CN113116785A - Cleaning massage shower gel and preparation method thereof - Google Patents

Cleaning massage shower gel and preparation method thereof Download PDF

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Publication number
CN113116785A
CN113116785A CN202110497903.5A CN202110497903A CN113116785A CN 113116785 A CN113116785 A CN 113116785A CN 202110497903 A CN202110497903 A CN 202110497903A CN 113116785 A CN113116785 A CN 113116785A
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parts
particles
zein
polylactic acid
massage
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何平蓉
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0241—Containing particulates characterized by their shape and/or structure
    • A61K8/0279—Porous; Hollow
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36—Carboxylic acids; Salts or anhydrides thereof
    • A61K8/368—Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60—Sugars; Derivatives thereof
    • A61K8/602—Glycosides, e.g. rutin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/63—Steroids; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/645—Proteins of vegetable origin; Derivatives or degradation products thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/731—Cellulose; Quaternized cellulose derivatives
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/85—Polyesters
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706—Algae
    • A61K8/9722—Chlorophycota or Chlorophyta [green algae], e.g. Chlorella
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/008—Preparations for oily skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/10—Washing or bathing preparations
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    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/28—Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants
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    • A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
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    • A61K2800/60—Particulates further characterized by their structure or composition
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    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/60—Particulates further characterized by their structure or composition
    • A61K2800/65—Characterized by the composition of the particulate/core
    • A61K2800/651—The particulate/core comprising inorganic material
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    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract

The invention relates to the field of washing and caring products, and discloses a cleaning and massaging bath cream and a preparation method thereof. The shower gel comprises the following components in parts by weight: 3-4 parts of mother chrysanthemum extract, 0.5-2.5 parts of citron fruit peel extract, 1-2 parts of chlorella extract, 2-3 parts of tea saponin, 4.5-5.5 parts of alkyl glycoside, 3-4 parts of cleaning massage particles, 0.1-0.3 part of disodium ethylenediamine tetraacetic acid, 0.05-0.1 part of sodium benzoate and 60-70 parts of water; the cleaning massage particles comprise an activated carbon core layer and a porous zein/polylactic acid composite coating layer coated outside the activated carbon core layer. In the cleaning massage particles used by the invention, the porous zein/polylactic acid is adopted to coat the active carbon, so that the active carbon can be prevented from damaging the skin, the cleaning massage particles have better massaging and cutin removing effects, and the oil removing effect of the active carbon cannot be adversely affected.

Description

Cleaning massage shower gel and preparation method thereof
Technical Field
The invention relates to the field of washing and caring products, in particular to a cleaning and massaging bath cream and a preparation method thereof.
Background
At present, a chemically synthesized surfactant is mostly adopted in the shower gel to play a role in deoiling and cleaning, but due to strong alkalinity, the shower gel can generate irritation to skin and even cause anaphylactic reaction; some shower gel adopts activated carbon to replace a chemically synthesized surfactant to a certain extent, and the porous property of the activated carbon is utilized to absorb oil stains, sweat stains, human body secretions and the like, so that the shower gel has a cleaning effect. For example, patent document CN202011044137.9 discloses an oil-controlling and soothing body wash and a preparation method thereof, wherein the body wash is prepared by compounding natural plant massage extract, bio-based surfactant and biomass activated carbon, and plays roles of controlling oil and regulating water-oil balance of skin together. However, although activated carbon can promote the removal of body surface stains by utilizing the excellent adsorption capacity and the friction mechanical effect, the activated carbon has poor comfort and is easy to cause skin abrasion when being applied to the skin due to high hardness and surface roughness of the activated carbon.
Disclosure of Invention
In order to solve the technical problems, the invention provides a cleansing massage bath lotion and a preparation method thereof. The cleaning massage bath cream adopts cleaning massage particles with unique structures, has good oil removal, cutin removal and massage effects, and can not cause damage to skin.
