting oxidation of systemic cells and destroying oxygen free radicals which can accelerate aging of human body.
(4) In the invention, the added rose essential oil is an extract of rose, is widely applied to cosmetics, health products and foods, has the effects of resisting bacteria, calming, regulating endocrine, promoting metabolism and the like, and is called 'liquid gold'. However, in the process of producing the rose essential oil, most of the byproduct rose dregs can only be treated as waste, which wastes resources and pollutes the environment. Studies have proved that the rose dregs contain comprehensive amino acid components, vitamin C, anthocyanin components and flavonoid compounds, and have good capacities of resisting oxidation and removing free radicals. Therefore, the mask mud takes the rose dregs as the main component, has the effects of whitening, replenishing water, locking water and the like, reduces the cost, avoids resource waste and improves the economic benefit.
(5) In the invention, the resveratrol and the UV-filtering agent are added to be polyphenol compounds, and the main sources are plants such as giant knotweed rhizome, grape, peanut and the like. Resveratrol is a very strong antioxidant, and can remove or inhibit the generation of free radicals, thereby playing the role of antioxidation and simultaneously having the function of water replenishing. And reports prove that the resveratrol which is a plant hormone can reduce melanin synthesis, thereby achieving the whitening effect. Although resveratrol has the above advantages, it is poorly soluble in water, but is dissolved in a polyhydric alcohol (e.g., glycerin), and is sensitive to UV, which induces decomposition of resveratrol, and the like, and thus its use in cosmetics is greatly limited. However, many years of research by scientists have demonstrated that the combination of resveratrol with UV-filters and polyols also has: preventing or reducing UV-induced breakdown of resveratrol; enhances dermal permeability and thus improves bioavailability; recrystallization of the resveratrol is avoided, and the solubility is improved; enhancing the stability of the cosmetic formulation.
(6) In the invention, the added procyanidin is a bioflavonoid with a special molecular structure, and the polyhydroxy structure in the structure ensures that the bioflavonoid has special antioxidant activity and free radical scavenging capability, is widely applied in the field of cosmetics and enjoys the reputation of skin vitamins and oral cosmetics. The combined use of procyanidin and hydroxytyrosol has been reported to have a synergistic effect, reduce the synthesis of melanin, maintain the synthesis of collagen, and improve the skin elasticity, so as to achieve the effects of whitening and moisturizing.
(7) In the invention, the added oat beta-glucan can regulate blood sugar, improve immunity, resist tumors, resist aging and the like, and the excellent effect of the oat beta-glucan in radiation resistance is discovered by scientists in recent years, thus gradually drawing wide attention all over the world. The results of numerous animal and plant experiments show that the radiation-resistant effect of the beta-1, 3-D-glucan derived from the oat is the strongest, so the beta-1, 3-D-glucan of the oat is also called as the immune polysaccharide. The biological activity of the beta-1, 3-D-glucan of the oat mainly embodies the following aspects: 1) regulating immunity of human body; 2) anti-tumor; 3) radiation resistance; 4) anti-inflammatory effects; 5) promoting the repair of the organism and healing the wound; 6) and (5) moisturizing.
(8) According to the invention, the added preservative has good synergistic effect, small usage amount, strong bactericidal power and strong lasting effect, can provide comprehensive preservative protection for daily chemical products, effectively prevents microorganisms from generating drug resistance to the preservative, and has high preservative safety and comprehensive guarantee.
The daily chemical product with the anti-radiation moisturizing oil and the preparation method thereof have the advantages that the raw material formula is scientific and reasonable, the raw materials are blended according to a reasonable proportion, the active ingredients of different raw materials are fully fused and complemented, the economic benefit, the social benefit and the popularization value are higher, the daily chemical product belongs to a pure natural skin care product, the daily chemical product does not contain essence, pigment, hormone, whitening agent and fluorescent agent, has obvious effects of whitening, moisturizing and locking water on skin, also has the effects of resisting radiation, moistening and moisturizing and sun-blocking, is natural and safe in components, has no toxic or side effect, has no stimulation, and is suitable for people with various skin qualities.
The foregoing shows and describes the general principles, essential features, and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, and the preferred embodiments of the present invention are described in the above embodiments and the description, and are not intended to limit the present invention. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (9)
1. A daily chemical product with anti-radiation moisturizing oil and a preparation method thereof are characterized in that: the feed comprises the following raw materials in parts by weight: 60-80 parts of mango seed essential oil, 40-50 parts of ginseng total saponin extract, 30-40 parts of pawpaw extract, 10-15 parts of rose essential oil, 15-20 parts of resveratrol, 10-15 parts of UV-filtering agent, 10-15 parts of procyanidine, 3-5 parts of olive oil, 8-15 parts of oat beta-glucan and a proper amount of preservative and purified water;
the preparation method of the radiation-resistant moisturizing oil daily chemical product comprises the following steps:
s1: weighing the raw materials in parts by weight;
s2: soaking mango seed essential oil, ginseng total saponin extract and pawpaw extract in purified water for 10-15h, wherein the ratio of the amount of the added purified water to the amount of the extract is 1-1.5: 1, boiling for 3-4h, and keeping the boiling state for 6-8h with slow fire to obtain a mixed solution;
s3: filtering the mixed solution, sequentially adding rose essential oil, resveratrol, UV-filtering agent, procyanidine, olive oil, oat beta-glucan and preservative into the filtrate, and uniformly mixing;
s4: cooling to room temperature, cooling the filtrate, and filtering again to obtain filtrate, namely the anti-radiation moisturizing oil daily chemical product;
s5: sterilizing, packaging, and bottling.
