CN112439377A - A reation kettle for preparing antirust liquid - Google Patents
A reation kettle for preparing antirust liquid Download PDFInfo
- Publication number
- CN112439377A CN112439377A CN201910810442.5A CN201910810442A CN112439377A CN 112439377 A CN112439377 A CN 112439377A CN 201910810442 A CN201910810442 A CN 201910810442A CN 112439377 A CN112439377 A CN 112439377A
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- CN
- China
- Prior art keywords
- reation kettle
- kettle main
- reaction
- main part
- sampling
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
Abstract
The invention discloses a reaction kettle for preparing antirust liquid, which comprises a reaction kettle main body, a stirring shaft, a heating pipe and a sampling assembly, wherein the stirring shaft is arranged in the reaction kettle main body, the top of the stirring shaft is fixedly connected with an output shaft of a motor through a coupler, and the motor is fixedly arranged at the top end of the reaction kettle main body. This a reation kettle for preparing antirust liquid sees the reaction preparation process in real time through the observation window, if there is unusually in the discovery reaction, promote first handle and make the piston piece move to stopper upper port, rotate the second handle simultaneously and will block up the nut and move to the stopper lower port, the reaction liquid flows in the sampling bottle along with the sampling subassembly pore, the completion sample detects, thereby can be real-time reaction solution reaction condition in the detection reation kettle, and then carry out real-time adjustment to the reaction liquid, guarantee reation kettle preparation antirust liquid quality.
Description
Technical Field
The invention relates to the technical field of reaction kettles, in particular to a reaction kettle for preparing antirust liquid.
Background
A pale yellow liquid, an industrial liquid preparation, is excellent in coatability; the surface of the ferrous metal is rust-proof and oxidation-resistant. The solution is water-soluble antirust solution; volatile toxic substances are not generated; the product is not suitable for direct contact of a human body, is suitable for surface rust prevention treatment of working procedures, indoor and outdoor steel, iron, aluminum, alloy products and the like, and has a one-time spraying rust prevention period of more than 8 months; if the storage period needs to be prolonged, soaking, spraying or coating once every half year is recommended.
When various raw materials are put into a reaction kettle to react to prepare the antirust liquid, more or less reaction for generating impurities can be generated, if the reaction is not timely adjusted, the impurities generated in the preparation of the antirust liquid are too much, and the quality of the antirust liquid is further influenced.
Disclosure of Invention
The invention aims to overcome the defects of the prior art, and provides a reaction kettle for preparing antirust liquid, which comprises a reaction kettle main body, a stirring shaft, a heating pipe and a sampling assembly, wherein the stirring shaft is arranged in the reaction kettle main body, the top of the stirring shaft is fixedly connected with an output shaft of a motor through a coupler, the motor is fixedly arranged at the top end of the reaction kettle main body, feed inlets are respectively arranged in the left direction and the right direction of the motor, the feed inlets are communicated with an inner cavity of the reaction kettle main body, the heating pipe is arranged below the stirring shaft, the bottom end of the heating pipe is fixedly connected with an electric heating sheet, the electric heating sheet is fixedly arranged at the bottom of the reaction kettle main body, a plurality of support columns are fixedly arranged at the bottom end of the reaction kettle main body, a discharge outlet is fixedly connected at the left lower part, the positive surface of the reaction kettle main body is provided with an observation window.
Preferably, the sampling component includes piston piece, jam nut, lead screw, first handle, connecting rod, second handle, sampling bottle and stopper, place the sampling component in the lead screw, lead screw right-hand member and second handle fixed connection, and lead screw left part threaded connection have the jam nut, and block up the nut bottom and cover the sampling bottle top, sampling bottle threaded connection is in the sampling component bottom, block up nut top sliding connection has the piston piece, and the right-hand stopper that is equipped with of piston piece, stopper fixed connection is inboard in the sampling component roof, place the sampling component top in the piston piece top and open the spout that has, piston piece top rotates with the connecting rod to be connected, and the connecting rod top rotates with reation kettle main part right-hand member to be connected, connecting rod middle part fixed mounting has first handle.
Preferably, the surfaces of the piston block and the blocking nut are sleeved with waterproof rubber layers.
Preferably, two ports are arranged at the left end of the limiting block, and the two ports sequentially correspond to the piston block and the blocking nut from top to bottom.
Compared with the prior art, the invention has the beneficial effects that: this a reation kettle for preparing antirust liquid sees the reaction preparation process in real time through the observation window, if there is unusually in the discovery reaction, promote first handle and make the piston piece move to stopper upper port, rotate the second handle simultaneously and will block up the nut and move to the stopper lower port, the reaction liquid flows in the sampling bottle along with the sampling subassembly pore, the completion sample detects, thereby can be real-time reaction solution reaction condition in the detection reation kettle, and then carry out real-time adjustment to the reaction liquid, guarantee reation kettle preparation antirust liquid quality.
