CN113529244B - Preparation facilities of flame retardant fiber surface fabric - Google Patents
Preparation facilities of flame retardant fiber surface fabric Download PDFInfo
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- CN113529244B CN113529244B CN202110640399.XA CN202110640399A CN113529244B CN 113529244 B CN113529244 B CN 113529244B CN 202110640399 A CN202110640399 A CN 202110640399A CN 113529244 B CN113529244 B CN 113529244B
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- retardant
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- barrel
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- 239000003063 flame retardant Substances 0.000 title claims abstract description 66
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 title claims abstract description 62
- 239000004744 fabric Substances 0.000 title claims abstract description 48
- 239000000835 fiber Substances 0.000 title claims abstract description 36
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 239000000843 powder Substances 0.000 claims abstract description 44
- 238000007789 sealing Methods 0.000 claims abstract description 14
- 238000002156 mixing Methods 0.000 claims abstract description 7
- 238000003756 stirring Methods 0.000 claims description 24
- 238000011010 flushing procedure Methods 0.000 claims description 11
- 238000007664 blowing Methods 0.000 claims description 6
- 238000003780 insertion Methods 0.000 claims description 4
- 230000037431 insertion Effects 0.000 claims description 4
- 239000007921 spray Substances 0.000 claims description 3
- 238000004043 dyeing Methods 0.000 abstract description 25
- 239000002775 capsule Substances 0.000 abstract description 17
- 239000002131 composite material Substances 0.000 abstract description 16
- 238000009987 spinning Methods 0.000 abstract description 11
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract description 8
- 238000005406 washing Methods 0.000 abstract description 7
- 238000001035 drying Methods 0.000 abstract description 6
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 238000012360 testing method Methods 0.000 abstract description 5
- 229910021529 ammonia Inorganic materials 0.000 abstract description 4
- -1 drying Chemical compound 0.000 abstract description 3
- 230000001590 oxidative effect Effects 0.000 abstract description 3
- 238000004806 packaging method and process Methods 0.000 abstract description 3
- 230000000391 smoking effect Effects 0.000 abstract description 3
- 238000009941 weaving Methods 0.000 abstract description 3
- ADCOVFLJGNWWNZ-UHFFFAOYSA-N antimony trioxide Chemical compound O=[Sb]O[Sb]=O ADCOVFLJGNWWNZ-UHFFFAOYSA-N 0.000 description 24
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 12
- 238000002485 combustion reaction Methods 0.000 description 9
- 238000003860 storage Methods 0.000 description 7
- 230000000694 effects Effects 0.000 description 6
- 238000005096 rolling process Methods 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- MXRIRQGCELJRSN-UHFFFAOYSA-N O.O.O.[Al] Chemical compound O.O.O.[Al] MXRIRQGCELJRSN-UHFFFAOYSA-N 0.000 description 4
- 230000009471 action Effects 0.000 description 4
- 238000000354 decomposition reaction Methods 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- UOCLXMDMGBRAIB-UHFFFAOYSA-N 1,1,1-trichloroethane Chemical compound CC(Cl)(Cl)Cl UOCLXMDMGBRAIB-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 241000208125 Nicotiana Species 0.000 description 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000003763 carbonization Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000009970 fire resistant effect Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 238000009940 knitting Methods 0.000 description 1
- 238000010907 mechanical stirring Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000004080 punching Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
Images
Classifications
-
- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/50—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads
- D03D15/513—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads heat-resistant or fireproof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B23/00—Component parts, details, or accessories of apparatus or machines, specially adapted for the treating of textile materials, not restricted to a particular kind of apparatus, provided for in groups D06B1/00 - D06B21/00
- D06B23/20—Arrangements of apparatus for treating processing-liquids, -gases or -vapours, e.g. purification, filtration or distillation
- D06B23/205—Arrangements of apparatus for treating processing-liquids, -gases or -vapours, e.g. purification, filtration or distillation for adding or mixing constituents of the treating material
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
- D06B3/02—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fibres, slivers or rovings
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/45—Oxides or hydroxides of elements of Groups 3 or 13 of the Periodic Table; Aluminates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/47—Oxides or hydroxides of elements of Groups 5 or 15 of the Periodic Table; Vanadates; Niobates; Tantalates; Arsenates; Antimonates; Bismuthates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
- D06M23/12—Processes in which the treating agent is incorporated in microcapsules
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/30—Flame or heat resistance, fire retardancy properties
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Mechanical Engineering (AREA)
- Artificial Filaments (AREA)
Abstract
The invention provides a preparation device of a flame-retardant fiber fabric, which relates to the field of flame-retardant fabrics and comprises the steps of preparation of flame-retardant fibers, production of powder bags and comprehensive spinning of composite fabrics; the preparation process comprises the following steps: the preparation of the flame-retardant fiber comprises the steps of dip-dyeing a flame retardant, drying, ammonia smoking, oxidizing, washing and drying again; the production of the powder capsule comprises powder mixing, powder packaging and sealing test; the comprehensive spinning of the composite fabric comprises spinning of flame-retardant fibers, mixed weaving of the powder bag and the flame-retardant yarns, and the powder bag and the flame-retardant yarns are combined to form the composite fabric.
