CN112609448A - Fabric capable of repelling mosquitoes lastingly and preparation method thereof - Google Patents
Fabric capable of repelling mosquitoes lastingly and preparation method thereof Download PDFInfo
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- CN112609448A CN112609448A CN202011393392.4A CN202011393392A CN112609448A CN 112609448 A CN112609448 A CN 112609448A CN 202011393392 A CN202011393392 A CN 202011393392A CN 112609448 A CN112609448 A CN 112609448A
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- 239000004744 fabric Substances 0.000 title claims abstract description 144
- 241000255925 Diptera Species 0.000 title claims abstract description 33
- 230000001846 repelling effect Effects 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- 238000000034 method Methods 0.000 claims abstract description 18
- 230000001442 anti-mosquito Effects 0.000 claims abstract description 11
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 45
- 238000009991 scouring Methods 0.000 claims description 45
- 238000004061 bleaching Methods 0.000 claims description 37
- 239000000243 solution Substances 0.000 claims description 31
- 238000005406 washing Methods 0.000 claims description 30
- 239000007788 liquid Substances 0.000 claims description 29
- 239000003795 chemical substances by application Substances 0.000 claims description 25
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 24
- 239000012224 working solution Substances 0.000 claims description 20
- 238000007639 printing Methods 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- 239000002585 base Substances 0.000 claims description 15
- 230000001590 oxidative effect Effects 0.000 claims description 15
- 239000003513 alkali Substances 0.000 claims description 14
- 238000010025 steaming Methods 0.000 claims description 13
- 238000004043 dyeing Methods 0.000 claims description 12
- 230000008569 process Effects 0.000 claims description 12
- 239000008367 deionised water Substances 0.000 claims description 10
- 229910021641 deionized water Inorganic materials 0.000 claims description 10
- 238000005096 rolling process Methods 0.000 claims description 10
- 238000001035 drying Methods 0.000 claims description 8
- 229920000058 polyacrylate Polymers 0.000 claims description 8
- 239000012744 reinforcing agent Substances 0.000 claims description 8
- 239000000344 soap Substances 0.000 claims description 8
- 238000005517 mercerization Methods 0.000 claims description 7
- 102000004190 Enzymes Human genes 0.000 claims description 6
- 108090000790 Enzymes Proteins 0.000 claims description 6
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 6
- 238000007598 dipping method Methods 0.000 claims description 6
- 239000000986 disperse dye Substances 0.000 claims description 6
- 229940088598 enzyme Drugs 0.000 claims description 6
- 239000000077 insect repellent Substances 0.000 claims description 6
- 230000002265 prevention Effects 0.000 claims description 6
- 239000000984 vat dye Substances 0.000 claims description 6
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 5
- 229920002472 Starch Polymers 0.000 claims description 5
- 238000004040 coloring Methods 0.000 claims description 5
- 238000009980 pad dyeing Methods 0.000 claims description 5
- 230000009467 reduction Effects 0.000 claims description 5
- 238000007493 shaping process Methods 0.000 claims description 5
- 238000009999 singeing Methods 0.000 claims description 5
- 235000010413 sodium alginate Nutrition 0.000 claims description 5
- 229940005550 sodium alginate Drugs 0.000 claims description 5
- 239000000661 sodium alginate Substances 0.000 claims description 5
- JVBXVOWTABLYPX-UHFFFAOYSA-L sodium dithionite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])=O JVBXVOWTABLYPX-UHFFFAOYSA-L 0.000 claims description 5
- 235000019698 starch Nutrition 0.000 claims description 5
- 239000008107 starch Substances 0.000 claims description 5
- 108090000145 Bacillolysin Proteins 0.000 claims description 3
- 108091005658 Basic proteases Proteins 0.000 claims description 3
- 108010059892 Cellulase Proteins 0.000 claims description 3
- 108091005507 Neutral proteases Proteins 0.000 claims description 3
- 102000035092 Neutral proteases Human genes 0.000 claims description 3
- 229940106157 cellulase Drugs 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 238000007790 scraping Methods 0.000 claims description 3
- VGKYEIFFSOPYEW-UHFFFAOYSA-N 2-methyl-4-[(4-phenyldiazenylphenyl)diazenyl]phenol Chemical compound Cc1cc(ccc1O)N=Nc1ccc(cc1)N=Nc1ccccc1 VGKYEIFFSOPYEW-UHFFFAOYSA-N 0.000 claims description 2
