CN113476386A - 一种漱口液及其制备方法 - Google Patents
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Abstract
本发明公开了一种漱口液及其制备方法，按照重量份数计包括：海藻酸钠15～22份、聚乙烯醇6～10份、N‑琥珀酰壳聚糖3～8份、D‑异抗坏血酸2～5份、葡萄糖酸氯己定0.4～0.8份、菊花12～20份、金银花12～20份、荔枝壳10～15份、紫茉莉15～20份、麦门冬10～16份、壳聚糖8～14份、茅术醇4～8份、榄香醇3～5份、椰油酰基谷氨酸三乙醇胺盐2～6份、抗菌剂0.1～0.15份、纯水50～100份。
Description
技术领域
本发明属于漱口液技术领域，具体涉及一种漱口液及其制备方法。
背景技术
随着社会生活水平的提高，人们对口腔清洁卫生及健康越来越重视，在该方面的花费也越来越多。越来越多的人意识到仅靠早晚刷牙一次的生活习惯已经不能满足自身健康口腔的迫切需求，因此各种各样的漱口液应运而生，发展迅速。我国漱口的历史较刷牙悠久。虽然使用牙刷及牙线也是去除菌斑的有效措施，但是菌斑控制的方法较难科学掌握，而且乏味、费时、费力，特别对身心残疾的患者难以完成，缺乏动机的人也难以使用，对这部分人来说漱口液将是一种理想的最佳代替方法。实践研究证明，漱口液使用起来很方便、快捷且容易掌握，实际可行、既适合在家中进行日常的口腔护理，又适合工作、出差时便携使用。特别是追求高品质生活的青年人群，急切希望用各种手段使口气清新，漱口液则可在短时间内达到该效果。同时漱口液具有杀菌抑菌效能，在刷牙破坏牙菌斑生物膜特性后，其使用效果更佳。在刷牙后使用漱口液，比仅仅单独刷牙能更有效的控制牙菌斑，从而消除口腔中的污垢，起到净化口腔的功能。
发明内容
本发明的目的是提供一种漱口液，按照重量份数计包括：海藻酸钠15～22份、聚乙烯醇6～10份、N-琥珀酰壳聚糖3～8份、D-异抗坏血酸2～5份、葡萄糖酸氯己定0.4～0.8份、菊花12～20份、金银花12～20份、荔枝壳10～15份、紫茉莉15～20份、麦门冬10～16份、壳聚糖8～14份、茅术醇4～8份、榄香醇3～5份、椰油酰基谷氨酸三乙醇胺盐2～6份、抗菌剂0.1～0.15份、纯水50～100份。
进一步地，所述抗菌剂为金丝桃素。
一种漱口液的制备方法，其制备方法包括以下步骤：
S1：将菊花、金银花、荔枝壳、紫茉莉、麦门冬洗涤干净，晒干，磨粉过500～800目网筛，然后浸渍在乙醇水溶液中2～4天，备用。
S2：将海藻酸钠、聚乙烯醇、N-琥珀酰壳聚糖加入到纯水中，升温至60～80℃搅拌1.5～3h，然后将温度将至室温后加入D-异抗坏血酸、葡萄糖酸氯己定、茅术醇、榄香醇、椰油酰基谷氨酸三乙醇胺盐、抗菌剂继续搅拌1～2h。
S3：将步骤S1中得到的混合液过滤，离心，取上清液加入到步骤S2中，静置1～2天后便可得到。
进一步地，所述步骤S1中的乙醇水溶液的质量浓度为42～60％。
进一步地，所述步骤S3中的离心速率为6000～8000rpm/min，离心时间为10～15min。
与现有技术相比，本发明具有如下有益效果：
本发明中，采用海藻酸钠、聚乙烯醇、N-琥珀酰壳聚糖、D-异抗坏血酸、葡萄糖酸氯己定、菊花、金银花、荔枝壳、紫茉莉、麦门冬、壳聚糖、茅术醇、榄香醇、椰油酰基谷氨酸三乙醇胺盐、抗菌剂、纯水制备出一种漱口水，具有控制牙菌斑，消除口腔中的污垢，起到净化口腔的功能，同时添加草本植物有效清新口气，起到消炎杀菌等功效。
具体实施方式
下面对本发明实施例作具体详细的说明，本实施例在本发明技术方案为前提下进行实施，给出了详细的实施方式和具体的操作过程，应当指出，对于本技术领域的普通技术人员来说，在不脱离本发明原理的前提下，还可以做出若干改进和润饰，这些改进和润饰也应视为本发明的保护范围。
实施例1
一种漱口液，按照重量份数计包括：海藻酸钠15份、聚乙烯醇6份、N-琥珀酰壳聚糖3份、D-异抗坏血酸2份、葡萄糖酸氯己定0.4份、菊花12份、金银花12份、荔枝壳10份、紫茉莉15份、麦门冬10份、壳聚糖8份、茅术醇4份、榄香醇3份、椰油酰基谷氨酸三乙醇胺盐2份、纯水50份。
具体包括以下步骤：
S1：将菊花、金银花、荔枝壳、紫茉莉、麦门冬洗涤干净，晒干，磨粉过500～800目网筛，然后浸渍在质量浓度为42％的乙醇水溶液中2天，备用。
S2：将海藻酸钠、聚乙烯醇、N-琥珀酰壳聚糖加入到纯水中，升温至60℃搅拌1.5h，然后将温度将至室温后加入D-异抗坏血酸、葡萄糖酸氯己定、茅术醇、榄香醇、椰油酰基谷氨酸三乙醇胺盐、抗菌剂继续搅拌1h。
