CN112999117A - Cleansing water with water phase and oil phase high-stability system, preparation method and application - Google Patents

Cleansing water with water phase and oil phase high-stability system, preparation method and application Download PDF

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Publication number
CN112999117A
CN112999117A CN202110239865.3A CN202110239865A CN112999117A CN 112999117 A CN112999117 A CN 112999117A CN 202110239865 A CN202110239865 A CN 202110239865A CN 112999117 A CN112999117 A CN 112999117A
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water
oil
phase
parts
makeup
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Chinese (zh)
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方丽霞
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Jingde Wanfang Commodity Co ltd
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Jingde Wanfang Commodity Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/14Preparations for removing make-up
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/48Thickener, Thickening system
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

Abstract

The invention provides makeup remover with a water phase and oil phase high-stability system, a preparation method and application, wherein the makeup remover comprises the following components in parts by weight: 0-2 parts of silicone oil, 3-5 parts of vegetable oil, 1-4 parts of synthetic esters, 2-3.5 parts of hydrocarbon grease, 1.5-4.5 parts of thickening agent, 2.5-4.5 parts of gellan gum, 5-8 parts of humectant, 0.005-0.01 part of preservative, 4-5 parts of surfactant, 0.2-0.5 part of electrolyte and 0.05-0.09 part of antioxidant; wherein the relative density of the synthetic ester is 1.14-1.15, and the thickener is pectin. By adding vegetable oil, synthetic esters, hydrocarbon grease, thickening agent, gellan gum and the like as main effective components of the makeup removing water, the problems of complicated use process, undesirable makeup removing effect, complex preparation process and high production cost of the double-layer makeup removing water are well solved. The makeup removing water provided by the invention can remove more than 90% of makeup within 1min, has obvious effect, adopts natural raw materials, and can achieve the effects of skin care and skin nourishing on the basis of being mild, not irritating and not damaging the skin.

Description

Cleansing water with water phase and oil phase high-stability system, preparation method and application
Technical Field
The invention belongs to the technical field of daily chemicals, and particularly relates to makeup remover with a water phase and oil phase high-stability system, a preparation method and application.
Background
Makeup is a metaphor of eticity, and most women make up at work or in life, and even without drawing color makeup, use sunscreen or isolation products to protect against ultraviolet rays, radiation from computers, and pollutants in the air. Excessive cosmetics and grease dirt are left on the skin, so that pores are blocked, the skin color is dull, and the health of the skin is affected. The makeup removing work is needed before the rest at night, and the best care for the face skin is achieved. If eye makeup and lip makeup are heavy, such as applying lipstick and eyeliner, partial color makeup is removed with a lip-specific makeup remover prior to full-face cleaning. The cleansing water has the advantage of being more refreshing than other cleansing products, but because the cleansing water contains less oil and more surfactants and alcohols, the cleansing water needs to be used together with makeup cotton. Dry makeup removal cotton can pull on the skin of the face, causing skin barrier damage and causing problems with the skin of the face.
Color cosmetics include BB cream, lipstick, lip gloss, eyebrow pencil, eye shadow, blush, etc. Most color cosmetics are oil-soluble or oil-dispersible and contain a large amount of oil, wax or silicone oil, because of the need for sweat resistance and moisture resistance. These make-up products are highly conformable after application to the face, and are difficult to clean with conventional cleansing products (e.g., soap bases, synthetic skin cleansing formulations). The makeup remover oil (cleansing oil) is oil added with an emulsifier, can be easily blended with color makeup and oil stain on the face according to the principle of similarity and intermiscibility, and takes away dirt on the face in a water emulsification mode during washing to play a role in makeup removal. Although the cleansing effect of the cleansing oil is good and the makeup remover can remove makeup from the surface of the skin, the cleansing oil is usually not mild enough in texture and can affect the skin to a certain extent after long-term use. Yet another reason is that the cleansing oil must be emulsified to achieve good cleansing, and if not completely emulsified, it can cause clogging of the pores and acne or acne on the face.