- WBCXRDHKXHADQF-UHFFFAOYSA-N 4,11-diamino-2-(3-methoxypropyl)naphtho[2,3-f]isoindole-1,3,5,10-tetrone Chemical compound O=C1C2=CC=CC=C2C(=O)C2=C1C(N)=C(C(N(CCCOC)C1=O)=O)C1=C2N WBCXRDHKXHADQF-UHFFFAOYSA-N 0.000 claims description 2
- 229960001506 brilliant green Drugs 0.000 claims description 2
- HXCILVUBKWANLN-UHFFFAOYSA-N brilliant green cation Chemical compound C1=CC(N(CC)CC)=CC=C1C(C=1C=CC=CC=1)=C1C=CC(=[N+](CC)CC)C=C1 HXCILVUBKWANLN-UHFFFAOYSA-N 0.000 claims description 2
- HRMOLDWRTCFZRP-UHFFFAOYSA-L disodium 5-acetamido-3-[(4-acetamidophenyl)diazenyl]-4-hydroxynaphthalene-2,7-disulfonate Chemical compound [Na+].OC1=C(C(=CC2=CC(=CC(=C12)NC(C)=O)S(=O)(=O)[O-])S(=O)(=O)[O-])N=NC1=CC=C(C=C1)NC(C)=O.[Na+] HRMOLDWRTCFZRP-UHFFFAOYSA-L 0.000 claims description 2
- TUXJTJITXCHUEL-UHFFFAOYSA-N disperse red 11 Chemical compound C1=CC=C2C(=O)C3=C(N)C(OC)=CC(N)=C3C(=O)C2=C1 TUXJTJITXCHUEL-UHFFFAOYSA-N 0.000 claims description 2
- 230000003449 preventive effect Effects 0.000 claims description 2
- 238000007670 refining Methods 0.000 claims description 2
- HHKPGQSPFVLKMV-UHFFFAOYSA-N vat olive green b Chemical compound N1C(C2=C(C(C3=CC=CC=C3C2=O)=O)C=C2)=C2C2=CC=C3C(=O)C4=CC=CC=C4C4=CC=C1C2=C43 HHKPGQSPFVLKMV-UHFFFAOYSA-N 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 11
- 206010020751 Hypersensitivity Diseases 0.000 abstract description 2
- 208000026935 allergic disease Diseases 0.000 abstract description 2
- 230000007815 allergy Effects 0.000 abstract description 2
- 230000000638 stimulation Effects 0.000 abstract description 2
- 231100000956 nontoxicity Toxicity 0.000 abstract 1
- 230000000704 physical effect Effects 0.000 abstract 1
- 239000004753 textile Substances 0.000 description 8
- 206010003399 Arthropod bite Diseases 0.000 description 3
- 239000002131 composite material Substances 0.000 description 3
- 238000009940 knitting Methods 0.000 description 3
- 241000238631 Hexapoda Species 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 230000003385 bacteriostatic effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 231100000989 no adverse effect Toxicity 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/38—Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with hydrogen peroxide or peroxides of metals; with persulfuric, permanganic, pernitric, percarbonic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
- D06M16/003—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic with enzymes or microorganisms
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/04—After-treatment with organic compounds
- D06P5/08—After-treatment with organic compounds macromolecular
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/10—After-treatment with compounds containing metal
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/20—Physical treatments affecting dyeing, e.g. ultrasonic or electric
- D06P5/2066—Thermic treatments of textile materials
- D06P5/2077—Thermic treatments of textile materials after dyeing
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Microbiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dispersion Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention discloses a fabric capable of repelling mosquitoes lastingly and a preparation method thereof. After the fabric is treated by the method disclosed by the invention, the fabric can keep a good anti-mosquito effect after being washed for 50 times, the physical properties of the fabric, such as appearance, strength and the like, are not lost, and the fabric has no stimulation to skin, no allergy phenomenon, safety to a human body, no toxicity and comfort to wear.
Description
Technical Field
The invention belongs to the technical field of special fabrics, and particularly relates to a fabric capable of repelling mosquitoes permanently and a preparation method thereof.
Background
The textile fabric is mainly used for manufacturing home textiles, clothes or medical textiles and has various types. With the diversification of market demands, the functionality of the fabric is more and more valued by people. Along with the continuous improvement of living standard, people have higher and higher requirements on the function of the garment fabric, besides the requirement of normal warm keeping function of the garment, the garment also has the requirement of mosquito bite prevention, and along with the hot summer, the mosquito bite phenomenon is too old for adults and children. Skin is red and swollen slightly after being bitten by mosquitoes and insects, diseases are infected seriously, and daily life is seriously influenced. Therefore, the development of a textile fabric capable of preventing mosquito bites and having good washability is an engineering with great market and social benefits.
