CN112807786A - Cold settling tank for defatted cannabidiol in industrial hemp - Google Patents

Cold settling tank for defatted cannabidiol in industrial hemp Download PDF

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Publication number
CN112807786A
CN112807786A CN202110170828.1A CN202110170828A CN112807786A CN 112807786 A CN112807786 A CN 112807786A CN 202110170828 A CN202110170828 A CN 202110170828A CN 112807786 A CN112807786 A CN 112807786A
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CN
China
Prior art keywords
tank
stirring
blanking
cold
wall
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Pending
Application number
CN202110170828.1A
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Chinese (zh)
Inventor
孙田
孙科
吴义务
陈昕
梁小勇
陈桂杭
潘池
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Jinban Machinery Co ltd
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Jinban Machinery Co ltd
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Publication date
Application filed by Jinban Machinery Co ltd filed Critical Jinban Machinery Co ltd
Priority to CN202110170828.1A priority Critical patent/CN112807786A/en
Publication of CN112807786A publication Critical patent/CN112807786A/en
Pending legal-status Critical Current

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/01—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements
    • B01D29/03—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements self-supporting
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/62—Regenerating the filter material in the filter
    • B01D29/64—Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element
    • B01D29/6469—Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element scrapers
    • B01D29/6484—Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element scrapers with a translatory movement with respect to the filtering element
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0004—Crystallisation cooling by heat exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F21/00—Dissolving
    • B01F21/10—Dissolving using driven stirrers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/11—Stirrers characterised by the configuration of the stirrers
    • B01F27/19—Stirrers with two or more mixing elements mounted in sequence on the same axis
    • B01F27/191—Stirrers with two or more mixing elements mounted in sequence on the same axis with similar elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/90—Heating or cooling systems
    • B01F35/92—Heating or cooling systems for heating the outside of the receptacle, e.g. heated jackets or burners
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/90—Heating or cooling systems
    • B01F2035/98—Cooling

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)

Abstract

The invention discloses a cold-sinking tank for degreasing cannabidiol in industrial hemp, which comprises a cold-sinking tank body, a fine control blanking device, a support frame, a refrigerating machine, a controller, a material stirring and dissolving device and a dynamic dewaxing filtering device, wherein the support frame is arranged on the upper wall of the cold-sinking tank body; the material stirring and dissolving device comprises a stirring and filtering tank, a stirring motor, an electric push rod, a motor fixing plate, a rotating shaft, a stirring blade, a lower fixing frame, a bearing plate, a lower connecting rod and a lower baffle. The invention belongs to the technical field of extraction and separation of natural phytochemicals, and particularly provides a cold settling tank for defatted cannabidiol in industrial hemp, which is convenient for accurately controlling the proportion of ethanol and an extract, is convenient for uniform mixing and dissolving of materials, and effectively separates filtrate and flocculent floating substances.

