CN112646650A - Worm gear and worm gear oil and preparation method thereof - Google Patents
Worm gear and worm gear oil and preparation method thereof Download PDFInfo
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- CN112646650A CN112646650A CN202011532419.3A CN202011532419A CN112646650A CN 112646650 A CN112646650 A CN 112646650A CN 202011532419 A CN202011532419 A CN 202011532419A CN 112646650 A CN112646650 A CN 112646650A
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/045—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution and non-macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/02—Hydroxy compounds
- C10M2207/023—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
- C10M2207/026—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings with tertiary alkyl groups
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
- C10M2207/127—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids polycarboxylic
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
- C10M2209/104—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only
- C10M2209/1045—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only used as base material
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
- C10M2215/064—Di- and triaryl amines
- C10M2215/065—Phenyl-Naphthyl amines
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
- C10M2215/223—Five-membered rings containing nitrogen and carbon only
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/08—Thiols; Sulfides; Polysulfides; Mercaptals
- C10M2219/082—Thiols; Sulfides; Polysulfides; Mercaptals containing sulfur atoms bound to acyclic or cycloaliphatic carbon atoms
- C10M2219/083—Dibenzyl sulfide
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/10—Heterocyclic compounds containing sulfur, selenium or tellurium compounds in the ring
- C10M2219/104—Heterocyclic compounds containing sulfur, selenium or tellurium compounds in the ring containing sulfur and carbon with nitrogen or oxygen in the ring
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
- C10M2223/041—Triaryl phosphates
Abstract
The invention belongs to the technical field of metal surface treatment, and particularly relates to worm gear oil and a preparation method thereof. The worm gear oil comprises the following components in parts by weight: 45-80 parts of synthetic lubricating oil PAG, 0.8-1.6 parts of composite antioxidant, 1-5 parts of extreme pressure antiwear agent, 0.05-0.5 part of metal passivator, 1-2.5 parts of corrosion inhibitor and 20-50ppm of defoaming agent. The selected amine antioxidant and the phenol antioxidant are compounded for use, so that the thermal oxidation stability of the worm and gear oil can be obviously improved, and meanwhile, the extreme pressure antiwear additive, the metal passivator and the corrosion inhibitor are selected to further improve the wear resistance, corrosion resistance and rust resistance of the worm and gear oil.
Description
Technical Field
The invention belongs to the technical field of metal surface treatment, and particularly relates to worm gear oil and a preparation method thereof.
Background
The worm and worm gear mechanism has the characteristics of small volume, large transmission speed ratio, stable operation, low noise, large output torque and the like, is usually used for transmitting the motion and the power between two staggered shafts, and has been widely applied. In the worm gear transmission, because the sliding between tooth surfaces is large, the contact time of the teeth is relatively longer than that of the gear transmission, and the friction wear and the heating condition are more serious, the lubrication by adopting common gear oil is not suitable.
The worm gear lubricating oil plays an important role in the transmission of the worm gear, can reduce friction and abrasion, improves the transmission efficiency of the worm gear pair, prolongs the service life of the worm gear, and the like. Along with the development of equipment towards the direction of high speed and heavy load, the problems of short service life, large worm wheel abrasion and the like of the conventional worm gear lubricating oil are often exposed, the transmission efficiency of the worm gear is influenced, and the operation cost is increased.
Disclosure of Invention
The invention aims to provide the worm and gear oil which has excellent thermal oxidation stability and wear resistance and also has excellent corrosion resistance and rust resistance.
The worm gear oil provided by the invention comprises the following components in parts by weight: 45-80 parts of synthetic lubricating oil PAG, 0.8-1.6 parts of composite antioxidant, 1-5 parts of extreme pressure antiwear agent, 0.05-0.5 part of metal passivator, 1-2.5 parts of corrosion inhibitor and 20-50ppm of defoaming agent.
Among these, synthetic lube PAGs can be: PAG VG150, PAG VG320, PAG VG460, or PAG VG 680.
The composite antioxidant is prepared by compounding an amine antioxidant and a phenol antioxidant according to the mass ratio of 3: 5.
