CN112430508B - Disinfectant powder atomizing device cleaning agent, application and cleaning method thereof - Google Patents

Disinfectant powder atomizing device cleaning agent, application and cleaning method thereof Download PDF

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Publication number
CN112430508B
CN112430508B CN202011426978.6A CN202011426978A CN112430508B CN 112430508 B CN112430508 B CN 112430508B CN 202011426978 A CN202011426978 A CN 202011426978A CN 112430508 B CN112430508 B CN 112430508B
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atomizing device
cleaning
powder
parts
powder atomizing
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CN112430508A (en
Inventor
王荣
罗伟
阮雨虹
魏俊祥
黄颖
李莹
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Fujian Pulido Technology Co ltd
Zibo Xinourui Environmental Protection Technology Co ltd
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Fujian Pulido Technology Co ltd
Zibo Xinourui Environmental Protection Technology Co ltd
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02Anionic compounds
    • C11D1/12Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/14Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
    • C11D1/146Sulfuric acid esters
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B3/00Cleaning by methods involving the use or presence of liquid or steam
    • B08B3/04Cleaning involving contact with liquid
    • B08B3/08Cleaning involving contact with liquid the liquid having chemical or dissolving effect
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2003Alcohols; Phenols
    • C11D3/2006Monohydric alcohols
    • C11D3/2017Monohydric alcohols branched
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2003Alcohols; Phenols
    • C11D3/2041Dihydric alcohols
    • C11D3/2044Dihydric alcohols linear

Abstract

A disinfectant powder atomizing device cleaning agent, application and a cleaning method thereof belong to the technical field of atomizing device cleaning. Potassium hydrogen persulfate is easy to separate out crystals from liquid mist in the atomization process, and particularly easy to separate out crystals near the spraying small holes of the atomization device, so that the small holes are blocked. The cleaning agent consisting of 28-32 parts of ethylene glycol, 18-22 parts of isopropanol, 0.8-1.2 parts of sodium dodecyl sulfate and 47-51 parts of water can be used for cleaning a disinfection powder atomization device, and particularly, the cleaning agent for the disinfection powder atomization device can be easily permeated into disinfection powder with crystals separated out by adopting a heating, volatilization and atomization mode, so that the crystals are dissolved inside and outside the disinfection powder atomization device, the disinfection powder atomization device is sufficiently and efficiently cleaned, the using amount is small, the preparation cost is low, and the use is convenient.

