CN112730366A - Method for rapidly judging wrapping uniformity of fully water-soluble liquid anti-caking agent on fertilizer - Google Patents
Method for rapidly judging wrapping uniformity of fully water-soluble liquid anti-caking agent on fertilizer Download PDFInfo
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- CN112730366A CN112730366A CN202011590697.4A CN202011590697A CN112730366A CN 112730366 A CN112730366 A CN 112730366A CN 202011590697 A CN202011590697 A CN 202011590697A CN 112730366 A CN112730366 A CN 112730366A
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
- G01N21/64—Fluorescence; Phosphorescence
- G01N21/645—Specially adapted constructive features of fluorimeters
- G01N21/6456—Spatial resolved fluorescence measurements; Imaging
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
- G01N21/64—Fluorescence; Phosphorescence
- G01N21/645—Specially adapted constructive features of fluorimeters
- G01N21/6456—Spatial resolved fluorescence measurements; Imaging
- G01N2021/646—Detecting fluorescent inhomogeneities at a position, e.g. for detecting defects
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Abstract
The invention discloses a method for rapidly judging the wrapping uniformity of a fully water-soluble liquid anti-caking agent on a fertilizer, which comprises the following steps: adding fluorescent powder accounting for 0.05-0.2% of the liquid anti-caking agent into the full-aqueous liquid anti-caking agent, fully and uniformly mixing, spraying the liquid anti-caking agent on the surface of the fertilizer, irradiating by using a fluorescent lamp, and judging whether the anti-caking agent added on the surface of the fertilizer is uniformly wrapped or not and whether the dosage of the added anti-caking agent is proper or not by using fluorescent reflection light on the surface of the fertilizer. The method has the advantages of low cost, simple operation, convenient use, intuitive judgment, strong detection foundation and high reference practicability, can quickly judge the uniformity of the fully water-soluble liquid anti-caking agent coated on the fertilizer by using the reflected light of the fluorescent lamp after irradiation on the surface of the fertilizer, truly reflects the reasonable addition amount of the anti-caking agent of the fertilizer in the production process, and can better guide the anti-caking agent to be reasonably added in the production process so as to ensure that the fertilizer is not caked, keeps loose for a long time, improves the appearance quality of the fertilizer, is convenient to store and use.
Description
Technical Field
The invention relates to a method for rapidly judging the wrapping uniformity of a fully water-soluble liquid anti-caking agent on a fertilizer, belonging to the technical field of fertilizer anti-caking agent detection methods.
Background
With the increasing new demands of crops and the increasing environmental protection, the fertilizer market is constantly changed, at present, fertilizer enterprises produce water-soluble fertilizers increasingly, the added fertilizer anti-caking agents are mainly water-soluble liquid anti-caking agents, and the liquid anti-caking agents are high in water solubility, clear, transparent and colorless, can not be used for visually judging the uniformity and uniformity of the wrapped fertilizers after being sprayed on the surfaces of the fertilizers and can not give early warning and precaution to the caking risk of the fertilizers after being stored.
In addition, since moisture contained in the fertilizer remains in the fertilizer in the form of a saturated solution and continuously permeates between fertilizer particles, it is crystallized out when the ambient temperature and humidity are changed. With the repetition of the "dissolution-crystallization" process, salt bridges are formed between the fertilizer granules, eventually leading to caking of the fertilizer. Therefore, whether the anti-caking agent is uniformly wrapped on the surface of the fertilizer is very important, and the anti-caking agent is also a precondition for ensuring the anti-caking effect. The anti-caking agent can effectively prevent salt bridges from being generated between fertilizer particles after the surface of the fertilizer is uniformly coated, and plays a positive anti-caking role.
The person skilled in the art of the patent CN205246510U proposes: the experimental device and the experimental method are used for evaluating the anti-caking effect of the anti-caking agent added fertilizer, the anti-caking effect of the anti-caking agent added fertilizer can be evaluated by using the experimental device, the using environment of the fertilizer needs to be simulated after the anti-caking agent added fertilizer enters the experimental device, the fertilizer is stored in the constant-temperature and constant-humidity box for a certain time under the condition of constant pressure, and the fertilizer is taken out to judge the quality of the anti-caking effect after the anti-caking agent is added by testing crushing pressure.
