CN105640803A - Anti-dandruff, anti-hair-loss and hair-care product and preparation method thereof - Google Patents
Anti-dandruff, anti-hair-loss and hair-care product and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
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- A61K2800/592—Mixtures of compounds complementing their respective functions
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Abstract
The invention relates to an anti-dandruff, anti-hair-loss and hair-care product and a preparation method thereof. A formula of the product comprises raw materials in parts by weight as follows: 1-5 parts of lavender essential oil, 1-3 parts of rosemary essential oil, 1-6 parts of fir essential oil and 86-92 parts of argan oil or jojoba oil. The preparation method of the product comprises steps as follows: (1) the lavender essential oil, the rosemary essential oil and the fir essential oil are evenly stirred after being mixed in parts by weight, and an essential oil mixture is obtained; (2) the essential oil mixture obtained in Step (1) is evenly mixed with the argan oil or jojoba oil in parts by weight, and thus the product is obtained. Multiple kinds of plant essential oil are matched scientifically and cooperate with one another to play roles of plant essential oil, and the product can quickly permeate to be absorbed by skin to realize anti-dandruff, anti-hair-loss and hair-care effects, can be applied to hair and scalps with various characteristics, is free of allergic reactions and toxic and side effects after usage, takes effect quickly and is good in anti-dandruff and hair-growth effect.
Description
Technical field
The invention belongs to hair-protecting health-care product, be specifically related to a kind of anti-dandruff, Anti-hair loss, hair products and preparation method thereof.
Background technology
Along with expanding economy, the quickening of modern life rhythm and the sharp increase of life stress, the sickness rate of the hair disease such as the dandruff is various, alopecia, withered and yellowish hairs is also more and more higher, brings very big puzzlement to the life of modern. The dandruff or alopecia not only affect attractive in appearance, and the psychology of patient also can be made to produce bad clear threads such as feeling oneself inferior, depressed, so that normal work, life and doings are affected by impact. Alopecia can be divided into seborrheic alopecia, sending alopecia early, alopecia areata, alopecia totalis, alopecia universalis and puerperal alopecia etc. by its symptom, and there is presently no specific medicament can hair growth.
The traditional Chinese medical science thinks that alopecia great majority cause due to physical function imbalance, and its pathogenesis is due to spirit and nutrition two reasons. Sad gloomy meeting causes that Liver and kidney heart spleen is all hindered, and makes hair lose nutrition and come off; Or due to blood addiction blood deficiency reality scalp Rhizoma Imperatae blood supply insufficiency, make atrichia nutrition, thus alopecia, therefore answer nourishing liver and kidney, invigorating blood circulation paralysis, rich in nutrition, expelling wind and removing dampness, the tired tissue regeneration promoting of change and hair growth accelerating, this type of disease can be cured. Through clinical observation, it has been found that these Chinese medicinal plant quintessence oil cosmetics are respectively provided with good effect for seborrheic alopecia, sending alopecia early, alopecia areata, alopecia totalis, alopecia universalis and puerperal alopecia etc., alleviate symptom, do not find untoward reaction simultaneously. The medicine have a headache for keeping tensions down on the market at present, calm the nerves, minded at rest and compound essential Oil shortcoming: the side effect of medicine is big, the actual effect of compound essential Oil is not reaching to due effect, and uses more complicated.
Summary of the invention
In order to solve the problems referred to above that prior art exists, the invention provides a kind of anti-dandruff, Anti-hair loss, hair products and preparation method thereof that can reduce the dandruff and alopecia can be suppressed.
The technical solution adopted in the present invention is:
A kind of anti-dandruff, Anti-hair loss, hair products, its formula includes the raw material of following weight portion:
Herba Lysimachiae foenum-graeci quintessence oil 1-5 part;Rosemary ethereal oil 1-3 part; Fir essential oil 1-6 part; Ah's glycerol and/or Jojoba oil 86-97 part.
Preferably: anti-dandruff, Anti-hair loss, hair products described above, its formula includes the raw material of following weight portion:
Herba Lysimachiae foenum-graeci quintessence oil 3 parts; Rosemary ethereal oil 2 parts; Fir essential oil 3 parts; Ah's glycerol or Jojoba oil 92 parts.