Description
Technical Field
The invention relates to the field of flame-retardant fabrics, in particular to a preparation device of a flame-retardant fiber fabric.
Background
Fire protection is to reduce the flammability of a material in a flame, slow down the flame propagation speed, and quickly self-extinguish and no longer shade-dyed after the flame is removed, and the combustion process of a fiber, i.e. from flaming combustion to becoming the final combustion product, needs to go through a series of complex physical and chemical changes, which have no obvious stage and can be generally divided into:
1) the fabric material is heated and cracked to generate combustible gas, non-combustible gas and carbonized residues;
2) flammable cracking, in which when the temperature reaches the ignition point or meets other fire sources, the fire is ignited and heat is released; and finishing the mixing of the tobacco.
3) The heat released causes the fibers to continue to crack and burn, causing the flame to spread.
The flame retardant principle of the existing flame retardant fabric is divided into two principles, one is to accelerate dehydration and carbonization of fibers to reduce combustible substances so as to achieve flame retardance, for example, ammonia treatment of the fabric and treatment of cotton cloth; the other is to change the internal structure of the fiber through a chemical process, reduce combustible components and achieve the purpose of flame retardance.
However, in view of the actual situation of the flame retardant fabric, although the flame retardant fabric has an excellent effect of preventing combustion, the flame retardant fabric is only limited to preventing combustion, and a layer of barrier is not applied on the surface of the fabric to isolate combustion before flame retardance, that is, for example, a firefighter participates in fire extinguishment, so that when the firefighter touches a fire source, the firefighter is protected based on the flame retardant fabric preventing combustion, but the fabric after flame retardance has impaired fiber strength due to the fact that the fabric has raised fire, and further, in the continuous activity of the firefighter, the fabric is damaged due to the decrease of fiber strength, so that the protection fails.
Based on special use scenes, a shielding layer is required to be formed before contacting a fire source, and the completeness of the flame-retardant fiber is protected to the maximum extent, so that an excellent flame-retardant protection effect is obtained.
Disclosure of Invention
The invention aims to provide a preparation device of a flame-retardant fiber fabric, which aims to solve the technical problem.
In order to solve the technical problems, the invention adopts the following technical scheme:
a preparation method of a flame-retardant fiber fabric is characterized by comprising the following steps: the method comprises the steps of preparing flame-retardant fibers, producing powder bags and comprehensively spinning composite fabrics;
the preparation process comprises the following steps:
1) the preparation of the flame-retardant fiber comprises the steps of dip-dyeing a flame retardant, drying, ammonia smoking, oxidizing, washing and drying again;
2) the production of the powder capsule comprises powder mixing, powder packaging and sealing test;
3) the comprehensive spinning of the composite fabric comprises spinning of flame-retardant fibers and mixed knitting of powder bags and the flame-retardant yarns;
wherein the powder comprises antimony trioxide and aluminum hydroxide, and the ratio of the antimony trioxide to the aluminum hydroxide is 6: 4;
the powder package is formed by taking a thermally decomposed capsule body as a wrapping object, and the powder is packaged by the wrapping object;
the air pressure in the air bag body is greater than the atmospheric pressure.