The specific technical scheme of the invention is as follows:
the cleaning massage bath cream comprises the following components in parts by weight: 3-4 parts of mother chrysanthemum extract, 0.5-2.5 parts of citron fruit peel extract, 1-2 parts of chlorella extract, 2-3 parts of tea saponin, 4.5-5.5 parts of alkyl glycoside, 1-2 parts of wood particles, 3-4 parts of cleaning massage particles, 0.1-0.3 part of disodium edetate, 0.05-0.1 part of sodium benzoate and 60-70 parts of water; the cleaning massage particles comprise an activated carbon core layer and a porous zein/polylactic acid composite coating layer coated outside the activated carbon core layer.
In the cleaning massage particles, the activated carbon core can play a role in removing oil by utilizing higher porosity, and the cleaning massage particles can play roles in massaging and removing cutin in the repeated smearing process of the shower gel. However, the active carbon with hard texture and rough surface is easy to cause skin damage when being directly contacted with the skin, therefore, the invention adopts the porous zein/polylactic acid to coat the active carbon, the polymer composite coating layer can endow the cleaning massage particles with smooth and softer surface, and can avoid the direct contact of the active carbon and the skin; in addition, in the composite coating layer, the zein and the polylactic acid both have higher hydrophobicity, so that the zein and the polylactic acid have an adsorption effect on oil stains, and the porous structure of the coating layer can ensure that the zein and the polylactic acid do not excessively influence the adsorption function of the activated carbon.
Preferably, the particle size of the cleaning massage particles is 80-120 μm, and the diameter of the activated carbon core layer is 40-50 μm.
Preferably, the preparation method of the cleaning massage particles is as follows:
(A) respectively dispersing polylactic acid and zein into water to prepare polylactic acid dispersion liquid and zein dispersion liquid; adding activated carbon into the polylactic acid dispersion liquid, after uniform dispersion, dropwise adding the zein dispersion liquid under stirring, continuously stirring for 40-60min, and filtering to obtain activated carbon @ zein/polylactic acid particles;
(B) and carrying out vacuum microwave treatment on the active carbon @ zein/polylactic acid particles, and then carrying out vacuum drying to obtain the clean massage particles.
After the active carbon @ zein/polylactic acid granules are prepared, the active carbon @ zein/polylactic acid granules are subjected to vacuum microwave treatment, air in the active carbon is vibrated to escape under the action of air pressure difference between the inside and outside of the granules and microwaves, and pores are formed in the zein/polylactic acid coating layer, so that the excessive influence of the coating layer on the adsorption effect of the active carbon is prevented.
In the composite coating layer, the polylactic acid has higher air permeability, and molecular chains of the polylactic acid form a net structure through physical entanglement, so that the polylactic acid is easily influenced by escaping air during vacuum microwave treatment to form larger pores; the zein molecular chains are crosslinked through hydrogen bonds and disulfide bonds, so that a zein/polylactic acid crosslinking network has certain mechanical strength, and a coating layer is prevented from being damaged in the preparation and use processes of the shower gel. Therefore, the invention adopts polylactic acid and zein to clad in a composite way, so that the cladding layer can form larger pores during vacuum microwave treatment and has higher mechanical strength, thereby endowing the cleaning massage particles with better oil removal function and effectively preventing the cleaning massage particles from damaging the skin.
Preferably, in step (A), the solid contents of the polylactic acid dispersion and the zein dispersion are 10 to 15 wt% and 6 to 8 wt%, respectively.
Preferably, in the step (A), the mass ratio of the polylactic acid to the zein to the activated carbon is 1.5-2.5:1: 0.5-1.
During the coating process, the amount of polylactic acid and zein can affect the function of the cleaning massage particles: if the consumption of the zein is too large, larger pores are difficult to form during vacuum microwave treatment, and the oil removal effect of the cleaning massage particles is not ideal; if the relative dosage of the polylactic acid is too large, the mechanical strength of the coating layer is too low, the coating layer is damaged in the preparation and use processes of the shower gel, and the rough surface of the active carbon is damaged after contacting with the skin.
Preferably, in the step (B), the vacuum degree of the vacuum microwave treatment is 0.03-0.05MPa, the power is 500-600W, and the treatment time is 15-25 min.
Preferably, the cleansing massage bath cream also comprises the following components in parts by weight: 1-2 parts of wood particles.