Preferably: the preparation method of above-mentioned Herba Lysimachiae foenum-graeci quintessence oil or fir essential oil, comprise the following steps:
(1) by the air-dry fresh inflorescence of lavandula angustifolia or fresh fir leaf, join immersion 2-3h in soak, obtain pretreated feedstock;
(2) described pretreated feedstock is placed in distilling apparatus and carries out air-distillation at 100-105 DEG C, after condensation, obtain condensed fluid;
(3) by described condensed fluid by equipped with the adsorption column of alcoholic solution and activated carbon carries out extracted many times, obtaining lixiviating solution;
(4) described lixiviating solution is carried out decompression distillation, obtains Herba Lysimachiae foenum-graeci quintessence oil or fir essential oil.
Further: when preparing Herba Lysimachiae foenum-graeci quintessence oil, the soak described in step (1) is mass concentration is the sodium chloride solution of 20%-25%; When preparing fir essential oil, the soak described in step (1) is water.
Further: the pressure of described decompression distillation is 0.1-1.0kP.
Preferably: the preparation method of above-mentioned rosemary ethereal oil, comprise the following steps:
(1) by leaf of Herba Rosmarini Officinalis material immersion polar organic solvent extracts 0.08-6h at 20-100 DEG C of temperature, obtain extracting solution, extracting solution is boiled off at 20-100 DEG C described polar organic solvent, obtains the mixture of rosemary ethereal oil and rosemary antioxidant;
(2) described mixture is immersed in nonpolar or weakly polar organic solvent, at 20-100 DEG C of temperature, 0.5-6h is extracted in circulation, is cooled to 5-30 DEG C, filters, gained filtrate is boiled off at 20-100 DEG C described nonpolar or weakly polar organic solvent, obtains rosemary ethereal oil.
Further: described leaf of Herba Rosmarini Officinalis material, described polar organic solvent and described nonpolar or weakly polar organic solvent weight be: 1:3-20:3-20.
The method preparing above-mentioned anti-dandruff, Anti-hair loss, hair products, including being made by step:
(1) stir after the Herba Lysimachiae foenum-graeci quintessence oil of above-mentioned weight portion, rosemary ethereal oil and fir essential oil being mixed, obtain blend of essential oils;
(2) blend of essential oils of gained in step (1) and Ah's glycerol of above-mentioned weight portion or Jojoba oil are sufficiently mixed uniformly, anti-dandruff, Anti-hair loss, hair products.
Herba Lysimachiae foenum-graeci quintessence oil energy balance skin fat secretion, for oiliness skin and oiliness hair quality, is provided that improvement all the better, the protection of the scalp of the hair dandruff that oil causes excessively and hair quality.
Rosemary ethereal oil has very strong contraction, tightens lax skin, also can alleviate the situation of hyperemia, swelling; Anti-dandruff is particularly helpful, improves the dandruff stimulating hair growth, stimulate cell division regeneration, skin renewal is had very big benefit, alopecia can be improved, the symptoms such as hair is sparse.
Fir, formal name used at school: Abiesfabri (Mast.) Craib, fir essential oil extracts from fir leaf, has moisturizing, moisturizing, anti-inflammation, pore refining, eliminating toxin and beautifying the skin, smoothing wrinkle dispel stricture of vagina, it is active to loosen, improve insomnia, promote metabolism, anti crease and anti senile prepared old effect.
Ah's glycerol is also known as macadamia nut oil, and it is squeezed by the nut being grown on Moroccan Ah Gan Shu and forms, and Ah's glycerol contains abundant fatty acid, sterol, vitamin e and phenolic compound.Including substantial amounts of essential fatty acid, unsaturated fatty acid and linoleic acid, these are all can not synthesize and must get from fat by body in people. Ah's glycerol has scientifically been confirmed that it contains its life E of the dimension of 2 times of olive oil, and the symptom that vitamin e lacks includes hair and dries up, and alopecia, wound healing is slow. Ah's glycerol is rich in unsaturated fatty acids such as omega3 and omega9, so it can easily by dry absorption with repair your impaired hair and hair follicle; Increase hair gloss; Non-greasy, can stop curly headed and distribute arbituarily; Do not stimulate, softening hair can be helped; Can be absorbed by hair at once, recover the moisture of hair; Help to suppress hair bifurcated and alopecia; Because the high-load of the vitamin e of Ah's glycerol, it also has the effect of highly significant in natural on-off cycles of hair growth.
