CN112451404B - Colorless and transparent color-changing blush and preparation method thereof - Google Patents
Colorless and transparent color-changing blush and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/368—Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/08—Preparations containing skin colorants, e.g. pigments for cheeks, e.g. rouge
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/26—Optical properties
- A61K2800/262—Transparent; Translucent
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
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Abstract
The invention relates to a colorless transparent color-changing blush and a preparation method thereof, which is characterized by comprising the following components in percentage by mass: 20 to 30 percent of octyl dodecanol stearoyl-oxy stearate, 10 to 20 percent of diisostearyl malate, 25 to 35 percent of dipentaerythritol hexaisononanoate, 8 to 15 percent of propylene glycol dibenzoate, 7 to 15 percent of isostearic acid, 3 to 6 percent of 10-hydroxystearic acid, 0.05 to 0.2 percent of bromous acid red and 0.05 to 0.15 percent of propyl hydroxybenzoate. The invention has the advantages of high transparency, no color, red color after being coated on skin, natural color and lasting coloring.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a colorless and transparent color-changing blush and a preparation method thereof.
Background
Blush is a cosmetic which is coated on a large face to make skin color ruddy, is one of important tools for modifying the face shape and beautifying the skin color, can make the whole face represent a natural, healthy and beautiful appearance after being used, and blush products are an indispensable part of large color cosmetics along with the vigorous development of the color cosmetics market.
Conventional blush matrices are both powdery and oily, and the coloring of both types of blush is achieved by spreading toner particles evenly over the skin surface. The powdery blush has low fit degree with the skin, and the face is easy to generate the phenomenon of powder floating; the oily blush has high fitting degree with the skin, but toner particles spread on the surface of the skin along with the secretion of skin grease are easy to wash, so that the removal and wearing of makeup are not lasting.
The bromic acid red series pigment is colored powder at normal temperature. If the colored bromous acid red powder is added into a cosmetic formula to prepare a colorless transparent system, the preparation is very difficult and needs to be reasonably matched with grease and a thickening agent in the formula. The transparent color-changing lipstick prepared in Chinese patent CN104352361A 'A transparent lipstick with variable color and a preparation method thereof' finally presents orange appearance color. The technical scheme for preparing the colorless transparent color-changing lipstick is not reported.
Disclosure of Invention
The invention aims to solve the technical problem of providing a colorless and transparent color-changing blush and a preparation method thereof, and the obtained blush has the advantages of colorless appearance, good transparency and simple preparation process.
In order to solve the technical problems, the invention adopts the following technical scheme: the colorless transparent color-changing blush is characterized by comprising the following components in percentage by mass: 20 to 30 percent of octyl dodecanol stearoyl-oxy stearate, 10 to 20 percent of diisostearyl malate, 25 to 35 percent of dipentaerythritol hexaisononanoate, 8 to 15 percent of propylene glycol dibenzoate, 7 to 15 percent of isostearic acid, 3 to 6 percent of 10-hydroxystearic acid, 0.05 to 0.2 percent of bromous acid red and 0.05 to 0.15 percent of propyl hydroxybenzoate.
The invention also provides a preparation method of the colorless and transparent color-changing blush, which is characterized by comprising the following steps: the method comprises the following steps:
A. weighing 20-30% of octyl dodecanol stearoyl-oxy stearate, 10-20% of diisostearyl malate, 25-35% of dipentaerythritol hexaisononanoate, 8-15% of propylene glycol dibenzoate, 7-15% of isostearic acid, 3-6% of 10-hydroxystearic acid, 0.05-0.2% of bromous acid red and 0.05-0.15% of propyl hydroxybenzoate according to the following mass ratio;
B. adding the 10-hydroxystearic acid into octyldodecanol stearoyloxy stearate for mixing, heating to 100-; then adding the dipentaerythritol hexaisononanoate, and continuing stirring for 2-4 min at the temperature of 100-;
C. adding the diisostearyl malate, the propylene glycol dibenzoate, the isostearic acid, the bromoform red and the propyl hydroxybenzoate into the transparent mixed solution obtained in the step B, and stirring the mixture by using a stirrer at the rotation speed of 400 rpm under the temperature of 100-110 ℃ until the mixture is uniformly dispersed to obtain a prefabricated solution;
D. and D, cooling the prefabricated liquid obtained in the step C to 75-85 ℃, then injecting the prefabricated liquid into a blush grinding tool, and cooling to room temperature to obtain the colorless and transparent color-changing blush.