Wherein the amine antioxidant is N-phenyl-alpha-naphthylamine;
the phenolic antioxidant is 2, 6-di-tert-butyl-p-cresol or 2, 4-dimethyl-6-tert-butylphenol.
The extreme pressure antiwear agent is one of tricresyl phosphate, sulfurized isobutylene, dibenzyl disulfide, amino thioester, or thiophosphoramine.
The metal passivator is one of benzotriazole, 2-mercaptobenzothiazole or 2-mercaptobenzothiazole sodium.
The corrosion inhibitor is barium dinonylnaphthalene sulfonate or dodecenylsuccinic acid.
The invention also provides a preparation method of the worm and gear oil, which comprises the step of mixing the synthetic lubricating oil, the composite antioxidant, the metal passivator, the corrosion inhibitor, the extreme pressure antiwear additive and the defoaming agent to obtain the worm and gear oil.
Has the advantages that:
according to the invention, the amine antioxidant and the phenol antioxidant are compounded for use, so that the thermal oxidation stability of the worm gear oil can be obviously improved, and meanwhile, the extreme pressure antiwear additive, the metal passivator and the corrosion inhibitor are selected to further improve the wear resistance, corrosion resistance and rust resistance of the worm gear oil.
Detailed Description
The present invention is further described below with reference to examples, but is not limited thereto.
Example 1
PAG 15045 parts of synthetic lubricating oil PAG VG, 0.45 part of N-phenyl-alpha-naphthylamine, 0.75 part of 2, 6-di-tert-butyl-p-cresol, 3 parts of tricresyl phosphate, 0.1 part of benzotriazole, 1 part of barium dinonyl naphthalene sulfonate and 20ppm of defoaming agent.
And mixing synthetic lubricating oil PAG VG150, N-phenyl-alpha-naphthylamine, 2, 6-di-tert-butyl-p-cresol, tricresyl phosphate, benzotriazole, barium dinonyl naphthalenesulfonate and a defoaming agent to obtain the worm gear oil.
Example 2
Synthetic lubricating oil PAG VG 32060 parts, N-phenyl-alpha-naphthylamine 0.45 parts, 2, 6-di-tert-butyl-p-cresol 0.75 parts, dibenzyl disulfide 3 parts, 2-mercaptobenzothiazole 0.2 parts, dodecenyl succinic acid 2 parts and defoaming agent 30 ppm.
The preparation method of the worm gear oil is the same as that of the embodiment 1.
Example 3
Synthetic lubricating oil PAG VG 46080 parts, N-phenyl-alpha-naphthylamine 0.45 part, 2, 4-dimethyl-6-tert-butylphenol 0.75 part, dibenzyl disulfide 5 parts, 2-mercaptobenzothiazole 0.5 part, dodecenylsuccinic acid 2.5 parts and defoaming agent 30 ppm.
The preparation method of the worm gear oil is the same as that of the embodiment 1.
Example 4
Synthetic lubricating oil PAG VG 32060 parts, N-phenyl-alpha-naphthylamine 0.3 parts, 2, 6-di-tert-butyl-p-cresol 0.5 parts, dibenzyl disulfide 2 parts, 2-mercaptobenzothiazole 0.5 parts, dodecenyl succinic acid 1.5 parts and defoaming agent 30 ppm.
The preparation method of the worm gear oil is the same as that of the embodiment 1.
Example 5
Synthetic lubricating oil PAG (PolyGenyl amine) VG 68070 parts, N-phenyl-alpha-naphthylamine 0.6 parts, 2, 6-di-tert-butyl-p-cresol 1 part, dibenzyl disulfide 3 parts, 2-mercaptobenzothiazole 0.2 part, dodecenyl succinic acid 2 parts and defoaming agent 50 ppm.
The preparation method of the worm gear oil is the same as that of the embodiment 1.
Comparative example 1
Synthetic lubricating oil PAG VG 32060 parts, N-phenyl-alpha-naphthylamine 1.2 parts, dibenzyl disulfide 3 parts, 2-mercaptobenzothiazole 0.2 part, dodecenyl succinic acid 2 parts and defoaming agent 30 ppm.