Jojoba oil, has another name called jojoba (Jojoba) oil, and rich in mineral substances, vitamin, protein, collagen protein, plant are cured, MytidyicAcid, moisten very much, without any taste and the oil more sliding oils and fats secreted like adipose gland. It has a high stability, resistant to high light, high temperature and keep structure constant, be the oil that can hide for a long time. It has good permeability, as long as there being space, can permeate; Also there is resistant to elevated temperatures speciality, and molecules align be very similar with the oils and fats of people, be that stability is high, the special good base oil of ductility, be suitable for oiliness sensitive skin, rheumatism, arthritis, gout people use, be good hair conditioner simultaneously. Coarse hair quality can be improved, be the optimum selection of Hair grooming oil, injure outside soft hair preventing hair to shine, hair can be helped pitch-black and prevention bifurcated.
The invention have the benefit that the present invention utilizes various plants quintessence oil to carry out scientific matching, collaborative effect playing plants essential oil, the concrete mechanism of action is as follows: 1, Herba Lysimachiae foenum-graeci quintessence oil multiple pure plants essential oil active factors of can arranging in pairs or groups complements each other, rapid osmotic hair follicle disinfecting, antimicrobial, promote cell regeneration, recover skin connective tissue, simultaneously balance skin top layer fat secretion, sensitive skin of releiving, recover skin oneself's maintenance function, strengthen skin resistance to external world, 2, pure Herba Lysimachiae foenum-graeci quintessence oil is as Joker oil, can with any Fragrance-Composite Essential Oils, after two kinds even quintessence oil of more than three or four kinds are allocated, its effect can growth at double, but the ratio that quintessence oil is allocated mutually is extremely important, require much skill parameter inside, Herba Lysimachiae foenum-graeci quintessence oil is formed compound essential Oil with rosemary ethereal oil and fir essential oil with the perfect golden ratio allotment of science by the present invention, abandon the drawback of folk prescription quintessence oil, multi-efficiency cooperates, it is greatly improved the effect of deep layer maintenance, the effect of the anti-bifurcated of anti-dandruff Anti-hair loss is reached by protecting hair root nutrients scalp, 3, the present invention is by joining in Ah's glycerol of excellent of defending the doctrine or the base oil of Jojoba oil after three kinds of quintessence oil scientific allocations, can rapidly permeate into and make skin absorption, reach effect anti-dandruff, hair care, Anti-hair loss, go for hair and the scalp of various feature, without anaphylaxis after using, have no side effect, and instant effect, anti-dandruff, hair-growing effects good.
Detailed description of the invention
6 specific embodiments are given below; explanation that the present invention will be further explained; it is noted that the present invention is not limited to following preferred forms; any those skilled in the art can draw other various forms of products under the enlightenment of the present invention; no matter but in its shape or structure, do any change; every have same or like with the application like technical scheme, all fall within protection scope of the present invention.
In the following embodiments, 1 weight portion acute pyogenic infection of finger tip 1g.
Embodiment 1
A kind of anti-dandruff, Anti-hair loss, hair products, including the raw material of following weight portion:
Herba Lysimachiae foenum-graeci quintessence oil 1 part; Rosemary ethereal oil 1 part; Fir essential oil 1 part; Ah's glycerol 86 parts.
The wherein preparation method of Herba Lysimachiae foenum-graeci quintessence oil, comprises the following steps:
(1) by the air-dry fresh inflorescence of lavandula angustifolia, joining concentration is immersion 2h in 20% sodium chloride solution, obtains pretreated feedstock;
(2) described pretreated feedstock is placed in distilling apparatus and carries out air-distillation at 100 DEG C, obtain condensed fluid;
(3) by described condensed fluid by carrying out extracted many times equipped with in the adsorption column of the alcoholic solution that mass concentration is 8% and activated carbon, lixiviating solution is obtained;
(4) by described lixiviating solution pressure be carry out under 0.1kP decompression distillation, obtain Herba Lysimachiae foenum-graeci quintessence oil.
The preparation method of rosemary ethereal oil, comprises the following steps:
(1) the leaf of Herba Rosmarini Officinalis material of 1 weight portion is immersed at 20 DEG C extraction 0.08h in the alcoholic solution that mass concentration is 8% of 3 weight portions, obtain extracting solution, extracting solution is boiled off solvent at 20 DEG C, obtains the mixture of rosemary ethereal oil and rosemary antioxidant;
(2) described mixture is immersed in the non-polar organic solvent of 3 weight portions, extracts 0.5h 20 DEG C of circulations, be cooled to 5 DEG C, filter, gained filtrate is boiled off solvent at 20 DEG C, obtains rosemary ethereal oil.
