CN113355924A - 一种染色助剂及其加工工艺 - Google Patents
一种染色助剂及其加工工艺 Download PDFInfo
- Publication number
- CN113355924A CN113355924A CN202010151815.5A CN202010151815A CN113355924A CN 113355924 A CN113355924 A CN 113355924A CN 202010151815 A CN202010151815 A CN 202010151815A CN 113355924 A CN113355924 A CN 113355924A
- Authority
- CN
- China
- Prior art keywords
- dyeing
- agent
- parts
- fiber
- softener
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000004043 dyeing Methods 0.000 title claims abstract description 118
- 238000005516 engineering process Methods 0.000 title abstract description 11
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 68
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims abstract description 54
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 50
- 239000000463 material Substances 0.000 claims abstract description 37
- 229940037003 alum Drugs 0.000 claims abstract description 29
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 28
- 229910052938 sodium sulfate Inorganic materials 0.000 claims abstract description 27
- 235000011152 sodium sulphate Nutrition 0.000 claims abstract description 27
- 241000196324 Embryophyta Species 0.000 claims abstract description 24
- 239000002105 nanoparticle Substances 0.000 claims abstract description 24
- 239000000049 pigment Substances 0.000 claims abstract description 21
- 239000001575 punica granatum l. bark extract Substances 0.000 claims abstract description 20
- -1 alkoxy silane Chemical compound 0.000 claims abstract description 19
- 230000014759 maintenance of location Effects 0.000 claims abstract description 19
- 239000010702 perfluoropolyether Substances 0.000 claims abstract description 19
- 229910000077 silane Inorganic materials 0.000 claims abstract description 18
- 239000004744 fabric Substances 0.000 claims abstract description 17
- 239000002131 composite material Substances 0.000 claims abstract description 16
- 239000000945 filler Substances 0.000 claims abstract description 11
- 239000002738 chelating agent Substances 0.000 claims description 30
- 239000003995 emulsifying agent Substances 0.000 claims description 30