According to the data, the world health organization advocates that the mosquito net is soaked with an insecticide, so that the fabric has the function of killing or expelling insects. Years of practice prove that good effects are generally obtained. However, after treatment, the durability of mosquito repelling is weak, so that the development of a mosquito repelling textile with good mosquito repelling effect and lasting efficacy and a bacteriostatic action is an urgent problem to be solved at present.
Disclosure of Invention
Aiming at the prior art, the invention provides a fabric capable of repelling mosquitoes permanently and a preparation method thereof, and aims to solve the problem that the existing mosquito-repellent fabric cannot repel mosquitoes for a long time.
In order to achieve the purpose, the invention adopts the technical scheme that: the preparation method of the fabric capable of repelling mosquitoes for a long time is provided, and comprises the following steps:
(1) singeing: removing fuzz on the surface of the fabric to obtain a singed fabric;
(2) scouring and bleaching: padding the singed fabric with scouring and bleaching working solution by adopting a two-dipping and two-rolling mode, and steaming at 90-110 ℃ for 55-70 min to obtain a scouring and bleaching fabric; in the process of padding scouring and bleaching working solution, the vehicle speed is 60-65 m/min, and the liquid carrying rate is 80-90%; the scouring and bleaching working solution comprises the following components in concentration: 10-12 g/L of scouring enzyme, 5-6 g/L of scouring agent, 3-8 g/L of alkali and 6-7 g/L of hydrogen peroxide;
(3) mercerizing: carrying out mercerizing treatment on the scouring and bleaching fabric by using alkali liquor with the concentration of 180-220 g/L to obtain mercerized fabric;
(4) shaping: setting the mercerized fabric at the temperature of 200-220 ℃ and the speed of 85-95 m/min, and rolling to ensure that no crease mark exists, thereby obtaining the set fabric;
(5) dyeing the bottom: dipping and pad-dyeing the mercerized fabric with the base solution to obtain a dyed fabric, wherein the speed of the dipping and pad process is 40-50 m/min, and the liquid carrying rate is 50-70%; the base dyeing solution comprises the following components in parts by mass: 30-50 parts of disperse dye, 10-20 parts of vat dye, 2-3 parts of back permeation preventive, 2-8 parts of infrared-proof regulator HW-013, 2-7 parts of fastness reinforcing agent and 10-60 parts of deionized water;
(6) printing: scraping printing paste on the dyed fabric at the speed of 40-50 m/min to obtain a printed fabric; the printing paste comprises the following components in parts by mass: 30-50 parts of disperse dye, 10-20 parts of vat dye, 10-015 parts of infrared-proof regulator HW-015 parts, 3-5 parts of fastness reinforcing agent, 2-3 parts of sodium alginate paste and 10-60 parts of deionized water;
(7) baking and coloring: baking the printed fabric for 1-2 min at the temperature of 205-210 ℃ at the speed of 40-50 m/min to obtain a color developing fabric;
(8) reduction, color development and soaping: placing the color-developing fabric in a reducing solution, and steaming for 20s at 130-140 ℃; oxidizing in an oxidizing solution for 30-40S; then washing for 60-90 s by using a soaping liquid to obtain a soaped fabric; the reducing solution comprises the following components in concentration: 75-80 g/L of sodium hydroxide, 100-110 g/L of sodium hydrosulfite and 15-18 g/L of starch; the oxidizing solution is hydrogen peroxide with the concentration of 2.5-3 g/L; the soap wash comprises the following components in concentrations: 3-4 g/L of soaping agent and 2-5 g/L of sodium hydroxide; soaping is carried out at a temperature of 95-98 ℃.
(9) Mosquito prevention treatment: padding the soaped fabric with an anti-mosquito finishing liquid, and then drying to obtain a finished fabric; the anti-mosquito finishing liquid comprises an anti-mosquito finishing agent with the concentration of 100-180 g/L and polyacrylate with the concentration of 20-50 g/L;
(10) pre-shrinking: and (4) performing preshrinking treatment on the finished fabric to obtain a finished product.
On the basis of the technical scheme, the invention can be further improved as follows.
