CN113368015A - Lip care cream for improving natural lip color and preparation method thereof - Google Patents
Lip care cream for improving natural lip color and preparation method thereof Download PDFInfo
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- CN113368015A CN113368015A CN202110761963.3A CN202110761963A CN113368015A CN 113368015 A CN113368015 A CN 113368015A CN 202110761963 A CN202110761963 A CN 202110761963A CN 113368015 A CN113368015 A CN 113368015A
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- oil
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a lip care cream for improving natural lip color and a preparation method thereof. The lip protecting cream contains oil-soluble rhodiola rosea, ligusticum wallichii extract and Dongganggui root water, and the three traditional Chinese medicines have a long application history in China and are famous medicines for promoting blood circulation and tonifying qi. By reasonable compounding and synergistic interaction, the effects of good anti-inflammatory repair, promotion of lip blood microcirculation and smoothness of lip cutin are achieved, and lip color can be obviously improved.
Description
Technical Field
The invention relates to the field of daily cosmetics, in particular to lip care cream for improving natural lip color and a preparation method thereof.
Background
The lips, which are the only parts of the five sense organs having color, have the greatest influence on the appearance of human complexion. There are about 16 layers of skin epithelial cells in other parts of the body, and the lips have only 3 to 5 layers of epithelial cells, so the color of the lips is mainly the color of blood in the subcutaneous capillaries. In addition, peeling of lips, i.e., the formation of a double layer without shedding of cells on the surface of the stratum corneum, also reduces the permeability of the stratum corneum and weakens the original color of the lips. In the plain state, too light or too dark a lip color is considered to be an unhealthy manifestation. Lip color is often used by consumers to change their own lip color, but this is only a temporary means. Lip care products currently on the market focus on moisturizing and lightening the lips, and few products are available that can meet the needs of consumers who are not convenient or able to use lip color cosmetics but want to improve their lip color.
CN109464367A discloses a daily lip balm containing Chinese medicinal extract, which comprises radix Arnebiae, semen Persicae, herba Lycopi, Coptidis rhizoma, Borneolum Syntheticum, vitamin E, cornu Bubali, essential oil and Cera flava.
CN109528547A discloses a night lip balm containing Chinese medicinal extracts, which comprises radix Ophiopogonis, herba Dendrobii, radix Paeoniae alba, radix Glehniae, vitamin E, fructus Schisandrae chinensis, oviductus Ranae, and Cera flava.
The above patent application adopts an immersion method and a water decoction method for extracting the traditional Chinese medicine raw materials, which are both traditional Chinese medicine extraction methods, not only take time, but also have low extraction efficiency. The formulation process is that beeswax is directly added into suspension after water and oil phases are stirred and mixed, so that certain water and oil separation can be generated in the process of cooling the material body, and the stability problems of sweating precipitation and the like can be generated in the later period due to incompatibility of the extract and the matrix component, so that the final use effect of the product is influenced.
At present, the application of a plurality of traditional Chinese medicine raw materials in the field of lip cosmetics is yet to be developed, appropriate components are selected in a targeted manner, the extraction and preparation processes are improved, and the effective and stable composition is obtained, which is particularly important for the new lip care subdivision field.
Disclosure of Invention
In order to solve the defects of the prior art, the invention uses oil-soluble rhodiola rosea, ligusticum wallichii extract and angelica sinensis root water. The three traditional Chinese medicines have a long application history in China, are famous medicines for promoting blood circulation and tonifying qi, and are rarely used for lip products in the field of cosmetics. Therefore, it is possible to try to apply these three ingredients to the lips and develop a lip care cosmetic capable of improving the natural lip color.
