CN109172398A - lipstick and preparation method - Google Patents
lipstick and preparation method Download PDFInfo
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- CN109172398A CN109172398A CN201811207096.3A CN201811207096A CN109172398A CN 109172398 A CN109172398 A CN 109172398A CN 201811207096 A CN201811207096 A CN 201811207096A CN 109172398 A CN109172398 A CN 109172398A
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- Prior art keywords
- lipstick
- alcohol
- mixture
- phase
- acid ester
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
- A61Q1/06—Lipsticks
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to cosmetic technical fields, and in order to improve the glossiness of lipstick, the invention discloses a kind of lipstick and preparation methods, wherein lipstick includes following component: polyethylene wax: 4-6% by mass percentage；Candelila wax: 0.5-1%；Beeswax: 2-4%；Ceresin: 5-8%；Pentaerythritol tetraoctyl stearate: 15-20%；Polyisobutene: 4-6%；Three isostearate of polyglycereol -2: 4-7%；Parleam: 5-10%；Jojoba seed oil: 1-3%；Butyrospermum parkii fruit rouge: 3-5%；Phenyl silicone oil class raw material: 15-20%；Double-docosyl alcohol or isooctadecanol or phytosterol dimerization Asia oleyl alcohol dimerized linoleic acid ester alcohol: 10-15%；CI77891:1%-10%；CI45410:1%-10%；CI15985:1%-10%；Tocopherol acetate: 0.5%-1%；Phenoxyethanol: 0.1%-0.5%.Lipstick of the invention has the advantages that glossiness is high.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of lipstick and preparation method.
Background technique
The present invention belongs to the relevant technologies related to the present invention for the description of background technique, be only used for explanation and just
In understanding summary of the invention of the invention, it should not be construed as applicant and be specifically identified to or estimate applicant being considered of the invention for the first time
The prior art for the applying date filed an application.
Recently as the improvement of people's living standards, more and more Mies that like to be beautiful begin to use color make-up class product, wherein
Lipstick is most widely used, moistens lipstick since its quality is not done, tends to smear out, color saturation is preferable, the most by market institute
Receive, user is also the most extensive.However the glossiness of lipstick currently on the market cannot reach the requirement of consumer.
Summary of the invention
The purpose of the embodiment of the present invention is that providing a kind of lipstick and preparation method, the lipstick of the method for the present invention preparation has pole
After good upper lip dissolves sense, good spreading property, is applied to lip, it can distribute such as the general gloss of shusu and high temperature
48 DEG C do not soften, do not generate stink for 6 months, and -15 DEG C of low temperature are not cracked for 6 months.
The purpose of the embodiment of the present invention is that be achieved through the following technical solutions:
The embodiment of first aspect present invention provides a kind of lipstick, by mass percentage includes following component:
Polyethylene wax: 4-6%；Candelila wax: 0.5-1%；Beeswax: 2-4%；Ceresin: 5-8%；Pentaerythrite four is different
Stearate: 15-20%；Polyisobutene: 4-6%；Three isostearate of polyglycereol -2: 4-7%；Parleam: 5-
10%；Jojoba seed oil: 1-3%；Butyrospermum parkii fruit rouge: 3-5%；Phenyl silicone oil class raw material: 15-20%；Double-docosyl alcohol is different
Stearyl alcohol or phytosterol dimerization Asia oleyl alcohol dimerized linoleic acid ester alcohol: 10-15%；CI77891:1%-10%；CI45410:
1%-10%；CI15985:1%-10%；Tocopherol acetate: 0.5%-1%；Phenoxyethanol: 0.1%-0.5%.
Further, the phenyl silicone oil class raw material is phenyl trimethicone.
Further, by mass percentage include following component:
Polyethylene wax: 4-6%；Candelila wax: 0.5-1%；Beeswax: 2-4%；Ceresin: 5-8%；Pentaerythrite four is different
Stearate: 15-20%；Polyisobutene: 4-6%；Three isostearate of polyglycereol -2: 4-7%；Parleam: 5-
10%；Jojoba seed oil: 1-3%；Butyrospermum parkii fruit rouge: 3-5%；Phenyl trimethicone: 15-20%；Double-docosyl alcohol
Or isooctadecanol or phytosterol dimerization Asia oleyl alcohol dimerized linoleic acid ester alcohol: 10-15%；CI77891:2%；CI45410:
1.5%；CI15985:2.5%；Tocopherol acetate: 0.5%；Phenoxyethanol: 0.5%.