Description

Cold settling tank for defatted cannabidiol in industrial hemp
Technical Field
The invention belongs to the technical field of extraction and separation of natural phytochemicals, and particularly relates to a cold settling tank for defatted cannabidiol in industrial cannabis sativa.
Background
Cannabis is an annual herb plant of significant medicinal value, belonging to the family Moraceae, the subfamily Cannabis. The main active ingredients of the hemp plant extract are three types: cannabidiol CBD, cannabinol CBN, tetrahydrocannabis THC, wherein THC is an addictive component. The hemp plant is mainly dependent on the concentration of THC, and the variety with THC less than 0.3% has no mental activity. Therefore, the European Union Committee sets a unified standard, and the THC content in the dry product of the planted hemp can not be higher than 0.3 percent, namely the dry product is called as 'industrial hemp'.
At present, more than 80 cannabinoids separated from cannabis are available, mainly comprising cannabidiol CBD, tetrahydrocannabis THC, cannabinol CBN, cannabigerol CBC and the like, and the research finds that CBD can block THC from influencing the human nervous system and has important pharmacological activity. In addition, in recent years, the research finds that CBD has a series of physiological functions of sedation and hypnosis, epilepsy treatment, neuroprotection, multiple sclerosis, rheumatoid arthritis, tumor treatment and the like, and is a natural active component with great application prospects in the fields of medicines and the like.
A cold precipitation tank, namely a cooling precipitation tank, is used in the dewaxing step of the process for extracting the degreased cannabidiol from the industrial hemp, and the crude extract of the extract generated after crushing, baking and leaching is dissolved by using ethanol solution, then the crude extract is frozen at the temperature of between 40 ℃ below zero and 5 ℃ below zero and filtered at the temperature, and the filtrate is collected to obtain CBDV enrichment;
the existing cryoprecipitation tank has poor dewaxing effect, long degreasing time and low efficiency, meshes are easy to be blocked due to excessive wax accumulated on a filter screen, but flocculent floaters are generated at low temperature of a CBD extract and are a continuous process, so that the cryoprecipitation tank which can be dynamically dewaxed and separated and is not easy to be blocked is urgently sought.
Disclosure of Invention
In order to solve the existing problems, the invention provides the cold settling tank for the defatted cannabidiol in the industrial hemp, which is convenient for accurately controlling the proportion of ethanol and the extract, is convenient for uniformly mixing and dissolving materials and effectively separating filtrate and flocculent floating substances.
The technical scheme adopted by the invention is as follows: the invention relates to a cold-sinking tank for degreasing cannabidiol in industrial hemp, which comprises a cold-sinking tank body, a fine control blanking device, a support frame, a refrigerator, a controller, a material stirring and dissolving device and a dynamic dewaxing filtering device, wherein the support frame is arranged on the upper wall of the cold-sinking tank body; the material stirring and dissolving device comprises a stirring and filtering tank, a stirring motor, an electric push rod, a motor fixing plate, a rotating shaft, stirring blades, a lower fixing frame, a bearing plate, a lower connecting rod and a lower baffle plate, wherein the stirring and filtering tank is arranged in the cold-sinking tank body and comprises a stirring tank and a filtering tank which are communicated, the stirring tank is arranged above the filtering tank, the electric push rod is arranged on the outer upper wall of the stirring and filtering tank, the motor fixing plate is arranged at the upper end of the electric push rod, the stirring motor is fixedly connected with the upper wall of the motor fixing plate, the upper end of the rotating shaft is rotatably arranged at the lower wall of the motor fixing plate, an output shaft of the stirring motor penetrates through the motor fixing plate and is connected with the upper end of the rotating shaft, the lower end of the rotating shaft penetrates through the upper wall of the stirring tank and is slidably arranged in the stirring tank, the lower end of the stirring tank is communicated with the filtering tank, the bearing plate is arranged at the lower end opening of the stirring tank, the upper wall of the bearing plate is arranged in an inverted table with a low middle part and four high edges, a blanking through hole is arranged at the center of the bearing plate, a limiting rod is arranged on the upper wall of the bearing plate and symmetrically arranged at two sides of the blanking through hole, the lower fixing frame is slidably arranged on the limiting rod, the limiting rod enables the lower fixing frame to only slide up and down along with the rotating shaft but can not rotate along with the rotating shaft, the lower end of the rotating shaft is rotatably arranged on the upper wall of the lower fixing frame, the lower connecting rod is arranged at the lower wall of the lower fixing frame and penetrates through the blanking through hole, the lower baffle is arranged at the lower end of the lower connecting rod and is arranged below the bearing plate, the cross-sectional area of the lower, the lower fixing frame drives the lower baffle plate to move upwards through the lower connecting rod, so that the lower baffle plate is tightly contacted and attached with the