CN112921666A - Agilawood emulsion with antiviral and bactericidal effects as well as preparation method and application thereof - Google Patents

Agilawood emulsion with antiviral and bactericidal effects as well as preparation method and application thereof Download PDF

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CN112921666A
CN112921666A CN202110110207.4A CN202110110207A CN112921666A CN 112921666 A CN112921666 A CN 112921666A CN 202110110207 A CN202110110207 A CN 202110110207A CN 112921666 A CN112921666 A CN 112921666A
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essential oil
oil
agilawood
emulsion
antiviral
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周日锋
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Guangxi Meihao Industrial Co ltd
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Guangxi Meihao Industrial Co ltd
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M23/00Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
    • D06M23/12Processes in which the treating agent is incorporated in microcapsules
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/005Compositions containing perfumes; Compositions containing deodorants
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M16/00Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/14Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
    • D21H21/36Biocidal agents, e.g. fungicidal, bactericidal, insecticidal agents

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Chemical & Material Sciences (AREA)
  • Biochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention provides agilawood emulsion with antiviral and bactericidal effects and a preparation method and application thereof. The agilawood emulsion comprises perfume microcapsules and water, wherein the mass concentration of the perfume microcapsules is 5-20%; the core material wrapped by the perfume microcapsule comprises composite oil and a nano antibacterial material, wherein the composite oil comprises: 1.5-3% of agilawood essential oil, 2-6% of sandalwood essential oil, 1-5% of lavender essential oil, 0.5-3% of ylang essential oil, 1-5% of lemon essential oil, 1-6% of eucalyptus essential oil, 1-5% of orange flower essential oil, 1-3% of benzoin essential oil and the balance of base oil, wherein the nano antibacterial material accounts for 10-15% of the core material mixture of the nano antibacterial material and the composite oil. The invention has natural fragrance, the fragrance is slowly released for a long time, and the invention has obvious antibacterial and antivirus effects, the killing rate to H1N1 influenza virus reaches 99.13%, and the killing rate to colibacillus, staphylococcus aureus and candida reaches more than 99%.