The embodiment of second aspect of the present invention provides a kind of preparation method of lipstick, includes the following steps:
Each component is weighed according to the mass percent；
By A phase and B heat phase to 85 DEG C -90 DEG C, is dissolved completely to pellucidity, mix, obtain the first mixture, it is described
A phase include polyethylene wax, candelila wax, beeswax and ceresin；The B phase includes pentaerythritol tetraoctyl stearate, gathers
Isobutene, three isostearate of polyglycereol -2, Parleam, jojoba seed oil, Butyrospermum parkii fruit rouge, phenyl silicone oil class are former
Material and alcohols, the alcohols are double-docosyl alcohol or isooctadecanol or phytosterol dimerization Asia oleyl alcohol dimerized linoleic acid ester alcohol；
It gradually adds C phase into the first mixture, after grinding uniformly, is heated to 85 DEG C -90 DEG C, be uniformly mixed, obtain the
Two mixtures；The C phase includes: CI77891, CI45410 and CI15985；
Second mixture is cooled to 80 DEG C, D is added into the second mixture, mixes, obtains third mixture；Institute
The D phase stated includes tocopherol acetate and Phenoxyethanol；
Third mixture is heated to 85 DEG C -90 DEG C, is cooled and shaped and obtains the lipstick.
According to the above aspect of the present invention, lipstick of the present invention and preparation method at least have the following beneficial effects:
In the present patent application using double-docosyl alcohol/isooctadecanol/phytosterol dimerization Asia oleyl alcohol dimerized linoleic acid ester alcohol and
Phenyl trimethicone is combined by certain proportion, and to prepare, high glaze is easy to apply and the mouth of easy long-term preservation
Red, the double-docosyl alcohol/isooctadecanol/phytosterol dimerization Asia oleyl alcohol dimerized linoleic acid ester alcohol of lipstick and phenyl of the application is poly-
Trimethicone substitutes traditional wool lipid and heavy flowing isomerization alkanes, and there is fabulous upper lip to dissolve sense, well
Spreading property, be applied to lip after, can distribute such as the general gloss of shusu and 48 DEG C of high temperature do not soften, do not produce for 6 months
Raw stink, -15 DEG C of low temperature are not cracked for 6 months.
Specific embodiment
The application is further introduced below with reference to embodiment.
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, it is described below of the invention
Specific embodiment.In the following description, what different " embodiment " or " embodiment " referred to is not necessarily the same embodiment.This
Outside, described below is only some embodiments of the present invention, can replace or merge combination between different embodiments, for
For those of ordinary skill in the art, without creative efforts, other embodiments can also be obtained.
Applicant has found through numerous studies: general moist lipstick is by various liquid and solid grease and different types of
Wax is mixed in a certain proportion.Lanolin and heavy flowing isomerization alkanes is widely used as imparting gloss in commercial product
Oil.Wherein wool lipid is easily because oxidation is easy to produce stink；Traditional heavy flowing isomerization alkanes because itself viscosity compared with
Height, the lipstick of production, which is easy to appear, applies non-uniform phenomenon.As consumer uses adornment effect requirement, especially mouth to moist lipstick
Glossiness requirement after red use is higher and higher, and existing technology has been unable to satisfy consumer's needs.The present invention overcome it is above-mentioned not
Foot, by strictly screening, selection pair-docosyl alcohol/isooctadecanol/phytosterol dimerization Asia oleyl alcohol dimerized linoleic acid ester alcohol and phenyl
Silicone oil raw material is combined by certain proportion, obtains that high glaze is easy to apply and the lipstick of easy long-term preservation, is disappeared with meeting
The person's of expense demand.
The embodiment of first aspect present invention provides a kind of lipstick, by mass percentage includes following component:
Polyethylene wax: 4-6%；Candelila wax: 0.5-1%；Beeswax: 2-4%；Ceresin: 5-8%；Pentaerythrite four is different
Stearate: 15-20%；Polyisobutene: 4-6%；Three isostearate of polyglycereol -2: 4-7%；Parleam: 5-
10%；Jojoba seed oil: 1-3%；Butyrospermum parkii fruit rouge: 3-5%；Phenyl silicone oil class raw material: 15-20%；Double-docosyl alcohol is different
Stearyl alcohol or phytosterol dimerization Asia oleyl alcohol dimerized linoleic acid ester alcohol: 10-15%；CI77891:1%-10%；CI45410:
1%-10%；CI15985:1%-10%；Tocopherol acetate: 0.5%-1%；Phenoxyethanol: 0.1%-0.5%.