The most common makeup removing products in the existing market are makeup removing oil and makeup removing water, the two products are filled in a container bottle and are troublesome to carry when the user goes out for a journey or on a business trip and cannot be carried when the user takes an airplane, and after the makeup removing oil or the makeup removing water is sealed, a large number of effective substances can volatilize and bacteria in the air can enter the container bottle and the container bottle is unsanitary when the container bottle is placed for a long time. The cleansing product combines the advantages of cleansing oil and cleansing water, has better cleansing effect than the cleansing water, is fresher, tender and not greasy than the cleansing oil during use, is mild and non-irritant, is particularly suitable for sensitive parts such as eyes, lips and the like, and is the double-layer cleansing water. However, double-layer cleansing water has several significant disadvantages during use: 1. the cleansing cream is required to be vigorously shaken before use, and part of consumers are likely to have unsatisfactory cleansing effect and poor use experience because the shaking force is insufficient and water and oil are not fully and uniformly mixed; 2. the oil phase and the water phase can be quickly layered after shaking up, so that a consumer needs to shake up repeatedly for many times when removing makeup which is difficult to remove, such as waterproof eyeliner, mascara and the like, the makeup removing time is long, and the makeup removing efficiency is low; 3. the proportion of the water phase to the oil phase in the makeup remover taken out in each use can not be ensured to be the same, so that the makeup removing effect of the same bottle of makeup remover used in each use is different, and a user can not well control the use of the makeup remover.
Disclosure of Invention
Aiming at the problems, the invention provides makeup remover with a water phase and oil phase high-stability system, a preparation method and application, aiming at solving the problems that the double-layer makeup remover in the prior art has a plurality of obvious defects in the using process: 1. shaking forcibly before use; 2. the oil phase and the water phase can be quickly layered after shaking up, and when the makeup remover is used, repeated shaking up needs to be carried out, the makeup removing time is long, and the makeup removing efficiency is low; 3. the proportion of the water phase and the oil phase in the cleansing liquid taken each time of use can not be ensured to be the same.
The makeup remover with the water phase and oil phase high-stability system comprises the following components in parts by weight: 0-2 parts of silicone oil, 3-5 parts of vegetable oil, 1-4 parts of synthetic esters, 2-3.5 parts of hydrocarbon grease, 1.5-4.5 parts of thickening agent, 2.5-4.5 parts of gellan gum, 5-8 parts of humectant, 0.005-0.01 part of preservative, 4-5 parts of surfactant, 0.2-0.5 part of electrolyte and 0.05-0.09 part of antioxidant; wherein the relative density of the synthetic ester is 1.14-1.15, and the thickener is pectin.
Still further, the synthetic ester is sucrose acetate isobutyrate.
Further, the humectant is one or more of glycerin, diglycerin, dipropylene glycol, propylene glycol, 1, 3-butylene glycol, PEG-6 and isoprene glycol.
Further, the preservative is one or more of chlorphenesin, polyaminopropyl biguanide, p-hydroxyacetophenone, imidazolidinyl urea, phenoxyethanol, ethylhexyl glycerol, caprylyl glycol and caprylyl hydroxamic acid.
Still further, the surfactant is one or more of PEG-7 glyceryl cocoate, poloxamer, PEG-6 caprylic/capric glyceride.
Still further, the antioxidant is one or more of butylated hydroxytoluene, pentaerythritol tetrakis (bis-tert-butylhydroxyhydrocinnamate) ester and tocopherol acetate.
Furthermore, the makeup remover also comprises 0.1-0.3 part of pigment, and the pigment is natural pigment.
The invention also provides a preparation method of the cleansing water with the water phase and oil phase high-stability system, which comprises the following steps:
1) adding water into a main kettle, premixing a thickening agent and a humectant uniformly, adding the mixture into water at room temperature, stirring and heating until the mixture is fully swelled, then adding a surfactant, stirring uniformly, cooling, adding an electrolyte and a preservative, stirring uniformly, standing, cooling, condensing into solid glue, and crushing the solid glue into uniform fluid glue by using a homogenizer;
2) mixing the oil and the antioxidant, heating until the oil and the antioxidant are dissolved and transparent, cooling, adding the pigment, and uniformly stirring;
3) adding the mixture obtained in the step 2) into the water phase of the main kettle under the condition of stirring until oil drops are suspended in the water phase, and discharging after uniformly stirring to obtain the makeup remover with the water phase and oil phase highly stable system.
