CN112500089A - Preparation method of high-viscosity ceramic tile adhesive - Google Patents

Preparation method of high-viscosity ceramic tile adhesive Download PDF

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Publication number
CN112500089A
CN112500089A CN202011620567.0A CN202011620567A CN112500089A CN 112500089 A CN112500089 A CN 112500089A CN 202011620567 A CN202011620567 A CN 202011620567A CN 112500089 A CN112500089 A CN 112500089A
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parts
viscosity
tile
following
portions
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吴伟
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/02Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
    • C04B28/04Portland cements
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474Uses not provided for elsewhere in C04B2111/00
    • C04B2111/00637Uses not provided for elsewhere in C04B2111/00 as glue or binder for uniting building or structural materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2201/00Mortars, concrete or artificial stone characterised by specific physical values
    • C04B2201/10Mortars, concrete or artificial stone characterised by specific physical values for the viscosity

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Adhesives Or Adhesive Processes (AREA)

Abstract

The invention discloses a preparation method of high-viscosity ceramic tile glue, belonging to the technical field of ceramic tile glue and comprising the following raw materials: inorganic portland cement, quartz sand, fine aggregate, biogum, latex powder, cellulose ether, a defoaming agent, alpha-ethyl cyanoacrylate, a tackifier, a stabilizer, a toughening agent, a polymerization inhibitor and a high molecular polymer; the mesh number of the quartz sand is 90-130 meshes; the viscosity of the cellulose ether is 700-58000 Pa.s; according to the invention, the components and the preparation method of the tile adhesive are limited, so that the viscosity of the tile adhesive is improved, and the viscosity of the tile adhesive and the tile is improved due to the matching of the alpha-ethyl cyanoacrylate, the tackifier, the stabilizer, the toughening agent, the polymerization inhibitor and the high molecular polymer; meanwhile, the fine bone powder can be well filled in gaps between the fine bone powder and the ceramic tiles, so that the viscosity of the ceramic tiles and the wall is effectively improved, and the ceramic tile adhesive and the wall surface cannot be hollowly bulged and fall off.