The oil-soluble rhodiola rosea extract contains geraniol, terpene compounds, linoleic acid, coumarin and other active ingredients, and has the effects of resisting oxidation, accelerating blood circulation, preventing ultraviolet injury and the like; the oil soluble rhizoma Ligustici Chuanxiong extract contains phthalide compounds, terpenoid compounds, and enol compounds, and has effects of inhibiting platelet aggregation and reducing blood plasma viscosity. The oil soluble part of the active ingredients of angelica is similar to that of ligusticum wallichii, and the water soluble part mainly contains angelica polysaccharide, ferulic acid, amino acid and the like, so that the Chinese angelica extract has the effects of enhancing the hematopoietic function, reducing the generation of free radicals and the like. In order to obtain more effective components and improve the extraction rate, the invention adopts the supercritical carbon dioxide extraction method to extract the rhodiola rosea and the ligusticum wallichii and adopts the enzymolysis ultrasonic extraction method to extract the angelica, compared with the traditional method, the two methods can avoid the damage of high temperature to the active components, and also have the advantages of high extraction rate, few byproducts, easy separation of products and the like.
In order to ensure that the oil-soluble ingredients and the water-soluble ingredients are better and jointly stably present in the same formula system, the natural emulsifier derived from olive oil and coconut oil is selected, has the functions of emulsification and moisture retention, and is less irritant compared with the traditional emulsifier.
In order to achieve the purpose, the invention provides the following technical scheme:
the invention provides lip care cream for improving natural lip color, which comprises 50-75 parts of angelica sinensis root water, 1-4 parts of oil-soluble rhodiola rosea extract, 1-4 parts of oil-soluble ligusticum wallichii extract and auxiliary materials acceptable in the field of cosmetics.
Preferably, the traditional Chinese medicine composition comprises 50-75 parts of angelica sinensis root water, 1-4 parts of oil-soluble rhodiola rosea extract, 1-4 parts of oil-soluble ligusticum wallichii extract, 0.01-0.1 part of chelating agent, 0.3-0.6 part of emulsifier A, 1-4 parts of emulsifier B, 8-16 parts of humectant and C14To C223-8 parts of fatty alcohol and 10-20 parts of emollient.
As a preference, the first and second liquid crystal compositions are,comprises 55-65 parts of angelica sinensis root water, 2-4 parts of oil-soluble rhodiola rosea extract, 2-4 parts of oil-soluble ligusticum wallichii extract, 0.01-0.1 part of sodium phytate, 0.4-0.5 part of emulsifier A, 2-3 parts of emulsifier B, 10-14 parts of humectant C14To C224-6 parts of fatty alcohol and 12-16 parts of an emollient.
Preferably, the oil-soluble rhodiola rosea extract and the oil-soluble ligusticum wallichii extract are respectively extracted from the root of rhodiola rosea and the root of ligusticum wallichii, and the extraction method is a supercritical carbon dioxide extraction method and comprises the following steps:
1) breaking the root of rhodiola crenulata or the rhizome of ligusticum wallichii into 100-200 meshes by wall breaking;
2) uniformly mixing the powder with 95% ethanol at a solid-to-liquid ratio of 1 (1-1.5) g/ml, and putting into an extraction kettle;
3) raising the extraction temperature to 35-45 ℃, introducing carbon dioxide to raise the pressure of an extraction kettle to 30MPa, soaking for 30-40 min, and dynamically extracting for 30-40 min at a flow rate of 25L/h;
4) introducing into a separating kettle, reducing temperature and pressure, collecting the solution from the bottom of the separating kettle, adding 6 times of caprylic/capric triglyceride, stirring, and mixing.
Preferably, the angelica sinensis root water is extracted from the root of angelica sinensis, and the extraction method is an enzymolysis ultrasonic extraction method, and comprises the following steps:
1) breaking the wall of the root of the angelica sinensis, crushing the angelica sinensis to 80-150 meshes, mixing the angelica sinensis and deionized water according to a ratio of 1:60, adjusting the pH to 6-7, and adjusting the temperature to 30-35 ℃;
2) adding protease, cellulase and pectinase according to a mass ratio of 0.3-0.6: 1-1.5: 1.5-3, wherein the mass ratio of the complex enzyme to the angelica powder is 0.002-0.004: 1;
3) after 2-3 h of enzymolysis, quickly heating to 90 ℃ to inactivate enzyme to obtain enzymolysis liquid;
4) transferring the enzymolysis liquid to a circulating ultrasonic extractor, and extracting for 0.5 h;
5) centrifuging for 20-30 min, and filtering for 2-3 times by a 600-mesh sieve to obtain the root water of the angelica sinensis.
