CN113429811A - 一种无机不粘复合涂层及其制备应用方法 - Google Patents

一种无机不粘复合涂层及其制备应用方法 Download PDF

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CN113429811A
CN113429811A CN202110813241.8A CN202110813241A CN113429811A CN 113429811 A CN113429811 A CN 113429811A CN 202110813241 A CN202110813241 A CN 202110813241A CN 113429811 A CN113429811 A CN 113429811A
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张来玉
邱国恩
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Henan Kelong Pinsheng Industrial Co ltd
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Abstract

本发明涉及一种无机不粘复合涂层及其制备应用方法，该涂层包括顶部不粘涂层和底部耐蚀层，顶部不粘涂层的重量份数的制备原料：第一丙烯酸树脂10‑30份，玻璃粉30‑50份，钛粉10‑30份，气相二氧化硅8‑10份，碳纤维40‑50份，石墨烯8‑10；底部耐蚀层的重量份数的制备原料：第二丙烯酸树脂90‑110份，低温玻璃粉20‑40份，助剂1‑2份。该涂层制备方法包括喷涂工艺和烧结工艺。本发明的涂层原料为无机材料，在使用过程中不会分解，使用安全；顶部不粘涂层的原料合理搭配，得到了不粘且耐刮性好的涂层；底部耐蚀层能够防止基材被腐蚀，具有抗热震，耐高温，耐刮伤，高附着力及高耐候性等特点。