Some water-soluble fertilizers in the market generally take urea, urea-based and nitro-compound fertilizers as main materials, the fertilizers are easier to agglomerate than conventional fertilizers, the corresponding anti-caking agents are water-soluble liquid anti-caking agents, the requirements on the anti-caking agents sprayed on the surfaces of the fertilizers are higher, and the anti-caking agents added are required to be completely and uniformly wrapped on the surfaces of the fertilizers to achieve ideal anti-caking effects, so that a method for quickly judging the wrapping uniformity of the water-soluble liquid anti-caking agents on the surfaces of the fertilizers is established to have far-reaching significance for measuring the quality of the anti-caking effects.
The increasing of the full water-soluble fertilizers in the current market provides a method for rapidly judging the wrapping uniformity of the full water-soluble liquid anti-caking agent on the fertilizer, and is particularly important.
Disclosure of Invention
The invention aims to provide a method for rapidly judging the wrapping uniformity of a fully water-soluble liquid anti-caking agent on a fertilizer. The method has the advantages of low cost, simple operation, convenient use, intuitive judgment, strong detection foundation and high reference practicability, can quickly judge the uniformity of the fully water-soluble liquid anti-caking agent coated on the fertilizer by using the reflected light of a fluorescent lamp after the fluorescent lamp irradiates on the surface of the fertilizer, can truly reflect the uniformity of the coated fertilizer on the surface of the fertilizer in the production process, can better guide the reasonable addition amount of the anti-caking agent in the production process, and ensures that the used liquid anti-caking agent is completely and uniformly coated on the surface of the fertilizer, thereby ensuring that the fertilizer is not caked, keeps loose for a long time, improves the appearance quality of the fertilizer, and is convenient to store and use.
The main technical problems to be solved by the invention are realized by the following scheme:
a method for rapidly judging the wrapping uniformity of a fully water-soluble liquid anti-caking agent on a fertilizer is characterized by comprising the following steps:
(1) adding fluorescent powder into a fully water-soluble liquid anti-caking agent according to the amount accounting for 0.05-0.2 percent of the liquid anti-caking agent, uniformly stirring for 10-30min to completely dissolve the fluorescent powder, and fully and uniformly mixing to ensure that the liquid anti-caking agent presents a corresponding color;
(2) spraying a certain amount of water-soluble liquid anti-caking agent on the surface of the fertilizer, and then taking 10-30 g of the granular fertilizer sprayed with the water-soluble liquid anti-caking agent; the uniform degree of surface wrapping of the fertilizer sprayed with the liquid anticaking agent is judged by using fluorescent lamp irradiation and through fluorescent reflected light reflected by the surface of the granular fertilizer;
(3) evaluation standard of wrapping uniformity: the surface of the fertilizer is irradiated by a fluorescent lamp, and when the whole surface of the fertilizer has uniform fluorescent reflection light, the liquid anti-caking agent is completely and uniformly wrapped on the fertilizer, so that the anti-caking effect is relatively good; when the surface of the fertilizer partially generates fluorescence reflection light, the anti-caking agent on the surface of the fertilizer is not uniformly wrapped, and the anti-caking effect is relatively poor; when the fluorescence reflection light is not seen on the surface of the fertilizer, the liquid anticaking agent is not added on the surface of the fertilizer, and the fertilizer is easy to agglomerate.
The stronger the fluorescence reflection light, the larger the surface area of visible light on the surface of the fertilizer, which shows that the more the wrapping addition amount of the liquid anti-caking agent is, the better the anti-caking performance is; on the contrary, the fluorescence reflection light is weak, and the smaller the surface area of visible light on the surface of the fertilizer, the smaller the wrapping addition amount of the liquid anti-caking agent is, and the anti-caking performance is poorer.
The fluorescent powder is organic fluorescent powder, the particle size is 800-1200 meshes, the particles are fine, and the dispersion is easy. The organic fluorescent powder is organic red fluorescent powder, organic yellow fluorescent powder, organic blue fluorescent powder or organic green fluorescent powder.
The fluorescent lamp is a hand-held ultraviolet fluorescent lamp.
