CN112745750A - Interior wall ceramic coating and preparation method thereof - Google Patents
Interior wall ceramic coating and preparation method thereof Download PDFInfo
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- CN112745750A CN112745750A CN201911039664.8A CN201911039664A CN112745750A CN 112745750 A CN112745750 A CN 112745750A CN 201911039664 A CN201911039664 A CN 201911039664A CN 112745750 A CN112745750 A CN 112745750A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1687—Use of special additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2289—Oxides; Hydroxides of metals of cobalt
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2296—Oxides; Hydroxides of metals of zinc
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Plant Pathology (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses an interior wall ceramic coating and a preparation method thereof, wherein the interior wall ceramic coating consists of a component A, a component B and a component C, wherein the component A comprises 20-25 parts by weight of methyltrimethoxysilane and 10-15 parts by weight of dimethyldimethoxysilane; the component B comprises 5-25 parts of pigment, 10-25 parts of filler, 25-30 parts of water, 10-15 parts of polyurethane resin, 10-15 parts of acrylic resin, 3-6 parts of isocyanate, 1-2 parts of non-stick auxiliary agent, 1-2 parts of dispersing agent, 0.5-2 parts of wetting agent, 1-2 parts of defoaming agent and 1-2 parts of ultraviolet absorbent; the component C is 1-2 parts by weight of glacial acetic acid. Compared with the traditional emulsion paint, the interior wall ceramic coating provided by the invention has the advantages of high hardness (4H), super-hydrophobicity, stain resistance (doodling resistance), strong weather resistance, antibiosis and mildew resistance, and the like, and is green and environment-friendly.
Description
Technical Field
The invention relates to the technical field of coatings, in particular to an interior wall ceramic coating and a preparation method thereof.
Background
The interior wall coating is the latex paint for general decoration. The latex paint is an emulsion material and is divided into two categories, namely polyvinyl acetate emulsion and acrylic emulsion, according to different base materials. The emulsion paint uses water as diluent, is a material with convenient construction, safety, water washing resistance and good air permeability, and can be prepared into different colors according to different color matching schemes. However, the latex paint interior wall coating usually contains formaldehyde, formaldehyde is easy to volatilize, formaldehyde has pungent odor, and when the formaldehyde content in the air is too high, formaldehyde is easy to affect human health, so that the interior wall is easy to emit gas with pungent odor after decoration, and the human health is easy to affect.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide an internal wall ceramic coating and a preparation method thereof.
The invention adopts the specific technical scheme that:
an interior wall ceramic coating comprises a component A, a component B and a component C, wherein the component A comprises 20-25 parts by weight of methyltrimethoxysilane and 10-15 parts by weight of dimethyldimethoxysilane; the component B comprises 5-25 parts of pigment, 10-25 parts of filler, 25-30 parts of water, 10-15 parts of polyurethane resin, 10-15 parts of acrylic resin, 3-6 parts of isocyanate, 1-2 parts of non-stick auxiliary agent, 1-2 parts of dispersing agent, 0.5-2 parts of wetting agent, 1-2 parts of defoaming agent and 1-2 parts of ultraviolet absorbent; the component C is 1-2 parts by weight of glacial acetic acid.
Further, the pigment is selected from any one or more of titanium dioxide, iron oxide red, carbon black, copper chromium black, cobalt blue and permanent violet.
Further, the filler is an inorganic filler.
Furthermore, the inorganic filler is composed of 5-10 parts by weight of nano zinc oxide, 5-10 parts by weight of nano silicon dioxide and 1-3 parts by weight of cobalt hydroxide.
Further, the non-stick auxiliary agent is selected from one or more of dimethylhydroxy silicone oil and fluorine-containing hydroxy silicone oil.
Further, the dispersing agent is selected from one or more of sodium hexametaphosphate, sodium pyrophosphate, sodium styrene sulfonate, polyether modified organic silicon and sodium naphthenate sulfate.
Further, the wetting agent is polyether modified siloxane.
Further, the defoaming agent is selected from one or more of a water-based silicone defoaming agent and a mineral oil defoaming agent.
Further, the ultraviolet absorbent is selected from one or more of salicylic acid esters, benzophenones, benzotriazoles and triazines.
Correspondingly, the invention also provides a preparation method of the interior wall ceramic coating, which comprises the following steps:
(1) preparing a component B: adding polyurethane resin, acrylic resin, isocyanate and water in a formula amount into a container, stirring for a certain time at a certain rotating speed, and pouring pigment, filler, a leveling agent, a non-stick auxiliary agent, a dispersing agent, a wetting agent, a defoaming agent and an ultraviolet absorbent into the container, and stirring uniformly at a certain rotating speed; preparing a component A and a component C;
(2) and mixing the component B and the component C, stirring for a certain time at a certain rotating speed, adding methyltrimethoxysilane and dimethyldimethoxysilane, and continuously stirring for a certain time at a certain rotating speed to obtain the ceramic coating.