Double-docosyl alcohol/isooctadecanol/phytosterol dimerization Asia oleyl alcohol dimerized linoleic acid ester alcohol contains dimeric dibasic acid ester and plant
The two groups of sterol, wherein the gloss of lipstick can be improved in the structure of distinctive hexatomic ring.
Above scheme can achieve improve lipstick gloss purpose, herein below on the basis of provide preferred embodiment:
In some embodiments of the invention, the phenyl silicone oil class raw material is phenyl trimethicone.
In some embodiments of the invention, by mass percentage include following component:
Polyethylene wax: 4-6%；Candelila wax: 0.5-1%；Beeswax: 2-4%；Ceresin: 5-8%；Pentaerythrite four is different
Stearate: 15-20%；Polyisobutene: 4-6%；Three isostearate of polyglycereol -2: 4-7%；Parleam: 5-
10%；Jojoba seed oil: 1-3%；Butyrospermum parkii fruit rouge: 3-5%；Phenyl trimethicone: 15-20%；Double-docosyl alcohol
Or isooctadecanol or phytosterol dimerization Asia oleyl alcohol dimerized linoleic acid ester alcohol: 10-15%；CI77891:2%；CI45410:
1.5%；CI15985:2.5%；Tocopherol acetate: 0.5%；Phenoxyethanol: 0.5%.
In the present patent application using double-docosyl alcohol/isooctadecanol/phytosterol dimerization Asia oleyl alcohol dimerized linoleic acid ester alcohol and
Phenyl trimethicone is combined by certain proportion, and to prepare, high glaze is easy to apply and the mouth of easy long-term preservation
Red, the double-docosyl alcohol/isooctadecanol/phytosterol dimerization Asia oleyl alcohol dimerized linoleic acid ester alcohol of lipstick and phenyl of the application is poly-
Trimethicone substitutes traditional wool lipid and heavy flowing isomerization alkanes, and there is fabulous upper lip to dissolve sense, well
Spreading property, be applied to lip after, can distribute such as the general gloss of shusu and 48 DEG C of high temperature do not soften, do not produce for 6 months
Raw stink, -15 DEG C of low temperature are not cracked for 6 months.
The embodiment of second aspect of the present invention provides a kind of preparation method of lipstick, includes the following steps:
Each component is weighed according to the mass percent；
By A phase and B heat phase to 85 DEG C -90 DEG C, is dissolved completely to pellucidity, mix, obtain the first mixture, it is described
A phase include polyethylene wax, candelila wax, beeswax and ceresin；The B phase includes pentaerythritol tetraoctyl stearate, gathers
Isobutene, three isostearate of polyglycereol -2, Parleam, jojoba seed oil, Butyrospermum parkii fruit rouge, phenyl silicone oil class are former
Material and alcohols, the alcohols are double-docosyl alcohol or isooctadecanol or phytosterol dimerization Asia oleyl alcohol dimerized linoleic acid ester alcohol；
It gradually adds C phase into the first mixture, after grinding uniformly, is heated to 85 DEG C -90 DEG C, be uniformly mixed, obtain the
Two mixtures；The C phase includes: CI77891, CI45410 and CI15985；
Second mixture is cooled to 80 DEG C, D is added into the second mixture, mixes, obtains third mixture；Institute
The D phase stated includes tocopherol acetate and Phenoxyethanol；
Third mixture is heated to 85 DEG C -90 DEG C, is cooled and shaped and obtains the lipstick.
The solution of the present invention is further elaborated combined with specific embodiments below:
Embodiment 1
A kind of preparation method of high glaze lipstick, it is characterised in that: weight percentage, including following components,
Specifically it is shown in Table 1
Table 1
Raw material is got out according to formulation ratio:
By A phase and B heat phase to 85 DEG C -90 DEG C, is dissolved completely to pellucidity, stirred evenly, obtain the first mixture；
It takes the first mixture of part to be added in three-roll grinder, gradually adds C phase, mixed after grinding uniformly with residue first
Object is heated to 85 DEG C -90 DEG C while stirring, is allowed to uniformly mixed, obtains the second mixture；
Second mixture is cooled to 80 DEG C, D is added into the second mixture, is stirred evenly, obtains third mixing
Object；
Third mixture is heated to 85 DEG C -90 DEG C, is poured into mold, is cooled to -5 DEG C, is freezed 10 minutes, shaping and demoulding
Obtain product.
