CN110314621A - A kind of wormwood essential oil microcapsules and preparation method thereof - Google Patents

A kind of wormwood essential oil microcapsules and preparation method thereof Download PDF

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Publication number
CN110314621A
CN110314621A CN201910545597.0A CN201910545597A CN110314621A CN 110314621 A CN110314621 A CN 110314621A CN 201910545597 A CN201910545597 A CN 201910545597A CN 110314621 A CN110314621 A CN 110314621A
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China
Prior art keywords
essential oil
wormwood
oil
capsule skin
preparation
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Pending
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CN201910545597.0A
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Chinese (zh)
Inventor
李铭春
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Dongguan Jan Yue Garment Co Ltd
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Dongguan Jan Yue Garment Co Ltd
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Priority to CN201910545597.0A priority Critical patent/CN110314621A/en
Publication of CN110314621A publication Critical patent/CN110314621A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02Making microcapsules or microballoons
    • B01J13/04Making microcapsules or microballoons by physical processes, e.g. drying, spraying
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0003Compounds of unspecified constitution defined by the chemical reaction for their preparation
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M16/00Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M23/00Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
    • D06M23/12Processes in which the treating agent is incorporated in microcapsules

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Textile Engineering (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Biochemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Dispersion Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of wormwood essential oil microcapsules and preparation method thereof, it include: capsule skin, the intradermal portion of capsule is filled with essential oil wick, wormwood essential oil passes through the molecular gap slow release of capsule skin, capsule skin is high molecular material, and essential oil microcapsules surface is active, can be welded together with textile by washing to impregnate to be bonded, bonding force is big, has good water-wash resistance.Capsule skin does not react with water and air, wormwood essential oil and extraneous contact has effectively been isolated, so that wormwood essential oil is can according to need slow release, make the clothing of wormwood essential oil, repeatedly still there is after washing long acting antibiotic, sterilization, it eliminates the unusual smell antipruritic, active and other effects, wormwood incense has promoting flow of qi by warming channel, and it is socks that antibacterial anti-inflammatory, which eliminates the unusual smell and other effects, towel, the preferred combination of the common textile such as underpants.