Description

一种无机不粘复合涂层及其制备应用方法
技术领域
本发明涉及一种高温不粘涂料，尤其是一种无机不粘复合涂层及其制备方法。
背景技术
现有技术针对铁基不粘涂料采取的技术方案为：现有涂料使用聚四氟乙烯乳液和聚醚砜树脂作为原料，采用一定比例混合的形式实现铁基不粘涂料的制作。
该技术的缺点为：
(1)不耐刮(不能用铁铲).不耐高温(温度超260度以上会分解有害气体)。
(2)涂层容易脱落，使用寿命短(普遍使用一个月后会出现粘锅现象)。
发明内容
本发明是要提供一种无机不粘复合涂层及其制备应用方法，用于解决铁基涂层不耐刮、不耐高温以及使用寿命短的问题。
为实现上述目的，本发明采用的技术方案是：一种无机不粘复合涂层，包括顶部不粘涂层和底部耐蚀层，
所述顶部不粘涂层包括以下重量份数的制备原料：
第一丙烯酸树脂10-30份，玻璃粉30-50份，钛粉10-30份，气相二氧化硅8-10份，碳纤维40-50份，石墨烯8-10；按顺序将物料投入研磨缸分散10分钟后，进行研磨至合格细度≤30um；
所述底部耐蚀层包括以下重量份数的制备原料：
第二丙烯酸树脂90-110份，低温玻璃粉20-40份，助剂1-2份；按顺序将物料投入研磨缸分散10分钟后，进行研磨至合格细度≤30um。
进一步，所述无机不粘复合涂层的涂层硬度：三菱铅笔＞9H
进一步，所述无机不粘复合涂层的耐温时效：≤500℃，＞1000h
一种无机不粘复合涂层的制备应用方法，包括：喷涂工艺、烧结工艺和使用方法，
所述喷涂工艺：
1)喷涂：采用空气喷涂，选用的普通喷枪的技术参数如下：
喷枪口径：1.0-2.0mm；
喷涂压力：2.0Kgf/cm2～4.0Kgf/cm2；
喷涂距离：15～25cm；
2)工艺要求：
(1)喷涂环境需要相对干燥，通风，无尘，降低因环境因素影响到喷涂的质量；
(2)喷涂前使用150-200目丝网过滤；
(3)涂层厚度，底部耐蚀层厚度为25μm--35μm；顶部不粘涂层厚度为15μm-25μm；
(4)喷涂时要注意涂层均匀、平整，防止涂膜厚度过薄遮盖不好，过厚易流挂、气泡现象出现；
所述烧结工艺：
1)底部耐蚀层表干150-170℃烘烤5-8分钟，然后对基材进行降温，待基材表面温度降至常温，即可进行顶部不粘涂层喷涂；
2)顶部不粘涂层固化温度为1段排水工段150～170℃/5-8分钟、2段排胶工段350～370℃/5-8分钟，3段固化段645～655℃/8-10分钟；
所述使用方法：
1)所述无机不粘复合涂层产品制备时要佩戴好合适的防护用具；
2)处理废弃物时要遵守废弃物处理的有关规定；
3)应急措施：
(1)浆料溅入眼睛时，即用大量清水冲洗至少5分钟，然后视情况接受医生治疗；
(2)吸入分解的气体时，应立即到新鲜空气的地方；
(3)涂料粘在皮肤上时，请用肥皂和水彻底清洗；
4)包装.贮存与运输
(1)所述无机不粘复合涂层产品应该在干燥，避雨，遮阳的环境中存放，在温度5-40℃环境下存放；
(2)运输按非危险品规则办理；
(3)正常保存环境下，所述无机不粘复合涂层产品保存期为6个月，超过保存期视产品变化情况使用。
本发明的有益效果在于：
1.涂层原料为无机材料，在使用过程中不会分解，使用安全；顶部不粘涂层的原料合理搭配，得到了不粘且耐刮性好的涂层。
2.底部耐蚀层能够防止基材被腐蚀，由于耐蚀层和不粘涂层的主要成分分别为低温玻璃粉和玻璃粉，形成高密度和稳定的无机玻璃态涂层，抗热震，耐高温，耐刮伤，高附着力及高耐候性。
附图说明
图1是本发明的一种无机不粘复合涂层结构示意图。
具体实施方式
下面结合附图与实施例对本发明作进一步说明。
本发明为解决铁基(低碳钢，铸铁，不锈钢，铁合金等)不粘涂层存在不耐刮、不耐高温及使用寿命短的问题所采取的技术方案为：
一种无机不粘复合涂层，包括顶部不粘涂层1和底部耐蚀层2，见图1，
顶部不粘涂层1包括以下重量份数的制备原料：
第一丙烯酸树脂10-30份，玻璃粉30-50份，钛粉10-30份，气相二氧化硅8-10份，碳纤维40-50份，石墨烯8-10；按顺序将物料投入研磨缸分散10分钟后，进行研磨至合格细度≤30um；
底部耐蚀层2包括以下重量份数的制备原料：
第二丙烯酸树脂90-110份，低温玻璃粉20-40份，助剂1-2份；按顺序将物料投入研磨缸分散10分钟后，进行研磨至合格细度≤30um。
性能参数：
1、涂层硬度(三菱铅笔＞9H)
2、涂层耐温时效(≤500℃，＞1000h)
一种无机不粘复合涂层的制备应用方法，其特征在于，包括：喷涂工艺、烧结工艺和使用方法，
所述喷涂工艺：
1)喷涂：采用空气喷涂，选用的普通喷枪的技术参数如下：
喷枪口径：1.0-2.0mm；
喷涂压力：2.0Kgf/cm2～4.0Kgf/cm2；
喷涂距离：15～25cm；
2)工艺要求：
(1)喷涂环境需要相对干燥，通风，无尘，降低因环境因素影响到喷涂的质量；
(2)喷涂前使用150-200目丝网过滤；
(3)涂层厚度，底部耐蚀层厚度为25μm--35μm；顶部不粘涂层厚度为15μm-25μm；
(4)喷涂时要注意涂层均匀、平整，防止涂膜厚度过薄遮盖不好，过厚易流挂、气泡现象出现；
所述烧结工艺：
1)底部耐蚀层表干150-170℃烘烤5-8分钟，然后对基材进行降温，待基材表面温度降至常温，即可进行顶部不粘涂层喷涂；
2)顶部不粘涂层固化温度为1段排水工段150～170℃/5-8分钟、2段排胶工段350～370℃/5-8分钟，3段固化段645～655℃/8-10分钟；
所述使用方法：
1)所述无机不粘复合涂层产品制备时要佩戴好合适的防护用具；
2)处理废弃物时要遵守废弃物处理的有关规定；
3)应急措施：
(1)浆料溅入眼睛时，即用大量清水冲洗至少5分钟，然后视情况接受医生治疗；
(2)吸入分解的气体时，应立即到新鲜空气的地方；
(3)涂料粘在皮肤上时，请用肥皂和水彻底清洗；
4)包装.贮存与运输
(1)所述无机不粘复合涂层产品应该在干燥，避雨，遮阳的环境中存放，在温度5-40℃环境下存放；
(2)运输按非危险品规则办理；
(3)正常保存环境下，所述无机不粘复合涂层产品保存期为6个月，超过保存期视产品变化情况使用。

