CN113372749A - Flame-retardant water-in-water artistic coating and preparation method thereof - Google Patents
Flame-retardant water-in-water artistic coating and preparation method thereof Download PDFInfo
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- CN113372749A CN113372749A CN202110890232.9A CN202110890232A CN113372749A CN 113372749 A CN113372749 A CN 113372749A CN 202110890232 A CN202110890232 A CN 202110890232A CN 113372749 A CN113372749 A CN 113372749A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/29—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for multicolour effects
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- Life Sciences & Earth Sciences (AREA)
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Abstract
The invention discloses a flame-retardant water-in-water artistic coating and a preparation method thereof, wherein the flame-retardant water-in-water artistic coating is prepared from the following raw materials in parts by weight: 7-13 parts of granulation protective glue, 1-15 parts of base paint protective glue, 0-75 parts of toning base paint and 8-15 parts of continuous phase. The invention effectively solves the fire-proof problem of the water-in-water artistic paint which is popularized and applied as the artistic paint on the inner wall, has the properties of fire resistance, environmental protection, smell elimination, rich color, exquisite texture, mildew resistance and moisture resistance, integrates the advantages of a plurality of wall decorations, and can better meet the upgrading requirement of urban building design on decorative and finishing materials.
Description
Technical Field
The invention relates to a flame-retardant water-in-water artistic coating and a preparation method thereof, belonging to the technical field of decoration materials.
Background
With the rapid development of the house and land industry, the upgrading requirement of the urban building design on decorative and finishing materials is generated, a plurality of series products in the technical field of water-in-water multicolor are successfully promoted to be pushed to the market by the prosperous real estate market, and most products can be used as artistic paint to be popularized and applied in a large area on the inner wall after formula optimization. However, most wall surface coating products of the inner wall do not have fireproof requirements, and the inner wall tool has specific requirements on the fireproof grade of the coating, so that the requirement of common home decoration on the fireproof coating is great while the requirement on decoration is met.
Disclosure of Invention
The technical problem to be solved by the invention is to provide a flame-retardant water-in-water artistic paint and a preparation method thereof, wherein the flame-retardant water-in-water artistic paint can be used as a coating material of an inner wall and has a fireproof requirement, so that the defects of the prior art are overcome.
In order to solve the technical problems, the technical scheme adopted by the invention is as follows:
the flame-retardant water-in-water artistic coating is mainly prepared from the following raw materials in parts by weight: 7-13 parts of granulation protective glue, 1-15 parts of base paint protective glue, 0-75 parts of toning base paint and 8-15 parts of continuous phase;
the granulation protection glue comprises the following components: 3-15 parts of protective rubber powder, 75-97 parts of water, 1-1 part of thickening agent O-1 part of mildew preventive, 0.1-1 part of bactericide and 1-1 part of pH regulator O-1 part;
the base paint protective adhesive comprises the following components: 5-20 parts of protective rubber powder, 75-95 parts of water, 0.1-1 part of mildew preventive, 0.1-1 part of bactericide and 1-1 part of pH regulator O-1;
the toning base paint comprises the following components: 35-65 parts of water, 0.5-1.5 parts of cellulose, 0.1-1 part of wetting agent, 0.1-1 part of mildew inhibitor, 0.1-l part of dispersant, 0.5-1.5 parts of antifreeze, 0.05-0.5 part of defoaming agent, 0-5 parts of titanium dioxide, 1-25 parts of flame-retardant filler, 1-10 parts of wollastonite powder, 1-10 parts of talcum micropowder, 15-45 parts of emulsion, 0.5-1.5 parts of film-forming assistant, 0.1-1 part of bactericide, 0.1-1 part of pH regulator and 2-10 parts of basic paint protective adhesive;
the continuous phase comprises the following components: 15-45 parts of water, 0.1-1 part of mildew preventive, 0.5-1.5 parts of antifreeze, 0.01-0.15 part of defoamer, 0.5-1.5 parts of anti-sticking agent, 35-65 parts of emulsion, 1-3 parts of film forming additive, 0.1-0.5 part of pH regulator, 15-45 parts of thickening pre-conditioning water and 1 part of thickener O;
as a preferable scheme, the flame-retardant water-in-water artistic paint is prepared by mixing one or more of aluminum hydroxide or magnesium hydroxide or other magnesium-based inorganic flame-retardant powder.