- 238000003756 stirring Methods 0.000 claims description 29
- 239000012752 auxiliary agent Substances 0.000 claims description 28
- 239000000243 solution Substances 0.000 claims description 21
- 239000002904 solvent Substances 0.000 claims description 18
- 239000000839 emulsion Substances 0.000 claims description 15
- 235000011127 sodium aluminium sulphate Nutrition 0.000 claims description 12
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 10
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical group [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 10
- 238000002156 mixing Methods 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 8
- 239000001632 sodium acetate Substances 0.000 claims description 7
- 235000017454 sodium diacetate Nutrition 0.000 claims description 7
- 239000002994 raw material Substances 0.000 claims description 6
- ZORQXIQZAOLNGE-UHFFFAOYSA-N 1,1-difluorocyclohexane Chemical compound FC1(F)CCCCC1 ZORQXIQZAOLNGE-UHFFFAOYSA-N 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 5
- 239000000986 disperse dye Substances 0.000 claims description 5
- 238000011049 filling Methods 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 239000011259 mixed solution Substances 0.000 claims description 5
- 229910052757 nitrogen Inorganic materials 0.000 claims description 5
- 125000006353 oxyethylene group Chemical group 0.000 claims description 5
- 239000002245 particle Substances 0.000 claims description 5
- 238000007789 sealing Methods 0.000 claims description 5
- 239000001593 sorbitan monooleate Substances 0.000 claims description 5
- 229940035049 sorbitan monooleate Drugs 0.000 claims description 5
- 235000011069 sorbitan monooleate Nutrition 0.000 claims description 5
- 238000005303 weighing Methods 0.000 claims description 5
- 239000011787 zinc oxide Substances 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 230000001153 anti-wrinkle effect Effects 0.000 claims 1
- 125000003916 ethylene diamine group Chemical group 0.000 claims 1
- 239000000835 fiber Substances 0.000 abstract description 51
- 238000005562 fading Methods 0.000 abstract description 16
- 238000002845 discoloration Methods 0.000 abstract description 5