S3：将步骤S1中得到的混合液过滤，离心，取上清液加入到步骤S2中，静置1天后便可得到；其中离心速率为6000rpm/min，离心时间为10min。
实施例2
一种漱口液，按照重量份数计包括：海藻酸钠22份、聚乙烯醇10份、N-琥珀酰壳聚糖8份、D-异抗坏血酸5份、葡萄糖酸氯己定0.8份、菊花20份、金银花20份、荔枝壳15份、紫茉莉20份、麦门冬16份、壳聚糖14份、茅术醇8份、榄香醇5份、椰油酰基谷氨酸三乙醇胺盐6份、纯水100份。
具体包括以下步骤：
S1：将菊花、金银花、荔枝壳、紫茉莉、麦门冬洗涤干净，晒干，磨粉过800目网筛，然后浸渍在质量浓度为60％的乙醇水溶液中4天，备用。
S2：将海藻酸钠、聚乙烯醇、N-琥珀酰壳聚糖加入到纯水中，升温至80℃搅拌1.5～3h，然后将温度将至室温后加入D-异抗坏血酸、葡萄糖酸氯己定、茅术醇、榄香醇、椰油酰基谷氨酸三乙醇胺盐、抗菌剂继续搅拌2h。
S3：将步骤S1中得到的混合液过滤，离心，取上清液加入到步骤S2中，静置2天后便可得到；其中离心速率为8000rpm/min，离心时间为15min。
实施例3
一种漱口液，按照重量份数计包括：海藻酸钠18份、聚乙烯醇8份、N-琥珀酰壳聚糖5份、D-异抗坏血酸3份、葡萄糖酸氯己定0.6份、菊花15份、金银花15份、荔枝壳12份、紫茉莉17份、麦门冬12份、壳聚糖10份、茅术醇5份、榄香醇4份、椰油酰基谷氨酸三乙醇胺盐4份、纯水70份。
具体包括以下步骤：
S1：将菊花、金银花、荔枝壳、紫茉莉、麦门冬洗涤干净，晒干，磨粉过600目网筛，然后浸渍在质量浓度为50％的乙醇水溶液中3天，备用。
S2：将海藻酸钠、聚乙烯醇、N-琥珀酰壳聚糖加入到纯水中，升温至70℃搅拌2h，然后将温度将至室温后加入D-异抗坏血酸、葡萄糖酸氯己定、茅术醇、榄香醇、椰油酰基谷氨酸三乙醇胺盐、抗菌剂继续搅拌1.5h。
S3：将步骤S1中得到的混合液过滤，离心，取上清液加入到步骤S2中，静置1.5天后便可得到；其中离心速率为7000rpm/min，离心时间为12min。
实施例4
一种漱口液，按照重量份数计包括：海藻酸钠20份、聚乙烯醇9份、N-琥珀酰壳聚糖7份、D-异抗坏血酸4份、葡萄糖酸氯己定0.7份、菊花18份、金银花18份、荔枝壳14份、紫茉莉18份、麦门冬14份、壳聚糖12份、茅术醇7份、榄香醇4份、椰油酰基谷氨酸三乙醇胺盐5份、纯水90份。
具体包括以下步骤：
S1：将菊花、金银花、荔枝壳、紫茉莉、麦门冬洗涤干净，晒干，磨粉过500～800目网筛，然后浸渍在质量浓度为55％的乙醇水溶液中3天，备用。
S2：将海藻酸钠、聚乙烯醇、N-琥珀酰壳聚糖加入到纯水中，升温至75℃搅拌2.5h，然后将温度将至室温后加入D-异抗坏血酸、葡萄糖酸氯己定、茅术醇、榄香醇、椰油酰基谷氨酸三乙醇胺盐、抗菌剂继续搅拌1.7h。
S3：将步骤S1中得到的混合液过滤，离心，取上清液加入到步骤S2中，静置1.5天后便可得到；其中离心速率为7500rpm/min，离心时间为14min。
Claims (5)
1.一种漱口液，其特征在于，按照重量份数计包括：海藻酸钠15～22份、聚乙烯醇6～10份、N-琥珀酰壳聚糖3～8份、D-异抗坏血酸2～5份、葡萄糖酸氯己定0.4～0.8份、菊花12～20份、金银花12～20份、荔枝壳10～15份、紫茉莉15～20份、麦门冬10～16份、壳聚糖8～14份、茅术醇4～8份、榄香醇3～5份、椰油酰基谷氨酸三乙醇胺盐2～6份、抗菌剂0.1～0.15份、纯水50～100份。
2.根据权利要求1所述的一种漱口液，其特征在于，所述抗菌剂为金丝桃素。
3.根据权利要求1所述的一种漱口液的制备方法，其特征在于，所述制备方法包括以下步骤：
S1：将菊花、金银花、荔枝壳、紫茉莉、麦门冬洗涤干净，晒干，磨粉过500～800目网筛，然后浸渍在乙醇水溶液中2～4天，备用；
S2：将海藻酸钠、聚乙烯醇、N-琥珀酰壳聚糖加入到纯水中，升温至60～80℃搅拌1.5～3h，然后将温度将至室温后加入D-异抗坏血酸、葡萄糖酸氯己定、茅术醇、榄香醇、椰油酰基谷氨酸三乙醇胺盐、抗菌剂继续搅拌1～2h；
S3：将步骤S1中得到的混合液过滤，离心，取上清液加入到步骤S2中，静置1～2天后便可得到。
4.根据权利要求1所述的一种漱口液的制备方法，其特征在于，所述步骤S1中的乙醇水溶液的质量浓度为42～60％。
5.根据权利要求1所述的一种漱口液的制备方法，其特征在于，所述步骤S3中的离心速率为6000～8000rpm/min，离心时间为10～15min。
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