Description

Agilawood emulsion with antiviral and bactericidal effects as well as preparation method and application thereof
Technical Field
The invention relates to the technical field of materials, in particular to agilawood emulsion with antiviral and bactericidal effects and a preparation method and application thereof.
Background
Common articles used repeatedly for a long time in daily life, such as curtains, can breed bacteria due to the fact that the articles are affected with damp and the like in the process of household use; in addition, the cloth area is large, and bacteria and viruses in the air are easy to adhere and propagate; when influenza occurs in family members, the influenza virus can easily parasitize on the family members, and the probability of other family members infecting the influenza is increased.
If the daily necessities which are repeatedly used for a long time and are inconvenient to clean are endowed with the functions of resisting virus and sterilizing, the problem of rapid propagation of viruses and bacteria can be effectively solved, and the household environment is healthier.
Disclosure of Invention
The invention aims to solve the technical problem of providing agilawood emulsion with antiviral and bactericidal effects and a preparation method and application thereof. The agilawood antibacterial agent has good antitoxic and bactericidal effects, and the antibacterial effect of the agilawood is greatly enhanced by utilizing the medicinal effect of the agilawood and combining a novel nontoxic antibacterial agent. The curtain fabric processed by the molecular embedding technology, the slow release technology and the like can effectively solve the problem that the curtain is no longer a virus and bacterium carrier, so that the home environment is more environment-friendly and healthy.
In order to solve the technical problems, the invention adopts the following technical scheme:
an agilawood emulsion with antiviral and antibacterial effects comprises perfume microcapsules and water, wherein the mass concentration of the perfume microcapsules is 5-20%; wherein:
the core material wrapped by the perfume microcapsule comprises composite oil, wherein the composite oil comprises the following components in percentage by weight:
1.5-3% of agilawood essential oil, 2-6% of sandalwood essential oil, 1-5% of lavender essential oil, 0.5-3% of ylang essential oil, 1-5% of lemon essential oil, 1-6% of eucalyptus essential oil, 1-5% of orange flower essential oil, 1-3% of benzoin essential oil and the balance of base oil.
Further, the composite oil comprises the following components in percentage by weight: 2% of agilawood essential oil, 4% of sandalwood essential oil, 3% of lavender essential oil, 1% of ylang-ylang essential oil, 3% of lemon essential oil, 3% of eucalyptus leaf essential oil, 2.5% of orange flower essential oil, 1.5% of benzoin essential oil and 80% of base oil.
Further, the core material wrapped by the perfume microcapsule also comprises a CSNM medical nano antibacterial material which is sourced from China center (Guangzhou) nano material Co., Ltd, and the CSNM medical nano antibacterial material corresponds to the patent application number 201911352358X. In the mixture of the CSNM medical nano antibacterial material and the composite oil, the mass percentage of the CSNM medical nano antibacterial material is 10-20%.
Further, the perfume microcapsule is 30 microns.
Further, the base oil is selected from jojoba oil, sweet almond oil, grape seed oil, rose hip oil, olive oil, etc., and can be common base oil.
The preparation method of the agilawood emulsion with the antiviral and bactericidal effects comprises the following steps:
(1) mixing lignum Aquilariae Resinatum essential oil, lignum Santali albi essential oil, Lavender essential oil, cananga odorata essential oil, fructus Citri Limoniae essential oil, folium Eucalypti Globueli essential oil, neroli essential oil, Benzonum essential oil, and base oil at a certain proportion, and alcoholizing at 35-45 deg.C for 24 hr;
(2) mixing the treated compound oil and the nano antibacterial material in proportion to obtain a mixture;
(3) preparing the mixture into perfume microcapsule by microcapsule coating technology;
(4) mixing the perfume microcapsule with water, and stirring to obtain emulsion with perfume microcapsule mass concentration of 5-20%.
In the invention, the agilawood emulsion with the antiviral and bactericidal effects can be applied to the production and preparation of articles for daily use which need to be repeatedly used for a long time and are inconvenient to clean, such as the production of curtains or other cloth materials, and can also be applied to the production and preparation of paper.
The application of the agilawood emulsion with the antiviral and bactericidal effects in producing the curtain comprises the following steps:
and (2) putting the prepared agilawood emulsion with the antiviral and bactericidal effects into a water tank of textile fabric finishing equipment, slowly immersing the continuously passing curtain fabric into the water tank, and performing shaping and drying in a drying oven with the temperature controlled at 150 ℃ to obtain the curtain fabric with the agilawood compound fragrance and the antibacterial function. At present, the curtain with the fragrance of the agilawood and the antibacterial effect is not reported.
The technical scheme of the invention has the following beneficial effects:
(1) has fragrant and fragrant natural fragrance.
(2) The fragrance is slowly released for a long time, and the fragrance can be washed for more than 10 times after being tested for more than two years.
(3) Has obvious antibacterial and antivirus effects, and is proved by detection: the killing rate to H1N1 influenza virus reaches 99.13%, and the killing rate to colibacillus, staphylococcus aureus and candida reaches more than 99%.
Drawings
Fig. 1 is a diagram of a curtain fabric product obtained by applying the agilawood emulsion of example 3 in curtain production.
Detailed Description
In order to make the technical problems, technical solutions and advantages to be solved by the present invention clearer, the following detailed description is given with reference to specific embodiments.
The CSNM medical nano antibacterial material is from China center (Guangzhou) nano material Co., Ltd, and the corresponding patent application number of the CSNM medical nano antibacterial material is 201911352358X.
Example 1
An agilawood emulsion with antiviral and antibacterial effects comprises perfume microcapsules and water, wherein the mass concentration of the perfume microcapsules is 5%; wherein:
the core material wrapped by the perfume microcapsule comprises composite oil and a CSNM medical nano antibacterial material, wherein the CSNM medical nano antibacterial material accounts for 10%, and the composite oil comprises the following components in percentage by weight:
1.5% of agilawood essential oil, 2% of sandalwood essential oil, 1% of lavender essential oil, 0.5% of ylang-ylang essential oil, 1% of lemon essential oil, 1% of eucalyptus leaf essential oil, 1% of orange flower essential oil, 1% of benzoin essential oil and the balance of base oil.
The base oil is selected from jojoba oil.
The preparation method of the agilawood emulsion comprises the following steps:
(1) mixing lignum Aquilariae Resinatum essential oil, lignum Santali albi essential oil, Lavender essential oil, cananga odorata essential oil, fructus Citri Limoniae essential oil, folium Eucalypti Globueli essential oil, neroli essential oil, Benzonum essential oil, and base oil at a certain proportion, and alcoholizing at 35-45 deg.C for 24 hr;
(2) mixing the treated composite oil and the CSNM medical nano antibacterial material in proportion to obtain a mixture;
(3) preparing the mixture into perfume microcapsules with the diameter of about 30 microns by a microcapsule wrapping technology;
(4) mixing the perfume microcapsule with water, and stirring to obtain emulsion.
Example 2
An agilawood emulsion with antiviral and antibacterial effects comprises perfume microcapsules and water, wherein the mass concentration of the perfume microcapsules is 20%; wherein:
the core material wrapped by the perfume microcapsule comprises composite oil and a CSNM medical nano antibacterial material, wherein the CSNM medical nano antibacterial material accounts for 20%, and the composite oil comprises the following components in percentage by weight:
3% of agilawood essential oil, 6% of sandalwood essential oil, 5% of lavender essential oil, 3% of ylang-ylang essential oil, 5% of lemon essential oil, 6% of eucalyptus leaf essential oil, 5% of orange flower essential oil, 3% of benzoin essential oil and the balance of base oil.
The base oil is selected from olive oil.
The preparation method of the agilawood emulsion comprises the following steps:
(1) mixing lignum Aquilariae Resinatum essential oil, lignum Santali albi essential oil, Lavender essential oil, cananga odorata essential oil, fructus Citri Limoniae essential oil, folium Eucalypti Globueli essential oil, neroli essential oil, Benzonum essential oil, and base oil at a certain proportion, and alcoholizing at 35-45 deg.C for 24 hr;
(2) mixing the treated composite oil and the CSNM medical nano antibacterial material in proportion to obtain a mixture;
(3) preparing the mixture into perfume microcapsules with the diameter of about 30 microns by a microcapsule wrapping technology;
(4) mixing the perfume microcapsule with water, and stirring to obtain emulsion.
Example 3
An agilawood emulsion with antiviral and antibacterial effects comprises perfume microcapsules and water, wherein the mass concentration of the perfume microcapsules is 10%; wherein:
the core material wrapped by the perfume microcapsule comprises composite oil and a CSNM medical nano antibacterial material, wherein the CSNM medical nano antibacterial material accounts for 15%, and the composite oil comprises the following components in percentage by weight:
2% of agilawood essential oil, 4% of sandalwood essential oil, 3% of lavender essential oil, 1% of ylang-ylang essential oil, 3% of lemon essential oil, 3% of eucalyptus leaf essential oil, 2.5% of orange flower essential oil, 1.5% of benzoin essential oil and 80% of base oil.
The base oil is selected from grape seed oil.
The preparation method of the agilawood emulsion comprises the following steps:
(1) mixing lignum Aquilariae Resinatum essential oil, lignum Santali albi essential oil, Lavender essential oil, cananga odorata essential oil, fructus Citri Limoniae essential oil, folium Eucalypti Globueli essential oil, neroli essential oil, Benzonum essential oil, and base oil at a certain proportion, and alcoholizing at 35-45 deg.C for 24 hr;
(2) mixing the treated composite oil and the CSNM medical nano antibacterial material in proportion to obtain a mixture;
(3) preparing the mixture into perfume microcapsules with the diameter of about 30 microns by a microcapsule wrapping technology;
(4) mixing the perfume microcapsule with water, and stirring to obtain emulsion.
Application examples
The agilawood emulsion with the antiviral and bactericidal effects can be applied to the production and preparation of articles for daily use which need to be repeatedly used for a long time and are inconvenient to clean, such as the production of curtains or other cloth materials, and can also be applied to the production and preparation of paper.
The application of the agilawood emulsion with the antiviral and bactericidal effects in the example 3 in the curtain production comprises the following steps:
the prepared agilawood emulsion with the antiviral and bactericidal effects is placed in a water tank of textile fabric finishing equipment, a curtain fabric passing through continuously is slowly immersed in the water tank, and is shaped and dried by a drying box controlling the temperature at 150 ℃, so that the curtain fabric containing the agilawood compound fragrance and having the antibacterial function is manufactured, and the product diagram is shown in fig. 1.
The prepared curtain fabric is analyzed and detected in a microbiological analysis and detection center in Guangdong province, and detection items comprise antiviral activity detection and antibacterial (bacteriostatic) detection.
1. Antiviral Activity assay
Detection basis and method: ISO 18184: 2014 (E);
the test results are as follows:
Figure BDA0002916336080000041
Figure BDA0002916336080000051
2. antibacterial (bacteriostatic) assay
Detection basis and method: GB/T20944.2-2007 absorption method, GB/T20944.3-2008 oscillation method;
the test results are as follows:
Figure BDA0002916336080000052
Figure BDA0002916336080000061
therefore, the emulsion of the invention has obvious antibacterial and antivirus effects, and the detection proves that: the killing rate to H1N1 influenza virus reaches 99.13%, and the killing rate to colibacillus and staphylococcus aureus reaches more than 99%.
While the foregoing is directed to the preferred embodiment of the present invention, it will be understood by those skilled in the art that various changes and modifications may be made without departing from the spirit and scope of the invention as defined in the appended claims.