- 241000894006 Bacteria Species 0.000 abstract description 4
- 241000700605 Viruses Species 0.000 abstract description 4
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 4
- 230000001681 protective effect Effects 0.000 abstract description 4
- 239000000975 dye Substances 0.000 description 21
- 230000000694 effects Effects 0.000 description 10
- 238000005406 washing Methods 0.000 description 6
- 230000037303 wrinkles Effects 0.000 description 6
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 3
- 238000004061 bleaching Methods 0.000 description 3
- 239000000460 chlorine Substances 0.000 description 3
- 229910052801 chlorine Inorganic materials 0.000 description 3
- 238000004040 coloring Methods 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 238000004945 emulsification Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000011241 protective layer Substances 0.000 description 3
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 230000005281 excited state Effects 0.000 description 2
- 230000002147 killing effect Effects 0.000 description 2
- 230000001954 sterilising effect Effects 0.000 description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/445—Use of auxiliary substances before, during or after dyeing or printing
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/60—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing polyethers
- D06P1/613—Polyethers without nitrogen
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/642—Compounds containing nitrogen
- D06P1/647—Nitrogen-containing carboxylic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65131—Compounds containing ether or acetal groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/655—Compounds containing ammonium groups
- D06P1/66—Compounds containing ammonium groups containing quaternary ammonium groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/67341—Salts or hydroxides of elements different from the alkaline or alkaline-earth metals or with anions containing those elements
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67391—Salts or oxidising-compounds mixtures