bottom wall of the bearing plate, the lower baffle plate blocks the blanking through hole, so that the material in the stirring tank is prevented from leaking, a stirring motor can conveniently drive a rotating shaft to rotate, the rotating shaft drives stirring blades to rotate to stir ethanol and extract, so that the extract crude extract is dissolved in the ethanol, the uniform mixing and stirring are ensured to be completely dissolved, the lower fixing frame, the lower connecting rod and the lower baffle plate cannot rotate along with the rotation of the rotating shaft because the limiting rod limits the lower fixing frame, when the blanking is needed, the electric push rod is controlled to contract and move downwards, the electric push rod drives the motor fixing plate to move downwards, the motor fixing plate pushes the rotating shaft to move downwards, the rotating shaft pushes the lower fixing frame to move downwards along the limiting rod, the lower fixing, the dynamic dewaxing and filtering device comprises a sliding motor, a partition plate, a sliding lead screw, an auxiliary slide bar, a fixed plate, a motor fixing frame, an inclined filter screen and a scraper blade, wherein the filter tank comprises a filter cavity and an impurity discharging cavity, the partition plate is arranged between the filter cavity and the impurity discharging cavity, the upper end of the partition plate is provided with a clearance gap, the inclined filter screen is obliquely arranged on the partition plate and between the side walls of the filter cavity, one end, close to the partition plate, of the inclined filter screen is higher than one end, far away from the partition plate, of the inclined filter screen, the fixed plate is fixedly connected with the upper wall in the impurity discharging cavity, the sliding lead screw penetrates through the clearance gap and is rotatably arranged between the fixed plate and the side wall of the filter cavity, the auxiliary slide bar penetrates through the clearance gap and is rotatably arranged between the fixed plate and the side wall of the filter cavity, the sliding motor is arranged on a motor fixing frame, an output shaft of the sliding motor is connected with the sliding lead screw, the scraper is arranged on the sliding lead screw and the auxiliary sliding rod in a sliding manner, the lower wall of the scraper is obliquely arranged, the lower wall of the scraper is inclined to be the same as the inclined angle of the inclined filter screen, the lower wall of the scraper is in contact with the upper wall of the inclined filter screen, the sliding motor drives the sliding lead screw to rotate, the sliding lead screw rotates to drive the scraper to slide along the sliding lead screw and the auxiliary sliding rod, the auxiliary sliding rod limits the scraper, the scraper scrapes off sediments and floaters filtered on the inclined filter screen in the sliding process, the sediments and floaters are prevented from being accumulated on the inclined filter screen for a long time to cause the blockage of the inclined filter screen, the wax is dynamically scraped and removed, the filtering is ensured to be smooth, the inclined filter screen, the discharging pipe is convenient for discharge the fluid after filtering, agitator tank outer wall cover is equipped with freezing chamber, freezing chamber outer wall parcel is equipped with the cotton layer that keeps warm, the intercommunication is equipped with out the tuber pipe between the air outlet of refrigerator and the freezing chamber, the air intake intercommunication of refrigerator is equipped with the air-supply line, the air-supply line runs through the cold sink jar side wall and locates outside the cold sink jar body, and the refrigerator absorbs the cold sink jar external hot air compression refrigeration and carries air conditioning to freezing intracavity through going out the tuber pipe, makes its cooling through freezing the inside material heat of chamber absorption agitator tank to freezing the storage in to the agitator tank.
Further, the fine control blanking device comprises a blanking tank, a first blanking barrel, a second blanking barrel, a three-way pipe, a first electromagnetic valve and a second electromagnetic valve, wherein the blanking tank is arranged on the support frame, the blanking tank is arranged in a hollow cavity with an opening at the upper part, the first blanking barrel and the second blanking barrel are arranged in the blanking tank, the first blanking barrel is provided with a first feed inlet, the second blanking barrel is provided with a second feed inlet, two ports at the upper end of the three-way pipe penetrate through the blanking tank and are respectively communicated with the first blanking barrel and the second blanking barrel, one port at the lower end of the three-way pipe penetrates through the cold sinking tank body and is communicated with the stirring tank, the first electromagnetic valve and the second electromagnetic valve are respectively arranged on two ports at the upper end of the three-way pipe, the first blanking barrel is controlled by the first electromagnetic valve to be communicated with the three-way pipe, the second electromagnetic valve is convenient to control the communication between the, the side wall of the discharging tank is provided with a first transparent observation window and a second transparent observation window respectively, the first transparent observation window and the second transparent observation window are convenient for observing the liquid levels of the first discharging barrel and the second discharging barrel, one side of the first transparent observation window and one side of the second transparent observation window are respectively provided with scale marks, and the scale marks, the first transparent observation window and the second transparent observation window are convenient for accurately controlling the proportion of materials, so that the extraction quality of the degreased cannabidiol is improved.