The invention also provides application of the makeup remover with the water-phase oil-phase high-stability system on the bearing body, wherein the makeup remover with the water-phase oil-phase high-stability system is uniformly coated on the bearing body, and the content of the makeup remover on the bearing body is saturated.
Furthermore, the carrier is absorbent cotton or non-woven fabric.
According to the makeup remover with the water phase and oil phase high-stability system, the silicone oil, the vegetable oil, the synthetic ester, the hydrocarbon oil, the thickening agent, the gellan gum, the humectant, the preservative, the surfactant, the electrolyte and the antioxidant are added to serve as main effective components of the makeup remover, so that the problems of complicated use process, unsatisfactory makeup removing effect, complex preparation process and high production cost of the double-layer makeup remover are well solved. The makeup removing water provided by the invention can remove more than 90% of makeup within 1min, has obvious effect, adopts natural raw materials, and can achieve the effects of skin care and skin nourishing on the basis of being mild, not irritating and not damaging the skin.
Additional features and advantages of the invention will be set forth in the description which follows, and in part will be obvious from the description, or may be learned by practice of the invention. The objectives and other advantages of the invention will be realized and attained by the structure particularly pointed out in the written description and claims hereof as well as the appended drawings.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below, and it is obvious that the drawings in the following description are some embodiments of the present invention, and those skilled in the art can also obtain other drawings according to the drawings without creative efforts.
FIG. 1 shows a flow chart of a method for preparing makeup remover according to an embodiment of the present invention;
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are some, but not all, embodiments of the present invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The main components of the conventional cleansing water comprise:
1) water, about 90%, to replenish stratum corneum water, to dissolve other components;
2) alcohols, bringing cool feeling, bacteriostasis and dissolving components;
3) a humectant which maintains the moisture of the stratum corneum, maintains good feeling in use, and dissolves other components;
4) a softening agent. The skin is lubricated and moistened;
5) emollient, to lubricate and moisturize the skin;
6) a surfactant having a high HLB and a solvent for solubilizing the raw material components;
7) a buffering agent for adjusting the pH value of the product;
7) the preservative is used for preventing the makeup remover from being corrupted and breeding bacteria so as to prolong the service life of the makeup remover;
8) astringent, algefacient, and appropriate amount of essence to make the cleansing water have better use feeling.
Compared with common lotion, the formula of the makeup remover contains more surfactants, humectants and alcohol compounds, and the cleansing effect on the skin is improved. However, many components in the traditional makeup removing aquatic products are derivatives of petrochemical industry, which not only have irritation to skin and potential harm to human health, poor biodegradation during discharge and environmental pollution, but also inevitably have residues of forbidden substances such as dioxane, ethylene oxide and the like which are harmful to human health in the production process. Similarly, the effective components of the traditional makeup removing wet tissue are mainly surfactant, a small amount of emulsifier and a small amount of oil-soluble agent, and the traditional makeup removing wet tissue is also harmful.
In addition, the makeup remover in the prior art mainly comprises three types, namely makeup remover oil, makeup remover water and double-layer makeup remover water, and the double-layer makeup remover water has better comprehensive feedback in use, but the makeup remover water still has more problems in the actual use process and needs to be improved. The specific problems include:
1. the cleansing cream is required to be vigorously shaken before use, and part of consumers are likely to have unsatisfactory cleansing effect and poor use experience because the shaking force is insufficient and water and oil are not fully and uniformly mixed;
2. the oil phase and the water phase can be quickly layered after shaking up, so that a consumer needs to shake up repeatedly for many times when removing makeup which is difficult to remove, such as waterproof eyeliner, mascara and the like, the makeup removing time is long, and the makeup removing efficiency is low;
3. the proportion of the water phase to the oil phase in the makeup remover taken out in each use can not be ensured to be the same, so that the makeup removing effect of the same bottle of makeup remover used in each use is different, and a user can not well control the use of the makeup remover.