Further, the speed of padding the scouring and bleaching working solution in the step (2) is 60m/min, and the liquid carrying rate is 85%; padding the scouring and bleaching working solution, and steaming for 60min at 100 ℃; the bleaching working solution comprises the following components in concentration: 10g/L scouring enzyme, 5g/L scouring agent, 5g/L alkali and 7g/L hydrogen peroxide.
Further, the refining enzyme is alkaline protease 2709, neutral protease ZS724 or cellulase; the scouring agent is soap, Ramipron A or washing powder; the alkali is sodium hydroxide or potassium hydroxide.
Further, the mercerization treatment in the step (3) comprises the following steps: padding the scouring and bleaching fabric with 180-220 g/L alkali liquor with strong tension to ventilate for 60S, then carrying out five-washing and five-washing dealkalization at 75-80 ℃, washing with 90-95 ℃ water until the pH value of the fabric surface is 7.0-8.5, and finishing mercerization.
Further, the speed of padding the base dyeing solution in the step (5) is 45m/min, and the solution carrying rate is 60%.
Further, the speed of padding the printing paste in the step (6) is 45 m/min.
Further, the disperse dye is at least one of disperse black P-G, disperse turquoise blue S-BG, disperse red S-2G and disperse yellow brown S-2R; the vat dye is at least one of vat black G, vat black GM, vat blue CLF, vat blue BS-03, vat red FBB, vat red 6B, vat yellow RK, vat bright yellow 5GF, vat brown RN, vat brown BR, vat brilliant green FFB, vat olive green B and vat grey NC.
Further, the concentration of the mosquito-proof finishing agent in the mosquito-proof finishing liquid is 160g/L, and the concentration of polyacrylate is 40 g/L.
Further, the mosquito-proof finishing agent is a mosquito-proof agent SPA-01.
By adopting the method, the fabric with good mosquito-proof effect can be prepared, and the fabric can still keep good mosquito-proof effect after being washed for many times, so that the aim of repelling mosquitoes for a long time can be fulfilled.
The invention has the beneficial effects that: the invention adopts the mosquito-proof finishing agent and the polyacrylate to process and finish the textile which is frequently contacted with the human body, and under the process conditions of specific temperature, time and the like, a mosquito-repellent medicine film which is insoluble in water and common organic solvents is formed on the surface of the fiber, and the medicine film is firmly attached to the surface of the textile, can emit smell aversive to mosquitoes for a long time, and is unwilling to stay on the textile to achieve the aim of repelling the mosquitoes.
Physical indexes such as appearance, strength and the like of the fabric treated by the method have no adverse effect; after being washed by water for 50 times, the mosquito-proof effect is good; the anti-mosquito finished fabric has no stimulation and allergy to skin, is safe and nontoxic to human bodies and is comfortable to wear.
Detailed Description
The following examples are provided to illustrate specific embodiments of the present invention.
Example 1
The fabric capable of repelling mosquitoes for a long time is prepared by the following steps:
(1) singeing: taking CVC (composite warp knitting) with the specification of 20 × 16/120 × 60 × 63 for camouflage, and removing fuzz on the surface of the fabric to obtain a singed fabric;
(2) scouring and bleaching: padding the singed fabric with scouring and bleaching working solution by adopting a two-padding and two-rolling mode, and steaming at 100 ℃ for 60min to obtain a scouring and bleaching fabric; in the process of padding scouring and bleaching working solution, the vehicle speed is 60m/min, and the liquid carrying rate is 85 percent; the scouring and bleaching working solution comprises the following components in concentration: 270910 g/L of alkaline protease, 5g/L of soap, 5g/L of sodium hydroxide and 7g/L of hydrogen peroxide;
(3) mercerizing: padding the scouring and bleaching fabric with 180-220 g/L alkali liquor with strong tension to ventilate for 60S, then carrying out five-washing and five-washing dealkalization at 75-80 ℃, washing with 90-95 ℃ water until the pH value of the fabric surface is 7.0-8.5, and finishing mercerization.