Further, the controller is electrically connected with the first electromagnetic valve, the second electromagnetic valve, the electric push rod, the stirring motor, the sliding motor and the refrigerator respectively.
Further, the side wall of the cold-sinking tank body is provided with a touch screen, the touch screen is electrically connected with the controller, and the touch screen is convenient for controlling the device to adjust the refrigerating temperature of the refrigerating machine.
Further, arrange miscellaneous chamber lateral wall and be equipped with row miscellaneous mouthful, the cold heavy jar of body is close to row miscellaneous mouthful one side and is equipped with gets the material mouth, get the articulated miscellaneous door that is equipped with in the material mouth, arrange miscellaneous door and row miscellaneous mouthful be convenient for take out arrange the wax that miscellaneous intracavity scraper blade scraped.
Furthermore, the bottom wall of the cold-sinking tank body is provided with supporting legs, and the cold-sinking tank body is conveniently erected by the supporting legs.
The invention with the structure has the following beneficial effects: the cold settling tank of degreased cannabidiol in this scheme industry cannabis sativa is reasonable in design, and is easy and simple to handle, and the accurate control ethanol and extract ratio of being convenient for makes things convenient for material homogeneous mixing to dissolve, and effective separation filtrating and flocculent floater can effectively improve the work efficiency of dewaxing in the degreased cannabidiol extraction technology.
Drawings
FIG. 1 is a schematic diagram of a cryoprecipitation tank for defatted cannabidiol in industrial cannabis in accordance with the present invention;
FIG. 2 is a sectional view of a cryoprecipitation tank for defatted cannabidiol in industrial cannabis in accordance with the present invention;
fig. 3 is a schematic view of the combined structure of the material stirring and dissolving device and the dynamic dewaxing and filtering device of the cold settling tank for the defatted cannabidiol in the industrial hemp.
The accompanying drawings, which are included to provide a further understanding of the invention and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention and together with the description serve to explain the principles of the invention and not to limit the invention. In the drawings: 1. a cold sinking tank body, 2, a fine control blanking device, 3, a support frame, 4, a refrigerator, 5, a controller, 6, a material stirring and dissolving device, 7, a dynamic dewaxing and filtering device, 8, a stirring and filtering tank, 9, a stirring motor, 10, an electric push rod, 11, a motor fixing plate, 12, a rotating shaft, 13, a stirring blade, 14, a lower fixing frame, 15, a bearing plate, 16, a lower connecting rod, 17, a lower baffle plate, 18, a stirring tank, 19, a filtering tank, 20, a blanking through hole, 21, a limiting rod, 22, a sliding motor, 23, a baffle plate, 24, a sliding lead screw, 25, an auxiliary sliding rod, 26, a fixing plate, 27, a motor fixing frame, 28, an inclined filter screen, 29, a scraping plate, 30, a filtering cavity, 31, a impurity discharging cavity, 32, an air avoiding gap, 33, a discharging pipe, 34, a freezing cavity, 35, a heat preservation cotton layer, 36, an air outlet pipe, 37, an air inlet pipe, 39. the device comprises a first feeding barrel, a first feeding barrel 40, a second feeding barrel 41, a three-way pipe 42, a first electromagnetic valve 43, a second electromagnetic valve 44, a first transparent observation window 45, a second transparent observation window 46, scale marks 47, a touch screen 48, a trash discharging port 49, a material taking port 50, a trash discharging door 51 and supporting legs.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments; all other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
As shown in fig. 1-3, the cryoprecipitation tank for defatted cannabidiol in industrial hemp of the present invention comprises a cryoprecipitation tank body 1, a fine control blanking device 2, a support frame 3, a refrigerator 4, a controller 5, a material stirring and dissolving device 6 and a dynamic dewaxing filter device 7, wherein the support frame 3 is arranged on the upper wall of the cryoprecipitation tank body 1, the fine control blanking device 2 is arranged at the upper end of the support frame 3, the refrigerator 4, the controller 5, the material stirring and dissolving device 6 and the dynamic dewaxing filter device 7 are arranged in the cryoprecipitation tank body 1, and the material stirring and dissolving device 6 is arranged above the dynamic dewaxing filter device 7; the material stirring and dissolving device 6 comprises a stirring and filtering tank 8, a stirring motor 9, an electric push rod 10, a motor fixing plate 11, a rotating shaft 12, stirring blades 13, a lower fixing frame 14, a bearing plate 15, a lower connecting rod 16 and a lower baffle plate 17, wherein the stirring and filtering tank 8 is arranged in the cold-sinking tank body 1, the stirring and filtering tank 8 comprises a stirring tank 18 and a filtering tank 19 which are communicated, the stirring tank 18 is arranged above the