The preparation method of the flame-retardant water-in-water artistic coating comprises the following steps:
(1) weighing the raw material components according to the raw material ratio;
(2) preparing a granulation protective adhesive: adding water, protective rubber powder, a thickening agent, a mildew preventive, a bactericide and a pH regulator into a first reactor according to the raw material ratio for mixing treatment to obtain granulation protective rubber;
(3) preparing a base paint protective adhesive: adding water, protective rubber powder, a mildew preventive, a bactericide and a pH regulator into a second reactor according to the raw material ratio for mixing treatment to obtain base paint protective rubber;
(4) preparing a toning base paint: adding water, cellulose, a wetting agent, a mildew preventive, a dispersing agent, an antifreezing agent, a defoaming agent, titanium dioxide, a flame-retardant filler, wollastonite powder, talc micro powder, an emulsion, a film-forming assistant, a bactericide and a pH regulator into a third reactor according to the raw material ratio for mixing, fully and uniformly stirring, and then adding the base paint protective adhesive to obtain the toning base paint;
(5) and (3) granulation: sequentially adding the toned base paints with various colors into the granulation protective glue for granulation to obtain colored particles;
(6) preparation of the continuous phase: adding water, a mildew preventive, an antifreezing agent, a defoaming agent, an anti-sticking agent, an emulsion, a film-forming aid and a pH regulator into a fourth reactor according to the raw material ratio for mixing treatment, and then adding thickening pre-conditioning water and a thickening agent into the fourth reactor at a constant speed to obtain a continuous phase;
(7) and (4) adding the continuous phase in the step (6) into the colored particles in the step (5), and uniformly mixing to obtain the flame-retardant water-in-water artistic coating.
The preparation method of the flame-retardant water-in-water artistic coating specifically comprises the following mixing treatment process in the step (2): adding 65% of formula water into a spare reactor, adding a thickening agent in a 40-mesh screen filtering mode at the stirring speed of 350-500rpm, stirring for 20-30min, and standing for 2-4 h to obtain spare thickened slurry; adding 35% of the rest formula water into the first reactor, adding the mildew preventive, the bactericide and the pH regulator at the stirring speed of 100 plus 300rpm, then adding the protective rubber powder at the stirring speed of 350 plus 500rpm, stirring for 20-30min, mixing the prepared standby thickening slurry with the mixed standby thickening slurry, and stirring for 5-10 min.
The preparation method of the flame-retardant water-in-water artistic coating specifically comprises the following mixing treatment process in the step (3): adding water into a second reactor, adding the preservative, the bactericide and the pH regulator at the stirring speed of 100-300rpm, then adding the protective rubber powder at the stirring speed of 350-500rpm, and stirring for 20-30 min.
The preparation method of the flame-retardant water-in-water artistic coating specifically comprises the following mixing treatment process in the step (4): adding water into a third reactor, adding cellulose, a wetting agent, a mildew preventive, a dispersing agent, an antifreezing agent, a defoaming agent, titanium dioxide, a flame-retardant filler, wollastonite powder, talc micro powder, an emulsion, a film-forming assistant and a bactericide at the stirring speed of 100-300rpm, stirring for 5-10min, filtering by a 120-mesh filter screen, then adding a pH regulator, stirring at the speed of 350-500rpm for 5-10min, finally adding the base paint protective adhesive prepared in the step (3), and stirring for 10-15 min.
The preparation method of the flame-retardant water-in-water artistic coating specifically comprises the following mixing treatment process in the step (6): adding water into a fourth reactor, adding a mildew preventive, an antifreezing agent, a defoaming agent, an anti-sticking agent, an emulsion, a film-forming aid and a pH regulator into the fourth reactor at the stirring speed of 100-300rpm, stirring for 10-15min at the stirring speed of 200-350rpm, mixing the mixed solution of the blended thickening pre-conditioning water and the thickening agent, and stirring for 5-10 min.
Has the advantages that: compared with the prior art, the flame-retardant filler is added into the toning base paint, so that the fire-proof problem of popularization and application of the water-in-water artistic paint as an artistic paint on an inner wall is effectively solved. The interior wall artistic coating has the advantages of fire resistance, environmental protection, odor elimination, rich colors, exquisite texture, mildew resistance and moisture resistance, integrates the advantages of a plurality of wall decorations, and fully shows the characteristics of the interior wall artistic coating. Meanwhile, the mechanical spraying replaces manual manufacturing, the construction cost is low, the technology copying and popularization are very simple, the market popularization is facilitated, and the upgrading requirement of the urban building design on the decorative and finishing materials is better met. The invention has the advantages that the invention completely realizes the fireproof, primer-free and finish coat construction on the inner wall, only needs one-time spraying construction and forming, greatly reduces the waste of manpower and material resources, and has great social contribution value to safe decoration.