(4) Shaping: setting the mercerized fabric at the temperature of 200 ℃ at the speed of 90m/min, and rolling to ensure that no crease mark exists, thereby obtaining the set fabric;
(5) dyeing the bottom: dip pad dyeing the base liquor to the mercerized fabric to obtain the dyed base fabric, wherein the speed of the padding process is 45m/min, and the liquor carrying rate is 60%; the base dyeing solution comprises the following components in parts by mass: 40 parts of disperse black P-G, 15 parts of reduced black G, 2 parts of back permeation preventing agent, 5 parts of infrared-proof regulator HW-015 parts, 5 parts of fastness reinforcing agent and 60 parts of deionized water;
(6) printing: padding printing paste on the dyed fabric at the speed of 45m/min to obtain a printed fabric; the printing paste comprises the following components in parts by mass: 40 parts of disperse black P-G, 15 parts of reduced black G, HW-018 parts of infrared-proof regulator, 4 parts of fastness reinforcing agent, 2 parts of sodium alginate paste and 60 parts of deionized water;
(7) baking and coloring: baking the printed fabric for 2min at 205 ℃ at the speed of 45m/min to obtain a color-developing fabric;
(8) reduction, color development and soaping: placing the color-developing fabric in a reducing solution, and steaming at 135 ℃ for 20 s; oxidizing in the oxidizing solution for 30 s; then washing for 80s by using a soaping liquid to obtain a soaped fabric; the reducing solution comprises the following components in concentration: 75g/L of sodium hydroxide, 105g/L of sodium hydrosulfite and 16g/L of starch; the oxidizing solution is hydrogen peroxide with the concentration of 3 g/L; the soap wash comprises the following components in concentrations: soaping agent 4g/L and sodium hydroxide 2 g/L; soaping was carried out at a temperature of 95 ℃.
(9) Mosquito prevention treatment: padding the soaped fabric with an anti-mosquito finishing liquid, and then drying to obtain a finished fabric, wherein the liquid carrying rate in the padding process is 60%, and the drying temperature is 135 ℃; the mosquito-proof finishing liquid comprises a mosquito-proof agent SPA-01 with the concentration of 160g/L and polyacrylate with the concentration of 40 g/L;
(10) pre-shrinking: and (4) performing preshrinking treatment on the finished fabric to obtain a finished product.
Example 2
The fabric capable of repelling mosquitoes for a long time is prepared by the following steps:
(1) singeing: taking CVC (composite warp knitting) with the specification of 20 × 16/120 × 60 × 63 for camouflage, and removing fuzz on the surface of the fabric to obtain a singed fabric;
(2) scouring and bleaching: padding the singed fabric with scouring and bleaching working solution by adopting a two-padding and two-rolling mode, and steaming at 90 ℃ for 70min to obtain a scouring and bleaching fabric; in the process of padding scouring and bleaching working solution, the vehicle speed is 65m/min, and the liquid carrying rate is 80 percent; the scouring and bleaching working solution comprises the following components in concentration: neutral protease ZS 72412 g/L, Ramipron A6 g/L, sodium hydroxide 3g/L and hydrogen peroxide 6 g/L;
(3) mercerizing: padding the scouring and bleaching fabric with 180-220 g/L alkali liquor with strong tension to ventilate for 60S, then carrying out five-washing and five-washing dealkalization at 75-80 ℃, washing with 90-95 ℃ water until the pH value of the fabric surface is 7.0-8.5, and finishing mercerization
(4) Shaping: setting the mercerized fabric at 220 ℃ at the speed of 95m/min, and rolling to ensure that no crease mark exists, thereby obtaining the set fabric;
(5) dyeing the bottom: dip pad dyeing the base liquor to the mercerized fabric to obtain the dyed base fabric, wherein the speed of the padding process is 40m/min, and the liquor carrying rate is 70%; the base dyeing solution comprises the following components in parts by mass: 30 parts of disperse black P-G, 20 parts of reduced black G, 2 parts of back permeation preventing agent, 2 parts of infrared-proof regulator HW-018 parts, 2 parts of fastness reinforcing agent and 50 parts of deionized water;
(6) printing: padding printing paste on the dyed fabric at the speed of 40m/min to obtain a printed fabric; the printing paste comprises the following components in parts by mass: 30 parts of disperse black P-G, 20 parts of reduced black G, 20 parts of infrared-proof regulator HW-015 parts, 5 parts of fastness reinforcing agent, 2 parts of sodium alginate paste and 50 parts of deionized water;
(7) baking and coloring: baking the printed fabric for 1min at the temperature of 210 ℃ at the speed of 50m/min to obtain a color-developing fabric;
(8) reduction, color development and soaping: placing the color-developing fabric in a reducing solution, and steaming at 130 ℃ for 20 s; oxidizing in the oxidizing solution for 40 s; then washing for 90s by using a soaping liquid to obtain a soaped fabric; the reducing solution comprises the following components in concentration: 80g/L of sodium hydroxide, 100g/L of sodium hydrosulfite and 18g/L of starch; the oxidizing solution is hydrogen peroxide with the concentration of 3 g/L; the soap wash comprises the following components in concentrations: soaping agent 3g/L and sodium hydroxide 5 g/L; soaping was carried out at a temperature of 98 ℃.