The fertilizer is a granulated fertilizer which is urea, a nitro compound fertilizer or a urea-based compound fertilizer, and the nutrient concentration is higher.
The method has the advantages of low cost, simple operation, convenient use, intuitive judgment, strong detection foundation and high reference practicability, can quickly judge the uniformity of the fully water-soluble liquid anti-caking agent coated on the fertilizer by using the reflected light of the fluorescent lamp after being irradiated on the surface of the fertilizer, can truly reflect the coating uniformity of the added anti-caking agent on the surface of the fertilizer in the production process of the fertilizer, can better guide the reasonable adding amount of the anti-caking agent in the production process of the fertilizer, ensures that the used liquid anti-caking agent is completely and uniformly coated on the surface of the fertilizer, ensures that the fertilizer is not caked, keeps loose for a long time, improves the appearance quality of the fertilizer, and is convenient to store and use.
Detailed Description
The invention will be further described with reference to specific examples:
example 1:
the method for rapidly judging the wrapping uniformity of the fully water-soluble liquid anti-caking agent on the fertilizer comprises the following steps of:
(1) adding organic blue fluorescent powder in an amount which accounts for 0.05 percent of the liquid anti-caking agent into the fully water-soluble liquid anti-caking agent, wherein the particle size and the mesh number of the organic blue fluorescent powder are 800 meshes, stirring at a constant speed for 10min to completely dissolve the organic blue fluorescent powder, and fully and uniformly mixing, wherein the liquid anti-caking agent presents transparent light blue liquid;
(2) spraying 1.0 kilogram of fully water-soluble blue liquid anti-caking agent on the surface of each ton of granular urea (46%), taking out 10 grams of granular urea (46%) sprayed with the fully water-soluble blue liquid anti-caking agent, irradiating the granular urea by using a fluorescent lamp, and judging the uniform degree of surface wrapping of the urea sprayed with the liquid anti-caking agent through blue light reflected by the fluorescent lamp;
(3) evaluation standard of wrapping uniformity: the surface of the urea is irradiated by a fluorescent lamp, and the whole fertilizer only has 1/5 surface blue reflected light, which shows that the liquid anti-caking agent is not uniformly wrapped on the fertilizer and only has about 20 percent of the normal anti-caking effect, so the anti-caking effect is greatly reduced.
Spraying 5.0 kilograms of fully water-soluble blue liquid anti-caking agent on each ton of granular urea (46%) by the same method, and taking 10 grams of granular urea (46%) sprayed with the fully water-soluble blue liquid anti-caking agent; the surface of the granular urea (46%) is irradiated by a fluorescent lamp, and only the surface of the whole fertilizer has uniform blue reflected light, which indicates that the anti-caking agent is uniformly coated on the fertilizer.
The particle urea (46%) sprayed with the fully water-soluble blue liquid anti-caking agent is detected by a CN205246510U device, and the obtained data is shown in the attached table I, which shows that the method provided by the invention is real and effective in judging and evaluating the coating uniformity of the fully water-soluble blue liquid anti-caking agent on the surface of the fertilizer, and the method is simple to operate, convenient to use, intuitive in judgment, strong in detection foundation and high in reference practicability.
A first attached table:
item | Full water-soluble anti-caking agent | Full water-soluble anti-caking agent | Full water-soluble anti-caking agent |
Adding amount of | 0 | 1.0 kg/ton | 5.0 kg/ton |
Uniformity of wrapping | Is not wrapped | Is not wrapped uniformly | Completely wrapped uniformly |
Anti-caking rate% | 0 | 20 | 95 |
Example 2:
the method for rapidly judging the wrapping uniformity of the fully water-soluble liquid anti-caking agent on the fertilizer comprises the following steps of:
(1) adding organic yellow fluorescent powder into a fully water-soluble liquid anti-caking agent according to the amount accounting for 0.1 percent of the liquid anti-caking agent, wherein the particle size of the organic yellow fluorescent powder is 1000 meshes, uniformly stirring for 20min at a uniform speed to completely dissolve the organic yellow fluorescent powder, and fully and uniformly mixing, wherein the liquid anti-caking agent presents transparent light yellow liquid;
(2) spraying 5.0 kilograms of water-soluble yellow liquid anti-caking agent on the surface of each ton of urea-based compound fertilizer (30-5-5), taking out 20 grams of water-soluble yellow liquid anti-caking agent sprayed urea-based compound fertilizer (30-5-5), irradiating by using a fluorescent lamp, and judging the uniform degree of surface wrapping of the compound fertilizer after the liquid anti-caking agent is sprayed on the compound fertilizer through yellow light reflected by the fluorescent lamp;
(3) evaluation standard of wrapping uniformity: the surface of the urea-based compound fertilizer is irradiated by a fluorescent lamp, and yellow reflected light rays are emitted from the surface of the whole fertilizer, so that the liquid anti-caking agent is completely and uniformly wrapped on the fertilizer, and the anti-caking effect can reach more than 90%.