Therefore, the invention provides cleansing water with a water phase and oil phase high-stability system, which comprises the following components in parts by weight: 0-2 parts of silicone oil, 3-5 parts of vegetable oil, 1-4 parts of synthetic esters, 2-3.5 parts of hydrocarbon grease, 1.5-4.5 parts of thickening agent, 2.5-4.5 parts of gellan gum, 5-8 parts of humectant, 0.005-0.01 part of preservative, 4-5 parts of surfactant, 0.2-0.5 part of electrolyte and 0.05-0.09 part of antioxidant; wherein the relative density of the synthetic ester is 1.14-1.15, and the thickener is pectin.
Still further, the synthetic ester is sucrose acetate isobutyrate.
Further, the humectant is one or more of glycerin, diglycerin, dipropylene glycol, propylene glycol, 1, 3-butylene glycol, PEG-6 and isoprene glycol.
Further, the preservative is one or more of chlorphenesin, polyaminopropyl biguanide, p-hydroxyacetophenone, imidazolidinyl urea, phenoxyethanol, ethylhexyl glycerol, caprylyl glycol and caprylyl hydroxamic acid.
Still further, the surfactant is one or more of PEG-7 glyceryl cocoate, poloxamer, PEG-6 caprylic/capric glyceride.
Still further, the antioxidant is one or more of butylated hydroxytoluene, pentaerythritol tetrakis (bis-tert-butylhydroxyhydrocinnamate) ester and tocopherol acetate.
Furthermore, the makeup remover also comprises 0.1-0.3 part of pigment, and the pigment is natural pigment.
The invention provides makeup remover with a water phase and oil phase high-stability system, in particular to makeup remover with suspended oil droplets. The stable suspended oil phase in the water phase can be discharged to form a stable system, and the makeup removing effect can reach an ideal state. The oil phase collocation in the invention is the combination of various types of grease according to a specific proportion, and the oil phase collocation has excellent dissolving capacity for products of vegetable oil systems, products of silicone oil systems and products of mineral oil systems, which is also a key factor for improving makeup removing effect. The addition of a thickener can further increase the stability, allowing better suspension of the oil droplets. The oil phase of the double-layer makeup remover can be uniformly and stably suspended in the water phase, shaking is not needed during use, oil and water are uniformly discharged during taking, the phenomenon of uneven taking of the oil and the water phase is avoided, the advantages of low irritation, fresh skin feeling, good makeup removing effect and the like of the double-layer makeup remover are completely kept, various inconveniences in the use process of the double-layer makeup remover can be solved, and the makeup removing efficiency is greatly improved. The makeup remover has low production cost, does not relate to a complex process in the preparation process, can be used for stably producing a large amount of makeup remover, and provides a new high-quality and low-price makeup remover for consumers.
The makeup remover with the water phase and oil phase high-stability system comprises the following main components: silicone oil, vegetable oil, synthetic esters, hydrocarbon oils, pectin, gellan gum, and the like. Wherein, the synthetic ester is sucrose acetate isobutyrate which is generally used as food additive, has good compatibility with various types of grease, has relative density of 1.14-1.15, and has wetting dispersion force on pigment. Besides adjusting the density of the oil phase, the cleansing oil has excellent removal capability on color cosmetics such as eye shadow, lipstick, foundation and the like. Pectin as thickener is a natural high molecular polysaccharide substance, and is usually a food additive prepared by extracting and refining one or more of pericarp and pomace of fructus Citri Grandis, fructus Citri Limoniae, Mandarin orange, and fructus Mali Pumilae, and can be used as thickener, gelatinizer, stabilizer, and tissue forming agent. Meanwhile, the pectin has the function of automatically balancing pH, and can form a protective film on the surface of skin when being applied to makeup remover, so that the facial skin is adjusted to a normal acid-base balance state. After the pectin and the gellan gum are compounded according to a specific proportion, the gellan gum has more excellent suspension stability due to a synergistic effect generated by crosslinking, and the suspension stability of the grease can be effectively improved. The gellan gum has a suspension effect because molecules can automatically aggregate to form a double-helix structure after being dissolved in water, and the addition of electrolyte initiates polymerization crosslinking between double helices. When the double helix is further aggregated to form a three-dimensional network structure, water molecules are trapped to generate a gel phenomenon.