In wooden granule, because the unique fan-shaped structure of wood fibre, can give wooden granule higher porosity, make it can adsorb the greasy dirt of body surface, simultaneously, wooden granule can exert the effect of getting rid of cutin through the friction mechanical effect, and because its soft texture, can avoid causing the damage to skin, and play the massage effect.
The soft texture can give better massage effect to the wood particles, but simultaneously, the pores are easy to deform and shrink in the using process, which is not beneficial to the absorption of oil stains; the active carbon in the core layer of the cleaning massage particles is not easy to deform, can keep better oil removal effect, but can also cause higher hardness of the cleaning massage particles and relatively poorer massage effect. Therefore, the shower gel provided by the invention has good cleaning and massaging functions by compounding the wood particles and the cleaning and massaging particles.
Preferably, the preparation method of the wood particles comprises the following steps: pulverizing wood into particles with particle size of 50-100 μm, and loosening at 180 deg.C and 0.5-0.8MPa for 40-80min to obtain wood particles.
At high temperature, water in the wood particles is evaporated, and at the same time, the cellulose is partially decomposed thermally, so that the wood particles are loose and soft in texture, the skin is not damaged, and the adsorption performance is better.
A method for preparing the cleansing massage bath cream comprises the following steps:
(1) heating water, maintaining the temperature at 65-75 deg.C, adding tea saponin and alkyl glycoside, mixing, adding cleaning massage particles, and mixing to obtain primary mixed solution;
(2) cooling the primary mixed liquid to 42-46 ℃, adding the chamomile extract, the citron fruit peel extract and the chlorella extract, mixing uniformly, adding the disodium edetate and the sodium benzoate, and fully mixing to obtain the cleaning massage bath cream.
A method for preparing the cleansing massage bath cream comprises the following steps:
(1) adding the wood particles into a part of water, and heating for 1-2h at 80-90 ℃ to obtain wood particle dispersion liquid;
(2) heating the rest water, maintaining the temperature at 65-75 deg.C, adding tea saponin and alkyl glycoside, mixing, adding wood particle dispersion liquid and cleaning massage particles, and mixing to obtain primary mixed liquid;
(3) cooling the primary mixed liquid to 42-46 ℃, adding the chamomile extract, the citron fruit peel extract and the chlorella extract, mixing uniformly, adding the disodium edetate and the sodium benzoate, and fully mixing to obtain the cleaning massage bath cream.
Preferably, in the step (1), the mass ratio of the wood particles to the water is 1: 10-15.
Compared with the prior art, the invention has the following advantages:
(1) in the cleaning massage particles, the porous zein/polylactic acid is adopted to coat the active carbon, so that the active carbon can be prevented from damaging the skin, the cleaning massage particles have better massaging and cutin removing effects, and the oil removing effect of the active carbon cannot be adversely affected;
(2) in the cleaning massage particles, the zein and the polylactic acid are compounded and coated in a certain proportion, so that the coating layer has larger pores and higher mechanical strength, thereby endowing the cleaning massage particles with better deoiling function and effectively preventing the cleaning massage particles from damaging the skin;
(3) the wood particles and the cleaning massage particles are compounded, so that the bath cream can have better oil removal, cutin removal and massage effects.
Detailed Description
The present invention will be further described with reference to the following examples. The following examples are intended only to illustrate the invention in detail and are not intended to limit the scope of the invention in any way.
Example 1
The cleaning massage bath cream comprises the following components in parts by weight: 3.5 parts of mother chrysanthemum extract, 1.5 parts of citron fruit peel extract, 1.5 parts of chlorella extract, 2.5 parts of tea saponin, 5 parts of alkyl glycoside, 3.5 parts of cleaning massage particles, 0.2 part of disodium edetate, 0.08 part of sodium benzoate and 65 parts of water.