Preferably, the antimony trioxide and aluminum hydroxide inner powder is independent powder with clear particles, and the antimony trioxide and the aluminum hydroxide are uniformly mixed by a stirring device.
Preferably, the decomposition temperature of the capsule is 75 ℃, and the maximum temperature which can be borne by the capsule maintaining the shape is 72.6 ℃.
Preferably, the sealing test is to judge the sealing performance of the capsule by placing the capsule packed with the powder in water liquid on the premise that the capsule does not overflow bubbles and the powder.
Preferably, the powder bags are connected at the flame-retardant yarn positions at equal intervals to form the composite flame-retardant yarn, and the powder bags do not interfere with each other in the mixed spinning of the composite flame-retardant yarn.
Preferably, the powder receptacle is an elongate receptacle having a maximum thickness value less than three times the thickness value of the fire-resistant yarn.
Preferably, the flame retardant is tetra-light methyl chloroform, wherein the dip dyeing operation steps are as follows:
1) the fiber is placed in the flame retardant for dip dyeing, so that after the fiber is fully dip-dyed, the flame retardant is extruded out through rolling;
2) subsequently, the dip dyeing and rolling steps in the step 1) are repeated three times;
the dip dyeing and rolling steps are carried out for four times, and the dip dyeing time is set in a descending manner every time, wherein,
the first dip dyeing time is 42-48 minutes;
the second dip dyeing time is 32-39 minutes;
the third dip dyeing time is 24-31 minutes;
the fourth dip dyeing time is 14-19 minutes;
the temperature of the four-time dip dyeing is controlled within 25-39 ℃.
Preferably, the water solution after washing is stored through a storage tank, so that the flame retardant removed from the fibers is concentrated again in the separation and re-concentration step.
A preparation facilities of flame retardant fiber surface fabric which characterized in that: comprises a charging basket, a barrel cover and a stirring component;
a barrel cover matched with the charging barrel is arranged at the barrel opening of the charging barrel; the barrel cover is provided with a stirring assembly, the stirring assembly is inserted into the barrel cover in a crossed manner, and the stirring assembly and the barrel cover are arranged in a crossed manner after insertion;
the stirring subassembly includes the screw thread plug bush, screw thread plug bush and bung cross, inserts the axostylus axostyle in the screw thread plug bush, and the axostylus axostyle is than the two-way overhanging of screw thread plug bush, and the axostylus axostyle end connection outwards has a head, towards the inboard end connection of storage bucket towards the piece of blowing, one side of screw thread plug bush dorsad storage bucket is equipped with the spring, and the axostylus axostyle department is located to the spring housing, and the spring both ends respectively with head and screw thread plug bush looks fixed connection.
The flushing and blowing part comprises a sleeve, the sleeve is arranged in the charging barrel, a flushing plug matched with a pipe cavity of the sleeve is arranged on the inner side of the sleeve, and the flushing plug is connected with a coaxial rod and used for enabling a shaft lever to be inserted into the sleeve and slide with the sleeve; the plunger piston is characterized in that a return spring is further arranged in the plunger piston, the bottom of the return spring is connected with a sealing cover, the sealing cover is in threaded connection with the sleeve, the return spring is used for adjusting the relative position of the return spring to the plunger piston, and spray holes are uniformly distributed in the side wall of the sleeve.
The invention has the beneficial effects that:
1. according to the invention, the powder bag and the flame-retardant yarn are combined to form the composite fabric, and the composite fabric is used for swelling antimony trioxide and aluminum hydroxide powder out of the bag body under the action of air pressure based on the thermal decomposition of the bag body before contacting a fire source, and then the swelled antimony trioxide and aluminum hydroxide powder fall on the surface of clothes to form a flame-retardant layer, so that the combustion is further prevented, and a more excellent flame-retardant effect is achieved.