The invention makes up the defects in the background technology to a certain extent
Drawings
FIG. 1 is a schematic diagram of the overall structure of a reaction kettle for preparing antirust liquid according to the present invention;
FIG. 2 is a schematic view of a part of the structure of a reaction kettle for preparing antirust liquid according to the present invention;
FIG. 3 is a schematic view of a sampling assembly according to the present invention.
In the figure: 1. the reaction kettle comprises a reaction kettle main body, 2, a stirring shaft, 3, a heating pipe, 4, a sampling assembly, 5, a motor, 6, a feeding hole, 7, an electric heating sheet, 8, a supporting column, 9, a piston block, 10, a blocking nut, 11, a limiting block, 12, a screw rod, 13, a first handle, 14, a connecting rod, 15, a second handle, 16, a sampling bottle, 17, a discharging hole, 18 and an observation window.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-3, the present invention provides a technical solution: a reaction kettle for preparing antirust liquid comprises a reaction kettle main body 1, a stirring shaft 2, a heating pipe 3 and a sampling component 4, and is characterized in that the reaction kettle main body 1 is internally provided with the stirring shaft 2, the top of the stirring shaft 2 is fixedly connected with an output shaft of a motor 5 through a coupler, the motor 5 is fixedly installed at the top end of the reaction kettle main body 1, the motor 5 is provided with a feeding port 6 in the left direction and the right direction, the feeding port 6 is communicated with the inner cavity of the reaction kettle main body 1, the heating pipe 3 is arranged below the stirring shaft 2, the bottom end of the heating pipe 3 is fixedly connected with an electric heating sheet 7, the electric heating sheet 7 is fixedly installed at the bottom of the reaction kettle main body 1, the bottom end of the reaction kettle main body 1 is fixedly provided with a plurality of supporting columns 8, the left lower part of the, the inner cavity of the sampling component 4 is communicated with the reaction kettle main body 1, and the front surface of the reaction kettle main body 1 is provided with an observation window 18.
Preferably, the sampling assembly 4 comprises a piston block 9, a blocking nut 10, a screw rod 12, a first handle 13, a connecting rod 14, a second handle 15, a sampling bottle 16 and a limiting block 11, the screw rod 12 is rotatably connected with the sampling assembly 4, the right end of the screw rod 12 is fixedly connected with the second handle 15, the left part of the screw rod 12 is in threaded connection with the blocking nut 10, the blocking nut 10 is in sliding connection with the bottom of the sampling assembly 4, the bottom end of the blocking nut 10 covers the top end of the sampling bottle 16, the sampling bottle 16 is in threaded connection with the bottom of the sampling assembly 4, the top end of the blocking nut 10 is in sliding connection with the piston block 9, the limiting block 11 is arranged on the right side of the piston block 9, the limiting block 11 is positioned on the inner side of the top wall of the sampling assembly 4, the top of the piston block 9 is in sliding connection, and the top of the connecting rod 14 is rotatably connected with the right end of the reaction kettle main body 1, and a first handle 13 is fixedly arranged in the middle of the connecting rod 14.
Preferably, the surfaces of the piston block 9 and the blocking nut 10 are both covered with waterproof rubber layers.
Preferably, two ports are arranged at the left end of the limiting block 11, and the two ports sequentially correspond to the piston block 9 and the blocking nut 10 from top to bottom.
The working principle is as follows: the raw materials gets into 1 inner chamber of reation kettle main part by feed inlet 6, by the stirring of (mixing) shaft 2 and the heating of heating pipe 3, thereby accelerate the reaction of raw materials, and see the reaction preparation process in real time through observation window 18, if it is unusual to discover the reaction, promote first handle 13 and drive the motion of connecting rod 14, and then make piston block 8 remove to stopper 11 upper port, rotate second handle 15 simultaneously and drive the lead screw and rotate and move jam nut 10 to stopper 11 lower port, reaction liquid flows into sampling bottle 16 along sampling assembly 4 pore, after sampling bottle 16 samples and accomplishes, reverse push away first handle 13 and make piston block 8 reset, reverse second handle 15 simultaneously makes and blocks up that jam nut 10 resets and accomplish and seal sampling assembly 4 pore, take out sampling bottle 16 and detect the reaction.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (4)
1. The utility model provides a reation kettle for preparing antirust liquid, includes reation kettle main part (1), (mixing) shaft (2), heating pipe (3) and sample subassembly (4), its characterized in that, reation kettle main part (1) embeds there is (mixing) shaft (2), and (mixing) shaft (2) top passes through shaft coupling and motor (5) output shaft fixed connection, motor (5) fixed mounting is on reation kettle main part (1) top, both directions all are equipped with feed inlet (6) about motor (5), and feed inlet (6) communicate with each other with reation kettle main part (1) inner chamber, the (mixing) shaft (2) below is equipped with heating pipe (3), and heating pipe (3) bottom fixedly connected with electric heating piece (7), electric heating piece (7) fixed mounting is in reation kettle main part (1) bottom, reation kettle main part (1) bottom fixed mounting has a plurality of support columns (8), the utility model discloses a reactor, including reation kettle main part (1), sampling subassembly (4), reation kettle main part (1) left side below fixedly connected with discharge gate (17), and reation kettle main part (1) right side below is equipped with sampling component (4), sampling component (4) inner chamber communicates with each other with reation kettle main part (1), reation kettle main part (1) positive surface mounting has observation window (18).