Preferably, the emulsifier A is cetearyl olive oleate (and) sorbitan olive oleate with the HLB value of 9-11; may preferably be sold under the trade name Olivem 1000; emulsifier B cetearyl alcohol (and) cetearyl glucoside having a microHLB value of 7-9; the trade name Montanov 68 may be preferred.
Preferably, the humectant is selected from one or a combination of at least two of glycerin, diglycerin, polyglycerol-3, propylene glycol, dipropylene glycol, butylene glycol, pentylene glycol, isoprene glycol, and hexylene glycol, preferably glycerin and hexylene glycol.
Preferably, C is14-C22The fatty alcohol is selected from myristyl alcohol, cetyl alcohol, stearyl alcohol, cetearyl alcohol, and behenyl alcohol, preferably cetearyl alcohol.
Preferably, the emollient is selected from one or the combination of at least two of natural oil and synthetic oil, preferably shea butter and dipentaerythritol tetrahydroxystearate/tetraisostearate.
The invention also provides a preparation method of the lip care cream, which comprises the following steps:
1) weighing angelica root water, sodium phytate, cetearyl olive oleate (and) sorbitan olive oleate and a humectant according to parts by mass, heating to 70-75 ℃ until the mixture is melted uniformly, and mixing and stirring for 5-10 min until the mixture is completely uniform to obtain a phase A;
2) mixing rhodiola oil extract, Ligusticum chuanxiong extract, cetearyl alcohol (and) cetearyl glucoside, C14To C22Weighing fatty alcohol and an emollient according to parts by weight, heating to 70-75 ℃ until the fatty alcohol and the emollient are uniformly melted, mixing and stirring for 5-10 min until the fatty alcohol and the emollient are completely and uniformly dissolved to obtain a phase B;
3) keeping the temperature at 70-75 ℃, slowly pouring the phase B into the phase A, and homogenizing at 6000-6500 rpm for 10-12 min;
4) cooling to 45 ℃, and discharging to obtain the lip protecting cream.
The invention has the following beneficial effects: according to the invention, the extracts of the rhodiola rosea and the ligusticum wallichii are selected, the angelica sinensis is used for extracting water to replace pure water, and the extracts are added into a lip care emulsion matrix formula using a natural source emulsifier, and the effects of good anti-inflammatory repair, promotion of lip blood microcirculation and smoothness of lip cutin are achieved through reasonable compounding and synergistic interaction, so that consumers have healthy and natural lip color.
Detailed Description
Embodiments of the present application will be described in detail by examples, so that how to apply technical means to solve technical problems and achieve technical effects of the present application can be fully understood and implemented.
The raw materials and equipment used in the present application are all common raw materials and equipment in the field, and are all from commercially available products, unless otherwise specified. The methods used in this application are conventional in the art unless otherwise indicated.
There are many other possible embodiments of the present invention, which are not listed here, and the embodiments claimed in the claims of the present invention can be implemented.
The compositions of the present application are prepared by the following method.
The preparation method of the lip care cream for improving the natural lip color comprises the following steps:
weighing the components of the phase A according to parts by weight, heating to 70-75 ℃ until the components are uniformly melted, and mixing and stirring for 5-10 min until the components are completely uniform;
weighing the components of the phase B according to parts by weight, heating to 70-75 ℃ until the components are uniformly melted, and mixing and stirring for 5-10 min until the components are completely uniform;
step three, keeping the temperature at 70-75 ℃, slowly pouring the phase B into the phase A, and homogenizing at 6000-6500 rpm for 10-12 min;
step four, cooling to 45 ℃;
and fifthly, defoaming, discharging and filling to obtain a finished product.
The phase A comprises 50-75 parts of angelica sinensis root water, 0.01-0.1 part of chelating agent, 0.3-0.6 part of emulsifier A and 8-16 parts of humectant.