The present invention will be further described with reference to the following embodiments.
Detailed Description
Example 1: the flame-retardant water-in-water artistic coating comprises the following raw materials in parts by weight: 10 parts of granulation protective glue, 8 parts of base paint protective glue, 65 parts of toning base paint and 10 parts of continuous phase. The granulation protection glue comprises the following components: 10 parts of protective rubber powder, 85 parts of water, 0.8 part of thickening agent, 0.5 part of mildew preventive, 0.5 part of bactericide and 0.2 part of pH regulator; the base paint protective adhesive comprises the following components: 15 parts of protective rubber powder, 85 parts of water, 0.5 part of mildew preventive, 0.5 part of bactericide and 0.2 part of pH regulator. The toning base paint comprises the following components: 55 parts of water, 1.2 parts of cellulose, 0.5 part of wetting agent, 0.5 part of mildew preventive, 0.5 part of dispersant, 1.2 parts of antifreeze, 0.1 part of defoamer, 2 parts of titanium dioxide, 15 parts of flame-retardant filler, 5 parts of wollastonite powder, 5 parts of talcum micropowder, 30 parts of emulsion, 1.2 parts of film-forming assistant, 0.4 part of bactericide, 0.5 part of pH regulator and 8 parts of the base paint protective adhesive, wherein the flame-retardant filler is aluminum hydroxide. The continuous phase comprises the following components: 35 parts of water, 0.5 part of mildew preventive, 1.2 parts of antifreeze, 0.10 part of defoamer, 1.2 parts of anti-sticking agent, 50 parts of emulsion, 2 parts of film-forming additive, 0.3 part of pH regulator, 30 parts of thickening pre-conditioning water and 0.2 part of thickener.
The preparation of the flame-retardant water-in-water artistic coating is carried out according to the following process steps:
weighing raw material components according to a raw material ratio;
preparing granulation protection glue in step (2): adding water, protective rubber powder, a thickening agent, a mildew preventive, a bactericide and a pH regulator into a first reactor according to the raw material ratio for mixing treatment to obtain granulation protective rubber; the process of mixing material treatment is as follows: adding 65% of formula water into a spare reactor, adding a thickening agent in a 40-mesh screen filtering mode at the stirring speed of 350-500rpm, stirring for 20-30min, and standing for 2-4 h to obtain spare thickened slurry; adding 35% of the rest formula water into the first reactor, adding the mildew preventive, the bactericide and the pH regulator at the stirring speed of 100 plus 300rpm, then adding the protective rubber powder at the stirring speed of 350 plus 500rpm, stirring for 20-30min, mixing the prepared standby thickening slurry with the mixed standby thickening slurry, and stirring for 5-10 min.
Preparing a base paint protective adhesive in step (3): adding water, protective rubber powder, a mildew preventive, a bactericide and a pH regulator into a second reactor according to the raw material ratio for mixing treatment to obtain base paint protective rubber; the process of mixing material treatment is as follows: adding water into a second reactor, adding the preservative, the bactericide and the pH regulator at the stirring speed of 100-300rpm, then adding the protective rubber powder at the stirring speed of 350-500rpm, and stirring for 20-30 min.
Step (4) preparing toning base paint: adding water, cellulose, a wetting agent, a mildew preventive, a dispersing agent, an antifreezing agent, a defoaming agent, titanium dioxide, a flame-retardant filler, wollastonite powder, talc micro powder, an emulsion, a film-forming assistant, a bactericide and a pH regulator into a third reactor according to the raw material ratio for mixing, fully and uniformly stirring, and then adding the base paint protective adhesive to obtain the toning base paint; the process of mixing material treatment is as follows: adding water into a third reactor, adding cellulose, a wetting agent, a mildew preventive, a dispersing agent, an antifreezing agent, a defoaming agent, titanium dioxide, a flame-retardant filler, wollastonite powder, talc micro powder, an emulsion, a film-forming assistant and a bactericide at the stirring speed of 100-300rpm, stirring for 5-10min, filtering by a 120-mesh filter screen, then adding a pH regulator, stirring at the speed of 350-500rpm for 5-10min, finally adding the base paint protective adhesive prepared in the step (3), and stirring for 10-15 min.