The 10-hydroxystearic acid provided by the invention has a CAS number of 638-26-6 and is purchased from Dismann China Co.
Octyl dodecanol STEAROYL STEARATE, having the INCI name octyldecoyl STEARATE, serial number 07196 in the catalogue of names of used cosmetic raw materials (2015 edition) in china, was purchased from shanghai abrik trade ltd.
The dipentaerythritol HEXAISONONANOATE of the invention, having an English INCI name of DIPENTAERYTHRITYL Hexaisononanoate and a CAS number of 65870-97-5, is purchased from Shanghai Aibirk trade company, Inc.
The DIISOSTEARYL MALATE of the present invention, having an INCI name of DIISOSTEARYL MALATE, was numbered 02233 in catalog of names of used cosmetic raw materials (2015 edition) in China, and was purchased from Shanghai Kogyo International trade company, Inc.
The PROPYLENE GLYCOL DIBENZOATE of the present invention, having an INCI name PROPYLENE GLYCOL DIBENZOATE, was purchased from Shanghai Progai International trade company, Inc., having a serial number of 01386 in the catalogue of used cosmetic raw materials (2015 edition) in China.
The ISOSTEARIC ACID of the invention, the English INCI name ISOSTEARIC ACID, has the serial number of 07872 in Chinese catalogue of names of used cosmetic raw materials (2015 edition), and is purchased from Shanghai Aibi trade company Limited.
The RED bromate of the invention is RED 27, is called INCI (RED for identification) 27, has the serial number of 02832 in Chinese catalogue of names of used cosmetic raw materials (2015 edition), and is purchased from vast Sen International Inc. in Shanghai.
The hydroxypropyl hydroxybenzoate of the present invention, named PROPYLPARABEN by INCI, has a serial number of 05205 in the catalogue of used cosmetic raw materials (2015 edition) in China, and is available from Shanghai, Inc. of the ocean, university
The stirrer of the invention is commonly used as IKA RW20, available from Shanghai Schdman fluid technology, Inc.
The appearance of a colorless and transparent color-changing blush prepared according to the examples of the present invention was measured.
1. Blush color was measured.
Heating the paste prepared in the embodiment to a flowable liquid state, then injecting the paste into a cuvette with the size of 10 multiplied by 20 multiplied by 40mm, placing the cuvette into a groove of a colorimetric box of a WSL Lovibond colorimeter after solidification, enabling the cuvette to be tightly attached to a window of a color chip box, then starting a power supply, observing a view field, displaying the color of a sample on the left half part and the color of a calibration color filter on the right half part, and respectively adjusting a yellow color filter group, a red color filter group and a blue color filter group until the colors of the left part and the right part are completely consistent, wherein the value displayed by a display window of an instrument groove plate is the color of the sample to be detected. The results are shown in table 1:
TABLE 1
As can be seen from Table 1, the blush paste prepared in the examples of the present invention was colorless in color.
2. Blush clarity determination
The paste obtained in example 1 was poured into a 10X 20X 40mm cuvette, and after solidification, the paste was placed on a white board having black stripes, and the transparency was observed, as shown in FIG. 1, from which FIG. 1 it can be seen that the black stripes are clearly visible, and the paste obtained in the present invention has high apparent transparency.