In a specific embodiment, the phase A can comprise 55-65 parts of angelica sinensis root water, 0.01-0.1 part of sodium phytate, 0.4-0.5 part of emulsifier A and 10-14 parts of humectant.
The HLB value of the emulsifier A is 9-11, and preferably cetearyl olive oleate and sorbitan olive oleate. The humectant is selected from one or a combination of at least two of glycerin, diglycerin, polyglycerol-3, propylene glycol, dipropylene glycol, butanediol, pentanediol, isoprene glycol and hexanediol, and preferably glycerin and hexanediol.
Phase B is 1-4 parts of oil-soluble rhodiola rosea extract, 1-4 parts of oil-soluble ligusticum wallichii extract, 1-4 parts of emulsifier B and phase C14To C223-8 parts of fatty alcohol and 10-20 parts of emollient.
In a specific embodiment, the rhodiola oil extract is 2-4 parts, the ligusticum wallichii extract is 2-4 parts, the emulsifier B is 2-3 parts, and the emulsifier C is14To C224-6 parts of fatty alcohol and 12-16 parts of an emollient.
Wherein the HLB value of the emulsifier B is 7-9, and preferably cetearyl alcohol and cetearyl glucoside; the C14-C22 fatty alcohol is selected from one or a combination of at least two of myristyl alcohol, cetyl alcohol, stearyl alcohol, cetearyl alcohol and behenyl alcohol, and is preferably cetearyl alcohol. The emollient is selected from one or the combination of at least two of natural oil and synthetic oil, preferably shea butter and dipentaerythritol tetrahydroxystearate/tetraisostearate.
In order to realize special application, phase C can be added when preparing lip care cream.
In certain embodiments phase C may be an aromatizing or polyenergetic additive or preservative. In certain more specific embodiments, phase C may be 0.1 parts of caprylic glycol and 0.1 parts of caprylic glycerol.
The oil-soluble rhodiola rosea extract and the oil-soluble ligusticum wallichii extract are respectively extracted from the root of rhodiola rosea and the root of ligusticum wallichii, and the extraction method is a supercritical carbon dioxide extraction method and comprises the following steps:
1) breaking the root of rhodiola crenulata or the rhizome of ligusticum wallichii into 100-200 meshes by wall breaking;
2) uniformly mixing the powder with 95% ethanol at a solid-to-liquid ratio of 1 (1-1.5) g/ml, and putting into an extraction kettle;
3) raising the extraction temperature to 35-45 ℃, introducing carbon dioxide to raise the pressure of an extraction kettle to 30MPa, soaking for 30-40 min, and dynamically extracting for 30-40 min at a flow rate of 25L/h;
4) introducing into a separating kettle, reducing temperature and pressure, collecting the solution from the bottom of the separating kettle, adding 6 times of caprylic/capric triglyceride, stirring, and mixing.
The radix Angelicae sinensis water is extracted from radix Angelicae sinensis, and the extraction method is enzymolysis ultrasonic extraction method, and comprises the following steps:
1) breaking the wall of the root of the angelica sinensis, crushing the angelica sinensis to 80-150 meshes, mixing the angelica sinensis and deionized water according to a ratio of 1:60, adjusting the pH to 6-7, and adjusting the temperature to 30-35 ℃;
2) adding protease, cellulase and pectinase according to a mass ratio of 0.3-0.6: 1-1.5: 1.5-3, wherein the mass ratio of the complex enzyme to the angelica powder is 0.002-0.004: 1;
3) after 2-3 h of enzymolysis, quickly heating to 90 ℃ to inactivate enzyme to obtain enzymolysis liquid;
4) transferring the enzymolysis liquid to a circulating ultrasonic extractor, and extracting for 0.5 h;
5) centrifuging for 20-30 min, and filtering for 2-3 times by a 600-mesh sieve to obtain the root water of the angelica sinensis.
Examples
The compositions of the present application are prepared by the following method.