A method for preparing the cleansing massage bath cream comprises the following steps:
(1) preparing cleaning massage particles:
(1.1) respectively dispersing polylactic acid and zein into water to prepare polylactic acid dispersion liquid and zein dispersion liquid with solid contents of 12 wt% and 7 wt%, respectively; adding active carbon with the particle size of 40-50 mu m into polylactic acid dispersion liquid, uniformly dispersing, dropwise adding zein dispersion liquid under stirring, continuously stirring for 50min, and filtering to obtain active carbon @ zein/polylactic acid particles, wherein the mass ratio of polylactic acid to zein to active carbon is 2:1: 0.8;
(1.2) carrying out vacuum microwave treatment on the activated carbon @ zein/polylactic acid particles, wherein the vacuum degree is 0.04MPa, the power is 550W, the treatment time is 20min, and then carrying out vacuum drying to obtain clean massage particles with the particle size of 80-120 microns;
(2) heating water, maintaining at 70 deg.C, adding tea saponin and alkyl glycoside, mixing, adding cleaning massage particles, and mixing to obtain primary mixed solution;
(3) cooling the primary mixed liquid to 44 ℃, adding the chamomile extract, the citron fruit peel extract and the chlorella extract, mixing uniformly, adding the disodium ethylenediamine tetraacetic acid and the sodium benzoate, and fully mixing to obtain the cleansing massage bath lotion.
Example 2
The cleaning massage bath cream comprises the following components in parts by weight: 3 parts of mother chrysanthemum extract, 2.5 parts of citron fruit peel extract, 1 part of chlorella extract, 3 parts of tea saponin, 4.5 parts of alkyl glycoside, 3 parts of cleaning massage particles, 0.1 part of disodium ethylene diamine tetraacetate, 0.05 part of sodium benzoate and 60 parts of water.
A method for preparing the cleansing massage bath cream comprises the following steps:
(1) preparing cleaning massage particles:
(1.1) respectively dispersing polylactic acid and zein into water to prepare polylactic acid dispersion liquid and zein dispersion liquid with solid contents of 10 wt% and 8 wt%, respectively; adding active carbon with the particle size of 40-50 mu m into polylactic acid dispersion, uniformly dispersing, dropwise adding zein dispersion under stirring, continuously stirring for 40min, and filtering to obtain active carbon @ zein/polylactic acid particles, wherein the mass ratio of polylactic acid to zein to active carbon is 1.5:1: 0.5;
(1.2) carrying out vacuum microwave treatment on the activated carbon @ zein/polylactic acid particles, wherein the vacuum degree is 0.03MPa, the power is 500W, the treatment time is 25min, and then carrying out vacuum drying to obtain clean massage particles with the particle size of 80-120 microns;
(2) heating water, maintaining the temperature at 65 deg.C, adding tea saponin and alkyl glycoside, mixing, adding cleaning massage particles, and mixing to obtain primary mixed solution;
(3) cooling the primary mixed liquid to 42 ℃, adding the chamomile extract, the citron fruit peel extract and the chlorella extract, mixing uniformly, adding the disodium ethylenediamine tetraacetic acid and the sodium benzoate, and fully mixing to obtain the cleansing massage bath lotion.
Example 3
The cleaning massage bath cream comprises the following components in parts by weight: 4 parts of mother chrysanthemum extract, 0.5 part of citron fruit peel extract, 2 parts of chlorella extract, 2 parts of tea saponin, 5.5 parts of alkyl glycoside, 4 parts of cleaning massage particles, 0.3 part of disodium ethylene diamine tetraacetate, 0.1 part of sodium benzoate and 70 parts of water.
A method for preparing the cleansing massage bath cream comprises the following steps:
(1) preparing cleaning massage particles:
(1.1) respectively dispersing polylactic acid and zein into water to prepare polylactic acid dispersion liquid and zein dispersion liquid with solid contents of 15 wt% and 6 wt%, respectively; adding active carbon with the particle size of 40-50 mu m into polylactic acid dispersion liquid, uniformly dispersing, dropwise adding zein dispersion liquid under stirring, continuously stirring for 60min, and filtering to obtain active carbon @ zein/polylactic acid particles, wherein the mass ratio of polylactic acid to zein to active carbon is 2.5:1: 1;
(1.2) carrying out vacuum microwave treatment on the activated carbon @ zein/polylactic acid particles, wherein the vacuum degree is 0.05MPa, the power is 600W, the treatment time is 15min, and then carrying out vacuum drying to obtain clean massage particles with the particle size of 80-120 microns;
(2) heating water, maintaining at 75 deg.C, adding tea saponin and alkyl glycoside, mixing, adding cleaning massage particles, and mixing to obtain primary mixed solution;
(3) cooling the primary mixed liquid to 46 ℃, adding the chamomile extract, the citron fruit peel extract and the chlorella extract, mixing uniformly, adding the disodium ethylenediamine tetraacetic acid and the sodium benzoate, and fully mixing to obtain the cleaning massage bath cream.