Comparative example 1
The step of lipstick preparation method of comparative example 1 is with embodiment 1 is identical, and component is as shown in table 2:
Table 2
Comparative example 2
The step of lipstick preparation method of comparative example 2 is with embodiment 1 is identical, and component is as shown in table 2:
Table 3
The preparation method of comparative example 1 and comparative example 2 is identical as the preparation method of embodiment 1, and only raw material is different.
Testing example
Experimental method: three sections of embodiments are tested using BYK glossiness tester.
Experimental principle: sample surfaces are exposed to 60 ° of incidence angles by BYK glossiness tester built-in light source, in mirror surface
The reflectivity of light, unit Gu (Gloss Unit) are measured at reflection, following table is known as G value, and G value is bigger, and person's glossiness is higher.
Experimental procedure: 1) 3 section lipsticks together 48 DEG C under the conditions of are placed into 30min；2) three sections of lipsticks are respectively placed in white
In color paper, membrane 90um is carried out using device for drawing die；3) 5min under the conditions of being placed in 48 DEG C again takes out and cooling, laggard wait do
The measurement of row G value, G value are the average value that 5 points of BYK glossiness tester measurement are taken.
Lipstick G value test result is as shown in table 4
Table 4
Experimental result: by comparison: sub- using double-docosyl alcohol/isooctadecanol/phytosterol dimerization in embodiment 1
The combination of oleyl alcohol dimerized linoleic acid ester alcohol and phenyl trimethicone can be obviously improved glossiness in lipstick formula.
It should be noted that above-described embodiment can be freely combined as needed.Described above is only of the invention preferred
Embodiment is not intended to restrict the invention, for those skilled in the art, the present invention can have it is various change and
Variation.All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in this hair
Within bright protection scope.
Claims (4)
1. a kind of lipstick, which is characterized in that by mass percentage include following component:
Polyethylene wax: 4-6%；Candelila wax: 0.5-1%；Beeswax: 2-4%；Ceresin: 5-8%；The different tristearin of pentaerythrite four
Acid esters: 15-20%；Polyisobutene: 4-6%；Three isostearate of polyglycereol -2: 4-7%；Parleam: 5-10%；Suddenly
Bar seed oil suddenly: 1-3%；Butyrospermum parkii fruit rouge: 3-5%；Phenyl silicone oil class raw material: 15-20%；Double-docosyl alcohol or isooctadecanol
Or phytosterol dimerization Asia oleyl alcohol dimerized linoleic acid ester alcohol: 10-15%；CI77891:1%-10%；CI45410:1%-10%；
CI15985:1%-10%；Tocopherol acetate: 0.5%-1%；Phenoxyethanol: 0.1%-0.5%.
2. lipstick according to claim 1, which is characterized in that the phenyl silicone oil class raw material is the poly- trimethyl silicane of phenyl
Oxygen alkane.
3. lipstick according to claim 1, which is characterized in that by mass percentage include following component:
Polyethylene wax: 4-6%；Candelila wax: 0.5-1%；Beeswax: 2-4%；Ceresin: 5-8%；The different tristearin of pentaerythrite four
Acid esters: 15-20%；Polyisobutene: 4-6%；Three isostearate of polyglycereol -2: 4-7%；Parleam: 5-10%；Suddenly
Bar seed oil suddenly: 1-3%；Butyrospermum parkii fruit rouge: 3-5%；Phenyl trimethicone: 15-20%；Double-docosyl alcohol is different hard
Lipidol or phytosterol dimerization Asia oleyl alcohol dimerized linoleic acid ester alcohol: 10-15%；CI77891:2%；CI45410:1.5%；
CI15985:2.5%；Tocopherol acetate: 0.5%；Phenoxyethanol: 0.5%.
