CN112411229A - Method for manufacturing sorghum stalk fiber pulp for packaging paper by ultrasonic wave - Google Patents

Method for manufacturing sorghum stalk fiber pulp for packaging paper by ultrasonic wave Download PDF

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Publication number
CN112411229A
CN112411229A CN202011220436.3A CN202011220436A CN112411229A CN 112411229 A CN112411229 A CN 112411229A CN 202011220436 A CN202011220436 A CN 202011220436A CN 112411229 A CN112411229 A CN 112411229A
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China
Prior art keywords
manufacturing
feeding
pulp
stalk fiber
pumping
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CN202011220436.3A
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Chinese (zh)
Inventor
刘洁
王安睿
赵晓兵
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Jiangxi Zhongzhu Biomass Technology Co ltd
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Jiangxi Zhongzhu Biomass Technology Co ltd
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Priority to CN202011220436.3A priority Critical patent/CN112411229A/en
Publication of CN112411229A publication Critical patent/CN112411229A/en
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    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21BFIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
    • D21B1/00Fibrous raw materials or their mechanical treatment
    • D21B1/04Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C7/00Digesters
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21DTREATMENT OF THE MATERIALS BEFORE PASSING TO THE PAPER-MAKING MACHINE
    • D21D1/00Methods of beating or refining; Beaters of the Hollander type
    • D21D1/20Methods of refining

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  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Mechanical Engineering (AREA)
  • Paper (AREA)

Abstract

The invention provides a method for manufacturing sorghum stalk fiber pulp for packaging paper by ultrasonic waves, and belongs to the technical field of pulping and papermaking. The method comprises the following steps: the method comprises the following steps of feeding raw sorghum stalks into a crusher by a conveying belt to be crushed to 3-5 cm, removing dust, screening by a diamond vibrating screen, feeding into a digester, steaming for 8 hours at the water temperature of 85-105 ℃, feeding into a high-concentration mill by a feeder to perform coarse grinding, adding water to dilute to the concentration of 2.0%, feeding into an ultrasonic reactor by a pump, performing ultrasonic treatment, pumping into a slag remover to remove heavy slag, pumping good pulp into a cylinder thickener to be washed and concentrated to the concentration of 2.5-3.0%, and pumping into a coarse pulp tank for later use. The invention is based on the technical principle of ultrasonic waves, uses sorghum stalks as raw materials to prepare the fiber pulp for the packaging paper, not only solves the burden of farmers, but also relieves the problem of shortage of papermaking raw materials. Moreover, the method generates less black liquor and has better environmental protection property; the prepared sorghum stalk fiber pulp has excellent performance and is suitable for manufacturing packing paper.