The preparation method of fir essential oil, comprises the following steps:
(1) by fresh fir leaf, be added to the water immersion 2h, obtains pretreated feedstock;
(2) described pretreated feedstock is placed in distilling apparatus and carries out air-distillation at 100 DEG C, obtain condensed fluid;
(3) by described condensed fluid by carrying out extracted many times equipped with in the adsorption column of the alcoholic solution that mass concentration is 8% and activated carbon, lixiviating solution is obtained;
(4) by described lixiviating solution pressure be carry out under 0.1kP decompression distillation, obtain fir essential oil.
The method preparing above-mentioned anti-dandruff, Anti-hair loss, hair products, including being made by step:
(1) stir after the Herba Lysimachiae foenum-graeci quintessence oil of gained, rosemary ethereal oil and fir essential oil being mixed by above-mentioned weight, obtain blend of essential oils;
(2) blend of essential oils of gained in step (1) is poured in the Ah sweet's oil vessel being added with above-mentioned weight portion, stirring, fully dilute fusion, anti-dandruff, Anti-hair loss, hair products.
Embodiment 2
A kind of anti-dandruff, Anti-hair loss, hair products, including the raw material of following weight portion:
Herba Lysimachiae foenum-graeci quintessence oil 2 parts; Rosemary ethereal oil 1.5 parts; Fir essential oil 2 parts; Ah's glycerol 92 parts.
The wherein preparation method of Herba Lysimachiae foenum-graeci quintessence oil, comprises the following steps:
(1) by the air-dry fresh inflorescence of lavandula angustifolia, joining concentration is immersion 2.5h in 22% sodium chloride solution, obtains pretreated feedstock;
(2) described pretreated feedstock is placed in distilling apparatus and carries out air-distillation at 102 DEG C, obtain condensed fluid;
(3) by described condensed fluid by carrying out extracted many times equipped with in the adsorption column of the alcoholic solution that mass concentration is 9% and activated carbon, lixiviating solution is obtained;
(4) by described lixiviating solution pressure be carry out under 0.4kP decompression distillation, obtain Herba Lysimachiae foenum-graeci quintessence oil.
The preparation method of rosemary ethereal oil, comprises the following steps:
(1) the leaf of Herba Rosmarini Officinalis material of 1 weight portion is immersed at 40 DEG C extraction 1.2h in the alcoholic solution that mass concentration is 9% of 8 weight portions, obtain extracting solution, extracting solution is boiled off solvent at 40 DEG C, obtains the mixture of rosemary ethereal oil and rosemary antioxidant;
(2) described mixture is immersed in the weakly polar organic solvent of 8 weight portions, extracts 1h 40 DEG C of circulations, be cooled to 8 DEG C, filter, gained filtrate is boiled off solvent at 40 DEG C, obtains rosemary ethereal oil.
The preparation method of fir essential oil, comprises the following steps:
(1) by fresh fir leaf, be added to the water immersion 2.5h, obtains pretreated feedstock;
(2) described pretreated feedstock is placed in distilling apparatus and carries out air-distillation at 102 DEG C, obtain condensed fluid;
(3) by described condensed fluid by carrying out extracted many times equipped with in the adsorption column of the alcoholic solution that mass concentration is 9% and activated carbon, lixiviating solution is obtained;
(4) by described lixiviating solution pressure be carry out under 0.4kP decompression distillation, obtain fir essential oil.
The method preparing above-mentioned anti-dandruff, Anti-hair loss, hair products, including being made by step:
(1) stir after the Herba Lysimachiae foenum-graeci quintessence oil of gained, rosemary ethereal oil and fir essential oil being mixed by above-mentioned weight, obtain blend of essential oils;
(2) blend of essential oils of gained in step (1) is poured in the container of the Ah's glycerol being added with above-mentioned weight portion, stirring, fully dilute fusion, anti-dandruff, Anti-hair loss, hair products.
Embodiment 3
A kind of anti-dandruff, Anti-hair loss, hair products, including the raw material of following weight portion:
Herba Lysimachiae foenum-graeci quintessence oil 5 parts; Rosemary ethereal oil 3 parts; Fir essential oil 6 parts; Ah's glycerol 92 parts.
The wherein preparation method of Herba Lysimachiae foenum-graeci quintessence oil, comprises the following steps:
(1) by the air-dry fresh inflorescence of lavandula angustifolia, joining concentration is immersion 3h in 25% sodium chloride solution, obtains pretreated feedstock;
(2) described pretreated feedstock is placed in distilling apparatus and carries out air-distillation at 105 DEG C, obtain condensed fluid;
(3) by described condensed fluid by carrying out extracted many times equipped with in the adsorption column of the alcoholic solution that mass concentration is 10% and activated carbon, lixiviating solution is obtained;
(4) by described lixiviating solution pressure be carry out under 1.0kP decompression distillation, obtain Herba Lysimachiae foenum-graeci quintessence oil.