(9) Mosquito prevention treatment: padding the soaped fabric with an anti-mosquito finishing liquid, and then drying to obtain a finished fabric, wherein the padding liquid carrying rate is 55%, and the drying temperature is 130 ℃; the mosquito-proof finishing liquid comprises a mosquito-proof agent SPA-01 with the concentration of 100g/L and polyacrylate with the concentration of 50 g/L;
(10) pre-shrinking: and (4) performing preshrinking treatment on the finished fabric to obtain a finished product.
Example 3
The fabric capable of repelling mosquitoes for a long time is prepared by the following steps:
(1) singeing: taking CVC (composite warp knitting) with the specification of 20 × 16/120 × 60 × 63 for camouflage, and removing fuzz on the surface of the fabric to obtain a singed fabric;
(2) scouring and bleaching: padding the singed fabric with scouring and bleaching working solution in a two-padding and two-rolling mode, and steaming at 100 ℃ for 55min to obtain a scouring and bleaching fabric; the vehicle speed is 60m/min, and the liquid carrying rate is 90 percent; the scouring and bleaching working solution comprises the following components in concentration: 10g/L of cellulase, 6g/L of washing powder, 8g/L of sodium hydroxide and 7g/L of hydrogen peroxide;
(3) mercerizing: padding the scouring and bleaching fabric with 180-220 g/L alkali liquor with strong tension to ventilate for 60S, then carrying out five-washing and five-washing dealkalization at 75-80 ℃, washing with 90-95 ℃ water until the pH value of the fabric surface is 7.0-8.5, and finishing mercerization
(4) Shaping: setting the mercerized fabric at the temperature of 200 ℃ and the speed of 85m/min, and rolling to ensure that no crease mark exists, thereby obtaining the set fabric;
(5) dyeing the bottom: dip pad dyeing the base liquor to the mercerized fabric to obtain the dyed base fabric, wherein the speed of the padding process is 50m/min, and the liquor carrying rate is 50%; the base dyeing solution comprises the following components in parts by mass: 50 parts of disperse black P-G, 10 parts of reduced black G and 50 parts of deionized water;
(6) printing: scraping and printing the printing paste on the dyed fabric at the speed of 50m/min by using a rotary screen to obtain a printed fabric; the printing paste comprises the following components in parts by mass: 50 parts of disperse black P-G, 10 parts of reduced black G, 3 parts of sodium alginate paste and 50 parts of deionized water;
(7) baking and coloring: baking the printed fabric for 2min at 205 ℃ at the speed of 40m/min to obtain a color-developing fabric;
(8) reduction, color development and soaping: placing the color-developing fabric in a reducing solution, and steaming at 140 ℃ for 20 s; oxidizing in the oxidizing solution for 30 s; then washing for 60s by using a soaping liquid to obtain a soaped fabric; the reducing solution comprises the following components in concentration: 75g/L of sodium hydroxide, 110g/L of sodium hydrosulfite and 15g/L of starch; the oxidizing solution is hydrogen peroxide with the concentration of 2.5 g/L; the soap wash comprises the following components in concentrations: soaping agent 4g/L and sodium hydroxide 5 g/L; soaping was carried out at a temperature of 95 ℃.
(9) Mosquito prevention treatment: and padding the soaped fabric with the anti-mosquito finishing liquid, and then drying to obtain the finished fabric. The padding liquid rate is 70%, and the drying temperature is 140 ℃; the mosquito-proof finishing liquid comprises a mosquito-proof agent SPA-01 with the concentration of 180g/L and polyacrylate with the concentration of 20 g/L;
(10) pre-shrinking: and (4) performing preshrinking treatment on the finished fabric to obtain a finished product.
Analysis of results
The mosquito repellent effect of the fabrics obtained in each of the above examples before washing and after 50 times of washing was examined, and the results are shown in table 1.
TABLE 1 mosquito repellent Effect of fabrics
Fabric | Mosquito-repellent effect before washing (mg/m)2) | Mosquito-proof effect (mg/m) after washing for 50 times2) |
Example 1 | 1290 | 927 |
Example 2 | 1139 | 901 |
Example 3 | 1310 | 952 |
CVC camouflage | 860 | 227 |
As can be seen from Table 1, after the fabric is treated by the method disclosed by the invention, the anti-mosquito effect before washing is obviously improved, and after the fabric is washed for multiple times, a better anti-mosquito effect can be still maintained, so that the obtained fabric can durably prevent mosquitoes.
