CN112826765B - Ganoderma spore hair care essential oil for promoting hair growth and preparation method thereof - Google Patents
Ganoderma spore hair care essential oil for promoting hair growth and preparation method thereof Download PDFInfo
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- CN112826765B CN112826765B CN202110069662.4A CN202110069662A CN112826765B CN 112826765 B CN112826765 B CN 112826765B CN 202110069662 A CN202110069662 A CN 202110069662A CN 112826765 B CN112826765 B CN 112826765B
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- oil
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- ganoderma lucidum
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
Abstract
The application provides a ganoderma lucidum spore hair care essential oil capable of promoting hair growth and a preparation method thereof, the hair care essential oil is composed of ganoderma lucidum spore oil and rosemary essential oil, and the mass ratio of the ganoderma lucidum spore oil to the rosemary essential oil is 10: 1; the hair care essential oil adopts pure natural raw materials, is safe without any harmful substances to bodies, skins and the like in the preparation process, has no toxic or side effect, and can promote hair growth and repair hair follicles.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to ganoderma lucidum spore hair care essential oil for promoting hair growth and a preparation method thereof.
Background
With the continuous progress of society, various pressures such as work, study, life and the like are continuously increased, the environment is continuously worsened, and the eating habits of bad diet and the use of hair washing and protecting products with over-strong alkalinity and poor quality cause damage to hair and cause hair loss when the hair washing and protecting products are improperly used for hair waving, hair dyeing, hair washing, hair combing, hair blowing and the like. Resulting in severe hair follicle damage. According to the digital display of the scalp health research center of the Chinese health education association, more than 80% of the human scalp has sub-health problems of different degrees. With the gradual rise of health consciousness of people, people advocate that 'hairs are like human faces and need regular care and professional care'. At present, common washing and caring products on the market only can achieve the effect of cleaning hair and scalp, so that the hair is smooth and easy to comb. The effects of repairing hair follicles and preventing alopecia are not comprehensive.
In order to solve the problem of hair loss, the hair follicle regeneration of the scalp is promoted. The development of ganoderma lucidum spore hair-care essential oil capable of promoting hair growth has become a technical problem to be solved urgently in the field.
Disclosure of Invention
Aiming at the existing actual requirements, the invention provides the ganoderma lucidum spore essential oil capable of promoting hair growth and the preparation method thereof, so as to achieve the purpose of promoting hair growth.
Specifically, the method is realized by the following technical scheme:
firstly, the application provides the ganoderma lucidum spore hair care essential oil capable of promoting hair growth, wherein the hair care essential oil comprises ganoderma lucidum spore oil and rosemary essential oil; wherein the Ganoderma spore oil is preferably Ganoderma spore oil obtained from Ganoderma lucidum (one of Ganoderma lucidum); the mass ratio of the ganoderma lucidum spore oil to the rosemary essential oil is preferably 10: 1.
secondly, the application also provides a preparation method of the ganoderma lucidum spore hair-care essential oil for promoting hair growth, which comprises the following specific steps:
1) breaking the wall of Ganoderma spore powder to obtain wall-broken Ganoderma spore powder; in the obtained wall-broken ganoderma lucidum spore powder, the wall-broken rate of the ganoderma lucidum spore powder is at least 95%;
2) breaking the wall of Ganoderma spore powder by CO 2 Extracting Ganoderma spore oil by supercritical extraction; the extraction temperature is 38-42 ℃, the extraction pressure is 30-35Mpa, and the extraction time is 3-4 hours;
3) cleaning rosemary, removing impurities, cutting into segments of about 1cm, adding purified water, soaking for at least 2 hours, heating by using a heating sleeve at the temperature of 200 ℃, keeping the liquid in a boiling state, and refluxing water vapor by using a condensing tube to obtain crude extract oil; collecting the crude extract oil, and concentrating by using a rotary evaporator to obtain rosemary essential oil for later use; the rosemary is preferably selected from branches, leaves and flowers so as to obtain high-quality and pure essential oil; the rotary evaporator has temperature of 60 deg.C and pressure of 0.09Mpa
4) Mixing the ganoderma lucidum spore oil and the rosemary essential oil in proportion to obtain the ganoderma lucidum spore hair care essential oil capable of promoting hair growth.