4. a kind of preparation method of the described in any item lipsticks of claim 1-3, which comprises the steps of:
Each component is weighed according to the mass percent；
By A phase and B heat phase to 85 DEG C -90 DEG C, is dissolved completely to pellucidity, mix, obtain the first mixture, the A
It mutually include polyethylene wax, candelila wax, beeswax and ceresin；The B phase includes pentaerythritol tetraoctyl stearate, poly- isobutyl
Alkene, three isostearate of polyglycereol -2, Parleam, jojoba seed oil, Butyrospermum parkii fruit rouge, phenyl silicone oil class raw material and
Alcohols, the alcohols are double-docosyl alcohol or isooctadecanol or phytosterol dimerization Asia oleyl alcohol dimerized linoleic acid ester alcohol；
C phase is gradually added into the first mixture and is heated to 85 DEG C -90 DEG C after grinding uniformly, is uniformly mixed, and it is mixed to obtain second
Close object；The C phase includes: CI77891, CI45410 and CI15985；
Second mixture is cooled to 80 DEG C, D is added into the second mixture, mixes, obtains third mixture；Described
D phase includes tocopherol acetate and Phenoxyethanol；
Third mixture is heated to 85 DEG C -90 DEG C, is cooled and shaped and obtains the lipstick.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811207096.3A CN109172398A (en) | 2018-10-17 | 2018-10-17 | lipstick and preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811207096.3A CN109172398A (en) | 2018-10-17 | 2018-10-17 | lipstick and preparation method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109172398A true CN109172398A (en) | 2019-01-11 |
Family
ID=64945524
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811207096.3A Pending CN109172398A (en) | 2018-10-17 | 2018-10-17 | lipstick and preparation method |
Country Status (1)
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| CN (1) | CN109172398A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109846738A (en) * | 2019-03-13 | 2019-06-07 | 广州莱倩化妆品有限公司 | A kind of formula and preparation method thereof of moisturizing lipstick |
| CN110236970A (en) * | 2019-07-11 | 2019-09-17 | 中山市美源化妆品有限公司 | Lipstick |
| CN110559214A (en) * | 2019-09-06 | 2019-12-13 | 上海中翊日化有限公司 | high-gloss color-changing lipstick and preparation method thereof |
| CN110721122A (en) * | 2019-11-29 | 2020-01-24 | 苏州安特化妆品股份有限公司 | Rich-color, moist and light-color lipstick and preparation method thereof |
| CN110882192A (en) * | 2019-12-16 | 2020-03-17 | 泉后(广州)生物科技研究院有限公司 | Freckle removing stick and preparation method thereof |
| CN112386513A (en) * | 2019-08-19 | 2021-02-23 | 英妃(杭州)化妆品有限公司 | Color-changing lipstick and preparation method thereof |
| CN113081872A (en) * | 2021-04-14 | 2021-07-09 | 广州花出见生物科技有限公司 | Moistening and lasting lipstick |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103747773A (en) * | 2011-06-01 | 2014-04-23 | 株式会社资生堂 | Solid cosmetic for lips |
-
2018
- 2018-10-17 CN CN201811207096.3A patent/CN109172398A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103747773A (en) * | 2011-06-01 | 2014-04-23 | 株式会社资生堂 | Solid cosmetic for lips |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109846738A (en) * | 2019-03-13 | 2019-06-07 | 广州莱倩化妆品有限公司 | A kind of formula and preparation method thereof of moisturizing lipstick |
| CN110236970A (en) * | 2019-07-11 | 2019-09-17 | 中山市美源化妆品有限公司 | Lipstick |
| CN112386513A (en) * | 2019-08-19 | 2021-02-23 | 英妃(杭州)化妆品有限公司 | Color-changing lipstick and preparation method thereof |
| CN110559214A (en) * | 2019-09-06 | 2019-12-13 | 上海中翊日化有限公司 | high-gloss color-changing lipstick and preparation method thereof |
| CN110721122A (en) * | 2019-11-29 | 2020-01-24 | 苏州安特化妆品股份有限公司 | Rich-color, moist and light-color lipstick and preparation method thereof |
| CN110882192A (en) * | 2019-12-16 | 2020-03-17 | 泉后(广州)生物科技研究院有限公司 | Freckle removing stick and preparation method thereof |
| CN110882192B (en) * | 2019-12-16 | 2021-04-30 | 泉后(广州)生物科技研究院有限公司 | Freckle removing stick and preparation method thereof |
| CN113081872A (en) * | 2021-04-14 | 2021-07-09 | 广州花出见生物科技有限公司 | Moistening and lasting lipstick |
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Application publication date: 20190111 |