Example 4
The cleaning massage bath cream comprises the following components in parts by weight: 4 parts of mother chrysanthemum extract, 0.5 part of citron fruit peel extract, 2 parts of chlorella extract, 2 parts of tea saponin, 5.5 parts of alkyl glycoside, 3 parts of cleaning massage particles, 1 part of wood particles, 0.3 part of disodium ethylene diamine tetraacetate, 0.1 part of sodium benzoate and 70 parts of water.
A method for preparing the cleansing massage bath cream comprises the following steps:
(1) preparing cleaning massage particles:
(1.1) respectively dispersing polylactic acid and zein into water to prepare polylactic acid dispersion liquid and zein dispersion liquid with solid contents of 15 wt% and 6 wt%, respectively; adding active carbon with the particle size of 40-50 mu m into polylactic acid dispersion liquid, uniformly dispersing, dropwise adding zein dispersion liquid under stirring, continuously stirring for 60min, and filtering to obtain active carbon @ zein/polylactic acid particles, wherein the mass ratio of polylactic acid to zein to active carbon is 2.5:1: 1;
(1.2) carrying out vacuum microwave treatment on the activated carbon @ zein/polylactic acid particles, wherein the vacuum degree is 0.05MPa, the power is 600W, the treatment time is 15min, and then carrying out vacuum drying to obtain clean massage particles with the particle size of 80-120 microns;
(2) preparing wood particles: pulverizing wood into particles with particle size of 50-100 μm, and loosening at 175 deg.C under 0.6MPa for 1 hr to obtain wood particles;
(3) adding wood particles into a part of water, wherein the mass ratio of the wood particles to the water is 1:10, and heating for 1.5 hours at 85 ℃ to obtain wood particle dispersion liquid;
(4) heating the rest water and maintaining at 75 deg.C, adding tea saponin and alkyl glycoside, mixing, adding wood particle dispersion liquid and cleaning massage particles, and mixing to obtain primary mixed liquid;
(5) cooling the primary mixed liquid to 46 ℃, adding the chamomile extract, the citron fruit peel extract and the chlorella extract, mixing uniformly, adding the disodium ethylenediamine tetraacetic acid and the sodium benzoate, and fully mixing to obtain the cleaning massage bath cream.
Comparative example 1
This comparative example is different from example 1 in that the cleaning massage particles are replaced with an equal mass of activated carbon having a particle size of 80 to 120 μm.
Comparative example 2
This comparative example differs from example 1 in that step (1.2) is not carried out.
Comparative example 3
This comparative example differs from example 1 in that in step (1.1) the polylactic acid is exchanged for zein of equal mass.
Comparative example 4
This comparative example differs from example 1 in that in step (1.1) zein is replaced by polylactic acid of equal mass.
Comparative example 5
The difference between the comparative example and the example 2 is that in the step (1.1), the mass ratio of the polylactic acid to the zein to the activated carbon is 2:1: 0.8.
Comparative example 5
The difference between the comparative example and example 3 is that in step (1.1), the mass ratio of polylactic acid, zein and activated carbon is 2.5:1: 1.