Further, in the preparation method of the ganoderma lucidum spore hair-care essential oil for promoting hair growth, the CO in the step 2) is 2 The supercritical extraction process comprises the following steps: the extraction temperature is 38-42 ℃, the extraction pressure is 30-35Mpa, and the extraction time is 3-4 hours; the method comprises the following specific steps: a) adding Ganoderma spore powder into mixture of water, gelatin and starch or one of edible additives, bonding Ganoderma spore powder, mixing, extruding at room temperature, and naturally drying; b) drying, molding, placing into an extractor, introducing CO from the bottom of the extractor 2 Controlling the temperature to be 35-65 ℃ and the pressure20-35 MPa, and the extraction time is 1-35 hours; c) discharging CO containing Ganoderma spore oil from the upper part of the extractor 2 Introducing into a pressure-reducing separator, discharging Ganoderma spore oil from the bottom of the pressure-reducing separator, and introducing CO 2 Gas flows out of the top of the decompression separator; d) separating water and jelly from Ganoderma spore oil to obtain purified Ganoderma spore oil, and recovering defatted Ganoderma spore powder from the extractor. The yield of the ganoderma lucidum spore oil is 10 to 20 percent. In specific implementations, the supercritical CO 2 The method for extracting Ganoderma spore oil can also be referred to Ganoderma spore oil prepared by the method disclosed in Chinese patent with patent number ZL99123952.0 (invention name: a supercritical processing method of Ganoderma spore).
Compared with the prior art, the invention has the beneficial effects that: the invention adopts pure natural raw materials, and no harmful substances to human bodies, skins and the like are added in the preparation process. The product does not produce harmful substances during use. Is a hair care essential oil with high efficiency, safety and no toxic or side effect. And can promote hair growth and repair hair follicle. The scalp is brought into a healthy state to prevent hair loss.
Detailed Description
The invention is further illustrated by the following specific examples.
Examples raw materials, equipment sources:
the Ganoderma spore powder is Ganoderma spore powder from Ganodermatae of Huangshan mountain of Anhui province;
the wall breaking machine is purchased from Nanjing Nada ultra-micro technology limited company, and has a model of JRG-30, the cooling form is closed water cooling, the wall breaking rate is not less than 98%, and the wall breaking rate of spore powder reaches 92% -95%.
EXAMPLE 1 preparation of Ganoderma spore Hair caring essential oil
The preparation method comprises the following steps:
1) taking 100g ganoderma lucidum spore powder, and performing wall breaking treatment to obtain wall-broken spore powder;
2) by CO 2 The supercritical extraction comprises the following specific steps:
A) adding Ganoderma spore powder into mixture of water, gelatin and starch to make Ganoderma spore powder adhere and form, mixing, extruding at room temperature, and naturally drying;
B) loading dried and molded Ganoderma spore powder into an extractor, introducing CO from the bottom of the extractor 2 Controlling the temperature to be 40 ℃, the extraction pressure to be 32MPa and the extraction time to be 4 hours;
C) discharging CO containing Ganoderma spore oil from the upper part of the extractor 2 Introducing into a pressure-reducing separator, discharging Ganoderma spore oil from the bottom of the pressure-reducing separator, and introducing CO 2 Gas flows out of the top of the decompression separator;
D) d) separating and removing water and jelly in the ganoderma lucidum spore oil to obtain purified ganoderma lucidum spore oil, and recovering defatted ganoderma lucidum spore powder from an extractor, wherein the yield of the ganoderma lucidum spore oil is 15%.
3) Taking 100g of fresh rosemary, removing impurities by cleaning, cutting into sections of about 1cm, putting into a round-bottom flask, and adding purified water to soak for 2 hours; connecting a condensing pipe in the heating sleeve, heating the purified water soaked with rosemary to boil, keeping the temperature of the heating sleeve at 200 ℃, and extracting for 4 h; collecting the reflux crude essential oil, purifying with rotary evaporator at 60 deg.C under 0.09Mpa, and evaporating excessive water to obtain rosemary essential oil; the yield of rosemary essential oil was 1.2%.
4) Mixing the extracted ganoderma lucidum spore oil and rosemary essential oil 10:1, mixing to obtain the ganoderma lucidum spore hair-care essential oil.
Comparative example 1: example 1 Ganoderma lucidum spore oil obtained in step 2);
comparative example 2: example 1 rosemary essential oil obtained in step 3);
comparative example 3: example 1 mixing the ganoderma lucidum spore oil obtained in the step 2) and the rosemary essential oil obtained in the step 3) in a mass ratio;
comparative example 4: example 1 ganoderma lucidum spore oil obtained in step 2) and rosemary essential oil obtained in step 3) in a mass ratio of 8:2 and mixing.
Animal experiments
25 female mice of 12 weeks of age were selected. After the mice are raised in cages for 10 days, hairs at the corresponding positions on the backs of the mice are removed by using experimental animal depilatory, and the removal area is 2cm multiplied by 2 cm. The dehaired mice skin was pink in color and at rest of the hair.
18 mice with no damage in the unhairing area are selected and randomly divided into 3 model groups, 3 experiment A groups, 3 experiment B groups, 3 experiment C groups, 3 experiment D groups and 3 experiment E groups. The experimental steps are as follows: the hair removal area of the model group was not smeared with hair care essential oil. Experiment a group was evenly coated with ganoderma lucidum spore oil from one of control example 1. Experiment B group was applied with individual rosemary essential oil in control example 2. Experiment C group was applied with the ganoderma lucidum spore hair-care essential oil of example 1 at a ratio of 10:1, and experiment D group was applied with the ganoderma lucidum spore hair-care essential oil of example 5:5 (comparative example 3). Experiment E group was coated with Ganoderma spore hair care essential oil at a ratio of 8:2 (comparative example 4). The application is continued for 28 days.