2. The daily chemical product with the radiation-resistant moisturizing oil and the preparation method thereof according to claim 1, wherein the daily chemical product comprises: the feed comprises the following raw materials in parts by weight: 70 parts of mango seed essential oil, 45 parts of ginseng total saponin extract, 35 parts of pawpaw extract, 12 parts of rose essential oil, 17 parts of resveratrol, 12 parts of UV-filtering agent, 15 parts of procyanidine, 4 parts of olive oil, 10 parts of oat beta-glucan and a proper amount of preservative and purified water.
3. The daily chemical product with the radiation-resistant moisturizing oil and the preparation method thereof according to claim 1, wherein the daily chemical product comprises: the feed comprises the following raw materials in parts by weight: 80 parts of mango seed essential oil, 50 parts of ginseng total saponin extract, 40 parts of pawpaw extract, 15 parts of rose essential oil, 20 parts of resveratrol, 15 parts of UV-filtering agent, 15 parts of procyanidine, 5 parts of olive oil, 15 parts of oat beta-glucan and a proper amount of preservative and purified water.
4. The daily chemical product with the radiation-resistant moisturizing oil and the preparation method thereof according to claim 1, wherein the daily chemical product comprises: the feed comprises the following raw materials in parts by weight: 60 parts of mango seed essential oil, 40 parts of ginseng total saponin extract, 30 parts of pawpaw extract, 10 parts of rose essential oil, 15 parts of resveratrol, 10 parts of UV-filtering agent, 10 parts of procyanidine, 3 parts of olive oil, 8 parts of oat beta-glucan and a proper amount of preservative and purified water.
5. The daily chemical product with the radiation-resistant moisturizing oil and the preparation method thereof according to claim 1, wherein the daily chemical product comprises: the UV-filter is free titanium dioxide, zinc oxide or a mixture of the two.
6. The daily chemical product with the radiation-resistant moisturizing oil and the preparation method thereof according to claim 1, wherein the daily chemical product comprises: the preservative comprises the following substances in percentage by weight: 15-20% of chlorphenesin, 45-60% of 2-bromo-2-nitro-1, 3-propylene glycol, 15-30% of solubilizer and 0.1-0.5% of iminodisuccinic acid.
7. The daily chemical product with the radiation-resistant moisturizing oil and the preparation method thereof according to claim 6, wherein the daily chemical product comprises: the solubilizer adopts polyoxyethylene ether or polyoxypropylene ether.
8. The daily chemical product with the radiation-resistant moisturizing oil and the preparation method thereof according to claim 1, wherein the daily chemical product comprises: the sterilization and disinfection in the step S5 is sterilization at 85-95 ℃ for 30-45 min.
9. The daily chemical product with the radiation-resistant moisturizing oil and the preparation method thereof according to claim 1, wherein the daily chemical product comprises: the extraction method of the mango seed essential oil comprises the following steps:
s21: drying mango seeds, and crushing the mango seeds through 40-60 meshes to prepare mango seed powder for later use;
s22: spraying a small amount of water into the mango seed powder until the water content of the mango seed powder is 15-20%; refrigerating the mango seed powder at 0-4 ℃ for 20-30h, performing microwave treatment on the mango seed powder, and cooling to room temperature for later use;
s23: placing the mango seed powder subjected to microwave pretreatment in supercritical CO2Supercritical CO is carried out in an extraction kettle of an extraction device2Extracting, separating the extract in a separating tank to obtain coarse essential oil of mango seed from the bottom of the separating tank and CO from the top of the separating tank2，CO2After gasification, the mixture enters an extraction device for recycling; the supercritical CO2The extraction conditions were: under supercritical conditions, CO2The flow rate of the extraction is 10-35L/min, the extraction pressure is 20-40MPa, the extraction temperature is 30-50 ℃, the resolution temperature is 30-40 ℃, and the extraction time is 1-3 h; in the separation tank, the extract is subjected to reduced pressure separation and extraction, the pressure of the separation tank is 10-15MPa, and the temperature is 25-55 ℃;
s24: and placing the obtained mango kernel crude essential oil in a molecular distillation reaction kettle for molecular distillation to obtain the mango kernel essential oil.
In step S22, the microwave frequency is 200-450MHz, and the power is 600-800W; the microwave is treated by interval microwave; the interval microwave treatment mode is as follows: stopping the microwave for 1min after the microwave treatment is carried out for 30-45s, and then continuing the microwave treatment for 30-45s, wherein the total time of the interval microwave treatment is 120-150 s.
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Application publication date: 20211130 |