2. In the invention, the aluminum hydroxide forms fluid when contacting water, so that when the aluminum hydroxide is attached to the surface of the fabric, the problem that the structural strength of the fabric is reduced due to the fact that the flame-retardant fabric is burnt by a fire source, and further the fabric is damaged under continuous action, so that the protection strength is greatly reduced is solved.
Drawings
FIG. 1 is a schematic structural diagram of a device for preparing a flame-retardant fiber fabric according to the invention;
FIG. 2 is a schematic view of the split structure of the present invention;
FIG. 3 is a schematic view of the stirring assembly of the present invention;
FIG. 4 is a schematic cross-sectional view of a blow-molded article according to the present invention;
reference numerals: 1. a charging bucket; 2. a barrel cover; 3. a stirring assembly; 31. a handle head; 32. a shaft lever; 33. a spring; 34. inserting a thread; 35. punching and blowing the part; 351. sealing the cover; 352. a return spring; 353. plug flushing; 354. spraying a hole; 355. a sleeve.
Detailed Description
In order to make the technical means, the original characteristics, the achieved purposes and the effects of the invention easily understood, the invention is further described below with reference to the specific embodiments and the attached drawings, but the following embodiments are only the preferred embodiments of the invention, and not all embodiments. Based on the embodiments in the implementation, other embodiments obtained by those skilled in the art without any creative efforts belong to the protection scope of the present invention.
Specific embodiments of the present invention are described below.
Example 1
A preparation method of a flame-retardant fiber fabric comprises the steps of preparation of flame-retardant fibers, production of powder bags and comprehensive spinning of a composite fabric.
Wherein, the production of the powder capsule comprises powder mixing, powder packaging and sealing test;
the powder comprises antimony trioxide and aluminum hydroxide, the ratio of the antimony trioxide to the aluminum hydroxide is 6:4, the powder package is a capsule which is decomposed by heating and serves as a wrapping object, the powder is packaged by the wrapping object, the capsule is filled with nitrogen, and the air pressure value in the capsule is larger than the atmospheric pressure.
The antimony trioxide and the aluminum hydroxide are powder particles with distinct particles, and the antimony trioxide and the aluminum hydroxide are uniformly mixed by stirring equipment.
The decomposition temperature of the capsule body is 75 ℃, and the maximum temperature which can be borne by the capsule body maintaining the shape is 72.6 ℃.
The sealing test is to judge the sealing performance of the capsule by placing the capsule packed with powder into water liquid on the premise that the capsule does not overflow bubbles and powder.
In this embodiment, the powder bag and the flame-retardant yarn are combined to form a composite fabric, and the composite fabric is designed to bulge antimony trioxide and aluminum hydroxide powder from the bag body under the action of air pressure in the decomposition of the bag body before contacting with a fire source, and the expanded antimony trioxide and aluminum hydroxide powder fall on the surface of clothes to form a flame-retardant layer, so that combustion is further prevented, and a more excellent flame-retardant effect is achieved.
In this embodiment, when the aluminum hydroxide contacts water, a fluid is formed, so that when the aluminum hydroxide is attached to the surface of the fabric, the fire source is prevented from burning the flame-retardant fabric, the structural strength of the fabric is reduced, and further, under continuous action, the fabric is damaged, so that the protection strength is greatly reduced.
In this embodiment, the utricule has good sealed parcel dynamics at normal atmospheric temperature, promptly, wears the clothing that this composite fabric made, need not worry because of the utricule is under normal atmospheric temperature environment, and the utricule problem of breaking that appears is safe in utilization.
Example 2
A preparation method of a flame-retardant fiber fabric is characterized in that the comprehensive spinning of a composite fabric comprises spinning of flame-retardant fibers and mixed weaving of powder bags and flame-retardant yarns.
The powder bags are connected at equal intervals at the flame-retardant yarn positions to form the composite flame-retardant yarn, the powder bags do not mutually conflict and interfere in the mixed spinning of the composite flame-retardant yarn, the powder bags are slender bags, and the maximum thickness value of the slender bags is less than three times that of the flame-retardant yarn.