filtering tank 19, the electric push rod 10 is arranged on the outer upper wall of the stirring and filtering tank 8, the motor fixing plate 11 is arranged at the upper end of the electric push rod 10, the stirring motor 9 is fixedly connected with the upper wall of the motor fixing plate 11, the upper end of the rotating shaft 12 is rotatably arranged at the lower wall of the motor fixing plate 11, an output shaft of the stirring motor 9 penetrates through the motor fixing plate 11 to be connected with the upper end of the rotating shaft 12, the lower end of the rotating shaft 12 penetrates through the, stirring leaf 13 is located in agitator tank 18, agitator tank 18 is lower extreme open-ended cavity setting, agitator tank 18 lower extreme and filter tank 19 intercommunication, agitator tank 18 lower extreme opening part is located to loading board 15, and loading board 15 upper wall is the setting of the high radius mesa of low four sides in the middle of, and loading board 15 center department is equipped with unloading through-hole 20, loading board 15 upper wall is equipped with gag lever post 21, and the gag lever post 21 symmetry is located unloading through-hole 20 both sides, down mount 14 slides and locates on gag lever post 21, and pivot 12 lower extreme rotates and locates the upper wall of down mount 14, down connecting rod 16 locates down mount 14 lower wall, down connecting rod 16 runs through and locates in the unloading through-hole 20, down baffle 17 locates down connecting rod 16 lower extreme, and down baffle 17 locates loading board 15 below, and the cross-sectional area of down baffle 17 is greater than the cross-sectional area of unloading through-hole 20, developments wax removal filter equipment 7, Baffle 23, sliding screw 24, supplementary slide bar 25, fixed plate 26, motor mount 27, slant filter screen 28 and scraper blade 29, filter tank 19 includes filter chamber 30 and row miscellaneous chamber 31, baffle 23 is located between filter chamber 30 and the row miscellaneous chamber 31, and baffle 23 upper end is equipped with clearance breach 32, slant filter screen 28 slope is located on baffle 23 and between the filter chamber 30 lateral wall, and the height that slant filter screen 28 is close to baffle 23 one end is greater than slant filter screen 28 and keeps away from baffle 23 one end height, fixed plate 26 rigid coupling is located and is arranged miscellaneous chamber 31 interior upper wall, sliding screw 24 runs through clearance breach 32 and rotates and locate between fixed plate 26 and the filter chamber 30 lateral wall, supplementary slide bar 25 runs through clearance breach 32 and rotates and locates between fixed plate 26 and the filter chamber 30 lateral wall, sliding screw 24 and supplementary slide bar 25 parallel arrangement, sliding screw 24 and slant filter screen parallel arrangement, motor mount 27 is located on arranging miscellaneous chamber 31 inner upper wall, sliding motor 22 is located on motor mount 27, sliding motor 22's output shaft and slip lead screw 24 are connected, slip lead screw 24 and supplementary slide bar 25 are located in the slip of scraper blade 29, the slope of scraper blade 29 lower wall sets up, and scraper blade 29 lower wall inclination is the same with slant filter screen 28 inclination, and scraper blade 29 lower wall touches with slant filter screen 28 upper wall and connects, the intercommunication is equipped with discharging pipe 33 under the filter chamber 30, 18 outer wall covers of agitator tank are equipped with freezing chamber 34, the cotton layer 35 of heat preservation is equipped with in the parcel of freezing chamber 34 outer wall, the intercommunication is equipped with out tuber pipe 36 between the air outlet of refrigerator 4 and the freezing chamber 34, the air intake intercommunication of refrigerator 4 is equipped with air-supply line 37, air-supply line 37 runs through the cold sinking jar body 1 lateral wall and locates outside.
Wherein the fine control blanking device 2 comprises a blanking tank 38, a first blanking barrel 39, a second blanking barrel 40, a three-way pipe 41, a first electromagnetic valve 42 and a second electromagnetic valve 43, the discharging tank 38 is arranged on the support frame 3, the discharging tank 38 is arranged in a hollow cavity with an opening at the upper part, the first discharging barrel 39 and the second discharging barrel 40 are arranged in the discharging barrel 38, a first feeding hole is arranged on the first discharging barrel 39, a second feeding port is arranged on the second feeding barrel 40, two ports at the upper end of a three-way pipe 41 penetrate through the feeding barrel 38 and are respectively communicated with the first feeding barrel 39 and the second feeding barrel 40, one port at the lower end of the three-way pipe 41 penetrates through the cold-sinking tank body 1 and is communicated with the stirring tank 18, the first electromagnetic valve 42 and the second electromagnetic valve 43 are respectively arranged on two ports at the upper end of the three-way pipe 41, the side wall of the blanking tank 38 is respectively provided with a first transparent observation window 44 and a second transparent observation window 45, scale marks 46 are respectively arranged on one sides of the first transparent observation window 44 and the second transparent observation window 45; the controller 5 is respectively electrically connected with the first electromagnetic valve 42, the second electromagnetic valve 43, the electric push rod 10, the stirring motor 9, the sliding motor 22 and the refrigerator 4; the side wall of the cold-sinking tank body 1 is provided with a touch screen 47, the touch screen 47 is electrically connected with the controller 5, and the touch screen 47 is convenient for controlling the device and adjusting the refrigerating temperature of the refrigerating machine 4; arrange miscellaneous chamber 31 lateral wall and be equipped with row miscellaneous mouth 48, the cold heavy jar of body 1 is close to row miscellaneous mouth 48 one side and is equipped with material taking port 49, material taking port 49 internal hinge is equipped with row miscellaneous door 50 cold heavy jar of body 1 diapire is equipped with supporting leg 51.