The test was performed on the body washes of examples 1-4 and comparative examples 1-4, respectively, by randomly dividing 80 subjects between 20-40 years of age into 8 groups, and the test items and methods were as follows:
(1) the oil removal effect is as follows: respectively testing the skin oil content of the inner side of the forearm of the testee before and after the shower gel is used, calculating the reduction rate of the skin oil content of each tester, and averaging each group;
(2) exfoliating effect: before use, the inner forearm of each subject was tested for skin roughness; after using the shower gel for 30 days (the using period is once a day), detecting the skin roughness of the anterior and medial sides of each subject again, calculating the reduction rate, and taking the average value of each group;
(3) sensory evaluation: taking 1-2g of shower gel, massaging the inner side of the forearm of a subject for 2min, scoring the skin pain condition, wherein 0 score represents no pain, 10 scores represents that the pain is very obvious, and averaging values are taken for each group.
The test results are shown in Table 1.
TABLE 1
Figure BDA0003055184430000071
Figure BDA0003055184430000081
The test results of comparative example 1 and comparative example 1 show that: after the surface of the active carbon is coated with the zein/polylactic acid composite coating layer, the pain is obviously weakened, and the deoiling effect is not obviously reduced. The reason is that: the active carbon with hard texture and rough surface is easy to generate pain and even hurt the skin when being directly contacted with the skin, and after the active carbon is coated by adopting the porous zein/polylactic acid, the polymer composite coating layer can endow the cleaning massage particles with smooth and softer surface, and can avoid the direct contact of the active carbon and the skin; in addition, in the composite coating layer, the zein and the polylactic acid both have higher hydrophobicity, so that the zein and the polylactic acid have an adsorption effect on oil stains, and the porous structure of the coating layer can ensure that the zein and the polylactic acid do not excessively influence the adsorption function of the activated carbon.
Example 4 the partial cleaning massage particles of example 3 were replaced with equal quality wood particles, and the test results of comparative example 3 and example 4 show that: compared with the single cleaning massage particles, the combination of the cleaning massage particles and the wood particles can reduce the pain although the oil removal effect is influenced to a certain extent. The reason is that: the active carbon of the core layer of the cleaning massage particles is not easy to deform, can keep better oil removal effect, but can also cause higher hardness of the cleaning massage particles; the texture of the wood particles is soft, so that the wood particles are more comfortable when being smeared on the skin, but the soft texture can also cause the pores to be easily deformed and reduced in the using process, so that the wood particles are not beneficial to the absorption of oil stains.
The test results of comparative example 1 and comparative example 2 show that: the cleaning massage particles treated by vacuum microwave can improve the deoiling effect of the shower gel. The reason is that: in the vacuum microwave treatment process, under the action of the air pressure difference between the inside and the outside of the particles and microwaves, air in the activated carbon vibrates and escapes, and pores are formed in the zein/polylactic acid coating layer, so that the excessive influence of the coating layer on the oil absorption effect of the activated carbon is prevented.
Comparing the test results of example 1 and comparative example 3, and example 2 and comparative example 5, it can be seen that: the coating layer outside the active carbon does not contain polylactic acid or the content of the polylactic acid is too low, so that the deoiling effect of the shower gel is not ideal. The reason is that: the polylactic acid has higher air permeability, and molecular chains of the polylactic acid form a net structure through physical entanglement, and are easily influenced by escaping air during vacuum microwave treatment to form larger pores, so that the influence of the coating layer on the oil absorption effect of the activated carbon can be reduced, and the cleaning massage particles have better oil removal function.
Comparing the test results of example 1 and comparative example 4, and example 3 and comparative example 6, it can be seen that: the coating layer outside the active carbon does not contain zein or the content of the zein is too low, so that the comfort degree of the shower gel during smearing is not ideal. The reason is that: the zein molecular chains are crosslinked through hydrogen bonds and disulfide bonds, so that a zein/polylactic acid crosslinking network has certain mechanical strength, and a coating layer is prevented from being damaged in the preparation and use processes of the shower gel.
Although the present invention has been described in detail with reference to the embodiments, it will be understood by those skilled in the art that the embodiments may be modified or changed without departing from the spirit of the present invention within the scope of the appended claims.

Claims (10)

1. The cleansing massage bath cream is characterized by comprising the following components in parts by weight: 3-4 parts of mother chrysanthemum extract, 0.5-2.5 parts of citron fruit peel extract, 1-2 parts of chlorella extract, 2-3 parts of tea saponin, 4.5-5.5 parts of alkyl glycoside, 3-4 parts of cleaning massage particles, 0.1-0.3 part of disodium ethylenediamine tetraacetic acid, 0.05-0.1 part of sodium benzoate and 60-70 parts of water; the cleaning massage particles comprise an activated carbon core layer and a porous zein/polylactic acid composite coating layer coated outside the activated carbon core layer.