Description

Preparation method of high-viscosity ceramic tile adhesive
Technical Field
The invention belongs to the technical field of ceramic tile glue, and particularly relates to a preparation method of high-viscosity ceramic tile glue.
Background
The tile glue is a modern decoration material for sticking decoration materials such as ceramic tiles, face tiles, floor tiles and the like. The tile glue contains various additives, in particular to the functionality of the tile glue. The general ceramic tile glue is added with cellulose ether for water retention and thickening, and latex powder for increasing the adhesive force of the ceramic tile, and the addition of the latex powder can greatly increase the flexibility of the ceramic tile glue, improve the stress and increase the flexibility. Other additives are added into other tile adhesives with special function requirements. However, with the rapid development of cities, high-rise buildings in cities are clustered, and the tiles on the outer wall are easy to break cars and passersby after slipping off in a large area. The tile glue in the prior art is easy to have the problems of hollowing, falling, low bonding strength, high water absorption, cracking after expansion with heat and contraction with cold and the like.
In order to solve the defects of the prior art, the invention discloses a preparation method of high-viscosity ceramic tile glue, belonging to the technical field of ceramic tile glue and comprising the following raw materials: inorganic portland cement, quartz sand, fine aggregate, biogum, latex powder, cellulose ether, a defoaming agent, alpha-ethyl cyanoacrylate, a tackifier, a stabilizer, a toughening agent, a polymerization inhibitor and a high molecular polymer; the mesh number of the quartz sand is 90-130 meshes; the viscosity of the cellulose ether is 700-58000 Pa.s; according to the invention, the components and the preparation method of the tile adhesive are limited, so that the viscosity of the tile adhesive is improved, and the viscosity of the tile adhesive and the tile is improved due to the matching of the alpha-ethyl cyanoacrylate, the tackifier, the stabilizer, the toughening agent, the polymerization inhibitor and the high molecular polymer; meanwhile, the fine bone powder can be well filled in gaps between the fine bone powder and the ceramic tiles, so that the viscosity of the ceramic tiles and the wall is effectively improved, and the ceramic tile adhesive and the wall surface cannot be hollowly bulged and fall off.
Disclosure of Invention
Technical problem to be solved
Complex construction, low adhesive strength, high water absorption and hollowing
(II) technical scheme
The invention is realized by the following technical scheme:
the preparation method of the high-viscosity tile adhesive comprises the following steps of:
cement 550-650 parts
250 portions of quartz sand and 300 portions of
50-80 parts of fine aggregate
0.01-0.5 part of biological glue
Latex powder 25-50 parts
5-15 parts of cellulose ether
0.2 to 0.4 portion of defoaming agent
10-15 parts of alpha-ethyl cyanoacrylate.
Further, the tile glue is prepared from the following components in parts by weight:
cement 580 and 620 portions
260 portions and 290 portions of quartz sand
60-70 parts of fine aggregate
0.05-0.1 part of biological glue
30-40 parts of latex powder
8-12 parts of cellulose ether
0.35 to 0.38 portion of defoaming agent
12-14 parts of alpha-ethyl cyanoacrylate.
Further, the tile adhesive also comprises the following components in parts by weight: 5.4 to 7.4 portions of tackifier, 4.5 to 6.6 portions of stabilizer, 2.4 to 5.6 portions of toughener and 0.7 to 3.2 portions of polymerization inhibitor.
Further, the tile adhesive also comprises the following components in parts by weight: 20-200 parts of high molecular polymer.
Further, the cement is inorganic portland cement.
Furthermore, the mesh number of the quartz sand is 90-130 meshes.
Further, the viscosity of the cellulose ether is 700-58000 Pa.s.
Further, the method comprises the following steps:
the method comprises the following steps: preparing raw materials according to a raw material formula;
step two: mixing and stirring cement, quartz sand, fine aggregate, biogel, latex powder, cellulose ether and a defoaming agent uniformly according to a raw material formula;
step three: adding a tackifier, a stabilizer, a toughening agent and a polymerization inhibitor according to a raw material formula, mixing and stirring uniformly;
step four: adding 20-200 parts of high molecular polymer on the basis of the third step, and uniformly mixing and stirring;
step five: and (5) storing the ceramic tile glue.
(III) advantageous effects
Compared with the prior art, the invention has the following beneficial effects:
in order to solve the defects of the prior art, the invention improves the viscosity of the tile adhesive by limiting the components and the preparation method of the tile adhesive, and the alpha-ethyl cyanoacrylate, the tackifier, the stabilizer, the toughening agent, the polymerization inhibitor and the high molecular polymer are matched to improve the viscosity between the tile adhesive and the tile; meanwhile, the fine bone powder can be well filled in gaps between the fine bone powder and the ceramic tiles, so that the viscosity of the ceramic tiles and the wall is effectively improved, and the ceramic tile adhesive and the wall surface cannot be hollowly bulged and fall off.
Detailed Description
The preparation method of the high-viscosity tile adhesive comprises the following steps of:
cement 550-650 parts
250 portions of quartz sand and 300 portions of
50-80 parts of fine aggregate
0.01-0.5 part of biological glue
Latex powder 25-50 parts
5-15 parts of cellulose ether
0.2 to 0.4 portion of defoaming agent
10-15 parts of alpha-ethyl cyanoacrylate.
The tile adhesive is prepared from the following components in parts by weight:
cement 580 and 620 portions
260 portions and 290 portions of quartz sand
60-70 parts of fine aggregate
0.05-0.1 part of biological glue
30-40 parts of latex powder
8-12 parts of cellulose ether
0.35 to 0.38 portion of defoaming agent
12-14 parts of alpha-ethyl cyanoacrylate.
The tile adhesive comprises the following components in parts by weight: 5.4 to 7.4 portions of tackifier, 4.5 to 6.6 portions of stabilizer, 2.4 to 5.6 portions of toughener and 0.7 to 3.2 portions of polymerization inhibitor.
The tile adhesive comprises the following components in parts by weight: 20-200 parts of high molecular polymer.