Description

Disinfectant powder atomizing device cleaning agent, application and cleaning method thereof
Technical Field
A disinfectant powder atomizing device cleaning agent, application and a cleaning method thereof belong to the technical field of atomizing device cleaning.
Background
Potassium hydrogen persulfate is an effective disinfectant, is a white powdery solid capable of flowing freely at normal temperature, and is easily soluble in water. The acidity of the aqueous solution is caused by the generation of hydrogen ions due to the dissolution of potassium hydrogen sulfate in the complex salt. However, potassium hydrogen persulfate has much better stability under acidic conditions than neutral conditions, and rapidly decomposes under alkaline conditions. Its mechanism of killing microorganisms can be explained as: 1. under the condition of aqueous solution, potassium hydrogen persulfate releases nascent oxygen to directly carry out oxidation reaction on microbial cell wall protein. 2. Free hydroxyl groups are released, interfering with the microbial enzyme system, quickly leading to inactivation of the microbial protein molecules. Research shows that when potassium persulfate acts on small molecular organic matters, such as relatively long-chain aldehyde and amine organic matters, free hydroxyl is used for promoting the reaction. Toxic and harmful 'three-cause' byproducts are not generated, and only K + and SO4 are slightly increased (for example, the K + increment is 0.03ppm and the SO4 increment is 0.06ppm when the K + and the SO4 are added into the water body according to 0.5 ppm).
At present, potassium hydrogen persulfate is mostly applied to sterilization and disinfection of water, but is also suitable for prevention and disinfection of certain livestock diseases in the breeding industry, such as swine fever, due to the excellent effect of the potassium hydrogen persulfate on virus inactivation.
However, if the potassium hydrogen persulfate is sprayed in an atomizing mode, the potassium hydrogen persulfate is easy to separate out crystals from liquid mist in the atomizing process, particularly, the crystals are easy to separate out near the spraying holes of the atomizing device, so that the spraying holes are blocked, and sometimes, the dissolved disinfection powder is required to be atomized even at high temperature, so that the disinfection powder separated out of the crystals is carbonized and hardened and is insoluble in water, and the blockage is difficult.
Disclosure of Invention
The technical problem to be solved by the invention is as follows: overcomes the defects of the prior art, and provides a disinfectant powder atomizing device cleaning agent which is low in cost and quick in cleaning and dredging, application and a cleaning method thereof.
The technical scheme adopted by the invention for solving the technical problems is as follows: the utility model provides a disinfection powder atomizing device sanitizer which characterized in that: comprises the following components in parts by weight: 28-32 parts of ethylene glycol, 18-22 parts of isopropanol, 0.8-1.2 parts of sodium dodecyl sulfate and 47-51 parts of water.
The disinfectant powder is dissolved in the solvent and then sprayed out, the state change of a liquid system is large, particularly, the temperature of the system is rapidly reduced after the temperature of the system is raised in the atomization process, the disinfectant powder is easy to separate out crystals from the system, if the disinfectant powder is a high-temperature system, the crystallized disinfectant powder is easy to rapidly carbonize and condense to form compact solids to block a spraying opening, the common solvent is difficult to deeply penetrate into the disinfectant powder crystals, the above detergent can rapidly permeate into the disinfection part crystallized at the spraying opening, the crystals are dissolved and taken away inside and outside synchronously, the easily blocked part of the disinfectant powder atomization device is efficiently and fully cleaned, and the using amount and cleaning time of the detergent are saved. The sodium dodecyl sulfate can improve the permeation and solubilization effects of the detergent on disinfectant powder crystals, the glycol and the isopropanol can gradually dissolve crystals from the outside of the disinfectant powder crystals according to the proportion, the detergent has the characteristic of atomization, and the glycol and the isopropanol can volatilize into mist after being heated, so that the size of detergent liquid drops is reduced, and the detergent liquid drops can more easily enter the inside of the disinfectant powder crystals. Water acts as a carrier for the above ingredients.
Preferably, the composition comprises the following components in parts by weight: 30 parts of ethylene glycol, 20 parts of iso-diol, 1 part of sodium dodecyl sulfate and 49 parts of water. The optimal proportion can realize the most efficient and sufficient crystal cleaning of the precipitated disinfection powder.
The application of the disinfectant powder atomizing device cleaning agent is characterized in that: is used for cleaning the hydrogen potassium persulfate disinfection powder atomization device.
A cleaning method of a disinfection powder atomization device is characterized in that: the disinfectant powder atomizing device cleaning agent is prepared according to any one of the disinfectant powder atomizing device cleaning agents, and after the disinfectant powder atomizing device runs for any period of time, the disinfectant powder atomizing device cleaning agent is heated to 130-160 ℃ through a heating device and is sprayed out through a nozzle of the disinfectant powder atomizing device.