The invention has the beneficial effects that: the polyurethane resin, the acrylic resin and the isocyanate in the paint have the function of assisting film formation in cooperation, and can replace emulsion to improve the film formation effect, the film formation strength and the bonding property between a coating film and a material; according to the invention, inorganic raw materials such as nano zinc oxide, nano silicon dioxide and cobalt hydroxide are used as fillers, so that the particle size is smaller, the crystallization is more complete, the internal clearance of the coating is reduced, the antioxidant index and the strength of the coating are further improved, and the coating has antibacterial and mildewproof effects; the silane in the invention is hydrolyzed into silanol under the action of glacial acetic acid, a chemical cross-linking structure is formed among the silanol, and fillers such as nano zinc oxide, nano silicon dioxide, cobalt hydroxide and the like are solidified, so that the adhesive force of the coating is improved. Compared with the traditional emulsion paint, the interior wall ceramic coating provided by the invention has the advantages of high hardness (4H), super-hydrophobicity, stain resistance (doodling prevention), strong weather resistance, antibiosis and mildew resistance, and the like, and is green and environment-friendly.
Detailed Description
The present invention will be described in further detail with reference to examples, but the embodiments of the present invention are not limited thereto, and various substitutions and alterations can be made without departing from the technical idea of the present invention as described above, according to the common technical knowledge and the conventional means in the field.
Example 1
An interior wall ceramic coating comprises a component A, a component B and a component C, wherein the component A comprises 20 parts by weight of methyltrimethoxysilane and 10 parts by weight of dimethyldimethoxysilane; the component B comprises 5 parts of pigment, 10 parts of filler, 25 parts of water, 10 parts of polyurethane resin, 10 parts of acrylic resin, 3 parts of isocyanate, 1 part of dimethyl hydroxy silicone oil, 1 part of sodium hexametaphosphate, 0.5 part of polyether modified siloxane, 1 part of water-based organic silicon defoamer and 1 part of salicylate; the component C is 1 part by weight of glacial acetic acid; the inorganic filler is composed of 5 parts by weight of nano zinc oxide, 5 parts by weight of nano silicon dioxide and 1 part by weight of cobalt hydroxide.
The preparation method of the interior wall ceramic coating comprises the following steps:
(1) preparing a component B: adding polyurethane resin, acrylic resin, isocyanate and water in a formula amount into a container, stirring for a certain time at a certain rotating speed, and pouring pigment, filler, a leveling agent, a non-stick auxiliary agent, a dispersing agent, polyether modified siloxane, a defoaming agent and an ultraviolet absorbent into the container, and stirring uniformly at a certain rotating speed; preparing a component A and a component C;
(2) and mixing the component B and the component C, stirring for a certain time at a certain rotating speed, adding methyltrimethoxysilane and dimethyldimethoxysilane, and continuously stirring for a certain time at a certain rotating speed to obtain the ceramic coating.
Example 2
An interior wall ceramic coating comprises a component A, a component B and a component C, wherein the component A comprises 22 parts by weight of methyltrimethoxysilane and 11 parts by weight of dimethyldimethoxysilane; the component B comprises 10 parts of pigment, 15 parts of filler, 26 parts of water, 11 parts of polyurethane resin, 12 parts of acrylic resin, 4 parts of isocyanate, 1.3 parts of fluorine-containing hydroxyl silicone oil, 1.3 parts of sodium pyrophosphate, 0.8 part of polyether modified siloxane, 1.2 parts of mineral oil defoamer and 1.2 parts of benzophenone; the component C is glacial acetic acid 1.3 weight parts; the inorganic filler is composed of 7.5 parts by weight of nano zinc oxide, 7.5 parts by weight of nano silicon dioxide and 2 parts by weight of cobalt hydroxide.
The preparation method of the interior wall ceramic coating comprises the following steps:
(1) preparing a component B: adding polyurethane resin, acrylic resin, isocyanate and water in a formula amount into a container, stirring for a certain time at a certain rotating speed, and pouring pigment, filler, a leveling agent, a non-stick auxiliary agent, a dispersing agent, polyether modified siloxane, a defoaming agent and an ultraviolet absorbent into the container, and stirring uniformly at a certain rotating speed; preparing a component A and a component C;
(2) and mixing the component B and the component C, stirring for a certain time at a certain rotating speed, adding methyltrimethoxysilane and dimethyldimethoxysilane, and continuously stirring for a certain time at a certain rotating speed to obtain the ceramic coating.