Meanwhile, the invention also provides a preparation method of the cleansing water with the water phase and oil phase high-stability system, as shown in figure 1, the steps comprise:
1) adding water into a main kettle, premixing a thickening agent and a humectant uniformly, adding the mixture into water at room temperature, stirring and heating until the mixture is fully swelled, then adding a surfactant, stirring uniformly, cooling, adding an electrolyte and a preservative, stirring uniformly, standing, cooling, condensing into solid glue, and crushing the solid glue into uniform fluid glue by using a homogenizer;
2) mixing the oil and the antioxidant, heating until the oil and the antioxidant are dissolved and transparent, cooling, adding the pigment, and uniformly stirring;
3) adding the mixture obtained in the step 2) into the water phase of the main kettle under the condition of stirring until oil drops are suspended in the water phase, and discharging after uniformly stirring to obtain the makeup remover with the water phase and oil phase highly stable system.
In addition, through market research, professional women who obtain the result that the whole day is busy also feel too loaded down with the procedure of removing makeup water, removing makeup oil, hope that a can be fast, high-efficient, convenient removing makeup finished product appears to solve the problem that the procedure of removing makeup every day is too loaded down with trivial details. The makeup removing wet tissue is a novel makeup removing product appearing in the market in recent years, is deeply loved by consumers due to the outstanding advantages of convenience, rapidness, convenient carrying and the like, however, the makeup removing wet tissue in the prior art is mostly oil-soluble makeup removing wet tissue, the production cost is relatively high, the process is relatively complex, the product stability is relatively poor, the production process is very laborious, and the production cost is relatively high. Therefore, the invention provides the application of the makeup remover with the water-phase oil-phase high-stability system on the bearing body, the makeup remover with the water-phase oil-phase high-stability system is uniformly coated on the bearing body, and the content of the makeup remover on the bearing body is saturated. Wherein, the supporting body is absorbent cotton or non-woven fabrics.
Example 1
The makeup remover with the water phase and oil phase high-stability system comprises the following components in parts by weight: 1 part of silicone oil, 4 parts of vegetable oil, 3 parts of synthetic esters, 2.5 parts of hydrocarbon grease, 3 parts of thickening agent, 3 parts of gellan gum, 6 parts of humectant, 0.008 part of preservative, 4.5 parts of surfactant, 0.4 part of electrolyte, 0.06 part of antioxidant and 0.2 part of pigment; wherein the relative density of the synthetic ester is 1.14-1.15, and the thickener is pectin.
Wherein the synthetic ester is sucrose acetate isobutyrate; the humectant is glycerin; the preservative is chlorphenesin or phenoxyethanol; the surfactant is PEG-7 glyceryl cocoate; the antioxidant is butylated hydroxytoluene, pentaerythritol tetra (di-tert-butyl hydroxyhydrocinnamate) ester and tocopherol acetate.
A method for preparing cleansing water with a water phase and oil phase high-stability system comprises the following steps:
1) adding water into a main kettle, premixing a thickening agent and a humectant uniformly, adding the mixture into water at room temperature, stirring and heating until the mixture is fully swelled, then adding a surfactant, stirring uniformly, cooling, adding an electrolyte and a preservative, stirring uniformly, standing, cooling, condensing into solid glue, and crushing the solid glue into uniform fluid glue by using a homogenizer;
2) mixing the oil and the antioxidant, heating until the oil and the antioxidant are dissolved and transparent, cooling, adding the pigment, and uniformly stirring;
3) adding the mixture obtained in the step 2) into the water phase of the main kettle under the condition of stirring until oil drops are suspended in the water phase, and discharging after uniformly stirring to obtain the makeup remover with the water phase and oil phase highly stable system.
Example 2
The makeup remover with the water phase and oil phase high-stability system comprises the following components in parts by weight: 3 parts of vegetable oil, 1 part of synthetic ester, 2 parts of hydrocarbon grease, 1.5 parts of thickening agent, 2.5 parts of gellan gum, 5 parts of humectant, 0.005 part of preservative, 4 parts of surfactant, 0.2 part of electrolyte, 0.05 part of antioxidant and 0.1 part of pigment; wherein the relative density of the synthetic ester is 1.14-1.15, and the thickener is pectin.