The preparation method of rosemary ethereal oil, comprises the following steps:
(1) the leaf of Herba Rosmarini Officinalis material of 1 weight portion is immersed at 100 DEG C extraction 6h in the alcoholic solution that mass concentration is 10% of 20 weight portions, obtain extracting solution, extracting solution is boiled off solvent at 100 DEG C, obtains the mixture of rosemary ethereal oil and rosemary antioxidant;
(2) described mixture is immersed in the non-polar organic solvent of 20 weight portions, extracts 6h 100 DEG C of circulations, be cooled to 30 DEG C, filter, gained filtrate is boiled off solvent at 100 DEG C, obtains rosemary ethereal oil.
The preparation method of fir essential oil, comprises the following steps:
(1) by fresh fir leaf, joining concentration is immersion 3h in 25% sodium chloride solution, obtains pretreated feedstock;
(2) described pretreated feedstock is placed in distilling apparatus and carries out air-distillation at 105 DEG C, obtain condensed fluid;
(3) by described condensed fluid by carrying out extracted many times equipped with in the adsorption column of the alcoholic solution that mass concentration is 10% and activated carbon, lixiviating solution is obtained;
(4) by described lixiviating solution pressure be carry out under 1.0kP decompression distillation, obtain fir essential oil.
The method preparing above-mentioned anti-dandruff, Anti-hair loss, hair products, including being made by step:
(1) stir after the Herba Lysimachiae foenum-graeci quintessence oil of gained, rosemary ethereal oil and fir essential oil being mixed by above-mentioned weight, obtain blend of essential oils;
(2) blend of essential oils of gained in step (1) poured into be added with by the container of Ah's glycerol of above-mentioned weight, stirring, fully dilute fusion, anti-dandruff, Anti-hair loss, hair products.
Embodiment 4
A kind of anti-dandruff, Anti-hair loss, hair products, including the raw material of following weight portion:
Herba Lysimachiae foenum-graeci quintessence oil 1 part; Rosemary ethereal oil 1 part; Fir essential oil 1 part; Jojoba oil 86 parts.
The wherein preparation method of Herba Lysimachiae foenum-graeci quintessence oil, comprises the following steps:
(1) by the air-dry fresh inflorescence of lavandula angustifolia, joining concentration is immersion 2h in 23% sodium chloride solution, obtains pretreated feedstock;
(2) described pretreated feedstock is placed in distilling apparatus and carries out air-distillation at 100 DEG C, obtain condensed fluid;
(3) by described condensed fluid by carrying out extracted many times equipped with in the adsorption column of the alcoholic solution that mass concentration is 8% and activated carbon, lixiviating solution is obtained;
(4) by described lixiviating solution pressure be carry out under 0.6kP decompression distillation, obtain Herba Lysimachiae foenum-graeci quintessence oil.
The preparation method of rosemary ethereal oil, comprises the following steps:
(1) the leaf of Herba Rosmarini Officinalis material of 1 weight portion is immersed at 60 DEG C extraction 2h in the alcoholic solution that mass concentration is 8% of 12 weight portions, obtain extracting solution, extracting solution is boiled off solvent at 60 DEG C, obtains the mixture of rosemary ethereal oil and rosemary antioxidant;
(2) described mixture is immersed in the non-polar organic solvent of 12 weight portions, extracts 2h 60 DEG C of circulations, be cooled to 15 DEG C, filter, gained filtrate is boiled off solvent at 60 DEG C, obtains rosemary ethereal oil.
The preparation method of fir essential oil, comprises the following steps:
(1) by fresh fir leaf, joining concentration is immersion 2h in 23% sodium chloride solution, obtains pretreated feedstock;
(2) described pretreated feedstock is placed in distilling apparatus and carries out air-distillation at 100 DEG C, obtain condensed fluid;
(3) by described condensed fluid by carrying out extracted many times equipped with in the adsorption column of the alcoholic solution that mass concentration is 8% and activated carbon, lixiviating solution is obtained;
(4) by described lixiviating solution pressure be carry out under 0.6kP decompression distillation, i.e. fir essential oil.