Example 3
An interior wall ceramic coating consists of a component A, a component B and a component C, wherein the component A comprises 22.5 parts by weight of methyltrimethoxysilane and 12.5 parts by weight of dimethyldimethoxysilane; the component B comprises 15 parts by weight of pigment, 17.5 parts by weight of filler, 27.5 parts by weight of water, 12.5 parts by weight of polyurethane resin, 12.5 parts by weight of acrylic resin, 4.5 parts by weight of isocyanate, 1.5 parts by weight of dimethyl hydroxy silicone oil, 1.5 parts by weight of sodium styrene sulfonate, 1.25 parts by weight of polyether modified siloxane, 1.5 parts by weight of water-based organic silicon defoamer and 1.5 parts by weight of benzotriazole; the component C is 1.5 parts by weight of glacial acetic acid; the inorganic filler is composed of 7.5 parts by weight of nano zinc oxide, 7.5 parts by weight of nano silicon dioxide and 2 parts by weight of cobalt hydroxide.
The preparation method of the interior wall ceramic coating comprises the following steps:
(1) preparing a component B: adding polyurethane resin, acrylic resin, isocyanate and water in a formula amount into a container, stirring for a certain time at a certain rotating speed, and pouring pigment, filler, a leveling agent, a non-stick auxiliary agent, a dispersing agent, polyether modified siloxane, a defoaming agent and an ultraviolet absorbent into the container, and stirring uniformly at a certain rotating speed; preparing a component A and a component C;
(2) and mixing the component B and the component C, stirring for a certain time at a certain rotating speed, adding methyltrimethoxysilane and dimethyldimethoxysilane, and continuously stirring for a certain time at a certain rotating speed to obtain the ceramic coating.
Example 4
An interior wall ceramic coating comprises a component A, a component B and a component C, wherein the component A comprises 24 parts by weight of methyltrimethoxysilane and 14 parts by weight of dimethyldimethoxysilane; the component B comprises 20 parts of pigment, 22 parts of filler, 29 parts of water, 14 parts of polyurethane resin, 14 parts of acrylic resin, 5 parts of isocyanate, 1.8 parts of fluorine-containing hydroxyl silicone oil, 1.8 parts of polyether modified organic silicon, 1.8 parts of polyether modified siloxane, 1.7 parts of mineral oil defoaming agent and 1.7 parts of triazine; the component C is 1.9 parts by weight of glacial acetic acid; the inorganic filler is composed of 8 parts by weight of nano zinc oxide, 9 parts by weight of nano silicon dioxide and 2.5 parts by weight of cobalt hydroxide.
The preparation method of the interior wall ceramic coating comprises the following steps:
(1) preparing a component B: adding polyurethane resin, acrylic resin, isocyanate and water in a formula amount into a container, stirring for a certain time at a certain rotating speed, and pouring pigment, filler, a leveling agent, a non-stick auxiliary agent, a dispersing agent, polyether modified siloxane, a defoaming agent and an ultraviolet absorbent into the container, and stirring uniformly at a certain rotating speed; preparing a component A and a component C;
(2) and mixing the component B and the component C, stirring for a certain time at a certain rotating speed, adding methyltrimethoxysilane and dimethyldimethoxysilane, and continuously stirring for a certain time at a certain rotating speed to obtain the ceramic coating.
Example 5
An interior wall ceramic coating comprises a component A, a component B and a component C, wherein the component A comprises 25 parts by weight of methyltrimethoxysilane and 15 parts by weight of dimethyldimethoxysilane; the component B comprises 25 parts of pigment, 25 parts of filler, 30 parts of water, 15 parts of polyurethane resin, 15 parts of acrylic resin, 6 parts of isocyanate, 2 parts of dimethyl hydroxyl silicone oil, 2 parts of naphthenic sodium sulfate, 2 parts of polyether modified siloxane, 2 parts of organic silicon defoamer and 2 parts of salicylate; the component C is glacial acetic acid 2 parts by weight; the inorganic filler is composed of 10 parts by weight of nano zinc oxide, 10 parts by weight of nano silicon dioxide and 3 parts by weight of cobalt hydroxide.
The preparation method of the interior wall ceramic coating comprises the following steps:
(1) preparing a component B: adding polyurethane resin, acrylic resin, isocyanate and water in a formula amount into a container, stirring for a certain time at a certain rotating speed, and pouring pigment, filler, a leveling agent, a non-stick auxiliary agent, a dispersing agent, polyether modified siloxane, a defoaming agent and an ultraviolet absorbent into the container, and stirring uniformly at a certain rotating speed; preparing a component A and a component C;
(2) and mixing the component B and the component C, stirring for a certain time at a certain rotating speed, adding methyltrimethoxysilane and dimethyldimethoxysilane, and continuously stirring for a certain time at a certain rotating speed to obtain the ceramic coating.