Description

A kind of wormwood essential oil microcapsules and preparation method thereof
Technical field
The present invention relates to microcapsules fields, more particularly, to a kind of wormwood essential oil microcapsules and preparation method thereof.
Background technique
Microcapsules technology (Microencapsulation) is the technology that micro substance is wrapped in thin polymer film, is one Kind store solids, the microdisplay package technology of liquid, gas.In microencapsulation field, Wuster and Green are two greatnesses Pioneer.Microencapsulation starts from the thirties in last century, but develops very fast.Application range is expanded to textile, medicine, agriculture With chemicals, the every field such as adhesive and liquid crystal.With the development of society, the progress of science, consumption of the people to textile The raising of standard, functionalization textile come into being.Called function textile refers to high-tech technological means, passes through weaving Product final finishing makes common textile that there is the specific functions such as longer antibacterial, deodorization, sterilization, protection skin to have at present Most in product is that the high-volume cloth dyeing and finishing that textile industry dyeing uses is added, and lacking a kind of to be daily household auxiliary Assist liquid.
Summary of the invention
The present invention is to overcome above situation insufficient, it is desirable to provide a kind of technical solution that can solve the above problem.
A kind of wormwood essential oil microcapsules, comprising: capsule skin, the intradermal portion of capsule are filled with essential oil wick.
As a further solution of the present invention: the capsule skin is that high-molecular anti-bacteria material and ionized water dissolve mixed liquor preparation It forms.
As a further solution of the present invention: the ratio that the high-molecular anti-bacteria material and ionized water dissolve is 3:7.
As a further solution of the present invention: the essential oil wick is prepared from the following raw materials in parts by weight: food-grade food Grade P-Cymene 15-20%, Essential Oil From Pine Needles 3-5%, Geranium Essential 3-5%, cedar wood oil 3-5%, bergamot essential oil 1- 3%, orange oil 2-4% remaining to leave away water.
As a further solution of the present invention: the essential oil wick is prepared from the following raw materials in parts by weight: food-grade food Grade P-Cymene 15%, Essential Oil From Pine Needles 3%, Geranium Essential 3%, cedar wood oil 3%, bergamot essential oil 1%, orange oil 2% Remaining is water of leaving away.
As a further solution of the present invention: the essential oil wick is prepared from the following raw materials in parts by weight: food-grade food Grade P-Cymene 20%, Essential Oil From Pine Needles 5%, Geranium Essential 5%, cedar wood oil 5%, bergamot essential oil 3%, orange oil 4% Remaining is water of leaving away.
A kind of preparation method of wormwood essential oil microcapsules, the wormwood essential oil microcapsules include following preparation step:
Step 1: food-grade food-grade P-Cymene, Essential Oil From Pine Needles, Geranium Essential, cypress will the preparation of essential oil wick: be eaten Oil, bergamot essential oil, orange oil are added in mixing apparatus with water of leaving away and are mixed, and are cooled down, are obtained after the completion of mixing Essential oil solution;
Step 2: it the preparation of capsule skin solution: high-molecular anti-bacteria material be added in mixing apparatus with ionized water carries out Mixing, obtains capsule skin solution;
Step 3: capsule skin solution being added in mixing apparatus with essential oil solution and is mixed, then will be mixed molten Liquid is poured into different molds and is cooled and shaped, because the high molecular material in the different reason capsule skin solution of density can be automatic One layer of capsule skin is formed in essential oil solution surface, so that essential oil solution be wrapped up, forms the state that capsule skin is wrapped in essential oil wick, it is complete At the preparation of wormwood essential oil microcapsules.
As a further solution of the present invention: in the step 1: mixing apparatus is constant temperature stirring container, and mixing temperature is 20-25 DEG C, incorporation time 360-420min, the cooling reaction time is 2-4H
As a further solution of the present invention: in institute's step 2: mixing apparatus is constant temperature stirring container, and incorporation time is 120-180min。
As a further solution of the present invention: in the step 3, mixing temperature is 30-40 DEG C, incorporation time 300- 360min。
Compared with prior art, the beneficial effects of the present invention are: wormwood essential oil passes through the molecular gap slow release of capsule skin, Capsule skin is high molecular material, and essential oil microcapsules surface is active, can be welded together with textile by washing to impregnate to be bonded, Bonding force is big, has good water-wash resistance.Capsule skin does not react with water and air, and wormwood essential oil and outer has effectively been isolated The contact on boundary makes wormwood essential oil can according to need slow release, makes the clothing of wormwood essential oil, repeatedly still has after washing Long acting antibiotic, sterilization eliminate the unusual smell antipruritic, active and other effects, and wormwood incense has promoting flow of qi by warming channel, and antibacterial anti-inflammatory eliminates the unusual smell and other effects and to be Socks, towel, the preferred combination of the common textile such as underpants.