The method preparing above-mentioned anti-dandruff, Anti-hair loss, hair products, including being made by step:
(1) stir after the Herba Lysimachiae foenum-graeci quintessence oil of gained, rosemary ethereal oil and fir essential oil being mixed by above-mentioned weight, obtain blend of essential oils;
(2) blend of essential oils of gained in step (1) is poured in the container being added with the Jojoba oil by above-mentioned weight, stirring, fully dilute fusion, anti-dandruff, Anti-hair loss, hair products.
Embodiment 5
A kind of anti-dandruff, Anti-hair loss, hair products, including the raw material of following weight portion:
Herba Lysimachiae foenum-graeci quintessence oil 2 parts; Rosemary ethereal oil 1.5 parts; Fir essential oil 2 parts; Jojoba oil 92 parts.
The wherein preparation method of Herba Lysimachiae foenum-graeci quintessence oil, comprises the following steps:
(1) by the air-dry fresh inflorescence of lavandula angustifolia, joining concentration is immersion 2.5h in 22% sodium chloride solution, obtains pretreated feedstock;
(2) described pretreated feedstock is placed in distilling apparatus and carries out air-distillation at 102 DEG C, obtain condensed fluid;
(3) by described condensed fluid by carrying out extracted many times equipped with in the adsorption column of the alcoholic solution that mass concentration is 9% and activated carbon, lixiviating solution is obtained;
(4) by described lixiviating solution pressure be carry out under 0.8kP decompression distillation, obtain Herba Lysimachiae foenum-graeci quintessence oil.
The preparation method of rosemary ethereal oil, comprises the following steps:
(1) the leaf of Herba Rosmarini Officinalis material of 1 weight portion is immersed at 80 DEG C extraction 3h in the alcoholic solution that mass concentration is 9% of 16 weight portions, obtain extracting solution, extracting solution is boiled off solvent at 80 DEG C, obtains the mixture of rosemary ethereal oil and rosemary antioxidant;
(2) described mixture is immersed in the weakly polar organic solvent of 16 weight portions, extracts 5h 80 DEG C of circulations, be cooled to 24 DEG C, filter, gained filtrate is boiled off solvent at 80 DEG C, obtains rosemary ethereal oil.
The preparation method of fir essential oil, comprises the following steps:
(1) by fresh fir leaf, joining concentration is immersion 2.5h in 22% sodium chloride solution, obtains pretreated feedstock;
(2) described pretreated feedstock is placed in distilling apparatus and carries out air-distillation at 102 DEG C, obtain condensed fluid;
(3) by described condensed fluid by carrying out extracted many times equipped with in the adsorption column of the alcoholic solution that mass concentration is 9% and activated carbon, lixiviating solution is obtained;
(4) by described lixiviating solution pressure be carry out under 0.8kP decompression distillation, obtain fir essential oil.
The method preparing above-mentioned anti-dandruff, Anti-hair loss, hair products, including being made by step:
(1) stir after the Herba Lysimachiae foenum-graeci quintessence oil of gained, rosemary ethereal oil and fir essential oil being mixed by above-mentioned weight, obtain blend of essential oils;
(2) blend of essential oils of gained in step (1) is poured in the container being added with the Jojoba oil by above-mentioned weight, stirring, fully dilute fusion, anti-dandruff, Anti-hair loss, hair products.
Embodiment 6
A kind of anti-dandruff, Anti-hair loss, hair products, including the raw material of following weight portion:
Herba Lysimachiae foenum-graeci quintessence oil 5 parts; Rosemary ethereal oil 3 parts; Fir essential oil 6 parts; Jojoba oil 92 parts.
The wherein preparation method of Herba Lysimachiae foenum-graeci quintessence oil, comprises the following steps:
(1) by the air-dry fresh inflorescence of lavandula angustifolia, joining concentration is immersion 3h in 25% sodium chloride solution, obtains pretreated feedstock;
(2) described pretreated feedstock is placed in distilling apparatus and carries out air-distillation at 105 DEG C, obtain condensed fluid;
(3) by described condensed fluid by carrying out extracted many times equipped with in the adsorption column of the alcoholic solution that mass concentration is 10% and activated carbon, lixiviating solution is obtained;
(4) by described lixiviating solution pressure be carry out under 1.0kP decompression distillation, obtain Herba Lysimachiae foenum-graeci quintessence oil.
The preparation method of rosemary ethereal oil, comprises the following steps:
(1) the leaf of Herba Rosmarini Officinalis material of 1 weight portion is immersed at 100 DEG C extraction 6h in the alcoholic solution that mass concentration is 10% of 20 weight portions, obtain extracting solution, extracting solution is boiled off solvent at 100 DEG C, obtains the mixture of rosemary ethereal oil and rosemary antioxidant;
(2) described mixture is immersed in the non-polar organic solvent of 20 weight portions, extracts 6h 100 DEG C of circulations, be cooled to 30 DEG C, filter, gained filtrate is boiled off solvent at 100 DEG C, obtains rosemary ethereal oil.