2. The cleansing massage body wash as claimed in claim 1, wherein the particle size of the cleansing massage particles is 80 to 120 μm, and the diameter of the activated carbon core layer is 40 to 50 μm.
3. The cleansing massage body wash according to claim 1 or 2, wherein the cleansing massage particles are prepared by the following method:
(A) respectively dispersing polylactic acid and zein into water to prepare polylactic acid dispersion liquid and zein dispersion liquid; adding activated carbon into the polylactic acid dispersion liquid, after uniform dispersion, dropwise adding the zein dispersion liquid under stirring, continuously stirring for 40-60min, and filtering to obtain activated carbon @ zein/polylactic acid particles;
(B) and carrying out vacuum microwave treatment on the active carbon @ zein/polylactic acid particles, and then carrying out vacuum drying to obtain the clean massage particles.
4. The cleansing massage body wash of claim 3, wherein in step (A), the solids content of the polylactic acid dispersion and the zein dispersion are 10-15 wt% and 6-8 wt%, respectively.
5. The cleansing massage body wash of claim 3, wherein in step (A), the mass ratio of the polylactic acid, the zein and the activated carbon is 1.5-2.5:1: 0.5-1.
6. The cleansing massage body wash as claimed in claim 3, wherein in the step (B), the vacuum degree of the vacuum microwave treatment is 0.03-0.05MPa, the power is 500-600W, and the treatment time is 15-25 min.
7. The cleansing massage body wash of claim 1, further comprising the following components in parts by weight: 1-2 parts of wood particles.
8. The cleansing massage body wash as claimed in claim 7, wherein the preparation method of the wood particles is as follows: pulverizing wood into particles with particle size of 50-100 μm, and loosening at 180 deg.C and 0.5-0.8MPa for 40-80min to obtain wood particles.
9. A method of preparing a cleansing massage body wash according to any one of claims 1 to 8, comprising the steps of:
scheme A:
(1) heating water, maintaining the temperature at 65-75 deg.C, adding tea saponin and alkyl glycoside, mixing, adding cleaning massage particles, and mixing to obtain primary mixed solution;
(2) cooling the primary mixed liquid to 42-46 ℃, adding the chamomile extract, the citron fruit peel extract and the chlorella extract, mixing uniformly, adding disodium edetate and sodium benzoate, and fully mixing to obtain the cleaning massage bath cream;
scheme B:
(1) adding the wood particles into a part of water, and heating for 1-2h at 80-90 ℃ to obtain wood particle dispersion liquid;
(2) heating the rest water, maintaining the temperature at 65-75 deg.C, adding tea saponin and alkyl glycoside, mixing, adding wood particle dispersion liquid and cleaning massage particles, and mixing to obtain primary mixed liquid;
(3) cooling the primary mixed liquid to 42-46 ℃, adding the chamomile extract, the citron fruit peel extract and the chlorella extract, mixing uniformly, adding the disodium edetate and the sodium benzoate, and fully mixing to obtain the cleaning massage bath cream.