The preparation method of the lip care cream for improving the natural lip color comprises the following steps:
weighing the components of the phase A according to parts by weight, heating to 70-75 ℃ until the components are uniformly melted, and mixing and stirring for 5-10 min until the components are completely uniform;
weighing the components of the phase B according to parts by weight, heating to 70-75 ℃ until the components are uniformly melted, and mixing and stirring for 5-10 min until the components are completely uniform;
step three, keeping the temperature at 70-75 ℃, slowly pouring the phase B into the phase A, and homogenizing at 6000-6500 rpm for 10-12 min;
weighing and adding the components of the phase C according to parts by weight, homogenizing at 4000-4500 rpm for 1-2 min, and cooling to 45 ℃;
and fifthly, defoaming, discharging and filling to obtain a finished product.
In the preparation method, the component of the phase C does not influence the property of the lip care cream, and is only used for enhancing the fragrance and the like. When the caprylyl glycol, the glyceryl caprylate and the essence are not required to be added, and the functionality and the quality of the lip care cream are not influenced.
The oil-soluble rhodiola rosea extract and the oil-soluble ligusticum wallichii extract are respectively extracted from the root of rhodiola rosea and the root of ligusticum wallichii, and the extraction method is a supercritical carbon dioxide extraction method and comprises the following steps:
1) breaking the root of rhodiola crenulata or the rhizome of ligusticum wallichii into 100-200 meshes by wall breaking;
2) uniformly mixing the powder with 95% ethanol at a solid-to-liquid ratio of 1:1.5g/ml, and putting into an extraction kettle;
3) raising the extraction temperature to 35-45 ℃, introducing carbon dioxide to raise the pressure of an extraction kettle to 30MPa, soaking for 30-40 min, and dynamically extracting for 30-40 min at a flow rate of 25L/h;
4) introducing into a separating kettle, reducing temperature and pressure, collecting the solution from the bottom of the separating kettle, adding 6 times of caprylic/capric triglyceride, stirring, and mixing.
The radix Angelicae sinensis water is extracted from radix Angelicae sinensis, and the extraction method is enzymolysis ultrasonic extraction method, and comprises the following steps:
1) breaking the wall of the root of the angelica sinensis, crushing the angelica sinensis to 80-150 meshes, mixing the angelica sinensis and deionized water according to a ratio of 1:60, adjusting the pH to 6-7, and adjusting the temperature to 30-35 ℃;
2) adding a complex enzyme formed by mixing protease, cellulase and pectinase according to the mass ratio of 0.5:1.2:2.0, wherein the mass ratio of the complex enzyme to the Chinese angelica powder is 0.002-0.004: 1;
3) after 2-3 h of enzymolysis, quickly heating to 90 ℃ to inactivate enzyme to obtain enzymolysis liquid;
4) transferring the enzymolysis liquid to a circulating ultrasonic extractor, and extracting for 0.5 h;
5) centrifuging for 20-30 min, and filtering for 2-3 times by a 600-mesh sieve to obtain the root water of the angelica sinensis.
Table 1 shows the compositions (by mass) of the respective compositions in examples 1 to 10 and comparative examples 1 to 4. The compositions of the examples were prepared according to table 1 and using the methods described above, and the resulting compositions were subjected to efficacy testing.
TABLE 1
Comparative example
Comparative example 1: this comparative example provides a lip care composition in which the equivalent amount of deionized water is used in place of the water from the root of oriental paperbush as in example 1, and the remaining components and preparation are the same as in example 1.
Comparative example 2: this comparative example provides a lip care composition which, compared to example 1, does not contain the rhodiola oil extract, the remaining components and the preparation method are the same as example 1.
Comparative example 3: this comparative example provides a lip care composition which, compared to example 1, does not contain an oil-soluble chuanxiong rhizome extract, and the remaining components and preparation method are the same as example 1.
Comparative example 4: this comparative example provides a lip care composition, which compared to example 1, uses an equal amount of deionized water instead of the water of the roots of east dangshen, and an equal amount of caprylic/capric triglyceride instead of the oil-soluble rhodiola rosea extract and the oil-soluble ligusticum wallichii extract, and the rest of the components and the preparation method are the same as example 1.