The preparation method of the worm gear oil is the same as that of the embodiment 2.
Comparative example 2
Synthetic lubricating oil PAG VG 32060 parts, 2, 6-di-tert-butyl-p-cresol 1.2 parts, dibenzyl disulfide 3 parts, 2-mercaptobenzothiazole 0.2 part, dodecenyl succinic acid 2 parts and defoaming agent 30 ppm.
The preparation method of the worm gear oil is the same as that of the embodiment 2.
Comparative example 3
Synthetic lubricating oil PAG VG 32060 parts, N-phenyl-alpha-naphthylamine 0.4 parts, 2, 6-di-tert-butyl-p-cresol 0.8 parts, dibenzyl disulfide 3 parts, 2-mercaptobenzothiazole 0.2 parts, dodecenyl succinic acid 2 parts and defoaming agent 30 ppm.
The preparation method of the worm gear oil is the same as that of the embodiment 2.
Comparative example 4
Synthetic lubricating oil PAG VG 32060 parts, N-phenyl-alpha-naphthylamine 0.5 parts, 2, 6-di-tert-butyl-p-cresol 0.7 parts, dibenzyl disulfide 3 parts, 2-mercaptobenzothiazole 0.2 parts, dodecenyl succinic acid 2 parts and defoaming agent 30 ppm.
The preparation method of the worm gear oil is the same as that of the embodiment 2.
Comparative example 5
Synthetic lubricating oil PAG VG 32060 parts, octyl diphenylamine 0.45 part, 2, 6-di-tert-butyl-p-cresol 0.75 part, dibenzyl disulfide 3 parts, 2-mercaptobenzothiazole 0.2 part, dodecenyl succinic acid 2 parts, and defoaming agent 30 ppm.
The preparation method of the worm gear oil is the same as that of the embodiment 2.
The thermal oxidation stability of the worm and gear oils prepared in the examples of the present invention and the comparative examples is shown in Table 1.
TABLE 1
The present invention is not limited to the above-described embodiments, and any obvious improvements, substitutions or modifications can be made by those skilled in the art without departing from the spirit of the present invention.
Claims (8)
1. The worm and gear oil is characterized by comprising the following components in parts by weight: 45-80 parts of synthetic lubricating oil PAG, 0.8-1.6 parts of composite antioxidant, 1-5 parts of extreme pressure antiwear agent, 0.05-0.5 part of metal passivator, 1-2.5 parts of corrosion inhibitor and 20-50ppm of defoaming agent.
2. The worm-gear oil according to claim 1, characterized in that the synthetic lubricant PAG is: PAG VG150, PAG VG320, PAG VG460, or PAG VG 680.
3. The worm and gear oil as claimed in claim 1, wherein the compound antioxidant is compounded by an amine antioxidant and a phenol antioxidant according to a mass ratio of 3: 5.
4. The worm-gear oil according to claim 3, wherein the amine antioxidant is N-phenyl- α -naphthylamine; the phenolic antioxidant is 2, 6-di-tert-butyl-p-cresol or 2, 4-dimethyl-6-tert-butylphenol.
5. The worm-gear oil as claimed in claim 1, wherein the extreme pressure antiwear agent is one of tricresyl phosphate, sulfurized isobutylene, dibenzyl disulfide, aminothioester, or thiophosphoramine.
6. The worm-gear oil as claimed in claim 1, wherein the metal deactivator is one of benzotriazole, 2-mercaptobenzothiazole or sodium 2-mercaptobenzothiazole.
7. The worm-gear oil according to claim 1, wherein the corrosion inhibitor is barium dinonylnaphthalene sulfonate or dodecenylsuccinic acid.