Claims (4)

1.一种无机不粘复合涂层，其特征在于：包括顶部不粘涂层和底部耐蚀层，
所述顶部不粘涂层包括以下重量份数的制备原料：
第一丙烯酸树脂10-30份，玻璃粉30-50份，钛粉10-30份，气相二氧化硅8-10份，碳纤维40-50份，石墨烯8-10；按顺序将物料投入研磨缸分散10分钟后，进行研磨至合格细度≤30um；
所述底部耐蚀层包括以下重量份数的制备原料：
第二丙烯酸树脂90-110份，低温玻璃粉20-40份，助剂1-2份；按顺序将物料投入研磨缸分散10分钟后，进行研磨至合格细度≤30um。
2.根据权利要求1所述的无机不粘复合涂层，其特征在于：所述无机不粘复合涂层的涂层硬度：三菱铅笔＞9H。
3.根据权利要求1所述的无机不粘复合涂层，其特征在于：所述无机不粘复合涂层的耐温时效：≤500℃，＞1000h。
4.一种权利要求1-3任一所述的无机不粘复合涂层的制备应用方法，其特征在于，包括：喷涂工艺、烧结工艺和使用方法，
所述喷涂工艺：
1)喷涂：采用空气喷涂，选用的普通喷枪的技术参数如下：
喷枪口径：1.0-2.0mm；
喷涂压力：2.0Kgf/cm2～4.0Kgf/cm2；
喷涂距离：15～25cm；
2)工艺要求：
(1)喷涂环境需要相对干燥，通风，无尘，降低因环境因素影响到喷涂的质量；
(2)喷涂前使用150-200目丝网过滤；
(3)涂层厚度，底部耐蚀层厚度为25μm--35μm；顶部不粘涂层厚度为15μm-25μm；
(4)喷涂时要注意涂层均匀、平整，防止涂膜厚度过薄遮盖不好，过厚易流挂、气泡现象出现；
所述烧结工艺：
1)底部耐蚀层表干150-170℃烘烤5-8分钟，然后对基材进行降温，待基材表面温度降至常温，即可进行顶部不粘涂层喷涂；
2)顶部不粘涂层固化温度为1段排水工段150～170℃/5-8分钟、2段排胶工段350～370℃/5-8分钟，3段固化段645～655℃/8-10分钟；
所述使用方法：
1)所述无机不粘复合涂层产品制备时要佩戴好合适的防护用具；
2)处理废弃物时要遵守废弃物处理的有关规定；
3)应急措施：
(1)浆料溅入眼睛时，即用大量清水冲洗至少5分钟，然后视情况接受医生治疗；
(2)吸入分解的气体时，应立即到新鲜空气的地方；
(3)涂料粘在皮肤上时，请用肥皂和水彻底清洗；
4)包装.贮存与运输
(1)所述无机不粘复合涂层产品应该在干燥，避雨，遮阳的环境中存放，在温度5-40℃环境下存放；
(2)运输按非危险品规则办理；
(3)正常保存环境下，所述无机不粘复合涂层产品保存期为6个月，超过保存期视产品变化情况使用。
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