Wherein the cement is inorganic portland cement.
Wherein the mesh number of the quartz sand is 90-130 meshes.
Wherein the viscosity of the cellulose ether is 700-58000Pa & s.
The method comprises the following steps:
the method comprises the following steps: preparing raw materials according to a raw material formula;
step two: mixing and stirring cement, quartz sand, fine aggregate, biogel, latex powder, cellulose ether and a defoaming agent uniformly according to a raw material formula;
step three: adding a tackifier, a stabilizer, a toughening agent and a polymerization inhibitor according to a raw material formula, mixing and stirring uniformly;
step four: adding 20-200 parts of high molecular polymer on the basis of the third step, and uniformly mixing and stirring;
step five: and (5) storing the ceramic tile glue.
Example 1: the preparation method of the high-viscosity tile adhesive comprises the following steps of: 580 parts of cement, 260 parts of quartz sand, 60 parts of fine aggregate, 0.05 part of biological glue, 30 parts of latex powder, 8 parts of cellulose ether, 0.35 part of defoaming agent, 12 parts of alpha-ethyl cyanoacrylate, 5.4 parts of tackifier, 4.5 parts of stabilizer, 2.4 parts of toughening agent, 0.7 part of polymerization inhibitor and 20 parts of high molecular polymer. Wherein the cement is inorganic portland cement.
Wherein the mesh number of the quartz sand is 90-130 meshes.
Wherein the viscosity of the cellulose ether is 700-58000Pa & s.
The method comprises the following steps:
the method comprises the following steps: preparing raw materials according to a raw material formula;
step two: mixing and stirring cement, quartz sand, fine aggregate, biogel, latex powder, cellulose ether and a defoaming agent uniformly according to a raw material formula;
step three: adding a tackifier, a stabilizer, a toughening agent and a polymerization inhibitor according to a raw material formula, mixing and stirring uniformly;
step four: adding 20-200 parts of high molecular polymer on the basis of the third step, and uniformly mixing and stirring;
step five: and (5) storing the ceramic tile glue.
Example 2:
the preparation method of the high-viscosity tile adhesive comprises the following steps of: 600 parts of cement, 270 parts of quartz sand, 65 parts of fine aggregate, 0.07 part of biological glue, 35 parts of latex powder, 10 parts of cellulose ether, 0.37 part of defoaming agent, 13 parts of alpha-ethyl cyanoacrylate, 6 parts of tackifier, 5 parts of stabilizer, 3 parts of toughening agent, 1.5 parts of polymerization inhibitor and 150 parts of high molecular polymer.
Wherein the cement is inorganic portland cement.
Wherein the mesh number of the quartz sand is 90-130 meshes.
Wherein the viscosity of the cellulose ether is 700-58000Pa & s.
The method comprises the following steps:
the method comprises the following steps: preparing raw materials according to a raw material formula;
step two: mixing and stirring cement, quartz sand, fine aggregate, biogel, latex powder, cellulose ether and a defoaming agent uniformly according to a raw material formula;
step three: adding a tackifier, a stabilizer, a toughening agent and a polymerization inhibitor according to a raw material formula, mixing and stirring uniformly;
step four: adding 20-200 parts of high molecular polymer on the basis of the third step, and uniformly mixing and stirring;
step five: and (5) storing the ceramic tile glue.
Example 3:
the preparation method of the high-viscosity tile adhesive comprises the following steps of: 620 parts of cement, 290 parts of quartz sand, 70 parts of fine aggregate, 0.1 part of biological glue, 40 parts of latex powder, 12 parts of cellulose ether, 0.38 part of defoaming agent, 14 parts of alpha-ethyl cyanoacrylate, 7.4 parts of tackifier, 6.6 parts of stabilizer, 5.6 parts of toughening agent, 3.2 parts of polymerization inhibitor and 200 parts of high molecular polymer.
Wherein the cement is inorganic portland cement.
Wherein the mesh number of the quartz sand is 90-130 meshes.
Wherein the viscosity of the cellulose ether is 700-58000Pa & s.
The method comprises the following steps:
the method comprises the following steps: preparing raw materials according to a raw material formula;
step two: mixing and stirring cement, quartz sand, fine aggregate, biogel, latex powder, cellulose ether and a defoaming agent uniformly according to a raw material formula;
step three: adding a tackifier, a stabilizer, a toughening agent and a polymerization inhibitor according to a raw material formula, mixing and stirring uniformly;
step four: adding 20-200 parts of high molecular polymer on the basis of the third step, and uniformly mixing and stirring;
step five: and (5) storing the ceramic tile glue.
The tile glue prepared in example 1 and example 3 and the tile glue in the prior art are subjected to performance detection, and the following data are obtained:
Figure 72781DEST_PATH_IMAGE002
as can be seen from the table, the prepared ceramic tile adhesive has the performance which is superior to the standard of ceramic wall and floor tile adhesive JC/T547-2005 and the performance of the ceramic tile adhesive in the prior art by limiting the specific components and the preparation method of the ceramic tile adhesive.
The working principle is as follows:
according to the invention, the components and the preparation method of the tile adhesive are limited, so that the viscosity of the tile adhesive is improved, and the viscosity of the tile adhesive and the tile is improved due to the matching of the alpha-ethyl cyanoacrylate, the tackifier, the stabilizer, the toughening agent, the polymerization inhibitor and the high molecular polymer; meanwhile, the fine bone powder can be well filled in gaps between the fine bone powder and the ceramic tiles, so that the viscosity of the ceramic tiles and the wall is effectively improved, and the ceramic tile adhesive and the wall surface cannot be hollowly bulged and fall off.
While there have been shown and described what are at present considered the fundamental principles and essential features of the invention and its advantages, it will be apparent to those skilled in the art that the invention is not limited to the details of the foregoing exemplary embodiments, but is capable of other specific forms without departing from the spirit or essential characteristics thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.