In addition, the mechanical properties of the fabrics obtained before and after 50 washes were examined and the results are shown in table 2.
TABLE 2 mechanical Properties of the fabrics
As can be seen from Table 2, the mechanical properties of the fabric treated by the method of the present invention before washing are greatly improved, and the mechanical properties are excellent; and the fabric can still keep good mechanical property after being washed for many times, which shows that the fabric obtained by the method has good washing fastness.
While the present invention has been described in detail with reference to the embodiments, it should not be construed as limited to the scope of the patent. Various modifications and changes may be made by those skilled in the art without inventive faculty within the scope of the claims set forth herein.
Claims (10)
1. The preparation method of the fabric capable of repelling mosquitoes for a long time is characterized by comprising the following steps:
(1) singeing: removing fuzz on the surface of the fabric to obtain a singed fabric;
(2) scouring and bleaching: padding the singed fabric with scouring and bleaching working solution by adopting a two-dipping and two-rolling mode, and steaming at 90-110 ℃ for 55-70 min to obtain a scouring and bleaching fabric; in the process of padding scouring and bleaching working solution, the vehicle speed is 60-65 m/min, and the liquid carrying rate is 80-90%; the scouring and bleaching working solution comprises the following components in concentration: 10-12 g/L of scouring enzyme, 5-6 g/L of scouring agent, 3-8 g/L of alkali and 6-7 g/L of hydrogen peroxide;
(3) mercerizing: carrying out mercerizing treatment on the scouring and bleaching fabric by using alkali liquor with the concentration of 180-220 g/L to obtain mercerized fabric;
(4) shaping: setting the mercerized fabric at the temperature of 200-220 ℃ and the speed of 85-95 m/min, and rolling to ensure that no crease mark exists, thereby obtaining the set fabric;
(5) dyeing the bottom: dipping and pad-dyeing the mercerized fabric with the base solution to obtain a dyed fabric, wherein the speed of the dipping and pad process is 40-50 m/min, and the liquid carrying rate is 50-70%; the base dyeing solution comprises the following components in parts by mass: 30-50 parts of disperse dye, 10-20 parts of vat dye, 2-3 parts of back permeation preventive, 2-8 parts of infrared-proof regulator HW-013, 2-7 parts of fastness reinforcing agent and 10-60 parts of deionized water;
(6) printing: scraping printing paste on the dyed fabric at the speed of 40-50 m/min to obtain printed fabric; the printing paste comprises the following components in parts by mass: 30-50 parts of disperse dye, 10-20 parts of vat dye, 10-015 parts of infrared-proof regulator HW-015 parts, 3-5 parts of fastness reinforcing agent, 2-3 parts of sodium alginate paste and 10-60 parts of deionized water;
(7) baking and coloring: baking the printed fabric for 1-2 min at the temperature of 205-210 ℃ at the speed of 40-50 m/min to obtain a color developing fabric;
(8) reduction, color development and soaping: placing the color-developing fabric in a reducing solution, and steaming for 20s at 130-140 ℃; oxidizing in the oxidizing solution for 30-40 s; then washing for 60-90 s by using a soaping liquid to obtain a soaped fabric; the reducing solution comprises the following components in concentration: 75-80 g/L of sodium hydroxide, 100-110 g/L of sodium hydrosulfite and 15-18 g/L of starch; the oxidizing solution is hydrogen peroxide with the concentration of 2.5-3 g/L; the soap wash comprises the following components in concentrations: 3-4 g/L of soaping agent and 2-5 g/L of sodium hydroxide; soaping is carried out at a temperature of 95-98 ℃.
(9) Mosquito prevention treatment: padding the soaped fabric with an anti-mosquito finishing liquid, and then drying to obtain a finished fabric; the mosquito-proof finishing liquid comprises a mosquito-proof finishing agent with the concentration of 100-180 g/L and polyacrylate with the concentration of 20-50 g/L;
(10) pre-shrinking: and (4) performing preshrinking treatment on the finished fabric to obtain a finished product.
2. The preparation method of the fabric capable of repelling mosquitoes permanently as claimed in claim 1, wherein the preparation method comprises the following steps: the speed of padding the scouring and bleaching working solution in the step (2) is 60m/min, and the liquid carrying rate is 85 percent; padding the scouring and bleaching working solution, and steaming for 60min at 100 ℃; the bleaching working solution comprises the following components in concentration: 10g/L scouring enzyme, 5g/L scouring agent, 5g/L alkali and 7g/L hydrogen peroxide.