Effect example 1: lip color test
Test samples: examples 1 to 10 and comparative examples 1 to 4 were selected as test samples, wherein each group of samples was colorless and transparent.
Testing an instrument: color difference meter CM-700d (Meinengda)
Test objects: female volunteers with pale lip color between 20-40 years of age, 5 persons in each group
The test method comprises the following steps:
1. the volunteers continuously apply the test samples to the lips one week and one day, once in the morning, at noon and at night, and once in each time by using a lip brush;
2. measuring the red a value and the chroma C value of the lips before use, after use for one week and after 3 days of non-use by using a color difference meter;
3. the average of the test values of each group of volunteers was used to calculate the rate of change of the red a value, the chroma C value.
TABLE 2
TABLE 3
As can be seen from tables 2 and 3, the red color value and the color value of the lips of the volunteers who used the lip care creams prepared in the examples are significantly improved after one week, and the effect can still be maintained after 3 days of disuse, while the red color value and the color value of the lips of the volunteers who used the lip care creams prepared in the comparative examples are limited after one week, and the effect is greatly reduced after 3 days of disuse, which indicates that the effect of improving the natural lip color by using the rhodiola oil extract, the ligusticum oil extract and the angelica root in combination with water is better than that by using one of the components alone.
Effect example 2: lip print improvement test
Test samples: the samples of example 11 and comparative examples 1 to 6 were selected as test samples
Testing an instrument: antera 3D (Miravex, Ireland)
Test objects: female volunteers between the ages of 20-40 years, 5 persons per group
The test method comprises the following steps:
1. measuring lip wrinkles by using an Antera 3D, selecting the deepest wrinkle of the lips of each subject, analyzing the wrinkle depth and the average cross-sectional area of each subject, and taking the average value of each group of volunteers as an initial value;
2. smearing the test sample in the morning, at noon and at night every day, and smearing the test sample for 2 times back and forth each time;
3. lip wrinkles were measured 1 week and 2 weeks after product use using an andrera 3D, respectively, wrinkle depth and average cross-sectional area at the same location were analyzed, and the average of each group of volunteers was taken as one-week and two-week values;
4. the rate of change of the wrinkle depth and average cross-sectional area of the lip skin after the corresponding test sample was used was calculated for each group of volunteers.
Parameter interpretation:
ra: average roughness, an average of all deviations from a straight line within the evaluation length, irrespective of the vertical direction;
rq: root mean square roughness is the root mean square average of the roughness ordinate.
TABLE 4
TABLE 5
It can be seen from tables 4 and 5 that the lip gloss improving effect of the lip gloss cream prepared in the examples is significantly better than that of the comparative example, which shows that the lip gloss improving effect of one of the components is better when the rhodiola oil extract, the ligusticum chuanxiong extract and the angelicae root water are used in combination.
Claims (10)
1. A lip care cream for improving natural lip color is characterized by comprising 50-75 parts of Donggui root water, 1-4 parts of oil-soluble rhodiola rosea extract, 1-4 parts of oil-soluble ligusticum wallichii extract and auxiliary materials acceptable in the field of cosmetics.
2. The lip care cream according to claim 1, comprising 50-75 parts of angelica sinensis root water, 1-4 parts of oil-soluble rhodiola rosea extract, 1-4 parts of oil-soluble ligusticum wallichii extract, 0.01-0.1 part of chelating agent, 0.3-0.6 part of emulsifier A, 1-4 parts of emulsifier B, 8-16 parts of humectant C and C14To C223-8 parts of fatty alcohol and 10-20 parts of emollient.
3. The lip care cream according to claim 2, comprising 55 to 65 parts of angelica sinensis root water, 2 to 4 parts of oil-soluble rhodiola rosea extract, 2 to 4 parts of oil-soluble ligusticum wallichii extract, 0.01 to 0.1 part of sodium phytate, 0.4 to 0.5 part of emulsifier A, 2 to 3 parts of emulsifier B, 10 to 14 parts of humectant C and C14To C224-6 parts of fatty alcohol and 12-16 parts of an emollient.