Claims (8)

1. A preparation method of high-viscosity tile glue is characterized by comprising the following steps: the tile adhesive is prepared from the following components in parts by weight:
cement 550-650 parts
250 portions of quartz sand and 300 portions of
50-80 parts of fine aggregate
0.01-0.5 part of biological glue
Latex powder 25-50 parts
5-15 parts of cellulose ether
0.2 to 0.4 portion of defoaming agent
10-15 parts of alpha-ethyl cyanoacrylate.
2. The method for preparing a high-viscosity tile glue according to claim 1, wherein the method comprises the following steps: the tile adhesive is prepared from the following components in parts by weight:
cement 580 and 620 portions
260 portions and 290 portions of quartz sand
60-70 parts of fine aggregate
0.05-0.1 part of biological glue
30-40 parts of latex powder
8-12 parts of cellulose ether
0.35 to 0.38 portion of defoaming agent
12-14 parts of alpha-ethyl cyanoacrylate.
3. The method for preparing a high-viscosity tile glue according to claim 1, wherein the method comprises the following steps: the tile adhesive also comprises the following components in parts by weight: 5.4 to 7.4 portions of tackifier, 4.5 to 6.6 portions of stabilizer, 2.4 to 5.6 portions of toughener and 0.7 to 3.2 portions of polymerization inhibitor.
4. The method for preparing a high-viscosity tile glue according to claim 1, wherein the method comprises the following steps: the tile adhesive also comprises the following components in parts by weight: 20-200 parts of high molecular polymer.
5. The method for preparing a high-viscosity tile glue according to claim 1, wherein the method comprises the following steps: the cement is inorganic portland cement.
6. The method for preparing a high-viscosity tile glue according to claim 1, wherein the method comprises the following steps: the mesh number of the quartz sand is 90-130 meshes.
7. The method for preparing a high-viscosity tile glue according to claim 1, wherein the method comprises the following steps: the viscosity of the cellulose ether is 700-58000 Pa.s.
8. A method for preparing a high-viscosity tile glue according to claims 1-7, characterized in that: the method comprises the following steps:
the method comprises the following steps: preparing raw materials according to a raw material formula;
step two: mixing and stirring cement, quartz sand, fine aggregate, biogel, latex powder, cellulose ether and a defoaming agent uniformly according to a raw material formula;
step three: adding a tackifier, a stabilizer, a toughening agent and a polymerization inhibitor according to a raw material formula, mixing and stirring uniformly;
step four: adding 20-200 parts of high molecular polymer on the basis of the third step, and uniformly mixing and stirring;
step five: and (5) storing the ceramic tile glue.
CN202011620567.0A 2020-12-31 2020-12-31 Preparation method of high-viscosity ceramic tile adhesive Pending CN112500089A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103131335A (en) * 2011-11-28 2013-06-05 宝山钢铁股份有限公司 Preparation dedicated binder of microbeam analysis standard sample and blending method thereof
CN108083723A (en) * 2017-12-04 2018-05-29 华砂砂浆有限责任公司 A kind of glue for tile and preparation method thereof
CN109486428A (en) * 2018-12-12 2019-03-19 深圳麦德利宇航材料科技有限公司 A kind of adhesion technique of aero seat foaming body and sticky cloth
CN110317026A (en) * 2019-08-16 2019-10-11 佛山市德堡建材有限公司 A kind of glue for tile
CN110964466A (en) * 2019-11-25 2020-04-07 深圳市佳鑫一帆科技有限公司 Glue preparation method
CN111205031A (en) * 2018-11-22 2020-05-29 华砂砂浆有限责任公司 Ceramic tile glue

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103131335A (en) * 2011-11-28 2013-06-05 宝山钢铁股份有限公司 Preparation dedicated binder of microbeam analysis standard sample and blending method thereof
CN108083723A (en) * 2017-12-04 2018-05-29 华砂砂浆有限责任公司 A kind of glue for tile and preparation method thereof
CN111205031A (en) * 2018-11-22 2020-05-29 华砂砂浆有限责任公司 Ceramic tile glue
CN109486428A (en) * 2018-12-12 2019-03-19 深圳麦德利宇航材料科技有限公司 A kind of adhesion technique of aero seat foaming body and sticky cloth
CN110317026A (en) * 2019-08-16 2019-10-11 佛山市德堡建材有限公司 A kind of glue for tile
CN110964466A (en) * 2019-11-25 2020-04-07 深圳市佳鑫一帆科技有限公司 Glue preparation method

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