Spraying 3.0 kilograms of fully water-soluble yellow liquid anti-caking agent on the surface of each ton of urea-based compound fertilizer (30-5-5) by the same method, taking out 20 grams of the fully water-soluble yellow liquid anti-caking agent sprayed urea-based compound fertilizer (30-5-5) and irradiating by using a fluorescent lamp, and judging the uniform degree of surface wrapping of the compound fertilizer after the liquid anti-caking agent is sprayed by the compound fertilizer through yellow light reflected by the fluorescent lamp; the yellow reflected light on the surface of the whole fertilizer is only 1/2, which shows that the liquid anti-caking agent is not uniformly wrapped on the fertilizer and only has about 50 percent of the normal anti-caking effect, and the anti-caking effect is greatly reduced.
The urea-based compound fertilizer (30-5-5) sprayed with the fully water-soluble yellow liquid anti-caking agent is detected by adopting a CN205246510U device, and the obtained data is shown as attached table II, which shows that the method judges and evaluates the coating uniformity of the fully water-soluble yellow liquid anti-caking agent on the surface of the fertilizer, and is real and effective, and the method has the advantages of simple operation, convenient use, intuitive judgment, strong detection foundation and high reference practicability.
And B, attaching a table II:
item | Full water-soluble anti-caking agent | Full water-soluble anti-caking agent | Full water-soluble anti-caking agent |
Adding amount of | 0 | 3.0 kg/ton | 5.0 kg/ton |
Uniformity of wrapping | Is not wrapped | Is not wrapped uniformly | Completely wrapped uniformly |
Anti-caking rate% | 0 | 50 | 95 |
Example 3:
the method for rapidly judging the wrapping uniformity of the fully water-soluble liquid anti-caking agent on the fertilizer comprises the following steps of:
(1) adding organic green fluorescent powder with the particle size of 1200 meshes into a fully water-soluble liquid anti-caking agent according to the using amount of 0.2 percent, uniformly stirring for 30min to completely dissolve the organic green fluorescent powder, and fully and uniformly mixing to obtain transparent light green liquid;
(2) spraying 3.0 kg of water-soluble green liquid anti-caking agent on the surface of each ton of nitro-compound fertilizer (25-13-7), taking out 30 g of the water-soluble green liquid anti-caking agent sprayed nitro-compound fertilizer (25-13-7), irradiating by using a fluorescent lamp, and judging the uniform degree of surface wrapping of the compound fertilizer after the liquid anti-caking agent is sprayed on the compound fertilizer through green light reflected by the fluorescent lamp;
(3) evaluation standard of wrapping uniformity: the surface of the nitro compound fertilizer is irradiated by a fluorescent lamp, and the surface of the whole fertilizer 1/2 has green reflected light, which shows that the liquid anti-caking agent is completely and uniformly wrapped on the fertilizer, and the anti-caking effect can only reach 50%.
Spraying 1.0 kg of water-soluble green liquid anti-caking agent on the surface of each ton of nitro-compound fertilizer (25-13-7) by the same method, taking out 30 g of the water-soluble green liquid anti-caking agent sprayed nitro-compound fertilizer (25-13-7) and irradiating by using a fluorescent lamp, and judging the uniform degree of surface wrapping of the compound fertilizer after the liquid anti-caking agent is sprayed by the compound fertilizer through green light reflected by the fluorescent lamp; only 1/5 surfaces of the whole fertilizer have yellow-green reflected light, which shows that the liquid anti-caking agent is not uniformly wrapped on the fertilizer and only has about 20 percent of the normal anti-caking effect, and the anti-caking effect is greatly reduced.