The bromic acid red is colored powder, and the prepared product generally has color. The colorless transparent color-changing blush is prepared by mixing the bromic acid red with octyl dodecanol stearoyl-oxy stearate, diisostearyl malate, dipentaerythritol hexaisononanoate, propylene glycol dibenzoate, isostearic acid, 10-hydroxystearic acid and propyl hydroxybenzoate in a specific mass ratio, and the blush is colorless and transparent when viewed externally and is red when being smeared on the face. Based on the characteristics of an oil system, the skin-friendly skin care cream has high adhesion degree with skin when in use; meanwhile, when the bromocriptine in the formula is contacted with the skin, the lactone ring of the bromocriptine is hydrolyzed and opened to show red when meeting the moisture in the skin, and meanwhile, the other part of dibenzopyran is combined with the protein on the skin, so that the color is firmly locked, and the cosmetic effect is durable. Overcomes the technical defects of the prior oily blush with makeup, such as non-durability and easy decolorization.
The blush of the invention is colorless and transparent in appearance, gradually changes into light red over time when being contacted with the skin after being coated, and the color of the presented blush is natural and durable in coloring. The colorless and transparent color-changing blush prepared by the invention has high skin fitting degree, lasting makeup, good use feeling and high transparency, is suitable for various skin-type people, and simultaneously meets the requirements of fashion and aesthetic feeling which are continuously promoted by consumers through the inexistent color-changing process.
In conclusion, the invention has the advantages of high transparency, no color, natural color and lasting coloring, and the skin becomes red after being coated with the pigment.
Drawings
FIG. 1 is a photograph of a transparency test of a colorless and transparent color-changeable blush prepared as described in example 1.
Detailed Description
The following examples are given by way of illustration only, and the scope of the present invention is not limited thereto.
Example 1:
a colorless and transparent color-changing blush comprises the following components by mass percent as shown in Table 2:
TABLE 2 quality composition of colorless transparent color-changing blush
3g of 10-hydroxystearic acid, 26.75g of octyldodecanol stearoyloxy stearate, 35g of dipentaerythritol hexaisononanoate, 20g of diisostearyl malate, 8g of propylene glycol dibenzoate, 7g of isostearic acid, 0.2g of bromous acid red and 0.05g of propylparaben are weighed out according to the mass percentage shown in Table 2 for later use.
Dispersing 10-hydroxystearic acid in octyldodecanol stearoyloxystearate, heating to 100 ℃ and maintaining at that temperature, stirring with an IKA RW20 stirrer at 200rpm to complete dissolution;
adding dipentaerythritol hexaisononanoate, heating to 100 deg.C, maintaining the temperature, and stirring with IKA RW20 stirrer at 200rpm for 2min to obtain transparent mixture;
adding diisostearyl malate, propylene glycol dibenzoate, isostearic acid, red bromate, and propyl hydroxybenzoate into the mixture, heating to 100 deg.C, maintaining the temperature, and stirring with IKA RW20 at 200rpm to completely disperse uniformly;
and cooling the obtained mixture to 75 ℃, injecting the mixture into a blush grinding tool, and cooling to obtain the colorless and transparent color-changing blush.
Example 2:
a colorless and transparent color-changing blush comprises the following components in percentage by mass as shown in Table 3:
TABLE 3 transparent color-changing blush Mass composition
3.8g of 10-hydroxystearic acid, 25g of octyldodecanol stearoyloxystearate, 32.57g of dipentaerythritol hexaisononanoate, 12.5g of diisostearyl malate, 15g of propylene glycol dibenzoate, 11g of isostearic acid, 0.08g of bromous acid red and 0.05g of propylparaben are weighed out according to the mass percentages shown in Table 3 for later use.