Claims (9)

1. An agilawood emulsion with antiviral and bactericidal effects is characterized by comprising perfume microcapsules and water, wherein the mass concentration of the perfume microcapsules is 5-20%; wherein:
the core material wrapped by the perfume microcapsule comprises composite oil, wherein the composite oil comprises the following components in percentage by weight:
1.5-3% of agilawood essential oil, 2-6% of sandalwood essential oil, 1-5% of lavender essential oil, 0.5-3% of ylang essential oil, 1-5% of lemon essential oil, 1-6% of eucalyptus essential oil, 1-5% of orange flower essential oil, 1-3% of benzoin essential oil and the balance of base oil.
2. The agilawood emulsion with antiviral and antibacterial effects as claimed in claim 1, wherein the compound oil comprises the following components in percentage by weight:
2% of agilawood essential oil, 4% of sandalwood essential oil, 3% of lavender essential oil, 1% of ylang-ylang essential oil, 3% of lemon essential oil, 3% of eucalyptus leaf essential oil, 2.5% of orange flower essential oil, 1.5% of benzoin essential oil and 80% of base oil.
3. The agilawood emulsion with antiviral and bactericidal effects according to claim 1 or 2, wherein the core material wrapped by the perfume microcapsule further comprises a CSNM medical nano antibacterial material, and the mass ratio of the CSNM medical nano antibacterial material in the core material mixture of the CSNM medical nano antibacterial material and the composite oil is 10-20%.
4. The agilawood emulsion having antiviral and antibacterial effects according to claim 3, wherein the perfume microcapsule is 30 microns.
5. The antiviral and antibacterial eaglewood emulsion according to claim 4, wherein the base oil is selected from one or more of jojoba oil, sweet almond oil, grape seed oil, rose hip oil and olive oil.
6. The method for preparing agilawood emulsion with antiviral and antibacterial effects as claimed in claim 5, comprising the following steps:
(1) mixing lignum Aquilariae Resinatum essential oil, lignum Santali albi essential oil, Lavender essential oil, cananga odorata essential oil, fructus Citri Limoniae essential oil, folium Eucalypti Globueli essential oil, neroli essential oil, Benzonum essential oil, and base oil at a certain proportion, and alcoholizing at 35-45 deg.C for 24 hr;
(2) mixing the treated compound oil and the nano antibacterial material in proportion to obtain a mixture;
(3) preparing the mixture into perfume microcapsule by microcapsule coating technology;
(4) mixing the perfume microcapsule with water, and stirring to obtain emulsion with perfume microcapsule mass concentration of 5-20%.
7. The use of the agilawood emulsion with antiviral and antibacterial effects according to claim 5 in the production and preparation of cloth or paper stock.
8. The use of the agilawood emulsion with antiviral and antibacterial effects according to claim 5 in the production and preparation of curtains.
9. Use according to claim 8, characterized in that it comprises the following steps:
and (2) putting the prepared agilawood emulsion with the antiviral and bactericidal effects into a water tank of textile fabric finishing equipment, slowly immersing the continuously passing curtain fabric into the water tank, and performing shaping and drying in a drying oven with the temperature controlled at 150 ℃ to obtain the curtain fabric with the agilawood compound fragrance and the antibacterial function.
CN202110110207.4A 2021-01-26 2021-01-26 Agilawood emulsion with antiviral and bactericidal effects as well as preparation method and application thereof Pending CN112921666A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115141502A (en) * 2022-08-05 2022-10-04 青岛万源生物科技有限公司 Visible light catalytic bactericidal antiviral coating material and preparation method thereof
CN115387129A (en) * 2022-08-02 2022-11-25 厦门旭纶成纺织科技有限公司 Agilawood cloth preparation method

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CN111053089A (en) * 2019-12-23 2020-04-24 中星(广州)纳米材料有限公司 Nano sterilizing and formaldehyde removing composition and preparation method thereof

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115387129A (en) * 2022-08-02 2022-11-25 厦门旭纶成纺织科技有限公司 Agilawood cloth preparation method
CN115141502A (en) * 2022-08-05 2022-10-04 青岛万源生物科技有限公司 Visible light catalytic bactericidal antiviral coating material and preparation method thereof

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