The preparation method of fir essential oil, comprises the following steps:
(1) by fresh fir leaf, joining concentration is immersion 3h in 25% sodium chloride solution, obtains pretreated feedstock;
(2) described pretreated feedstock is placed in distilling apparatus and carries out air-distillation at 105 DEG C, obtain condensed fluid;
(3) by described condensed fluid by carrying out extracted many times equipped with in the adsorption column of the alcoholic solution that mass concentration is 10% and activated carbon, lixiviating solution is obtained;
(4) by described lixiviating solution pressure be carry out under 1.0kP decompression distillation, obtain fir essential oil.
The method preparing above-mentioned anti-dandruff, Anti-hair loss, hair products, including being made by step:
(1) stir after the Herba Lysimachiae foenum-graeci quintessence oil of gained, rosemary ethereal oil and fir essential oil being mixed by above-mentioned weight, obtain blend of essential oils;
(2) blend of essential oils of gained in step (1) is poured in the container being added with the Jojoba oil by above-mentioned weight, stirring, fully dilute fusion, anti-dandruff, Anti-hair loss, hair products.
By anti-dandruff, Anti-hair loss, the hair products of the present invention for 100 user, user is had one's hair wash every three days, 2-3 drips quintessence oil when hair washing be mixed in shampoo to use, or when back of having one's hair wash is sent out half-dried, take 2-3 drip be coated in after quintessence oil is crumpled in palm on hair use, observe 6 months, wherein 80 people have new hair generation or feedback hair to become many, minority has thin piliation, 96 people think anti-dandruff respond well, 100 people all think that hair quality improves after use, and the withered phenomenon of bifurcated reduces, and hair is glossy.
Claims (8)
1. anti-dandruff, Anti-hair loss, hair products, it is characterised in that its formula includes the raw material of following weight portion:
Herba Lysimachiae foenum-graeci quintessence oil 1-5 part; Rosemary ethereal oil 1-3 part; Fir essential oil 1-6 part; Ah's glycerol or Jojoba oil 86-97 part.
2. anti-dandruff, Anti-hair loss, hair products according to claim 1, it is characterised in that its formula includes the raw material of following weight portion: Herba Lysimachiae foenum-graeci quintessence oil 3 parts; Rosemary ethereal oil 2 parts; Fir essential oil 3 parts; Ah's glycerol and/or Jojoba oil 92 parts.
3. anti-dandruff, Anti-hair loss, hair products according to claim 1, it is characterised in that the preparation method of described Herba Lysimachiae foenum-graeci quintessence oil or fir essential oil, comprise the following steps:
(1) by the air-dry fresh inflorescence of lavandula angustifolia or fresh fir leaf, join immersion 2-3h in soak, obtain pretreated feedstock;
(2) described pretreated feedstock is placed in distilling apparatus and carries out air-distillation at 100-105 DEG C, after condensation, obtain condensed fluid;
(3) by described condensed fluid by equipped with the adsorption column of alcoholic solution and activated carbon carries out extracted many times, obtaining lixiviating solution;
(4) described lixiviating solution is carried out decompression distillation, obtains Herba Lysimachiae foenum-graeci quintessence oil or fir essential oil.
4. anti-dandruff, Anti-hair loss, hair products according to claim 3, it is characterised in that when preparing Herba Lysimachiae foenum-graeci quintessence oil, the soak described in step (1) is mass concentration is the sodium chloride solution of 20%-25%; When preparing fir essential oil, the soak described in step (1) is water.
5. anti-dandruff, Anti-hair loss, hair products according to claim 3, it is characterised in that the pressure of described decompression distillation is 0.1-1.0kP.
6. anti-dandruff, Anti-hair loss, hair products according to claim 1, it is characterised in that the preparation method of described rosemary ethereal oil, comprise the following steps:
(1) by leaf of Herba Rosmarini Officinalis material immersion polar organic solvent extracts 0.08-6h at 20-100 DEG C of temperature, obtain extracting solution, extracting solution is boiled off at 20-100 DEG C described polar organic solvent, obtains the mixture of rosemary ethereal oil and rosemary antioxidant;
(2) described mixture is immersed in nonpolar or weakly polar organic solvent, at 20-100 DEG C of temperature, 0.5-6h is extracted in circulation, is cooled to 5-30 DEG C, filters, gained filtrate is boiled off at 20-100 DEG C described polarity or weakly polar organic solvent, obtains rosemary ethereal oil.