The influence of single-ingredient essential oil and ganoderma lucidum spore hair care essential oil on hair growth: the mice all developed hair on day 10 after depilation. Experiment A, B the two groups clearly lags the hair growth rate of experiment c. At 28 days of the experiment, the skin on the back of the mouse and paraffin sections are cut and stained to observe the number of hair follicles. The number of hair follicles in the field of view of the experimental group was significantly greater than that of the model group. The number of hair follicles in each group of mice is shown in Table 1.
TABLE 1 number of hair follicles in mice of each group
Conclusion 1:
compared with the experiment A group, the experiment B group and the experiment C group, the P of the model group is less than 0.01, so the model group and the experiment group have significant difference.
The study found that the hair was grown first in group C, and the hair growth rate in A, B group lags behind that in group C, indicating that the ratio of ganoderma spore oil to rosemary essential oil is 10:1 has hair growth promoting effect.
Conclusion 2:
compared with the experiment C group, the experiment D group and the experiment E group, the P of the model group is less than 0.01, so the model group and the experiment group have significant difference.
Research shows that the hair follicle quantity of the experiment group D and the experiment group E is lower than that of the experiment group C, so that the ratio of the obtained ganoderma lucidum spore oil to the rosemary essential oil is 10: the hair growth promoting effect is most remarkable when 1 is used. The observation of the number of the hair follicles of the mice is an important basis for judging the hair growth condition of the mice.
The above examples show that the effect is most remarkable when the ratio of the ganoderma lucidum spore oil to the rosemary essential oil is 10:1, the growth of hair and hair follicles can be promoted, and in contrast, the fragrance emitted by the ganoderma lucidum spore oil and the rosemary essential oil is fresher and elegant and is suitable for different people.
Claims (7)
1. A Ganoderma spore essential oil for hair care with hair growth promoting effect is characterized by comprising Ganoderma spore oil and rosemary essence oil;
wherein the mass ratio of the ganoderma lucidum spore oil to the rosemary essential oil is 10:1, 1:1 or 4: 1.
2. The essential oil for hair care containing ganoderma lucidum spores for promoting hair growth as claimed in claim 1, wherein the ganoderma lucidum spores oil is ganoderma lucidum spores oil.
3. The method for preparing the ganoderma lucidum spore hair care essential oil capable of promoting hair growth according to claim 1 or 2, which is characterized by comprising the following steps:
1) breaking the wall of Ganoderma spore powder to obtain wall-broken Ganoderma spore powder;
2) breaking the wall of Ganoderma spore powder by CO 2 Extracting Ganoderma spore oil by supercritical extraction;
3) soaking herba Rosmarini officinalis in water for at least 2 hr, heating with heating jacket, and refluxing water vapor with condenser tube to obtain crude essential oil; collecting the crude extract oil, and concentrating by using a rotary evaporator to obtain rosemary essential oil for later use;
4) mixing the ganoderma lucidum spore oil and the rosemary essential oil in proportion to obtain the ganoderma lucidum spore hair care essential oil capable of promoting hair growth.
4. The method of claim 3, wherein the CO of step 2) is 2 Supercritical extraction processThe method comprises the following steps: the extraction temperature is 38-42 deg.C, the extraction pressure is 30-35Mpa, and the extraction time is 3-4 hr.
5. The method according to claim 3, wherein the rosemary of step 3) comprises rosemary branches and leaves and rosemary flowers.
6. The method of claim 3, wherein the heating with the heating jacket in step 3) is performed at a temperature of 200 ℃ and kept in a boiling state.
7. The method according to claim 3, wherein the rotary evaporator of step 3) has a temperature of 60 ℃ and a pressure of 0.09 MPa.
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105853286A (en) * | 2016-04-29 | 2016-08-17 | 山东复大生物科技有限公司 | Skin care product containing ganoderma lucidum spore oil and preparation method for ganoderma lucidum spores oil of skin care product |
| CN111135122A (en) * | 2020-03-09 | 2020-05-12 | 上海禾向健康科技发展有限公司 | Composition containing ganoderma lucidum extract and application thereof in moisturizing and anti-wrinkle cosmetics |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105853286A (en) * | 2016-04-29 | 2016-08-17 | 山东复大生物科技有限公司 | Skin care product containing ganoderma lucidum spore oil and preparation method for ganoderma lucidum spores oil of skin care product |
| CN111135122A (en) * | 2020-03-09 | 2020-05-12 | 上海禾向健康科技发展有限公司 | Composition containing ganoderma lucidum extract and application thereof in moisturizing and anti-wrinkle cosmetics |
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