The interior wall ceramic coatings of the above examples were subjected to performance tests, adhesion was tested according to GB/T9286-1978, hardness was determined according to GB/T6739-2006 colored paint and varnish pencil method, water absorption was determined according to GB1727-79, formaldehyde content was determined according to GB18582-2001 "Limited amount of harmful substances in interior finishing materials-interior wall coatings", and the test results are shown in the following table:
examples | Strength of adhesion | Hardness of | Water absorption rate | Content of Formaldehyde |
Example 1 | Level 1 | 6H | 3.01% | 0.01 |
Example 2 | Level 1 | 6H | 2.78% | 0.01 |
Example 3 | Level 0 | 6H | 2.06% | 0.01 |
Example 4 | Level 0 | 6H | 2.45% | 0.01 |
Example 5 | Level 1 | 6H | 2.67% | 0.01 |
Although the embodiments have been described, once the basic inventive concept is known, other variations and modifications can be made to the embodiments by those skilled in the art, so that the above embodiments are only examples of the present invention, and not intended to limit the scope of the present invention, and all equivalent structures or equivalent processes that can be used in the present specification or directly or indirectly applied to other related fields are encompassed by the present invention.
Claims (10)
1. The interior wall ceramic coating is characterized by comprising a component A, a component B and a component C, wherein the component A comprises 20-25 parts by weight of methyltrimethoxysilane and 10-15 parts by weight of dimethyldimethoxysilane; the component B comprises 5-25 parts of pigment, 10-25 parts of filler, 25-30 parts of water, 10-15 parts of polyurethane resin, 10-15 parts of acrylic resin, 3-6 parts of isocyanate, 1-2 parts of non-stick auxiliary agent, 1-2 parts of dispersing agent, 0.5-2 parts of wetting agent, 1-2 parts of defoaming agent and 1-2 parts of ultraviolet absorbent; the component C is 1-2 parts by weight of glacial acetic acid.
2. The interior wall ceramic coating according to claim 1, wherein the pigment is selected from any one or more of titanium dioxide, iron oxide red, carbon black, copper chromium black, cobalt blue and permanent violet.
3. An interior wall ceramic coating according to claim 1, wherein the filler is an inorganic filler.
4. The interior wall ceramic coating according to claim 3, wherein the inorganic filler comprises 5-10 parts by weight of nano zinc oxide, 5-10 parts by weight of nano silica and 1-3 parts by weight of cobalt hydroxide.
5. The interior wall ceramic coating according to claim 3, wherein the non-stick auxiliary agent is one or more selected from dimethylhydroxysiloxane oil and fluorinated hydroxysiloxane oil.
6. The interior wall ceramic coating according to claim 3, wherein the dispersant is one or more selected from sodium hexametaphosphate, sodium pyrophosphate, sodium styrene sulfonate, polyether modified silicone, and sodium naphthenate sulfate.
7. The interior wall ceramic coating of claim 3, wherein the wetting agent is a polyether modified siloxane.
8. The interior wall ceramic coating according to claim 3, wherein the defoaming agent is one or more selected from water-based silicone defoaming agent and mineral oil defoaming agent.
9. An interior wall ceramic coating according to claim 3, wherein the ultraviolet absorber is selected from one or more of the group consisting of salicylates, benzophenones, benzotriazoles, and triazines.
10. A method for preparing an interior wall ceramic coating according to any one of claims 1 to 9, comprising the steps of:
(1) preparing a component B: adding polyurethane resin, acrylic resin, isocyanate and water in a formula amount into a container, stirring for a certain time at a certain rotating speed, and pouring pigment, filler, a leveling agent, a non-stick auxiliary agent, a dispersing agent, a wetting agent, a defoaming agent and an ultraviolet absorbent into the container, and stirring uniformly at a certain rotating speed; preparing a component A and a component C;
(2) and mixing the component B and the component C, stirring for a certain time at a certain rotating speed, adding methyltrimethoxysilane and dimethyldimethoxysilane, and continuously stirring for a certain time at a certain rotating speed to obtain the ceramic coating.
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CN115320207A (en) * | 2022-08-16 | 2022-11-11 | 常熟宏巨新材料科技有限公司 | Mould-proof TPU thermoplastic polyurethane film |
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CN115320207A (en) * | 2022-08-16 | 2022-11-11 | 常熟宏巨新材料科技有限公司 | Mould-proof TPU thermoplastic polyurethane film |
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Application publication date: 20210504 |