Dispersing 10-hydroxystearic acid in octyldodecanol stearoyloxystearate, heating to 102 ℃ and maintaining at that temperature, stirring with an IKA RW20 stirrer at 230rpm to complete dissolution;
adding dipentaerythritol hexaisononanoate, heating to 103 deg.C, maintaining the temperature, and stirring with IKA RW20 stirrer at 230rpm for 2min to obtain transparent mixture;
adding diisostearyl malate, propylene glycol dibenzoate, isostearic acid, red bromate, and propyl hydroxybenzoate to the mixture, heating to 102 deg.C, maintaining the temperature, and stirring with IKA RW20 at 230rpm to completely disperse uniformly;
and cooling the obtained mixture to 78 ℃, injecting the mixture into a blush grinding tool, and cooling to obtain the colorless and transparent color-changing blush.
Example 3:
a colorless and transparent color-changing blush comprises the following components by mass percent as shown in Table 4:
TABLE 4 transparent color-changing blush Mass composition
Weighing 4.6g of 10-hydroxystearic acid, 24g of octyldodecanol stearoyloxystearate, 25g of dipentaerythritol hexaisononanoate, 19.15g of diisostearyl malate, 12g of propylene glycol dibenzoate, 15g of isostearic acid, 0.1g of bromous acid red, 0.2g of bisabolol and 0.15g of propylhydroxybenzoate for later use according to the mass percentages shown in Table 4.
Dispersing 10-hydroxystearic acid in octyldodecanol stearoyloxystearate, heating to 105 ℃ and maintaining at that temperature, stirring with an IKA RW20 stirrer at 250rpm to complete dissolution;
adding dipentaerythritol hexaisononanoate, heating to 105 deg.C, maintaining the temperature, and stirring with IKA RW20 stirrer at 250rpm for 3min to obtain transparent mixture;
adding diisostearyl malate, propylene glycol dibenzoate, isostearic acid, red bromate, and propyl hydroxybenzoate into the mixture, heating to 105 deg.C, maintaining the temperature, and stirring with IKA RW20 at 250rpm to completely disperse uniformly;
cooling the obtained mixture to 80 ℃, injecting the mixture into a blush grinding tool, and cooling to obtain the colorless and transparent color-changing blush.
Example 4:
a colorless and transparent color-changing blush comprises the following components in percentage by mass as shown in Table 5:
TABLE 5 transparent color-changing blush Mass composition
5g of 10-hydroxystearic acid, 30g of octyldodecanol stearoyloxy stearate, 26.85g of dipentaerythritol hexaisononanoate, 15g of diisostearyl malate, 12g of propylene glycol dibenzoate, 11g of isostearic acid, 0.05g of bromous acid red and 0.1g of propylparaben are weighed out according to the mass percentage shown in Table 5 for later use.
Dispersing 10-hydroxystearic acid in octyldodecanol stearoyloxystearate, heating to 108 ℃ and maintaining at that temperature, stirring with an IKA RW20 stirrer at 300rpm to complete dissolution;
adding dipentaerythritol hexaisononanoate, heating to 108 deg.C, maintaining the temperature, and stirring with IKA RW20 stirrer at 300rpm for 3min to obtain transparent mixture;
adding diisostearyl malate, propylene glycol dibenzoate, isostearic acid, red bromate, and propyl hydroxybenzoate into the mixture, heating to 108 deg.C, maintaining the temperature, and stirring with IKA RW20 at 300rpm to completely disperse uniformly;
and cooling the obtained mixture to 82 ℃, injecting the mixture into a blush grinding tool, and cooling to obtain the colorless and transparent color-changing blush.
Example 5:
a colorless and transparent color-changing blush comprises the following components in percentage by mass as shown in Table 6:
TABLE 6 transparent color-changing blush Mass composition
6g of 10-hydroxystearic acid, 20g of octyldodecanol stearoyloxy stearate, 34.85g of dipentaerythritol hexaisononanoate, 10g of diisostearyl malate, 14g of propylene glycol dibenzoate, 15g of isostearic acid, 0.1g of bromous acid red and 0.05g of propylparaben are weighed out according to the mass percentage shown in Table 6 for later use.