When the device is used specifically, extract crude extract and ethanol generated after extraction are poured into the first lower charging barrel 39 and the second lower charging barrel 40 through the first feeding port and the second feeding port respectively, liquid levels of the first lower charging barrel 39 and the second lower charging barrel 40 are observed through the first transparent observation window 44 and the second transparent observation window 45 respectively, the scale mark 46 is convenient for accurately controlling the feeding amount of the extract crude extract and the ethanol so as to accurately control the proportion of the extract crude extract and the ethanol, after the feeding is finished, an instruction is sent to the controller 5 through the touch screen 47 to control the first electromagnetic valve 42 and the second electromagnetic valve 43 to be opened, the extract crude extract and the ethanol in the first lower charging barrel 39 and the second lower charging barrel 40 slide down to the stirring tank 18 through the three-way pipe 41, an instruction is sent to the controller 5 through the touch screen 47 to control the stirring motor 9 to rotate, in an initial state, the electric push rod 10 is in an extension state, at the moment, the electric push rod 10 pushes the motor fixing, the motor fixing plate 11 drives the rotating shaft 12 to move upwards, the rotating shaft 12 moves upwards to drive the lower fixing frame 14 to move upwards, the lower fixing frame 14 drives the lower baffle 17 to move upwards through the lower connecting rod 16, so that the lower baffle 17 is tightly contacted and attached with the bottom wall of the bearing plate 15, the lower baffle 17 blocks the blanking through hole 20, so that materials in the stirring tank 18 are prevented from leaking, the extract crude jin paste and ethanol sliding downwards from the three-way pipe 41 slide downwards into the stirring tank 18, the stirring motor 9 drives the rotating shaft 12 to rotate, the rotating shaft 12 drives the stirring blade 13 to rotate to stir and mix the extract crude jin paste and ethanol to be fully dissolved, after stirring, an instruction is sent to the controller 5 through the touch screen 47 to control the stirring motor 9 to stop rotating, then an instruction is sent to the controller 5 through the touch screen 47 to control the refrigerator 4 to work, the refrigerating temperature of the refrigerator 4 is set through the touch screen 47, the refrigerator 4 absorbs hot air outside the cold sink tank body 1, the heat of the materials in the stirring tank 18 is absorbed by the freezing cavity 34 to cool the materials, so that the interior of the stirring tank 18 is frozen and stored, wax in the materials can be separated out along with low-temperature crystallization, after the materials are frozen for 4-12 hours, an instruction is sent to the controller 5 through the touch screen 47 to control the electric push rod 10 to shorten, the electric push rod 10 is controlled to contract and move downwards, the electric push rod 10 drives the motor fixing plate 11 to move downwards, the motor fixing plate 11 drives the rotating shaft 12 to move downwards, the rotating shaft 12 drives the lower fixing frame 14 to move downwards along the limiting rod 21, the lower fixing frame 14 drives the lower baffle 17 to move downwards through the lower connecting rod 16 so as to expose the blanking through hole 20, the materials in the stirring tank 18 flow out to the inclined filter screen 28 in the filtering tank 19 to be filtered, oil slides downwards to the filtering cavity 30 through the inclined filter screen 28 to be discharged through the discharge pipe 33, the inclined filter screen 28 effectively prevents the, wax separated out from oil is filtered on the inclined filter screen 28, in the filtering process, the sliding motor 22 is controlled to periodically rotate forwards and backwards through the touch screen 47, the sliding motor 22 drives the sliding screw rod 24 to rotate, the sliding screw rod 24 rotates to drive the scraper 29 to slide along the sliding screw rod 24 and the auxiliary slide rod 25, the auxiliary slide rod 25 limits the scraper 29, the scraper 29 scrapes and pushes sediments and floaters filtered on the inclined filter screen 28 in the sliding process to the impurity removing cavity 31, so that the sediments and floaters are prevented from being accumulated on the inclined filter screen 28 for a long time to cause the blockage of the inclined filter screen 28, impurities are dynamically scraped, the smooth filtering is ensured, after the operation is finished, the touch screen 47 sends an instruction to the controller 5 to control the sliding motor 22 to stop moving and control the electric telescopic rod to extend and reset so that the lower baffle 17 resets to block the, then the impurity discharging door 50 at one side of the cold-sink tank body 1 is opened to take out the scraped wax from the impurity discharging port 48.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (6)