The aperture of the spray opening of the disinfectant powder atomizing device is smaller, the disinfectant powder is separated out along with the crystallization of the disinfectant powder after the device runs for a period of time, the spray opening or the spray pipeline is narrower, the detergent in a solution state is difficult to pass through the spray opening or the spray pipeline under the action of surface tension, the cleaning efficiency of the interior of the spray opening or the spray pipeline can be reduced, and under the component proportion of the disinfectant powder atomizing device detergent, the detergent is easy to be heated, volatilized and atomized, the atomized detergent can easily enter the spray opening or the spray pipeline with the crystallization, further, the disinfectant powder can permeate into the crystallized disinfectant powder solid more easily, and the cleaning efficiency is higher.
The sterilizing powder atomizing device is a potassium hydrogen persulfate sterilizing powder atomizing device. The potassium hydrogen persulfate disinfection powder is extremely sensitive to state change, and is easy to separate out crystals, and the potassium hydrogen persulfate after crystallization is easy to carbonize and crystallize at high temperature.
The potassium hydrogen persulfate disinfection powder atomization device cleans 20s every 10min of atomization. The cleaning process can ensure that the sterilizing powder atomizing device is not completely blocked, meanwhile, the device is not excessively cleaned, the using amount of a cleaning agent and the sterilizing time are saved, and the sterilizing efficiency is improved.
The flow of the disinfectant powder atomizing device cleaner in the cleaning process is 4.5-5.5L/h. Too low a flow rate lengthens the cleaning time and results in insufficient penetration of the cleaning agent, while too high a flow rate results in waste of the cleaning agent.
Preferably, the flow rate is 5L/h. The optimized flow can realize full and rapid cleaning and disinfection powder crystallization, avoid waste and shorten the flow for cleaning.
Compared with the prior art, the invention has the beneficial effects that: the cleaning agent with proper components and proportion is used, crystals precipitated from the disinfection powder can be dissolved fully and efficiently, the penetration of the cleaning agent in the crystallized solid is accelerated by matching with a cleaning method of heating, volatilization and atomization, the cleaning is synchronously dissolved and cleaned from the inside and the outside of the crystallized solid, the blockage of a disinfection powder atomization device is prevented, the used cleaning agent is less in dosage and high in cleaning speed, the components of the cleaning agent are low in price and low in total cost, and the efficiency of the whole disinfection process is greatly improved.
Detailed Description
Examples 1 and 7 are preferred embodiments of the present invention, and the present invention will be further described with reference to the following examples.
Example 1
A disinfectant powder atomizing device cleaning agent is prepared by uniformly mixing 30kg of ethylene glycol, 20kg of isopropanol, 1kg of sodium dodecyl sulfate and 49kg of water.
Example 2
A disinfectant powder atomizing device cleaning agent is prepared by uniformly mixing 28kg of ethylene glycol, 22kg of isopropanol, 1kg of sodium dodecyl sulfate and 49kg of water.
Example 3
A disinfectant powder atomizing device cleaning agent is prepared by uniformly mixing 28kg of ethylene glycol, 22kg of isopropanol, 0.8kg of sodium dodecyl sulfate and 48.8kg of water.
Example 4
A disinfectant powder atomizing device cleaning agent is prepared by uniformly mixing 29kg of ethylene glycol, 19kg of isopropanol, 1kg of sodium dodecyl sulfate and 51kg of water.
Example 5
A disinfectant powder atomizing device cleaning agent is prepared by uniformly mixing 32kg of ethylene glycol, 20kg of isopropanol, 1kg of sodium dodecyl sulfate and 47kg of water.
Example 6
A disinfectant powder atomizing device cleaning agent is prepared by uniformly mixing 30kg of ethylene glycol, 20kg of isopropanol, 1.2kg of sodium dodecyl sulfate and 49kg of water.
Comparative example 1
A disinfectant powder atomizing device cleaning agent is prepared by uniformly mixing 25kg of ethylene glycol, 20kg of isopropanol, 1kg of sodium dodecyl sulfate and 49kg of water.
Comparative example 2
A disinfectant powder atomizing device cleaning agent is prepared by uniformly mixing 30kg of ethylene glycol, 15kg of isopropanol, 1kg of sodium dodecyl sulfate and 51kg of water.
Comparative example 3
A disinfectant powder atomizing device cleaning agent is prepared by uniformly mixing 30kg of ethylene glycol, 20kg of isopropanol, 0.5kg of sodium dodecyl sulfate and 50kg of water.
Comparative example 4
A disinfectant powder atomizing device cleaning agent is prepared by uniformly mixing 35kg of ethylene glycol, 20kg of isopropanol, 1.2kg of sodium dodecyl sulfate and 47kg of water.
Comparative example 5
A disinfectant powder atomizing device cleaning agent is prepared by uniformly mixing 30kg of ethylene glycol, 20kg of isopropanol, 0.8kg of sodium dodecyl sulfate and 40kg of water.
Comparative example 6
A disinfectant powder atomizing device cleaning agent is prepared by uniformly mixing 30kg of ethylene glycol, 25kg of isopropanol, 1kg of sodium dodecyl sulfate and 49kg of water.
Comparative example 7
A disinfectant powder atomizing device cleaning agent is prepared by uniformly mixing 30kg of ethylene glycol, 20kg of isopropanol, 1.5kg of sodium dodecyl sulfate and 51kg of water.