The nitro-compound fertilizer (25-13-7) sprayed with the fully water-soluble green liquid anticaking agent is detected by adopting a CN205246510U device, and the obtained data is shown in the attached table III, which shows that the method judges and evaluates the coating uniformity of the fully water-soluble green liquid anticaking agent on the surface of the fertilizer to be real and effective, and the method has the advantages of simple operation, convenient use, intuitive judgment, strong detection foundation and high reference practicability.
Attaching a third table:
item | Full water-soluble anti-caking agent | Full water-soluble anti-caking agent | Full water-soluble anti-caking agent |
Adding amount of | 0 | 1.0 kg/ton | 3.0 kg/ton |
Uniformity of wrapping | Is not wrapped | Is not wrapped uniformly | Not completely wrapped uniformly |
Anti-caking rate% | 0 | 20 | 55 |
。
Claims (5)
1. A method for rapidly judging the wrapping uniformity of a fully water-soluble liquid anti-caking agent on a fertilizer is characterized by comprising the following steps:
(1) adding fluorescent powder into a fully water-soluble liquid anti-caking agent according to the amount accounting for 0.05-0.2 percent of the liquid anti-caking agent, uniformly stirring for 10-30min at a uniform speed to completely dissolve the fluorescent powder, and fully and uniformly mixing to ensure that the liquid anti-caking agent presents a corresponding color;
(2) spraying a certain amount of water-soluble liquid anti-caking agent on the surface of the fertilizer, and then taking 10-30 g of the granular fertilizer sprayed with the water-soluble liquid anti-caking agent; the uniform degree of surface wrapping of the fertilizer sprayed with the liquid anticaking agent is judged by using fluorescent lamp irradiation and through fluorescent reflected light reflected by the surface of the granular fertilizer;
(3) evaluation standard of wrapping uniformity: the surface of the fertilizer is irradiated by a fluorescent lamp, and when the whole surface of the fertilizer has uniform fluorescent reflection light, the liquid anti-caking agent is completely and uniformly wrapped on the fertilizer, so that the anti-caking effect is relatively good; when the surface of the fertilizer partially generates fluorescence reflection light, the anti-caking agent on the surface of the fertilizer is not uniformly wrapped, and the anti-caking effect is relatively poor; when the fluorescence reflection light is not seen on the surface of the fertilizer, the liquid anticaking agent is not added on the surface of the fertilizer, and the fertilizer is easy to agglomerate.
The stronger the fluorescence reflection light, the larger the surface area of visible light on the surface of the fertilizer, which shows that the more the wrapping addition amount of the liquid anti-caking agent is, the better the anti-caking performance is; on the contrary, the fluorescence reflection light is weak, and the smaller the surface area of visible light on the surface of the fertilizer, the smaller the wrapping addition amount of the liquid anti-caking agent is, and the anti-caking performance is poorer.
2. The method for rapidly judging the wrapping uniformity of the fully water-soluble liquid anti-caking agent on the fertilizer according to claim 1, wherein the fluorescent powder is organic fluorescent powder with the particle size of 800-1200 meshes.
3. The method for rapidly judging the coating uniformity of the fully water-soluble liquid anti-caking agent on the fertilizer according to claim 2, wherein the organic fluorescent powder is organic red fluorescent powder, organic yellow fluorescent powder, organic blue fluorescent powder or organic green fluorescent powder.
4. The method for rapidly judging the uniform wrapping degree of the fully water-soluble liquid anti-caking agent on the fertilizer according to claim 1, which is characterized in that: the fluorescent lamp is a hand-held ultraviolet fluorescent lamp.
5. The method for rapidly judging the uniform wrapping degree of the fully water-soluble liquid anti-caking agent on the fertilizer according to claim 1, which is characterized in that: the fertilizer is a granulated fertilizer which is urea, a nitro compound fertilizer or a urea-based compound fertilizer.
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Cited By (1)
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CN113358603A (en) * | 2021-06-04 | 2021-09-07 | 中国核动力研究设计院 | Solution uniformity evaluation device and method |
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Application publication date: 20210430 |