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/002—Locally enhancing dye affinity of a textile material by chemical means
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Coloring (AREA)
Abstract
本发明公开了一种染色助剂及其加工工艺,包括水55‑60份、乙醇20‑30份、草木灰纳米颗粒18‑24份、石榴皮萃取液10‑12份、保色混料12‑18份、α‑全氟聚醚烷氧基硅烷3‑8份和染色颜料5‑10份,所述染色助剂中还包括复合填料。本发明通过水与乙醇相溶溶解混合物料,并配合石榴皮萃取液有效杀灭细菌病毒,使纤维具有抗菌性,染料均匀涂布纤维,并在其表面形成防护膜,元明粉和明矾促进上染并保色减少纤维染色褪色变色,柔顺剂、防皱剂和抗紫外线剂配合染料提高纤维强度,使其耐磨、耐水洗和耐用,提高了纤维布匹的整体性能。
Description
技术领域
本发明涉及织物印染领域,具体涉及一种染色助剂及其加工工艺。
背景技术
染色即染上颜色,也称上色,是指用化学的或其他的方法影响物质本身而使其着色。把纤维浸入一定温度下的染料水溶液中,染料就从水相向纤维中移动,此时水中的染料量逐渐减少,经过一段时间以后,就达到平衡状态。水中减少的染料,就是向纤维上移动的染料。在任意时间取出纤维,即使绞拧,染料也仍留在纤维中,并不能简单地使染料完全脱离纤维,这种染料结合在纤维中的现象,就称为染色。
纺织材料用染浴处理,使染料和纤维发生化学或物理化学结合,或在纤维上生成不溶性有色物质的工艺过程。染料应在纤维上有一定的耐水洗、晒、摩擦等性能,这种性能称为染色牢度。纺织物的染色,历史悠久。但是现有的染色助剂染色不能提高纤维性能,而且容易褪色,不便于长期使用。
因此,发明一种染色助剂及其加工工艺来解决上述问题很有必要。
发明内容
本发明的目的是提供一种染色助剂及其加工工艺,通过水与乙醇相溶为溶剂,便于溶解混合物料,并配合石榴皮萃取液有效杀灭细菌病毒,使纤维具有抗菌性,草木灰纳米颗粒、α-全氟聚醚烷氧基硅烷和乙二胺二邻羟苯基大乙酸钠配合,使染料均匀涂布纤维,并在其表面形成防护膜,元明粉和明矾促进上染并保色减少纤维染色褪色变色,柔顺剂、防皱剂和抗紫外线剂配合染料提高纤维强度,使其耐磨、耐水洗和耐用,提高了纤维布匹的整体性能,以解决技术中的上述不足之处。
为了实现上述目的,本发明提供如下技术方案:一种染色助剂,其中所使用的主料按重量计包括:水55-60份、乙醇20-30份、草木灰纳米颗粒18-24份、石榴皮萃取液10-12份、保色混料12-18份、α-全氟聚醚烷氧基硅烷3-8份和染色颜料5-10份,所述染色助剂中还包括复合填料;
所述复合填料由柔顺剂、螯合剂、防皱剂、乳化剂和抗紫外线剂组成,且柔顺剂、螯合剂、防皱剂、乳化剂和抗紫外线剂的添加质量比设置为柔顺剂:螯合剂:防皱剂:乳化剂:抗紫外线剂=3-5:1:3:6-10:2-4。
优选的,所述复合助剂与主料的质量比设置为10-15:1,所述草木灰纳米颗粒粒径设置为100-200nm,所述染色颜料设置为分散染料。
优选的,所述保色混料由元明粉和明矾组成,且元明粉与明矾的体积比设置为元明粉:明矾=2-3:4-6。
优选的,所述柔顺剂设置为酯基季铵盐,所述螯合剂设置为乙二胺二邻羟苯基大乙酸钠,所述防皱剂设置为浴中防皱柔软剂,所述乳化剂设置为氧乙烯20山梨醇酐单油酸酯,所述抗紫外线剂设置为氧化锌。
一种染色助剂的加工工艺,具体操作步骤为:
步骤一:准备原料,按比例量取一定重量份的水、乙醇、草木灰纳米颗粒、石榴皮萃取液、元明粉、明矾、α-全氟聚醚烷氧基硅烷、染色颜料、柔顺剂、螯合剂、防皱剂、乳化剂和抗紫外线剂;
步骤二:将三分之二体积的乙醇溶于水内制成染色溶剂,将元明粉和明矾混合均匀制成保色混料,备用;
步骤三:将保色混料倒入染色溶剂中,在染色溶剂中加入草木灰纳米颗粒、石榴皮萃取液、α-全氟聚醚烷氧基硅烷和染色颜料,中温环境下搅拌均匀制成染色基液;
步骤四:在染色基液中加入柔顺剂、螯合剂、防皱剂和抗紫外线剂,混合均匀后加入乳化剂,加热并充分搅拌至混合液呈乳化状态,通入氮气冷却至室温,将剩余三分之一体积的乙醇倒入混合乳液中,并再次搅拌均匀,使之稀释匀质;
步骤五:将稀释后的混合乳液取出并震荡脱泡,制成染色助剂,将染色助剂灌装并密封存储。
优选的,所述步骤三中搅拌加工环境设置为45-55℃,搅拌时间设置为30-45min。
优选的,所述步骤四中搅拌加工环境设置为70-80℃,搅拌时间设置为2-3h。
在上述技术方案中,本发明提供的技术效果和优点:
通过水与乙醇相溶为溶剂,便于溶解混合物料,并配合石榴皮萃取液有效杀灭细菌病毒,使纤维具有抗菌性,草木灰纳米颗粒、α-全氟聚醚烷氧基硅烷和乙二胺二邻羟苯基大乙酸钠配合,使染料均匀涂布纤维,并在其表面形成防护膜,元明粉和明矾促进上染并保色减少纤维染色褪色变色,柔顺剂、防皱剂和抗紫外线剂配合染料提高纤维强度,使其耐磨、耐水洗和耐用,提高了纤维布匹的整体性能。
具体实施方式
为了使本领域的技术人员更好地理解本发明的技术方案,下面对本发明作进一步的详细介绍。