4. The lip care cream of claim 3, wherein the oil-soluble rhodiola rosea extract and the oil-soluble ligusticum wallichii extract are respectively extracted from the root of rhodiola rosea and the root of ligusticum wallichii by a supercritical carbon dioxide extraction method, and the extraction method comprises the following steps:
1) breaking the root of rhodiola crenulata or the rhizome of ligusticum wallichii into 100-200 meshes by wall breaking;
2) uniformly mixing the powder with 95% ethanol at a solid-to-liquid ratio of 1 (1-1.5) g/ml, and putting into an extraction kettle;
3) raising the extraction temperature to 35-45 ℃, introducing carbon dioxide to raise the pressure of an extraction kettle to 30MPa, soaking for 30-40 min, and dynamically extracting for 30-40 min at a flow rate of 25L/h;
4) introducing into a separating kettle, reducing temperature and pressure, collecting the solution from the bottom of the separating kettle, adding 6 times of caprylic/capric triglyceride, stirring, and mixing.
5. The lip care lotion according to claim 3, wherein the root water of the angelica sinensis is extracted from the root of the angelica sinensis by an enzymatic ultrasonic extraction method, and the extraction method comprises the following steps:
1) breaking the wall of the root of the angelica sinensis, crushing the angelica sinensis to 80-150 meshes, mixing the angelica sinensis and deionized water according to a ratio of 1:60, adjusting the pH to 6-7, and adjusting the temperature to 30-35 ℃;
2) adding protease, cellulase and pectinase according to a mass ratio of 0.3-0.6: 1-1.5: 1.5-3, wherein the mass ratio of the complex enzyme to the angelica powder is 0.002-0.004: 1;
3) after 2-3 h of enzymolysis, quickly heating to 90 ℃ to inactivate enzyme to obtain enzymolysis liquid;
4) transferring the enzymolysis liquid to a circulating ultrasonic extractor, and extracting for 0.5 h;
5) centrifuging for 20-30 min, and filtering for 2-3 times by a 600-mesh sieve to obtain the root water of the angelica sinensis.
6. A lip cream according to claim 3, characterized in that emulsifier A has an HLB value of 9 to 11, preferably cetearyl olive oleate, sorbitan olive oleate; the emulsifier B has an HLB value of 7 to 9, and is preferably cetearyl alcohol or cetearyl glucoside.
7. A lip care cream according to claim 3, characterized in that the humectant is selected from one or a combination of at least two of glycerol, diglycerol, polyglycerin-3, propylene glycol, dipropylene glycol, butylene glycol, pentylene glycol, isoprene glycol, hexylene glycol, preferably glycerol and hexylene glycol.
8. The lip care cream of claim 3, wherein C is14To C22The fatty alcohol is selected from myristyl alcohol, cetyl alcohol, stearyl alcohol, cetearyl alcohol, and behenyl alcohol, preferably cetearyl alcohol.
9. A lip cream according to claim 3, characterized in that the emollient is selected from any one or a combination of at least two of natural and synthetic fats, preferably shea butter and dipentaerythritol tetrahydroxystearate/tetraisostearate.
10. A method of preparing a lip care cream according to claim 3, comprising the steps of:
1) weighing angelica root water, sodium phytate, cetearyl olive oleate (and) sorbitan olive oleate and a humectant according to parts by mass, heating to 70-75 ℃ until the mixture is melted uniformly, and mixing and stirring for 5-10 min until the mixture is completely uniform to obtain a phase A;
2) mixing rhodiola oil extract, Ligusticum chuanxiong extract, cetearyl alcohol (and) cetearyl glucoside, C14To C22Weighing fatty alcohol and an emollient according to parts by weight, heating to 70-75 ℃ until the fatty alcohol and the emollient are uniformly melted, mixing and stirring for 5-10 min until the fatty alcohol and the emollient are completely and uniformly dissolved to obtain a phase B;
3) keeping the temperature at 70-75 ℃, slowly pouring the phase B into the phase A, and homogenizing at 6000-6500 rpm for 10-12 min;
4) cooling to 45 ℃, and discharging to obtain the lip protecting cream.
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