3. The preparation method of the fabric capable of repelling mosquitoes permanently as claimed in claim 1 or 2, wherein: the refining enzyme is alkaline protease 2709, neutral protease ZS724 or cellulase; the scouring agent is soap, ramination A or washing powder; the alkali is sodium hydroxide or potassium hydroxide.
4. The preparation method of the fabric capable of permanently repelling mosquitoes according to claim 1, wherein the mercerization treatment in the step (3) comprises the following steps: padding the scouring and bleaching fabric with an alkali liquor with the concentration of 180-220 g/L by adopting a five-washing and five-washing mode, then steaming at 75-80 ℃ to remove alkali, and then washing with water at 90-95 ℃ until the pH value of the fabric surface is 7.0-7.3, thereby completing the mercerization treatment.
5. The preparation method of the fabric capable of repelling mosquitoes permanently as claimed in claim 1, wherein the preparation method comprises the following steps: the speed of padding the dyeing base solution in the step (5) is 45m/min, and the solution carrying rate is 60%.
6. The preparation method of the fabric capable of repelling mosquitoes permanently as claimed in claim 1, wherein the preparation method comprises the following steps: and (4) the speed of padding the printing paste in the step (6) is 45 m/min.
7. The preparation method of the fabric capable of repelling mosquitoes permanently as claimed in claim 1, wherein the preparation method comprises the following steps: the disperse dye is at least one of disperse black P-G, disperse turquoise blue S-BG, disperse red S-2G and disperse yellow brown S-2R; the vat dye is at least one of vat black G, vat black GM, vat blue CLF, vat blue BS-03, vat red FBB, vat red 6B, vat yellow RK, vat bright yellow 5GF, vat brown RN, vat brown BR, vat brilliant green FFB, vat olive green B and vat grey NC.
8. The preparation method of the fabric capable of repelling mosquitoes permanently as claimed in claim 1, wherein the preparation method comprises the following steps: the concentration of the mosquito-proof finishing agent in the mosquito-proof finishing liquid is 160g/L, and the concentration of polyacrylate is 40 g/L.
9. The preparation method of the fabric capable of repelling mosquitoes permanently as claimed in claim 1 or 8, wherein: the mosquito-proof finishing agent is a mosquito-proof agent SPA-01.
10. The durable mosquito repellent fabric prepared by the preparation method of any one of claims 1-9.
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CN102051819A (en) * | 2010-11-19 | 2011-05-11 | 志向(中国)集团有限公司 | Method for producing mosquito prevention textile fabric |
CN105926312A (en) * | 2016-07-12 | 2016-09-07 | 绵阳佳禧印染有限责任公司 | Printing and dyeing method for anti-ant antibacterial anti-infrared camouflage fabric and camouflage fabric |
WO2018018800A1 (en) * | 2016-07-26 | 2018-02-01 | 黄庄芳容 | Method for wet transfer printing of polyester fiber/cotton fiber union fabric |
WO2019000663A1 (en) * | 2017-06-27 | 2019-01-03 | 南通金仕达超微阻燃材料有限公司 | Production method for modal fiber and polyester filament interwoven broad-width jacquard double-color woven fabric |
CN109322153A (en) * | 2018-11-16 | 2019-02-12 | 无锡环中科技服务有限公司 | Mosquito proof camouflage facing material |
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2020
- 2020-12-03 CN CN202011393392.4A patent/CN112609448A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102051819A (en) * | 2010-11-19 | 2011-05-11 | 志向(中国)集团有限公司 | Method for producing mosquito prevention textile fabric |
CN105926312A (en) * | 2016-07-12 | 2016-09-07 | 绵阳佳禧印染有限责任公司 | Printing and dyeing method for anti-ant antibacterial anti-infrared camouflage fabric and camouflage fabric |
WO2018018800A1 (en) * | 2016-07-26 | 2018-02-01 | 黄庄芳容 | Method for wet transfer printing of polyester fiber/cotton fiber union fabric |
WO2019000663A1 (en) * | 2017-06-27 | 2019-01-03 | 南通金仕达超微阻燃材料有限公司 | Production method for modal fiber and polyester filament interwoven broad-width jacquard double-color woven fabric |
CN109322153A (en) * | 2018-11-16 | 2019-02-12 | 无锡环中科技服务有限公司 | Mosquito proof camouflage facing material |
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