1. A cold settling tank for defatted cannabidiol in industrial hemp is characterized in that: the device comprises a cold-sinking tank body, a fine control blanking device, a support frame, a refrigerator, a controller, a material stirring and dissolving device and a dynamic dewaxing and filtering device, wherein the support frame is arranged on the upper wall of the cold-sinking tank body; the material stirring and dissolving device comprises a stirring and filtering tank, a stirring motor, an electric push rod, a motor fixing plate, a rotating shaft, stirring blades, a lower fixing frame, a bearing plate, a lower connecting rod and a lower baffle plate, wherein the stirring and filtering tank is arranged in the cold-sinking tank body and comprises a stirring tank and a filtering tank which are communicated, the stirring tank is arranged above the filtering tank, the electric push rod is arranged on the outer upper wall of the stirring and filtering tank, the motor fixing plate is arranged at the upper end of the electric push rod, the stirring motor is fixedly connected with the upper wall of the motor fixing plate, the upper end of the rotating shaft is rotatably arranged at the lower wall of the motor fixing plate, an output shaft of the stirring motor penetrates through the motor fixing plate and is connected with the upper end of the rotating shaft, the lower end of the rotating shaft penetrates through the upper wall of the stirring tank and is slidably arranged in the stirring tank, the lower end of the stirring tank is communicated with the filtering tank, the bearing plate is arranged at the lower end opening of the stirring tank, the upper wall of the bearing plate is arranged in an inverted table top with a low middle and four high edges, a blanking through hole is arranged at the center of the bearing plate, a limiting rod is arranged on the upper wall of the bearing plate and symmetrically arranged at two sides of the blanking through hole, the lower fixing frame is slidably arranged on the limiting rod, the lower end of the rotating shaft is rotatably arranged on the upper wall of the lower fixing frame, the lower connecting rod is arranged at the lower wall of the lower fixing frame and penetrates through the blanking through hole, the lower baffle is arranged at the lower end of the lower connecting rod and is arranged below the bearing plate, the cross sectional area of the lower baffle is larger than that of the blanking through hole, the dynamic dewaxing filtering device comprises a sliding motor, a partition plate, a sliding lead, the baffle is arranged between the filter cavity and the impurity removing cavity, the upper end of the baffle is provided with a clearance gap, the oblique filter screen is obliquely arranged on the baffle and between the side walls of the filter cavity, one end of the oblique filter screen close to the baffle is higher than one end of the oblique filter screen far away from the baffle, the fixed plate is fixedly connected with the upper wall in the impurity removing cavity, the sliding lead screw is rotatably arranged between the fixed plate and the side wall of the filter cavity through the clearance gap, the auxiliary slide bar is rotatably arranged between the fixed plate and the side wall of the filter cavity through the clearance gap, the sliding lead screw is arranged in parallel with the auxiliary slide bar, the sliding lead screw is arranged in parallel with the oblique filter screen, the motor fixing frame is arranged on the upper wall in the impurity removing cavity, the sliding motor is arranged on the motor fixing frame, the output shaft of the sliding motor is connected with, scraper blade lower wall inclination is the same with slant filter screen inclination, and the scraper blade lower wall touches with slant filter screen upper wall and connects, filter chamber lower wall intercommunication is equipped with the discharging pipe, agitator tank outer wall cover is equipped with freezing chamber, freezing chamber outer wall parcel is equipped with the cotton layer of heat preservation, the intercommunication is equipped with out the tuber pipe between the air outlet of refrigerator and the freezing chamber, the air intake intercommunication of refrigerator is equipped with the air-supply line, the air-supply line runs through the cold sinking jar external wall and locates outside the cold sinking jar body.
2. The cryoprecipitation tank for defatted cannabidiol in industrial cannabis as claimed in claim 1, wherein: the fine control blanking device comprises a blanking tank, a first blanking barrel, a second blanking barrel, a three-way pipe, a first electromagnetic valve and a second electromagnetic valve, wherein the blanking tank is arranged on the support frame, the blanking tank is a hollow cavity with an opening at the upper part, the first blanking barrel and the second blanking barrel are arranged in the blanking tank, the first blanking barrel is provided with a first feed inlet, the second blanking barrel is provided with a second feed inlet, two ports at the upper end of the three-way pipe penetrate through the blanking tank and are communicated with the first blanking barrel, the second blanking barrel and the stirring tank respectively, one port at the lower end of the three-way pipe penetrates through a cold sinking tank body and is communicated with the stirring tank, the first electromagnetic valve and the second electromagnetic valve are arranged on two ports at the upper end of the three-way pipe respectively, the side wall of the blanking tank is provided with a first transparent observation window and.
3. The cryoprecipitation tank for defatted cannabidiol in industrial cannabis sativa as claimed in claim 2, wherein: the controller is respectively and electrically connected with the first electromagnetic valve, the second electromagnetic valve, the electric push rod, the stirring motor, the sliding motor and the refrigerator.
4. The cryoprecipitation tank for defatted cannabidiol in industrial cannabis as claimed in claim 1, wherein: the lateral wall of the cold sinking tank body is provided with a touch screen, and the touch screen is electrically connected with the controller.
5. The cryoprecipitation tank for defatted cannabidiol in industrial cannabis as claimed in claim 1, wherein: arrange miscellaneous chamber lateral wall and be equipped with row miscellaneous mouth, the cold heavy jar of body is close to row miscellaneous mouthful one side and is equipped with the material taking mouth, it is equipped with row miscellaneous door to get the articulated in the material taking mouth.
6. The cryoprecipitation tank for defatted cannabidiol in industrial cannabis as claimed in claim 1, wherein: the bottom wall of the cold-sinking tank body is provided with supporting legs.
CN202110170828.1A 2021-02-08 2021-02-08 Cold settling tank for defatted cannabidiol in industrial hemp Pending CN112807786A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202110170828.1A CN112807786A (en) 2021-02-08 2021-02-08 Cold settling tank for defatted cannabidiol in industrial hemp