Granulating in step (5): sequentially adding the toned base paints with various colors into the granulation protective glue for granulation to obtain colored particles;
step (6) preparation of the continuous phase: adding water, a mildew preventive, an antifreezing agent, a defoaming agent, an anti-sticking agent, an emulsion, a film-forming aid and a pH regulator into a fourth reactor according to the raw material ratio for mixing treatment, and then adding thickening pre-conditioning water and a thickening agent into the fourth reactor at a constant speed to obtain a continuous phase; the process of mixing material treatment is as follows: adding water into a fourth reactor, adding a mildew preventive, an antifreezing agent, a defoaming agent, an anti-sticking agent, an emulsion, a film-forming aid and a pH regulator into the fourth reactor at the stirring speed of 100-300rpm, stirring for 10-15min at the stirring speed of 200-350rpm, mixing the mixed solution of the blended thickening pre-conditioning water and the thickening agent, and stirring for 5-10 min.
And (7): and (5) adding the continuous phase in the step (6) into the colored particles in the step (5), and uniformly mixing to obtain the pigment.
The above embodiments are the best embodiments of the present invention. The embodiments of the present invention are not limited to the above-described examples, and various changes made without departing from the spirit of the present invention are within the scope of the present invention.
Claims (7)
1. The flame-retardant water-in-water artistic coating is characterized by comprising the following components in parts by weight: the feed is prepared from the following raw materials in parts by weight: 7-13 parts of granulation protective glue, 1-15 parts of base paint protective glue, 0-75 parts of toning base paint and 8-15 parts of continuous phase;
the granulation protection glue comprises the following components: 3-15 parts of protective rubber powder, 75-97 parts of water, 1-1 part of thickening agent O-1 part of mildew preventive, 0.1-1 part of bactericide and 1-1 part of pH regulator O-1 part;
the base paint protective adhesive comprises the following components: 5-20 parts of protective rubber powder, 75-95 parts of water, 0.1-1 part of mildew preventive, 0.1-1 part of bactericide and 1-1 part of pH regulator O-1;
the toning base paint comprises the following components: 35-65 parts of water, 0.5-1.5 parts of cellulose, 0.1-1 part of wetting agent, 0.1-1 part of mildew inhibitor, 0.1-l part of dispersant, 0.5-1.5 parts of antifreeze, 0.05-0.5 part of defoaming agent, 0-5 parts of titanium dioxide, 1-25 parts of flame-retardant filler, 1-10 parts of wollastonite powder, 1-10 parts of talcum micropowder, 15-45 parts of emulsion, 0.5-1.5 parts of film-forming assistant, 0.1-1 part of bactericide, 0.1-1 part of pH regulator and 2-10 parts of basic paint protective adhesive;
the continuous phase comprises the following components: 15-45 parts of water, 0.1-1 part of mildew preventive, 0.5-1.5 parts of antifreeze, 0.01-0.15 part of defoamer, 0.5-1.5 parts of anti-sticking agent, 35-65 parts of emulsion, 1-3 parts of film forming additive, 0.1-0.5 part of pH regulator, 15-45 parts of thickening pre-adjusting water and 1 part of thickener O.
2. The flame retardant water-in-water artistic coating of claim 1, wherein: the flame-retardant filler is one or more of aluminum hydroxide, magnesium hydroxide or other magnesium inorganic flame-retardant powder.