10. The method of claim 9, wherein in step (1) of protocol B, the mass ratio of wood particles to water is 1: 10-15.
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113876627A (en) * 2021-11-04 2022-01-04 何花 Fragrant mild antibacterial shower gel and preparation method thereof

Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1991006286A1 (en) * 1989-11-06 1991-05-16 Enzytech, Inc. Method for producing protein microspheres
JP2000226322A (en) * 1999-02-03 2000-08-15 Ichimaru Pharcos Co Ltd Agar or sodium alginate granule-containing cosmetic composition
JP2003342162A (en) * 2002-05-24 2003-12-03 Fancl Corp Skin cleaning composition
CN1562373A (en) * 2004-03-25 2005-01-12 上海交通大学 Method for preparing solid dosage forms type microsphere of alcohol soluble protein from source of plants
CN102836099A (en) * 2012-09-18 2012-12-26 曼秀雷敦(中国)药业有限公司 Activated carbon bead, facial cleanser comprising same and preparation methods thereof
FR2986968A1 (en) * 2012-02-21 2013-08-23 Laurent Schimmerling Exfoliating cosmetic solution based on pasteurized raw cork powder, used to prepare skin care products, comprises cream, shower gel or liquid soap, which is incorporated into the raw cork in powder form having varying particle size
CN103263374A (en) * 2013-05-28 2013-08-28 上海亚缇沐语生物科技有限公司 Calendula bath cream and preparation method thereof
CN103417390A (en) * 2013-07-23 2013-12-04 广州立白企业集团有限公司 Toothpaste containing carbon coating particles
CN106366590A (en) * 2016-08-29 2017-02-01 佛山市高明区尚润盈科技有限公司 Preparing method of polylactic acid photochromic master batch
CN109125112A (en) * 2018-07-23 2019-01-04 东莞市联洲知识产权运营管理有限公司 A kind of chitosan-based activated carbon shell nuclear particle and its preparation method and application that chitosan oligosaccharide/graphene is modified
CN109528619A (en) * 2019-01-30 2019-03-29 中吉亚科技(广州)有限公司 A kind of deodorizing type shower cream
CN112076109A (en) * 2020-09-24 2020-12-15 岭南师范学院 Shaddock peel pectin shower gel and preparation method thereof
CN112137907A (en) * 2020-09-28 2020-12-29 南京慧智莲华科技有限公司 Oil-control and relieving shower gel and preparation method thereof

Patent Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1991006286A1 (en) * 1989-11-06 1991-05-16 Enzytech, Inc. Method for producing protein microspheres
JP2000226322A (en) * 1999-02-03 2000-08-15 Ichimaru Pharcos Co Ltd Agar or sodium alginate granule-containing cosmetic composition
JP2003342162A (en) * 2002-05-24 2003-12-03 Fancl Corp Skin cleaning composition
CN1562373A (en) * 2004-03-25 2005-01-12 上海交通大学 Method for preparing solid dosage forms type microsphere of alcohol soluble protein from source of plants
FR2986968A1 (en) * 2012-02-21 2013-08-23 Laurent Schimmerling Exfoliating cosmetic solution based on pasteurized raw cork powder, used to prepare skin care products, comprises cream, shower gel or liquid soap, which is incorporated into the raw cork in powder form having varying particle size
CN102836099A (en) * 2012-09-18 2012-12-26 曼秀雷敦(中国)药业有限公司 Activated carbon bead, facial cleanser comprising same and preparation methods thereof
CN103263374A (en) * 2013-05-28 2013-08-28 上海亚缇沐语生物科技有限公司 Calendula bath cream and preparation method thereof
CN103417390A (en) * 2013-07-23 2013-12-04 广州立白企业集团有限公司 Toothpaste containing carbon coating particles
CN106366590A (en) * 2016-08-29 2017-02-01 佛山市高明区尚润盈科技有限公司 Preparing method of polylactic acid photochromic master batch
CN109125112A (en) * 2018-07-23 2019-01-04 东莞市联洲知识产权运营管理有限公司 A kind of chitosan-based activated carbon shell nuclear particle and its preparation method and application that chitosan oligosaccharide/graphene is modified
CN109528619A (en) * 2019-01-30 2019-03-29 中吉亚科技(广州)有限公司 A kind of deodorizing type shower cream
CN112076109A (en) * 2020-09-24 2020-12-15 岭南师范学院 Shaddock peel pectin shower gel and preparation method thereof
CN112137907A (en) * 2020-09-28 2020-12-29 南京慧智莲华科技有限公司 Oil-control and relieving shower gel and preparation method thereof

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
庄越等: "《实用药物制剂技术》", 31 January 1999 *
李立清等: "微波改性对活性炭及其甲醇吸附的影响", 《湖南大学学报》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113876627A (en) * 2021-11-04 2022-01-04 何花 Fragrant mild antibacterial shower gel and preparation method thereof

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