7. anti-dandruff, Anti-hair loss, hair products according to claim 6, it is characterised in that described leaf of Herba Rosmarini Officinalis material, described polar organic solvent and described nonpolar or weakly polar organic solvent weight ratio be: 1:3-20:3-20.
8. prepare method anti-dandruff as according to any one of claim 1-7, Anti-hair loss, hair products for one kind, it is characterised in that include being made by step:
(1) stir after the Herba Lysimachiae foenum-graeci quintessence oil of above-mentioned weight portion, rosemary ethereal oil and fir essential oil being mixed, obtain blend of essential oils;
(2) blend of essential oils of gained in step (1) is sufficiently mixed uniformly with Ah's glycerol of above-mentioned weight portion or Jojoba oil, obtains anti-dandruff, Anti-hair loss, hair products.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108567592A (en) * | 2017-10-19 | 2018-09-25 | 无锡市天爱装饰工程有限公司 | A kind of essential oil hair conditioner of Anti-hair loss |
| CN110934783A (en) * | 2018-09-21 | 2020-03-31 | 珠海伊斯佳科技股份有限公司 | Dandruff-removing and itching-relieving composition containing Chinese herbal medicines, silicone oil-free amino acid shampoo containing composition, and preparation method and application of silicone oil-free amino acid shampoo |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1654616A (en) * | 2005-01-24 | 2005-08-17 | 中国林业科学研究院林产化学工业研究所 | combined extraction method for rosemary essential oil and rosemary antioxidant |
| CN102949318A (en) * | 2012-12-03 | 2013-03-06 | 晓健科技（大连）有限公司 | Soapberry shampoo and preparation process thereof |
| CN103393569A (en) * | 2013-08-02 | 2013-11-20 | 太仓市伟基生物科技有限公司 | Preparation method for fleece-flower root nourishing shampoo |
| CN103585266A (en) * | 2013-11-07 | 2014-02-19 | 上海珍馨化工科技有限公司 | Patchouli compound essential oil |
| CN104031745A (en) * | 2014-06-27 | 2014-09-10 | 钟延华 | Method for extracting lavender essential oil |
| CN104274358A (en) * | 2014-09-05 | 2015-01-14 | 拉芳家化股份有限公司 | Scalp repair shampoo composition containing plant essential oil and preparation method thereof |
-
2016
- 2016-02-25 CN CN201610104568.7A patent/CN105640803B/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1654616A (en) * | 2005-01-24 | 2005-08-17 | 中国林业科学研究院林产化学工业研究所 | combined extraction method for rosemary essential oil and rosemary antioxidant |
| CN102949318A (en) * | 2012-12-03 | 2013-03-06 | 晓健科技（大连）有限公司 | Soapberry shampoo and preparation process thereof |
| CN103393569A (en) * | 2013-08-02 | 2013-11-20 | 太仓市伟基生物科技有限公司 | Preparation method for fleece-flower root nourishing shampoo |
| CN103585266A (en) * | 2013-11-07 | 2014-02-19 | 上海珍馨化工科技有限公司 | Patchouli compound essential oil |
| CN104031745A (en) * | 2014-06-27 | 2014-09-10 | 钟延华 | Method for extracting lavender essential oil |
| CN104274358A (en) * | 2014-09-05 | 2015-01-14 | 拉芳家化股份有限公司 | Scalp repair shampoo composition containing plant essential oil and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 马子川等: "《生活中的化学》", 30 June 2011, 北京师范大学出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108567592A (en) * | 2017-10-19 | 2018-09-25 | 无锡市天爱装饰工程有限公司 | A kind of essential oil hair conditioner of Anti-hair loss |
| CN110934783A (en) * | 2018-09-21 | 2020-03-31 | 珠海伊斯佳科技股份有限公司 | Dandruff-removing and itching-relieving composition containing Chinese herbal medicines, silicone oil-free amino acid shampoo containing composition, and preparation method and application of silicone oil-free amino acid shampoo |
| CN110934783B (en) * | 2018-09-21 | 2022-06-28 | 珠海伊斯佳科技股份有限公司 | Dandruff-removing and itching-relieving composition containing Chinese herbal medicines, silicone oil-free amino acid shampoo containing composition, and preparation method and application of silicone oil-free amino acid shampoo |
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