实施例1:
本发明提供了一种染色助剂,其中所使用的主料按重量计包括:水55份、乙醇200份、草木灰纳米颗粒18份、石榴皮萃取液10份、保色混料12份、α-全氟聚醚烷氧基硅烷3份和染色颜料5份,所述染色助剂中还包括复合填料;
所述复合填料由柔顺剂、螯合剂、防皱剂、乳化剂和抗紫外线剂组成,且柔顺剂、螯合剂、防皱剂、乳化剂和抗紫外线剂的添加质量比设置为柔顺剂:螯合剂:防皱剂:乳化剂:抗紫外线剂=3:1:3:6:2;
进一步的,在上述技术方案中,所述复合助剂与主料的质量比设置为10:1,所述草木灰纳米颗粒粒径设置为100nm,所述染色颜料设置为分散染料;
进一步的,在上述技术方案中,所述保色混料由元明粉和明矾组成,且元明粉与明矾的体积比设置为元明粉:明矾=2:4;
进一步的,在上述技术方案中,所述柔顺剂设置为酯基季铵盐,所述螯合剂设置为乙二胺二邻羟苯基大乙酸钠,所述防皱剂设置为浴中防皱柔软剂,所述乳化剂设置为氧乙烯20山梨醇酐单油酸酯,所述抗紫外线剂设置为氧化锌。
一种染色助剂的加工工艺,具体操作步骤为:
步骤一:准备原料,按比例量取一定重量份的水、乙醇、草木灰纳米颗粒、石榴皮萃取液、元明粉、明矾、α-全氟聚醚烷氧基硅烷、染色颜料、柔顺剂、螯合剂、防皱剂、乳化剂和抗紫外线剂;
步骤二:将三分之二体积的乙醇溶于水内制成染色溶剂,将元明粉和明矾混合均匀制成保色混料,备用;
步骤三:将保色混料倒入染色溶剂中,在染色溶剂中加入草木灰纳米颗粒、石榴皮萃取液、α-全氟聚醚烷氧基硅烷和染色颜料,45℃温度环境下搅拌30min,搅拌均匀后制成染色基液;
步骤四:在染色基液中加入柔顺剂、螯合剂、防皱剂和抗紫外线剂,混合均匀后加入乳化剂,加热溶液温度至70℃并充分搅拌至混合液呈乳化状态,搅拌时间设置为2h,通入氮气冷却至室温,将剩余三分之一体积的乙醇倒入混合乳液中,并再次搅拌均匀,使之稀释匀质;
步骤五:将稀释后的混合乳液取出并震荡脱泡,制成染色助剂,将染色助剂灌装并密封存储。
本实施例中制备的染色助剂质地均匀,乳化效果好,在对纤维布匹进行染色时,上料均匀涂布,染色效果好,能够有效杀菌灭霉,并在纤维表面形成一层保护层,减少其褪色变色,并提高纤维强度,使其耐磨、耐水洗和耐用,另外本实施例制备染色助剂后,使用该染色助剂对布匹进行染色并进一步对染色后的染色牢度进行测试,在日光作用下,染料吸收光能,分子处于激化态而变得极不稳定,容易产生某些化学反应,使染料分解褪色,导致染色织物经日晒后产生较大的褪色现象,从而将日晒牢度分为1-8级,本实施例测得结果为7级,在40℃皂洗温度下测试样品经试验、淋洗、晾干后即用“灰色褪色样卡”按国家规定标准评级,在五级九档皂洗牢度标准中,本实施例测得结果为5级,类似标准下,测得氯漂牢度为4级,摩擦牢度为4级,染色效果好且不易褪色,证明本实施例技术方案实际有效。
实施例2:
本发明提供了一种染色助剂,其中所使用的主料按重量计包括:水58份、乙醇25份、草木灰纳米颗粒22份、石榴皮萃取液11份、保色混料15份、α-全氟聚醚烷氧基硅烷5份和染色颜料8份,所述染色助剂中还包括复合填料;
所述复合填料由柔顺剂、螯合剂、防皱剂、乳化剂和抗紫外线剂组成,且柔顺剂、螯合剂、防皱剂、乳化剂和抗紫外线剂的添加质量比设置为柔顺剂:螯合剂:防皱剂:乳化剂:抗紫外线剂=4:1:3:8:3;
进一步的,在上述技术方案中,所述复合助剂与主料的质量比设置为13:1,所述草木灰纳米颗粒粒径设置为150nm,所述染色颜料设置为分散染料;
进一步的,在上述技术方案中,所述保色混料由元明粉和明矾组成,且元明粉与明矾的体积比设置为元明粉:明矾=2:5;
进一步的,在上述技术方案中,所述柔顺剂设置为酯基季铵盐,所述螯合剂设置为乙二胺二邻羟苯基大乙酸钠,所述防皱剂设置为浴中防皱柔软剂,所述乳化剂设置为氧乙烯20山梨醇酐单油酸酯,所述抗紫外线剂设置为氧化锌。
一种染色助剂的加工工艺,具体操作步骤为:
步骤一:准备原料,按比例量取一定重量份的水、乙醇、草木灰纳米颗粒、石榴皮萃取液、元明粉、明矾、α-全氟聚醚烷氧基硅烷、染色颜料、柔顺剂、螯合剂、防皱剂、乳化剂和抗紫外线剂;
步骤二:将三分之二体积的乙醇溶于水内制成染色溶剂,将元明粉和明矾混合均匀制成保色混料,备用;
步骤三:将保色混料倒入染色溶剂中,在染色溶剂中加入草木灰纳米颗粒、石榴皮萃取液、α-全氟聚醚烷氧基硅烷和染色颜料,50℃温度环境下搅拌40min,搅拌均匀后制成染色基液;
步骤四:在染色基液中加入柔顺剂、螯合剂、防皱剂和抗紫外线剂,混合均匀后加入乳化剂,加热溶液温度至75℃并充分搅拌至混合液呈乳化状态,搅拌时间设置为2.5h,通入氮气冷却至室温,将剩余三分之一体积的乙醇倒入混合乳液中,并再次搅拌均匀,使之稀释匀质;
步骤五:将稀释后的混合乳液取出并震荡脱泡,制成染色助剂,将染色助剂灌装并密封存储。