2. The reaction kettle for preparing antirust liquid according to claim 1, wherein the sampling assembly (4) comprises a piston block (9), a blocking nut (10), a screw rod (12), a first handle (13), a connecting rod (14), a second handle (15), a sampling bottle (16) and a limiting block (11), the screw rod (12) is rotatably connected with the sampling assembly (4), the right end of the screw rod (12) is fixedly connected with the second handle (15), the left part of the screw rod (12) is in threaded connection with the blocking nut (10), the blocking nut (10) is in sliding connection with the bottom of the sampling assembly (4), the bottom end of the blocking nut (10) covers the top end of the sampling bottle (16), the sampling bottle (16) is in threaded connection with the bottom of the sampling assembly (4), the top end of the blocking nut (10) is in sliding connection with the piston block (9), and the piston block (9) is provided with the limiting block (11), stopper (11) are located sampling component (4) roof inboard, piston piece (9) top sliding connection is in the open spout in sampling component (4) top, piston piece (9) top is rotated with connecting rod (14) and is connected, and connecting rod (14) top and reation kettle main part (1) right-hand member rotate to be connected, connecting rod (14) middle part fixed mounting has first handle (13).
3. The reaction kettle for preparing the antirust liquid according to claim 1, wherein the surfaces of the piston block (9) and the blocking nut (10) are covered with waterproof rubber layers.
4. The reaction kettle for preparing the antirust liquid according to claim 1, wherein two ports are arranged at the left end of the limiting block (11), and the two ports correspond to the piston block (9) and the blocking nut (10) from top to bottom in sequence.
Priority Applications (1)
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CN201910810442.5A CN112439377A (en) | 2019-08-29 | 2019-08-29 | A reation kettle for preparing antirust liquid |
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CN201910810442.5A CN112439377A (en) | 2019-08-29 | 2019-08-29 | A reation kettle for preparing antirust liquid |
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CN112439377A true CN112439377A (en) | 2021-03-05 |
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CN201910810442.5A Pending CN112439377A (en) | 2019-08-29 | 2019-08-29 | A reation kettle for preparing antirust liquid |
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Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
SU1040374A1 (en) * | 1982-04-28 | 1983-09-07 | Государственное Конструкторское Бюро Коксохимического Машиностроения Гипрококса | Sampler |
CN101035602A (en) * | 2004-08-06 | 2007-09-12 | 迪奥尼斯公司 | Separation system, components of a separation system and methods of making and using them |
US20130064610A1 (en) * | 2011-09-14 | 2013-03-14 | GuD Geotechnik und Dynamik GmbH | Suspension extraction device |
CN204841692U (en) * | 2015-08-13 | 2015-12-09 | 宁波大学 | Practical chemical industry reation kettle |
US20170297997A1 (en) * | 2014-09-24 | 2017-10-19 | Basf Se | Method for producing diesters of terephthalic acid with a dehydration of recirculated alcohol |
CN107551955A (en) * | 2017-10-10 | 2018-01-09 | 李云 | A kind of chemical industry reaction agitating device of separation of solid and liquid charging |
CN207655124U (en) * | 2017-11-01 | 2018-07-27 | 金丽梅 | A kind of highly effective reaction kettle facilitating sampling |
-
2019
- 2019-08-29 CN CN201910810442.5A patent/CN112439377A/en active Pending
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
SU1040374A1 (en) * | 1982-04-28 | 1983-09-07 | Государственное Конструкторское Бюро Коксохимического Машиностроения Гипрококса | Sampler |
CN101035602A (en) * | 2004-08-06 | 2007-09-12 | 迪奥尼斯公司 | Separation system, components of a separation system and methods of making and using them |
US20130064610A1 (en) * | 2011-09-14 | 2013-03-14 | GuD Geotechnik und Dynamik GmbH | Suspension extraction device |
US20170297997A1 (en) * | 2014-09-24 | 2017-10-19 | Basf Se | Method for producing diesters of terephthalic acid with a dehydration of recirculated alcohol |
CN204841692U (en) * | 2015-08-13 | 2015-12-09 | 宁波大学 | Practical chemical industry reation kettle |
CN107551955A (en) * | 2017-10-10 | 2018-01-09 | 李云 | A kind of chemical industry reaction agitating device of separation of solid and liquid charging |
CN207655124U (en) * | 2017-11-01 | 2018-07-27 | 金丽梅 | A kind of highly effective reaction kettle facilitating sampling |
Non-Patent Citations (1)
Title |
---|
廖传华: "《反应过程与设备》", 31 July 2008 * |
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Application publication date: 20210305 |