Wherein the synthetic ester is sucrose acetate isobutyrate; the humectant is glycerol, PEG-6 and isoprene glycol; the preservative is caprylyl hydroximic acid; the surfactant is PEG-6 caprylic/capric glyceride; the antioxidant is butylated hydroxytoluene, pentaerythritol tetra (di-tert-butyl hydroxyhydrocinnamate) ester and tocopherol acetate.
A method for preparing cleansing water with a water phase and oil phase high-stability system comprises the following steps:
1) adding water into a main kettle, premixing a thickening agent and a humectant uniformly, adding the mixture into water at room temperature, stirring and heating until the mixture is fully swelled, then adding a surfactant, stirring uniformly, cooling, adding an electrolyte and a preservative, stirring uniformly, standing, cooling, condensing into solid glue, and crushing the solid glue into uniform fluid glue by using a homogenizer;
2) mixing the oil and the antioxidant, heating until the oil and the antioxidant are dissolved and transparent, cooling, adding the pigment, and uniformly stirring;
3) adding the mixture obtained in the step 2) into the water phase of the main kettle under the condition of stirring until oil drops are suspended in the water phase, and discharging after uniformly stirring to obtain the makeup remover with the water phase and oil phase highly stable system.
Example 3
The makeup remover with the water phase and oil phase high-stability system comprises the following components in parts by weight: 2 parts of silicone oil, 5 parts of vegetable oil, 4 parts of synthetic esters, 3.5 parts of hydrocarbon grease, 4.5 parts of thickening agent, 4.5 parts of gellan gum, 8 parts of humectant, 0.01 part of preservative, 5 parts of surfactant, 0.5 part of electrolyte, 0.09 part of antioxidant and 0.3 part of pigment; wherein the relative density of the synthetic ester is 1.14-1.15, and the thickener is pectin.
Wherein the synthetic ester is sucrose acetate isobutyrate; the humectant is a mixture of glycerol, diglycerol, dipropylene glycol, propylene glycol, 1, 3-butanediol, PEG-6 and isoprene glycol in any proportion; the preservative is a mixture of chlorphenesin, polyaminopropyl biguanide, p-hydroxyacetophenone, imidazolidinyl urea, phenoxyethanol, ethylhexyl glycerol, caprylyl glycol and caprylyl hydroxamic acid in any proportion; the surfactant is a mixture of PEG-7 glyceryl cocoate, poloxamer and PEG-6 caprylic/capric glyceride in any proportion, and the antioxidant is butylated hydroxytoluene;
a method for preparing cleansing water with a water phase and oil phase high-stability system comprises the following steps:
1) adding water into a main kettle, premixing a thickening agent and a humectant uniformly, adding the mixture into water at room temperature, stirring and heating until the mixture is fully swelled, then adding a surfactant, stirring uniformly, cooling, adding an electrolyte and a preservative, stirring uniformly, standing, cooling, condensing into solid glue, and crushing the solid glue into uniform fluid glue by using a homogenizer;
2) mixing the oil and the antioxidant, heating until the oil and the antioxidant are dissolved and transparent, cooling, adding the pigment, and uniformly stirring;
3) adding the mixture obtained in the step 2) into the water phase of the main kettle under the condition of stirring until oil drops are suspended in the water phase, and discharging after uniformly stirring to obtain the makeup remover with the water phase and oil phase highly stable system.
The stability and makeup removing effect performance of the makeup removing water with the water phase and oil phase high-stability system prepared in 3 embodiments are detected, and the obtained result is that the makeup removing water and oil phase can be stably suspended in the water phase, the system can be kept stable under the environments of high temperature, low temperature, slight vibration, large-amplitude vibration, long-time standing and the like, the effect of the makeup removing water is remarkable, cosmetics can be quickly dissolved within 5s, and the makeup on the skin can be removed within 1min by more than 90%.
Although the present invention has been described in detail with reference to the foregoing embodiments, it will be understood by those of ordinary skill in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some technical features may be equivalently replaced; and such modifications or substitutions do not depart from the spirit and scope of the corresponding technical solutions of the embodiments of the present invention.