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202110170828.1A CN112807786A (en) 2021-02-08 2021-02-08 Cold settling tank for defatted cannabidiol in industrial hemp

Publications (1)

Publication Number Publication Date
CN112807786A true CN112807786A (en) 2021-05-18

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Family Applications (1)

Application Number Title Priority Date Filing Date
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Country Link
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113578117A (en) * 2021-08-06 2021-11-02 江苏国胶新材料有限公司 Water-based pressure-sensitive adhesive production device and production process thereof
CN113634006A (en) * 2021-07-16 2021-11-12 刘子豪 Food freezing and concentrating device
CN114250363A (en) * 2021-12-20 2022-03-29 清远市嘉禾稀有金属有限公司 Lime cream anti-settling process and treatment device thereof
CN116271875A (en) * 2023-01-17 2023-06-23 江苏润普食品科技股份有限公司 Evaporation and centrifugation integrated device for potassium citrate crystallization process

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113634006A (en) * 2021-07-16 2021-11-12 刘子豪 Food freezing and concentrating device
CN113578117A (en) * 2021-08-06 2021-11-02 江苏国胶新材料有限公司 Water-based pressure-sensitive adhesive production device and production process thereof
CN114250363A (en) * 2021-12-20 2022-03-29 清远市嘉禾稀有金属有限公司 Lime cream anti-settling process and treatment device thereof
CN116271875A (en) * 2023-01-17 2023-06-23 江苏润普食品科技股份有限公司 Evaporation and centrifugation integrated device for potassium citrate crystallization process
CN116271875B (en) * 2023-01-17 2023-10-20 江苏润普食品科技股份有限公司 Evaporation and centrifugation integrated device for potassium citrate crystallization process

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