8. The preparation method of the worm and gear oil according to claim 1, characterized by comprising the following steps: and mixing the synthetic lubricating oil, the composite antioxidant, the metal passivator, the corrosion inhibitor, the extreme pressure antiwear additive and the defoaming agent to obtain the worm gear oil.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2020114493404 | 2020-12-11 | ||
| CN202011449340 | 2020-12-11 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN112646650A true CN112646650A (en) | 2021-04-13 |
| CN112646650B CN112646650B (en) | 2022-08-19 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202011532419.3A Active CN112646650B (en) | 2020-12-11 | 2020-12-23 | Worm gear and worm gear oil and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113263300A (en) * | 2021-04-30 | 2021-08-17 | 四川固锐德科技有限公司 | Worm gear and worm for heavy-duty vehicle main reducing system and preparation method thereof |
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| JP2004331933A (en) * | 2003-05-10 | 2004-11-25 | Tonengeneral Sekiyu Kk | Lubricating oil composition |
| JP2008274190A (en) * | 2007-05-07 | 2008-11-13 | Cosmo Sekiyu Lubricants Kk | Gear oil composition |
| CN101469288A (en) * | 2007-12-25 | 2009-07-01 | 中国科学院兰州化学物理研究所 | Lubricant composition for exposed gear |
| CN102766508A (en) * | 2011-05-06 | 2012-11-07 | 中国石油天然气股份有限公司 | Long-life fully synthetic industrial gear lubricant composition |
| CN103194302A (en) * | 2013-04-19 | 2013-07-10 | 上海禾泰特种润滑技术有限公司 | Worm gear oil composition and preparation method thereof |
| CN103289797A (en) * | 2013-06-18 | 2013-09-11 | 上海禾泰特种润滑技术有限公司 | Worm and gear oil composition and preparation method thereof |
| CN103740444A (en) * | 2012-09-20 | 2014-04-23 | 中国石油化工股份有限公司 | Gear oil composition and applications thereof |
| CN104130823A (en) * | 2014-07-29 | 2014-11-05 | 中国石油化工股份有限公司 | Antioxidant composition, application thereof and industrial gear oil containing the same |
| CN104450107A (en) * | 2015-01-04 | 2015-03-25 | 吴江华威特种油有限公司 | Lubricating oil for gear |
| CN108587753A (en) * | 2018-06-22 | 2018-09-28 | 郑州正赢石化有限公司 | Gear lubricating oil composition |
-
2020
- 2020-12-23 CN CN202011532419.3A patent/CN112646650B/en active Active
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004331933A (en) * | 2003-05-10 | 2004-11-25 | Tonengeneral Sekiyu Kk | Lubricating oil composition |
| JP2008274190A (en) * | 2007-05-07 | 2008-11-13 | Cosmo Sekiyu Lubricants Kk | Gear oil composition |
| CN101469288A (en) * | 2007-12-25 | 2009-07-01 | 中国科学院兰州化学物理研究所 | Lubricant composition for exposed gear |
| CN102766508A (en) * | 2011-05-06 | 2012-11-07 | 中国石油天然气股份有限公司 | Long-life fully synthetic industrial gear lubricant composition |
| CN103740444A (en) * | 2012-09-20 | 2014-04-23 | 中国石油化工股份有限公司 | Gear oil composition and applications thereof |
| CN103194302A (en) * | 2013-04-19 | 2013-07-10 | 上海禾泰特种润滑技术有限公司 | Worm gear oil composition and preparation method thereof |
| CN103289797A (en) * | 2013-06-18 | 2013-09-11 | 上海禾泰特种润滑技术有限公司 | Worm and gear oil composition and preparation method thereof |
| CN104130823A (en) * | 2014-07-29 | 2014-11-05 | 中国石油化工股份有限公司 | Antioxidant composition, application thereof and industrial gear oil containing the same |
| CN104450107A (en) * | 2015-01-04 | 2015-03-25 | 吴江华威特种油有限公司 | Lubricating oil for gear |
| CN108587753A (en) * | 2018-06-22 | 2018-09-28 | 郑州正赢石化有限公司 | Gear lubricating oil composition |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113263300A (en) * | 2021-04-30 | 2021-08-17 | 四川固锐德科技有限公司 | Worm gear and worm for heavy-duty vehicle main reducing system and preparation method thereof |
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| CN112646650B (en) | 2022-08-19 |
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