Additional aspect and advantage of the invention will be set forth in part in the description, and will partially become from the following description Obviously, or practice through the invention is recognized.
Detailed description of the invention
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below There is attached drawing needed in technical description to be briefly described, it should be apparent that, the accompanying drawings in the following description is only this Some embodiments of invention without any creative labor, may be used also for those of ordinary skill in the art To obtain other drawings based on these drawings.
Fig. 1 is schematic structural view of the invention.
In figure: 1, capsule skin, 2, wormwood essential oil.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common Technical staff's every other embodiment obtained without making creative work belongs to the model that the present invention protects It encloses.
Referring to Fig. 1, in the embodiment of the present invention, a kind of wormwood essential oil microcapsules, comprising: capsule skin 1, inside the capsule skin 1 Filled with essential oil wick 2.
The capsule skin 1 is that high-molecular anti-bacteria material is prepared with ionized water dissolution mixed liquor.
The high-molecular anti-bacteria material and the ratio of ionized water dissolution are 3:7.
The essential oil wick is prepared from the following raw materials in parts by weight: food-grade food-grade P-Cymene 15-20%, pine needle Essential oil 3-5%, Geranium Essential 3-5%, cedar wood oil 3-5%, bergamot essential oil 1-3%, orange oil 2-4% remaining to leave away Water.
The essential oil wick is prepared from the following raw materials in parts by weight: food-grade food-grade P-Cymene 15%, pine needle essence Oil 3%, Geranium Essential 3%, cedar wood oil 3%, bergamot essential oil 1%, orange oil 2% remaining to leave away water.
The essential oil wick is prepared from the following raw materials in parts by weight: food-grade food-grade P-Cymene 20%, pine needle essence Oil 5%, Geranium Essential 5%, cedar wood oil 5%, bergamot essential oil 3%, orange oil 4% remaining to leave away water.
A kind of preparation method of wormwood essential oil microcapsules, 2 microcapsules of wormwood essential oil include following preparation step:
Step 1: food-grade food-grade P-Cymene, Essential Oil From Pine Needles, Geranium Essential, cypress will the preparation of essential oil wick: be eaten Oil, bergamot essential oil, orange oil are added in mixing apparatus with water of leaving away and are mixed, and are cooled down, are obtained after the completion of mixing Essential oil solution;
Step 2: it the preparation of 1 solution of capsule skin: high-molecular anti-bacteria material be added in mixing apparatus with ionized water carries out Mixing, obtains 1 solution of capsule skin;
Step 3: 1 solution of capsule skin being added in mixing apparatus with essential oil solution and is mixed, then will be mixed molten Liquid is poured into different molds and is cooled and shaped, because the high molecular material in different 1 solution of reason capsule skin of density can be automatic Form one layer of capsule skin 1 in essential oil solution surface, so that essential oil solution be wrapped up, form the shape that capsule skin 1 is wrapped in essential oil wick State completes the preparation of 2 microcapsules of wormwood essential oil.
In the step 1: mixing apparatus is constant temperature stirring container, and mixing temperature is 20-25 DEG C, incorporation time 360- 420min, cooling reaction time are 2-4H
In institute's step 2: mixing apparatus is constant temperature stirring container, incorporation time 120-180min.
In the step 3, mixing temperature is 30-40 DEG C, incorporation time 300-360min.
Wormwood essential oil passes through the molecular gap slow release of capsule skin, and capsule skin is high molecular material, essential oil microcapsules surface tool It is active, it can be welded together with textile by washing to impregnate to be bonded, bonding force is big, has good water-wash resistance.Capsule skin It does not react with water and air, wormwood essential oil and extraneous contact has effectively been isolated, can according to need wormwood essential oil Slowly release, makes the clothing of wormwood essential oil, repeatedly still has long acting antibiotic, sterilization after washing, eliminates the unusual smell antipruritic, active etc. Effect, wormwood incense have a promoting flow of qi by warming channel, and it is socks that antibacterial anti-inflammatory, which eliminates the unusual smell and other effects, towel, the common textile such as underpants it is excellent Choosing combination.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims Variation is included within the present invention.Any reference signs in the claims should not be construed as limiting the involved claims.