In this embodiment, the powder bag is long and thin utricule, and this setting can avoid because of the powder bag is too protruding in mixing weaving with fire-retardant yarn, the poor problem of the surface fabric comfort level that leads to, secondly, avoids relying on the powder bag as the contact to under the repeated contact friction, the utricule wearing and tearing problem that leads to.
Example 3
A preparation method of a flame-retardant fiber fabric comprises the steps of dip-dyeing a flame retardant, drying, ammonia smoking, oxidizing, washing and drying again.
Wherein the flame retardant is tetra-light methyl chloroform, and the dip dyeing comprises the following operation steps:
1) the fiber is placed in the flame retardant for dip dyeing, so that the flame retardant is extruded out through rolling after the fiber is fully dip-dyed;
2) subsequently, the dip dyeing and rolling steps in the step 1) are repeated three times;
the dip dyeing and rolling steps are carried out for four times, the dip dyeing time is set in a descending manner every time, wherein,
the first dip dyeing time is 42-48 minutes;
the second dip dyeing time is 32-39 minutes;
the third dip dyeing time is 24-31 minutes;
the fourth dip dyeing time is 14-19 minutes;
the temperature of the four-time dip dyeing is controlled within 25-39 ℃.
And (4) storing the water solution after washing through a storage tank so as to re-concentrate the flame retardant released from the fibers in the separation and re-concentration step.
In this embodiment, through repeated dip-dyeing many times for in the more abundant infiltration of fire retardant to the fibre, in order to obtain more outstanding flame retardant efficiency, simultaneously through the washing step, wash the fire retardant of too saturated in the dip-dyeing, in order after washing, through the separation reconcentration step under, concentrate the fire retardant that breaks away from in the fibre again, participate in the recycling.
Example 4
As shown in fig. 1-4, a device for preparing a flame-retardant fiber fabric comprises a charging basket 1, a barrel cover 2 and a stirring component 3; a barrel cover 2 matched with the charging barrel 1 is arranged at the barrel opening of the charging barrel 1; 2 departments of bung are equipped with stirring subassembly 3, stirring subassembly 3 is to 2 crossing insertions of bung, and stir subassembly 3 and bung 2 are the cross arrangement after inserting, stirring subassembly 3 includes screw thread plug bush 34, screw thread plug bush 34 and 2 cross insertions of bung, insert axostylus axostyle 32 in the screw thread plug bush 34, axostylus axostyle 32 is two-way overhanging than screw thread plug bush 34, axostylus axostyle 32 end connection outwards has a head 31, end connection towards the storage bucket 1 inboard has dash and blows piece 35, one side of screw thread plug bush 34 dorsad storage bucket 1 is equipped with spring 33, 32 departments are located to spring 33 cover, and spring 33 both ends are respectively with head 31 and screw thread plug bush 34 looks fixed connection.
Wherein, the flushing and blowing piece 35 comprises a sleeve 355, the sleeve 355 is arranged in the charging basket 1, a flushing plug 353 matched with the pipe cavity of the sleeve 355 is arranged at the inner side of the sleeve 355, and the flushing plug 353 is connected with the shaft 32 and is used for inserting the shaft 32 into the sleeve 355 and sliding with the sleeve 355; a return spring 352 is further arranged in the plunger 353, the bottom of the return spring 352 is connected with a sealing cover 351, the sealing cover 351 is connected with a sleeve 355 in a threaded mode and used for adjusting the relative position of the return spring 352 to the plunger 353, and spray holes 354 are uniformly arranged on the side wall of the sleeve 355.
In this embodiment, traditional mechanical stirring, because of the drive assembly noise magnitude of sound that adopts is big, the way, based on stirring subassembly 3 moves in storage bucket 1, stirs the processing to the powder, wherein stirs the processing and divide into two processes:
the handle 31 is pulled, and the impact blow piece 35 moves like a bullet in the charging basket 1 due to the elastic force accumulated by the spring 33 in the stretched state, and contacts with the powder, thereby achieving the purpose of mixing and stirring.