Examples 7 to 12 and comparative examples 8 to 14
An application and a cleaning method of a disinfection powder atomization device are provided, wherein the disinfection powder atomization device cleaning agent prepared in the embodiments 1-6 and the comparative examples 1-7 is used for cleaning the potassium hydrogen persulfate disinfection powder atomization device respectively. Preparing a solvent from 40kg of propylene glycol, 22kg of ethylene glycol, 0.5kg of sodium dodecyl sulfate and 37.5kg of water, wherein the weight ratio of potassium hydrogen persulfate to the solvent is 1: 25 preparing a disinfectant powder solution, pressurizing the disinfectant powder solution by a pump, conveying the disinfectant powder solution to an electric heating device, heating the disinfectant powder solution to 180 ℃, volatilizing and spraying the disinfectant powder solution, wherein a flowmeter is arranged on the pump, and the flow rate is 5L/h; every 10 minutes of the disinfectant powder solution atomized by the disinfectant powder atomizing device, the disinfectant powder atomizing device cleaning agent prepared in the embodiments 1-6 and the comparative examples 1-7 is conveyed to an electric heating pipe by a pump and heated to 145 ℃, and is sprayed out through a nozzle of the disinfectant powder atomizing device, a flowmeter is arranged on the pump, the flow rate is 5L/h, the cleaning time is 20s, and the record is that the cleaning time is examples 7-12 and the comparative examples 8-14.
Examples 13 to 15 and comparative examples 15 to 16
A method for cleaning a disinfectant powder atomizing device and a cleaning method thereof, wherein the disinfectant powder atomizing device cleaning agent prepared in the embodiment 1 is used for cleaning a potassium hydrogen persulfate disinfectant powder atomizing device. Preparing a solvent from 40kg of propylene glycol, 22kg of ethylene glycol, 0.5kg of sodium dodecyl sulfate and 37.5kg of water, wherein the weight ratio of potassium hydrogen persulfate to the solvent is 1: 25 preparing a disinfectant powder solution, pressurizing the disinfectant powder solution by a pump, conveying the disinfectant powder solution to an electric heating device, heating the disinfectant powder solution to 180 ℃, volatilizing and spraying the disinfectant powder solution, wherein a flowmeter is arranged on the pump, and the flow rate is 5L/h; and conveying the cleaning agent of the disinfection powder atomizing device prepared in the embodiment 1 to an electric heating pipe by a pump to heat to 130-160 ℃ every 10 minutes of the disinfection powder solution atomized by the disinfection powder atomizing device, and spraying the cleaning agent out of a nozzle of the disinfection powder atomizing device, wherein a flow meter is arranged on the pump. Specific heating temperature, flow and cleaning time are shown in the following table 1, wherein whether the blockage is caused is the blockage condition of the spraying opening after the disinfection powder atomization device circularly works for 1 hour.
TABLE 1 cleaning Process parameters
Figure DEST_PATH_IMAGE002
According to Table 1, the dissolution efficiency of the atomized detergent for the crystals of the disinfectant powder is lowered by the heating temperature of the detergent being too low, and a longer cleaning time is required at the same flow rate, so that eventually even if the flow rate is lowered to sufficiently heat the detergent and prolong the cleaning time, the crystal solids are not sufficiently dissolved. And when the temperature is too high, the disinfection powder crystals near the spraying opening are heated and carbonized and crystallized to form more compact solid, so that the cleaning agent is more difficult to enter the interior of the crystallized solid.
Performance testing
The disinfection powder atomization devices in examples 7-12 and comparative examples 8-14 were tested to be operated circularly until the blockage time, and the blockage process of the disinfection powder atomization device is characterized in that the pump pressure of the disinfection powder solution is increased firstly, and then the flow rate is slowly decreased, so the operation time is rounded down for 5 min.
The results of the performance testing are shown in Table 2 below.
Table 2 results of performance testing
Figure DEST_PATH_IMAGE004
According to table 2, when the content of sodium dodecyl sulfate exceeds the range of the present invention, the cleaning ability is greatly reduced because the absorption of water carrier is reduced due to its too high concentration, and the crystal can not be sufficiently dissolved as the glycol and the isopropanol enter the crystal, and the boiling point of the whole system is reduced due to the too high content of the glycol and the isopropanol in the system, the water content of the atomized cleaning agent is reduced at the same temperature, and the permeability to the crystal is reduced. The proportion of the ethylene glycol to the isopropanol ensures the dispersion effect of the atomized cleaning agent, and the finer the dispersion of the liquid drops, the better the cleaning effect.
The foregoing is directed to preferred embodiments of the present invention, other and further embodiments of the invention may be devised without departing from the basic scope thereof, and the scope thereof is determined by the claims that follow. However, any simple modification, equivalent change and modification of the above embodiments according to the technical essence of the present invention are within the protection scope of the technical solution of the present invention.