3. The method for preparing the flame-retardant water-in-water artistic coating as claimed in claim 1 or 2, which comprises the following steps:
(1) weighing the raw material components according to the raw material ratio;
(2) preparing a granulation protective adhesive: adding water, protective rubber powder, a thickening agent, a mildew preventive, a bactericide and a pH regulator into a first reactor according to the raw material ratio for mixing treatment to obtain granulation protective rubber;
(3) preparing a base paint protective adhesive: adding water, protective rubber powder, a mildew preventive, a bactericide and a pH regulator into a second reactor according to the raw material ratio for mixing treatment to obtain base paint protective rubber;
(4) preparing a toning base paint: adding water, cellulose, a wetting agent, a mildew preventive, a dispersing agent, an antifreezing agent, a defoaming agent, titanium dioxide, a flame-retardant filler, wollastonite powder, talc micro powder, an emulsion, a film-forming assistant, a bactericide and a pH regulator into a third reactor according to the raw material ratio for mixing, fully and uniformly stirring, and then adding the base paint protective adhesive to obtain the toning base paint;
(5) and (3) granulation: sequentially adding the toned base paints with various colors into the granulation protective glue for granulation to obtain colored particles;
(6) preparation of the continuous phase: adding water, a mildew preventive, an antifreezing agent, a defoaming agent, an anti-sticking agent, an emulsion, a film-forming aid and a pH regulator into a fourth reactor according to the raw material ratio for mixing treatment, and then adding thickening pre-conditioning water and a thickening agent into the fourth reactor at a constant speed to obtain a continuous phase;
(7) and (4) adding the continuous phase in the step (6) into the colored particles in the step (5), and uniformly mixing to obtain the flame-retardant water-in-water artistic coating.
4. The preparation method of the flame-retardant water-in-water artistic coating as claimed in claim 3, wherein the preparation method comprises the following steps: the process of mixing material treatment in the step (2) is as follows: adding 65% of formula water into a spare reactor, adding a thickening agent in a 40-mesh screen filtering mode at the stirring speed of 350-500rpm, stirring for 20-30min, and standing for 2-4 h to obtain spare thickened slurry; adding 35% of the rest formula water into the first reactor, adding the mildew preventive, the bactericide and the pH regulator at the stirring speed of 100 plus 300rpm, then adding the protective rubber powder at the stirring speed of 350 plus 500rpm, stirring for 20-30min, mixing the prepared standby thickening slurry with the mixed standby thickening slurry, and stirring for 5-10 min.
5. The preparation method of the flame-retardant water-in-water artistic coating as claimed in claim 3, wherein the preparation method comprises the following steps: the process of mixing material treatment in the step (3) is as follows: adding water into a second reactor, adding the preservative, the bactericide and the pH regulator at the stirring speed of 100-300rpm, then adding the protective rubber powder at the stirring speed of 350-500rpm, and stirring for 20-30 min.
6. The preparation method of the flame-retardant water-in-water artistic coating as claimed in claim 3, wherein the preparation method comprises the following steps: the process of mixing material treatment in the step (4) is as follows: adding water into a third reactor, adding cellulose, a wetting agent, a mildew preventive, a dispersing agent, an antifreezing agent, a defoaming agent, titanium dioxide, a flame-retardant filler, wollastonite powder, talc micro powder, an emulsion, a film-forming assistant and a bactericide at the stirring speed of 100-300rpm, stirring for 5-10min, filtering by a 120-mesh filter screen, then adding a pH regulator, stirring at the speed of 350-500rpm for 5-10min, finally adding the base paint protective adhesive prepared in the step (3), and stirring for 10-15 min.
7. The preparation method of the flame-retardant water-in-water artistic coating as claimed in claim 3, wherein the preparation method comprises the following steps: the process of mixing material treatment in the step (6) is as follows: adding water into a fourth reactor, adding a mildew preventive, an antifreezing agent, a defoaming agent, an anti-sticking agent, an emulsion, a film-forming aid and a pH regulator into the fourth reactor at the stirring speed of 100-300rpm, stirring for 10-15min at the stirring speed of 200-350rpm, mixing the mixed solution of the blended thickening pre-conditioning water and the thickening agent, and stirring for 5-10 min.
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| CN202110890232.9A CN113372749A (en) | 2021-08-04 | 2021-08-04 | Flame-retardant water-in-water artistic coating and preparation method thereof |
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| CN202110890232.9A CN113372749A (en) | 2021-08-04 | 2021-08-04 | Flame-retardant water-in-water artistic coating and preparation method thereof |
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2021
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107722774A (en) * | 2017-10-23 | 2018-02-23 | 河北晨阳工贸集团有限公司 | A kind of flame-retardant water burnt-in sand coating and preparation method thereof |
| CN108300047A (en) * | 2018-01-29 | 2018-07-20 | 河北晨阳工贸集团有限公司 | A kind of indoor anti-pollution water-water coating and preparation method thereof |
| CN110372265A (en) * | 2019-06-21 | 2019-10-25 | 河北晨阳工贸集团有限公司 | A kind of water burnt-in sand coating and preparation method thereof |
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Application publication date: 20210910 |