Claims (10)

1. a kind of wormwood essential oil microcapsules characterized by comprising capsule skin, the intradermal portion of capsule are filled with essential oil wick.
2. a kind of wormwood essential oil microcapsules according to claim 1, which is characterized in that the capsule skin is high-molecular anti-bacteria material Material is prepared with ionized water dissolution mixed liquor.
3. a kind of wormwood essential oil microcapsules according to claim 2, which is characterized in that the high-molecular anti-bacteria material with from The ratio of sub- water dissolution is 3:7.
4. a kind of wormwood essential oil microcapsules according to claim 1, which is characterized in that the essential oil wick is by following weight The raw material of proportion is made: food-grade food-grade P-Cymene 15-20%, Essential Oil From Pine Needles 3-5%, Geranium Essential 3-5%, cypress Oily 3-5%, bergamot essential oil 1-3%, orange oil 2-4% remaining to leave away water.
5. a kind of wormwood essential oil microcapsules according to claim 4, which is characterized in that the essential oil wick is by following weight The raw material of proportion is made: food-grade food-grade P-Cymene 15%, Essential Oil From Pine Needles 3%, Geranium Essential 3%, cedar wood oil 3%, Bergamot essential oil 1%, orange oil 2% remaining to leave away water.
6. a kind of wormwood essential oil microcapsules according to claim 4, which is characterized in that the essential oil wick is by following weight The raw material of proportion is made: food-grade food-grade P-Cymene 20%, Essential Oil From Pine Needles 5%, Geranium Essential 5%, cedar wood oil 5%, Bergamot essential oil 3%, orange oil 4% remaining to leave away water.
7. a kind of preparation method of wormwood essential oil microcapsules, using a kind of described in any item wormwood essential oils of claims 1-6 Microcapsules, the wormwood essential oil microcapsules include following preparation step:
Step 1: essential oil wick preparation: will eat food-grade food-grade P-Cymene, Essential Oil From Pine Needles, Geranium Essential, cedar wood oil, Bergamot essential oil, orange oil are added in mixing apparatus with water of leaving away and are mixed, and are cooled down after the completion of mixing, obtain essential oil Solution;
Step 2: the preparation of capsule skin solution: high-molecular anti-bacteria material be added in mixing apparatus mixing with ionized water, Obtain capsule skin solution;
Step 3: capsule skin solution being added in mixing apparatus with essential oil solution and is mixed, and then falls mixed solution Enter and be cooled and shaped in different molds, because the high molecular material in the different reason capsule skin solution of density can be automatically in essence Oil solution surface forms one layer of capsule skin, so that essential oil solution be wrapped up, forms the state that capsule skin is wrapped in essential oil wick, completes Chinese mugwort The preparation of careless essential oil microcapsules.
8. a kind of preparation method of wormwood essential oil microcapsules according to claim 7, which is characterized in that the step 1 In: mixing apparatus is constant temperature stirring container, and mixing temperature is 20-25 DEG C, incorporation time 360-420min, the cooling reaction time For 2-4H.
9. a kind of preparation method of wormwood essential oil microcapsules according to claim 7, which is characterized in that in institute's step 2: Mixing apparatus is constant temperature stirring container, incorporation time 120-180min.
10. a kind of preparation method of wormwood essential oil microcapsules according to claim 7, which is characterized in that the step 3 In, mixing temperature is 30-40 DEG C, incorporation time 300-360min.
CN201910545597.0A 2019-06-22 2019-06-22 A kind of wormwood essential oil microcapsules and preparation method thereof Pending CN110314621A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112111973A (en) * 2020-09-17 2020-12-22 深圳桃行科技股份有限公司 Preparation method of warm-keeping cloth with antibacterial and mite-inhibiting functions and cloth
CN112921666A (en) * 2021-01-26 2021-06-08 广西每好实业股份有限公司 Agilawood emulsion with antiviral and bactericidal effects as well as preparation method and application thereof
CN114164655A (en) * 2021-12-24 2022-03-11 绍兴罡龙针纺服饰有限公司 Antibacterial finishing process of rayon fabric

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112111973A (en) * 2020-09-17 2020-12-22 深圳桃行科技股份有限公司 Preparation method of warm-keeping cloth with antibacterial and mite-inhibiting functions and cloth
CN112921666A (en) * 2021-01-26 2021-06-08 广西每好实业股份有限公司 Agilawood emulsion with antiviral and bactericidal effects as well as preparation method and application thereof
CN114164655A (en) * 2021-12-24 2022-03-11 绍兴罡龙针纺服饰有限公司 Antibacterial finishing process of rayon fabric
CN114164655B (en) * 2021-12-24 2023-09-19 绍兴罡龙针纺服饰有限公司 Antibacterial finishing process of human cotton fabric

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Application publication date: 20191011

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