Claims (8)

1. The utility model provides a disinfection powder atomizing device sanitizer which characterized in that: the composition comprises the following components in parts by weight: 28-32 parts of ethylene glycol, 18-22 parts of isopropanol, 0.8-1.2 parts of sodium dodecyl sulfate and 47-51 parts of water.
2. The disinfectant powder atomizing device cleaner according to claim 1, wherein: the composition comprises the following components in parts by weight: 30 parts of ethylene glycol, 20 parts of isopropanol, 1 part of sodium dodecyl sulfate and 49 parts of water.
3. The use of a cleaning agent for a sterilizing powder atomizing device according to claim 1 or 2, characterized in that: is used for cleaning the hydrogen potassium persulfate disinfection powder atomization device.
4. A cleaning method of a disinfection powder atomization device is characterized in that: a detergent for a disinfecting powder atomizing device prepared by using the detergent for a disinfecting powder atomizing device according to any one of claims 1 to 2, wherein said detergent for a disinfecting powder atomizing device is heated to 130 to 160 ℃ by a heating device and sprayed out through a nozzle of the disinfecting powder atomizing device after the disinfecting powder atomizing device is operated for any period of time.
5. The method for cleaning a sterilizing powder atomizing device according to claim 3, wherein: the sterilizing powder atomizing device is a potassium hydrogen persulfate sterilizing powder atomizing device.
6. The method for cleaning a sterilizing powder atomizing device according to claim 3, wherein: the potassium hydrogen persulfate disinfection powder atomization device cleans 20s every 10min of atomization.
7. The method for cleaning a sterilizing powder atomizing device according to claim 3, wherein: the flow of the disinfectant powder atomizing device cleaner in the cleaning process is 4.5-5.5L/h.
8. The method for cleaning a sterilizing powder atomizing device according to claim 7, wherein: the flow rate is 5L/h.
CN202011426978.6A 2020-12-09 2020-12-09 Disinfectant powder atomizing device cleaning agent, application and cleaning method thereof Active CN112430508B (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0633415B2 (en) * 1988-12-02 1994-05-02 花王株式会社 Skin cleanser composition
WO2003104900A2 (en) * 2002-06-07 2003-12-18 Mallinckrodt Baker Inc. Microelectronic cleaning compositions containing oxidizers and organic solvents
US20100179368A1 (en) * 2008-11-07 2010-07-15 Aries Associates, Inc. Novel Chemistries, Solutions, and Dispersal Systems for Decontamination of Chemical and Biological Systems
CN101836659A (en) * 2010-04-12 2010-09-22 湖南圣雅凯生物科技有限公司 Compound potassium hydrogen persulfate disinfectant
BR112017014894A2 (en) * 2015-01-13 2018-06-19 Syngenta Participations Ag pesticide-active heterocyclic derivatives with sulfur-containing substituents

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