对比实施例1,本实施例中制备的染色助剂质地均匀,乳化效果好,在对纤维布匹进行染色时,上料均匀涂布,染色效果好,能够有效杀菌灭霉,并在纤维表面形成一层保护层,减少其褪色变色,并提高纤维强度,使其耐磨、耐水洗和耐用,另外本实施例制备染色助剂后,使用该染色助剂对布匹进行染色并进一步对染色后的染色牢度进行测试,在日光作用下,染料吸收光能,分子处于激化态而变得极不稳定,容易产生某些化学反应,使染料分解褪色,导致染色织物经日晒后产生较大的褪色现象,从而将日晒牢度分为1-8级,本实施例测得结果为8级,在40℃皂洗温度下测试样品经试验、淋洗、晾干后即用“灰色褪色样卡”按国家规定标准评级,在五级九档皂洗牢度标准中,本实施例测得结果为5级,类似标准下,测得氯漂牢度为4级,摩擦牢度为4级,染色效果好且不易褪色,证明本实施例技术方案实际有效。
实施例3:
本发明提供了一种染色助剂,其中所使用的主料按重量计包括:水60份、乙醇30份、草木灰纳米颗粒24份、石榴皮萃取液12份、保色混料18份、α-全氟聚醚烷氧基硅烷8份和染色颜料10份,所述染色助剂中还包括复合填料;
所述复合填料由柔顺剂、螯合剂、防皱剂、乳化剂和抗紫外线剂组成,且柔顺剂、螯合剂、防皱剂、乳化剂和抗紫外线剂的添加质量比设置为柔顺剂:螯合剂:防皱剂:乳化剂:抗紫外线剂=5:1:3:10:4;
进一步的,在上述技术方案中,所述复合助剂与主料的质量比设置为15:1,所述草木灰纳米颗粒粒径设置为200nm,所述染色颜料设置为分散染料;
进一步的,在上述技术方案中,所述保色混料由元明粉和明矾组成,且元明粉与明矾的体积比设置为元明粉:明矾=3:6;
进一步的,在上述技术方案中,所述柔顺剂设置为酯基季铵盐,所述螯合剂设置为乙二胺二邻羟苯基大乙酸钠,所述防皱剂设置为浴中防皱柔软剂,所述乳化剂设置为氧乙烯20山梨醇酐单油酸酯,所述抗紫外线剂设置为氧化锌。
一种染色助剂的加工工艺,具体操作步骤为:
步骤一:准备原料,按比例量取一定重量份的水、乙醇、草木灰纳米颗粒、石榴皮萃取液、元明粉、明矾、α-全氟聚醚烷氧基硅烷、染色颜料、柔顺剂、螯合剂、防皱剂、乳化剂和抗紫外线剂;
步骤二:将三分之二体积的乙醇溶于水内制成染色溶剂,将元明粉和明矾混合均匀制成保色混料,备用;
步骤三:将保色混料倒入染色溶剂中,在染色溶剂中加入草木灰纳米颗粒、石榴皮萃取液、α-全氟聚醚烷氧基硅烷和染色颜料,55℃温度环境下搅拌45min,搅拌均匀后制成染色基液;
步骤四:在染色基液中加入柔顺剂、螯合剂、防皱剂和抗紫外线剂,混合均匀后加入乳化剂,加热溶液温度至80℃并充分搅拌至混合液呈乳化状态,搅拌时间设置为3h,通入氮气冷却至室温,将剩余三分之一体积的乙醇倒入混合乳液中,并再次搅拌均匀,使之稀释匀质;
步骤五:将稀释后的混合乳液取出并震荡脱泡,制成染色助剂,将染色助剂灌装并密封存储。
对比实施例1和2,本实施例中制备的染色助剂质地均匀,乳化效果好,在对纤维布匹进行染色时,上料均匀涂布,染色效果好,能够有效杀菌灭霉,并在纤维表面形成一层保护层,减少其褪色变色,并提高纤维强度,使其耐磨、耐水洗和耐用,另外本实施例制备染色助剂后,使用该染色助剂对布匹进行染色并进一步对染色后的染色牢度进行测试,在日光作用下,染料吸收光能,分子处于激化态而变得极不稳定,容易产生某些化学反应,使染料分解褪色,导致染色织物经日晒后产生较大的褪色现象,从而将日晒牢度分为1-8级,本实施例测得结果为8级,在40℃皂洗温度下测试样品经试验、淋洗、晾干后即用“灰色褪色样卡”按国家规定标准评级,在五级九档皂洗牢度标准中,本实施例测得结果为5级,类似标准下,测得氯漂牢度为3级,摩擦牢度为4级,染色效果好且不易褪色,证明本实施例技术方案实际有效。
根据实施例1-3得出下表:
由上表可知,实施例2中原材料比例适中,加工温度适中,该实施例提供的方法最为适合染色助剂的生产制备,且该方法制备的染色助剂染色性能最优,因此,便于推广使用,另外,通过水与乙醇相溶为溶剂,便于溶解混合物料,并配合石榴皮萃取液有效杀灭细菌病毒,使纤维具有抗菌性,草木灰纳米颗粒、α-全氟聚醚烷氧基硅烷和乙二胺二邻羟苯基大乙酸钠配合,使染料均匀涂布纤维,并在其表面形成防护膜,元明粉和明矾促进上染并保色减少纤维染色褪色变色,柔顺剂、防皱剂和抗紫外线剂配合染料提高纤维强度,使其耐磨、耐水洗和耐用,提高了纤维布匹的整体性能。
以上只通过说明的方式描述了本发明的某些示范性实施例,毋庸置疑,对于本领域的普通技术人员,在不偏离本发明的精神和范围的情况下,可以用各种不同的方式对所描述的实施例进行修正。因此,上述描述在本质上是说明性的,不应理解为对本发明权利要求保护范围的限制,凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。
Claims (7)
1.一种染色助剂,其特征在于:其中所使用的主料按重量计包括:水55-60份、乙醇20-30份、草木灰纳米颗粒18-24份、石榴皮萃取液10-12份、保色混料12-18份、α-全氟聚醚烷氧基硅烷3-8份和染色颜料5-10份,所述染色助剂中还包括复合填料;
所述复合填料由柔顺剂、螯合剂、防皱剂、乳化剂和抗紫外线剂组成,且柔顺剂、螯合剂、防皱剂、乳化剂和抗紫外线剂的添加质量比设置为柔顺剂:螯合剂:防皱剂:乳化剂:抗紫外线剂=3-5:1:3:6-10:2-4。