Claims (10)

1. The cleansing water with the water phase and oil phase high-stability system is characterized in that: the composition comprises the following components in parts by weight: 0-2 parts of silicone oil, 3-5 parts of vegetable oil, 1-4 parts of synthetic esters, 2-3.5 parts of hydrocarbon grease, 1.5-4.5 parts of thickening agent, 2.5-4.5 parts of gellan gum, 5-8 parts of humectant, 0.005-0.01 part of preservative, 4-5 parts of surfactant, 0.2-0.5 part of electrolyte and 0.05-0.09 part of antioxidant; wherein the relative density of the synthetic ester is 1.14-1.15, and the thickener is pectin.
2. The makeup remover with the water-phase oil-phase high-stability system is characterized in that: the synthetic ester is sucrose acetate isobutyrate.
3. The makeup remover with the water-phase oil-phase high-stability system is characterized in that: the humectant is one or more of glycerol, diglycerol, dipropylene glycol, propylene glycol, 1, 3-butanediol, PEG-6 and isoprene glycol.
4. The makeup remover with the water-phase oil-phase high-stability system is characterized in that: the antiseptic is one or more of chlorphenesin, polyaminopropyl biguanide, p-hydroxyacetophenone, imidazolidinyl urea, phenoxyethanol, ethylhexyl glycerol, caprylyl glycol and caprylyl hydroximic acid.
5. The makeup remover with the water-phase oil-phase high-stability system is characterized in that: the surfactant is one or more of PEG-7 glyceryl cocoate, poloxamer and PEG-6 caprylic/capric glyceride.
6. The makeup remover with the water-phase oil-phase high-stability system is characterized in that: the antioxidant is one or more of butylated hydroxytoluene, pentaerythritol tetra (bis-tert-butyl hydroxyhydrocinnamate) ester and tocopherol acetate.
7. The cleansing water having a high stability system of an aqueous phase and an oil phase according to any one of claims 1 to 6, wherein: the makeup remover also comprises 0.1-0.3 part of pigment, and the pigment is natural pigment.
8. The method for preparing the cleansing water with the high stability system of the water phase and the oil phase as claimed in claim 7 is characterized in that: the steps include:
1) adding water into a main kettle, premixing a thickening agent and a humectant uniformly, adding the mixture into water at room temperature, stirring and heating until the mixture is fully swelled, then adding a surfactant, stirring uniformly, cooling, adding an electrolyte and a preservative, stirring uniformly, standing, cooling, condensing into solid glue, and crushing the solid glue into uniform fluid glue by using a homogenizer;
2) mixing the oil and the antioxidant, heating until the oil and the antioxidant are dissolved and transparent, cooling, adding the pigment, and uniformly stirring;
3) adding the mixture obtained in the step 2) into the water phase of the main kettle under the condition of stirring until oil drops are suspended in the water phase, and discharging after uniformly stirring to obtain the makeup remover with the water phase and oil phase highly stable system.
9. Use of a make-up remover with a highly stable system of aqueous and oily phases on a support according to claim 7, characterized in that: and uniformly coating the makeup removing water with the water-phase oil-phase high-stability system on the bearing body, wherein the makeup removing water content on the bearing body is saturated.
10. Use according to claim 9, characterized in that: the supporting body is absorbent cotton or non-woven fabric.
CN202110239865.3A 2021-03-04 2021-03-04 Cleansing water with water phase and oil phase high-stability system, preparation method and application Pending CN112999117A (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070065393A1 (en) * 2005-09-20 2007-03-22 L'oreal Make-up-removing composition
CN109966184A (en) * 2019-04-30 2019-07-05 广州玮弘祺生物科技有限公司 A kind of suspension oil droplet makeup remover and preparation method thereof
CN110420152A (en) * 2019-08-20 2019-11-08 中山中研化妆品有限公司 A kind of salubrious mild double-deck make up remover and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070065393A1 (en) * 2005-09-20 2007-03-22 L'oreal Make-up-removing composition
CN109966184A (en) * 2019-04-30 2019-07-05 广州玮弘祺生物科技有限公司 A kind of suspension oil droplet makeup remover and preparation method thereof
CN110420152A (en) * 2019-08-20 2019-11-08 中山中研化妆品有限公司 A kind of salubrious mild double-deck make up remover and preparation method thereof

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