Dispersing 10-hydroxystearic acid in octyldodecanol stearoyloxystearate, heating to 110 ℃ and maintaining at that temperature, stirring with an IKA RW20 stirrer at 400 rpm until complete dissolution;
adding dipentaerythritol hexaisononanoate, heating to 110 deg.C, maintaining the temperature, and stirring with IKA RW20 stirrer at 400 rpm for 4 min to obtain transparent mixture; adding diisostearyl malate, propylene glycol dibenzoate, isostearic acid, red bromate, and propyl hydroxybenzoate into the mixture, heating to 110 deg.C, maintaining the temperature, and stirring with IKA RW20 at 400 rpm to completely disperse uniformly; and cooling the obtained mixture to 85 ℃, injecting the mixture into a blush grinding tool, and cooling to obtain the colorless and transparent color-changing blush.
Claims (2)
1. The colorless transparent color-changing blush is characterized by comprising the following components in percentage by mass: 20 to 30 percent of octyl dodecanol stearoyl-oxy stearate, 10 to 20 percent of diisostearyl malate, 25 to 35 percent of dipentaerythritol hexaisononanoate, 8 to 15 percent of propylene glycol dibenzoate, 7 to 15 percent of isostearic acid, 3 to 6 percent of 10-hydroxystearic acid, 0.05 to 0.2 percent of bromous acid red and 0.05 to 0.15 percent of propyl hydroxybenzoate.
2. A preparation method of colorless and transparent color-changing blush is characterized in that: the method comprises the following steps:
A. weighing 20-30% of octyl dodecanol stearoyl-oxy stearate, 10-20% of diisostearyl malate, 25-35% of dipentaerythritol hexaisononanoate, 8-15% of propylene glycol dibenzoate, 7-15% of isostearic acid, 3-6% of 10-hydroxystearic acid, 0.05-0.2% of bromous acid red and 0.05-0.15% of propyl hydroxybenzoate according to the following mass ratio;
B. adding the 10-hydroxystearic acid into octyldodecanol stearoyloxy stearate for mixing, heating to 100-; then adding the dipentaerythritol hexaisononanoate, and continuing stirring for 2-4 min at the temperature of 100-;
C. adding the diisostearyl malate, the propylene glycol dibenzoate, the isostearic acid, the bromoform red and the propyl hydroxybenzoate into the transparent mixed solution obtained in the step B, and stirring the mixture by using a stirrer at the rotation speed of 400 rpm under the temperature of 100-110 ℃ until the mixture is uniformly dispersed to obtain a prefabricated solution;
D. and D, cooling the prefabricated liquid obtained in the step C to 75-85 ℃, then injecting the prefabricated liquid into a blush grinding tool, and cooling to room temperature to obtain the colorless and transparent color-changing blush.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JP2018080163A (en) * | 2016-11-04 | 2018-05-24 | 株式会社コーセー | Powdery solid makeup cosmetic |
| KR20180121037A (en) * | 2017-04-28 | 2018-11-07 | 주식회사 엘지생활건강 | Solid cosmetic composition |
| CN108938481A (en) * | 2018-07-02 | 2018-12-07 | 广州艾蓓生物科技有限公司 | A kind of discoloration lip gloss and preparation method thereof with maintenance effect |
| CN109125116A (en) * | 2018-11-07 | 2019-01-04 | 广州暨北生物科技有限公司 | A kind of U.S. face jelly lipstick of transparent color and preparation method thereof |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2018080163A (en) * | 2016-11-04 | 2018-05-24 | 株式会社コーセー | Powdery solid makeup cosmetic |
| KR20180121037A (en) * | 2017-04-28 | 2018-11-07 | 주식회사 엘지생활건강 | Solid cosmetic composition |
| CN108938481A (en) * | 2018-07-02 | 2018-12-07 | 广州艾蓓生物科技有限公司 | A kind of discoloration lip gloss and preparation method thereof with maintenance effect |
| CN109125116A (en) * | 2018-11-07 | 2019-01-04 | 广州暨北生物科技有限公司 | A kind of U.S. face jelly lipstick of transparent color and preparation method thereof |
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