2.根据权利要求1所述的一种染色助剂,其特征在于:所述复合助剂与主料的质量比设置为10-15:1,所述草木灰纳米颗粒粒径设置为100-200nm,所述染色颜料设置为分散染料。
3.根据权利要求1所述的一种染色助剂,其特征在于:所述保色混料由元明粉和明矾组成,且元明粉与明矾的体积比设置为元明粉:明矾=2-3:4-6。
4.根据权利要求1所述的一种染色助剂,其特征在于:所述柔顺剂设置为酯基季铵盐,所述螯合剂设置为乙二胺二邻羟苯基大乙酸钠,所述防皱剂设置为浴中防皱柔软剂,所述乳化剂设置为氧乙烯20山梨醇酐单油酸酯,所述抗紫外线剂设置为氧化锌。
5.根据权利要求1-4中任意一项所述的一种染色助剂的加工工艺,其特征在于:具体操作步骤为:
步骤一:准备原料,按比例量取一定重量份的水、乙醇、草木灰纳米颗粒、石榴皮萃取液、元明粉、明矾、α-全氟聚醚烷氧基硅烷、染色颜料、柔顺剂、螯合剂、防皱剂、乳化剂和抗紫外线剂;
步骤二:将三分之二体积的乙醇溶于水内制成染色溶剂,将元明粉和明矾混合均匀制成保色混料,备用;
步骤三:将保色混料倒入染色溶剂中,在染色溶剂中加入草木灰纳米颗粒、石榴皮萃取液、α-全氟聚醚烷氧基硅烷和染色颜料,中温环境下搅拌均匀制成染色基液;
步骤四:在染色基液中加入柔顺剂、螯合剂、防皱剂和抗紫外线剂,混合均匀后加入乳化剂,加热并充分搅拌至混合液呈乳化状态,通入氮气冷却至室温,将剩余三分之一体积的乙醇倒入混合乳液中,并再次搅拌均匀,使之稀释匀质;
步骤五:将稀释后的混合乳液取出并震荡脱泡,制成染色助剂,将染色助剂灌装并密封存储。
6.根据权利要求5所述的一种染色助剂的加工工艺,其特征在于:所述步骤三中搅拌加工环境设置为45-55℃,搅拌时间设置为30-45min。
7.根据权利要求5所述的一种染色助剂的加工工艺,其特征在于:所述步骤四中搅拌加工环境设置为70-80℃,搅拌时间设置为2-3h。
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202010151815.5A CN113355924A (zh) | 2020-03-06 | 2020-03-06 | 一种染色助剂及其加工工艺 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202010151815.5A CN113355924A (zh) | 2020-03-06 | 2020-03-06 | 一种染色助剂及其加工工艺 |
Publications (1)
Publication Number | Publication Date |
---|---|
CN113355924A true CN113355924A (zh) | 2021-09-07 |
Family
ID=77524168
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN202010151815.5A Pending CN113355924A (zh) | 2020-03-06 | 2020-03-06 | 一种染色助剂及其加工工艺 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN113355924A (zh) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115787326A (zh) * | 2022-11-29 | 2023-03-14 | 石狮市瑞鹰纺织科技有限公司 | 一种混纺纤维印染助剂及其制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB923394A (en) * | 1960-05-13 | 1963-04-10 | Dow Corning | A composition and process for dyeing non-siliceous textile fibres |
CN104831529A (zh) * | 2015-05-27 | 2015-08-12 | 天津滨海大田纺织有限公司 | 一种棉织物的抗菌整理剂及抗菌整理工艺 |
CN109098018A (zh) * | 2018-06-08 | 2018-12-28 | 姜永达 | 一种染色用助剂及其制备方法 |
-
2020
- 2020-03-06 CN CN202010151815.5A patent/CN113355924A/zh active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB923394A (en) * | 1960-05-13 | 1963-04-10 | Dow Corning | A composition and process for dyeing non-siliceous textile fibres |
US3504998A (en) * | 1960-05-13 | 1970-04-07 | Dow Corning | Dyeing textile coated with an aminoethylaminopropyl trialkoxy silane |