In addition, the shaft 32 is rapidly fired, compressing against the sleeve 355, i.e., compressing air through the plunger 353 into the sleeve 355, to further mix the powder as it is ejected through the orifice 354.
The foregoing shows and describes the general principles, essential features, and advantages of the invention. It should be understood by those skilled in the art that the present invention is not limited to the above embodiments, and the above embodiments and descriptions are only preferred examples of the present invention and are not intended to limit the present invention, and that various changes and modifications may be made without departing from the spirit and scope of the present invention, which fall within the scope of the claimed invention. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (1)
1. The utility model provides a preparation facilities of flame retardant fiber surface fabric for the mixing stirring of powder is handled, its characterized in that: comprises a charging basket (1), a basket cover (2) and a stirring component (3);
a barrel cover (2) matched with the charging barrel (1) is arranged at the barrel opening of the charging barrel (1); the barrel cover (2) is provided with a stirring component (3), the stirring component (3) is inserted into the barrel cover (2) in a crossed manner, and the stirring component (3) and the barrel cover (2) are arranged in a crossed manner after insertion;
the stirring assembly (3) comprises a threaded plug bush (34), the threaded plug bush (34) and the barrel cover (2) are crossed, a shaft rod (32) is inserted into the threaded plug bush (34), the shaft rod (32) extends outwards in a two-way mode compared with the threaded plug bush (34), the outward end part of the shaft rod (32) is connected with a handle head (31), the end part facing the inner side of the charging basket (1) is connected with a flushing and blowing piece (35), one side, back to the charging basket (1), of the threaded plug bush (34) is provided with a spring (33), the spring (33) is sleeved on the shaft rod (32), and two ends of the spring (33) are fixedly connected with the handle head (31) and the threaded plug bush (34) respectively;
the flushing and blowing piece (35) comprises a sleeve (355), the sleeve (355) is arranged in the charging basket (1), a flushing plug (353) matched with a pipe cavity of the sleeve is arranged on the inner side of the sleeve (355), and the flushing plug (353) is connected with the shaft rod (32) and used for inserting the shaft rod (32) into the sleeve (355) and sliding with the sleeve (355); the plunger (353) is further internally provided with a return spring (352), the bottom of the return spring (352) is connected with a sealing cover (351), the sealing cover (351) is connected with a sleeve (355) in an internal thread mode and used for adjusting the relative position of the return spring (352) to the plunger (353), and spray holes (354) are uniformly formed in the side wall of the sleeve (355).
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CN113529244B true CN113529244B (en) | 2022-08-26 |
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CN103694496A (en) * | 2013-09-16 | 2014-04-02 | 合肥中科阻燃新材料有限公司 | Preparation method of active magnesium hydroxide fire retardants |
CN105086416A (en) * | 2015-04-23 | 2015-11-25 | 广西华锑科技有限公司 | Antimony trioxide inorganic compound flame retardant masterbatch and preparation method thereof |
CN107142596B (en) * | 2017-06-24 | 2018-12-14 | 浙江西大门新材料股份有限公司 | The big jacquard curtain fabric of the fire-retardant complex function of health-care environment protection type negative oxygen ion |
CN107653505A (en) * | 2017-10-17 | 2018-02-02 | 高俊 | A kind of preparation method of flame retardant type sound insulation wall paper |
CN107557966A (en) * | 2017-10-17 | 2018-01-09 | 蓝星(成都)新材料有限公司 | A kind of composite flame-proof material and preparation method |
CN209133258U (en) * | 2018-12-20 | 2019-07-19 | 河南虹峰电缆股份有限公司 | One kind prevents pyrophoricity accident from expanding cable |
CN210994152U (en) * | 2019-07-10 | 2020-07-14 | 四川成邦药业有限公司 | Powder mixer |
CN213150443U (en) * | 2020-07-08 | 2021-05-07 | 安徽凌宇电缆科技有限公司 | High temperature resistant cable with local function of putting out a fire |
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