CN104831529A (zh) * | 2015-05-27 | 2015-08-12 | 天津滨海大田纺织有限公司 | 一种棉织物的抗菌整理剂及抗菌整理工艺 |
CN109098018A (zh) * | 2018-06-08 | 2018-12-28 | 姜永达 | 一种染色用助剂及其制备方法 |
Non-Patent Citations (1)
Title |
---|
陈科等: "氟硅材料在防水防油领域的研究进展", 《浙江化工》 * |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115787326A (zh) * | 2022-11-29 | 2023-03-14 | 石狮市瑞鹰纺织科技有限公司 | 一种混纺纤维印染助剂及其制备方法 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN103696296B (zh) | 一种活性染料用阳离子型无醛固色剂及其制备方法 | |
CN104744642B (zh) | 纳米二氧化钛改性固色剂乳液的制备方法 | |
CN103711011B (zh) | 一种微交联型聚甲基丙烯酰氧乙基三甲基氯化铵改性固色剂及其制备方法 | |
CN109267382A (zh) | 一种涤纶针织布的染色工艺 | |
CN101245563B (zh) | 一种环保酸性固色剂及其制备方法 | |
CN106337303A (zh) | 一种棉织物的活性染料染色方法 | |
Gao et al. | Silicone nanomicelle dyeing using the nanoemulsion containing highly dispersed dyes for polyester fabrics | |
CN108252130A (zh) | 海藻纤维/涤纶纤维混纺织物的轧染染色方法 | |
CN107558253A (zh) | 一种用还原染料染色人棉纤维的方法 | |
CN105986329A (zh) | 一种原液着色聚丙烯腈纤维及其制备方法 | |
Khattak et al. | Optimization of fastness and tensile properties of cotton fabric dyed with natural extracts of Marigold flower (Tagetes erecta) by pad-steam method | |
CN104404791A (zh) | 一种纤维素纤维的差异化无盐低碱染色工艺 | |
CN102965927B (zh) | 柞蚕丝纤维或其织物阳离子改性整理剂和其改性工艺方法 | |
CN113355924A (zh) | 一种染色助剂及其加工工艺 | |
CN106986953B (zh) | 一种用作分散剂的壳聚糖衍生物及其在纺织品印染中的应用 | |
CN101117765A (zh) | 一种Gemini型阳离子溶胶及提高织物染色牢度的方法 | |
Fang et al. | Pigment dyeing of polyamide‐epichlorohydrin cationized cotton fabrics | |
EP2978891B1 (en) | Reactive silica nanoparticles containing immobilized dye for permanent colouration of fibres | |
CN104358159B (zh) | 一种纤维素纤维的无盐低碱循环染色工艺 | |
CN110258141A (zh) | 一种提高醇类有机溶剂-水体系中活性染料固色率的方法 | |
CN109183447A (zh) | 海藻酸钙纤维的活性染料无盐染色方法 | |
CN104233850B (zh) | 一种涂料着色剂、制备方法及应用 | |
CN105220532A (zh) | 一种基于壳聚糖的纺织品印花用防迁移剂及其制备方法 | |
CN106337300A (zh) | 化纤面料的染色方法 | |
Sampaio et al. | Colored nanoparticles for ecological dyeing of cellulosic fibres |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
RJ01 | Rejection of invention patent application after publication |
Application publication date: 20210907 |
|
RJ01 | Rejection of invention patent application after publication |