Description

Method for manufacturing sorghum stalk fiber pulp for packaging paper by ultrasonic wave
Technical Field
The invention relates to the technical field of pulping and papermaking, in particular to a method for manufacturing sorghum stalk fiber pulp for packaging paper by ultrasonic waves.
Background
Plant fiber raw materials for papermaking can be roughly classified into three categories: wood fibers, grass fibers, cotton and hemp fibers. In recent years, forestry resources in China are disorderly cut and felled, so that the forestry resources in China are seriously damaged, and therefore the state increases the control strength on the forestry resources. The paper stock market has also been impacted.
The sorghum stalks are one of the varieties of crops, become useless objects after autumn, are thrown away by farmers in the field, and are burnt in the field after the spring of the next year, thereby not only increasing the pressure of environmental protection, but also wasting resources. Under the condition, if the sorghum stalks are used as raw materials and the characteristics of high fiber content are utilized to manufacture paper pulp, the resource utilization way of the sorghum stalks is expected to be expanded.
However, in general, grass plants are mostly vascular fibers, and contain therein foreign cells, which have many adverse effects on paper making, are poorly interlaced with fibers, directly affect the strength of paper, and have a large surface area, so that the absorbability of the foreign cells also affects the dimensional stability of paper. Therefore, the original pulping method utilizes alkaline cooking to disintegrate the mixed cell groups into single cell lines and strengthen washing, screening and purifying. The method can remove the mixed cells as much as possible, and can improve the strength of various physical indexes of the paper. But it is characterized in that a large amount of black liquor generated in the pulp in the cooking process can not be treated, if the black liquor is directly discharged, the black liquor can cause pollution, and if the black liquor is not discharged, the black liquor can not be stored for a long time.
Disclosure of Invention
The invention aims to provide a method for manufacturing sorghum stalk fiber pulp for packaging paper by ultrasonic waves aiming at the technical defects of the prior art, so as to solve the technical problem that the resource utilization way of sorghum stalks needs to be expanded.
The invention aims to solve another technical problem that the quality of the obtained paper pulp and the quality of the finished paper need to be improved when the sorghum stalks are used for pulping and papermaking.
The invention also aims to solve the technical problem of how to reduce the generation and the discharge of black liquor in the process of pulping and papermaking by using sorghum stalks.
In order to achieve the technical purpose, the invention adopts the following technical scheme:
the method for manufacturing the sorghum stalk fiber pulp for the packaging paper by ultrasonic waves comprises the following steps: the method comprises the following steps of feeding raw sorghum stalks into a crusher by a conveying belt to be crushed to 3-5 cm, removing dust, screening by a diamond vibrating screen, feeding into a digester, steaming for 8 hours at the water temperature of 85-105 ℃, feeding into a high-concentration mill by a feeder to perform coarse grinding, adding water to dilute to the concentration of 2.0%, feeding into an ultrasonic reactor by a pump, performing ultrasonic treatment, pumping into a slag remover to remove heavy slag, pumping good pulp into a cylinder thickener to be washed and concentrated to the concentration of 2.5-3.0%, and pumping into a coarse pulp tank for later use.
Preferably, the dust removal is realized by using a fan or a water washing device.
Preferably, after the rhombus vibrating screen is used for screening, the material is fed into the digester by a screw conveyor or a conveyer belt.
Preferably, the digester is a vertical pot or a pipe-connected digester.
Preferably, the ultrasonic reactor comprises a generator, a heat exchanger and a reaction vessel.
Preferably, the heavy slag is re-cooked before being sent to the digester.
The invention utilizes the special technical characteristics of ultrasonic waves to prepare the sorghum stalk fiber pulp. The ultrasonic wave is a sound wave with frequency beyond human hearing range, the ultrasonic wave is propagated by an elastic medium, when the ultrasonic wave is propagated, the particles in the elastic medium are vibrated, and energy is transferred through the medium according to the propagation direction of the ultrasonic wave, the wave can be divided into longitudinal wave and transverse wave, both the longitudinal wave and the transverse wave can be transferred in the solid, only the longitudinal wave can be transferred in the liquid and the gas, and an elastic weak area also exists in the reactor, namely, the gas core expands and grows under the action of gas or dust in the liquid, and is filled with surrounding liquid steam or gas, and the cavity collapses and breaks due to the great difference of internal and external pressure, so that the concentrated sound field energy is released in extremely short time and extremely small space. The medium is locally formed into high-temperature environment with hundreds of to thousands of K and atmosphere pressure environment exceeding hundreds of atmospheric pressure, and generates great impact force, so that the medium plays a role of intense stirring, simultaneously generates a large amount of micro bubbles, the micro bubbles are circularly continued when being used as new gas nuclei, the group cells of impurities in the primary pulp are disintegrated into single cells under the specific action of the micro bubbles, and then the single cells are washed, screened and purified. It can also have the same effect as soda cooking pulping, and can raise pulp quality and yield.
The invention is based on the technical principle of ultrasonic waves, uses sorghum stalks as raw materials to prepare the fiber pulp for the packaging paper, not only solves the burden of farmers, but also relieves the problem of shortage of papermaking raw materials to a certain extent. Moreover, the method generates less black liquor and has better environmental protection property; the prepared sorghum stalk fiber pulp has excellent performance and is suitable for manufacturing packing paper.
Drawings
FIG. 1 is a process flow diagram of the present invention.
Detailed Description
Hereinafter, specific embodiments of the present invention will be described in detail. Well-known structures or functions may not be described in detail in the following embodiments in order to avoid unnecessarily obscuring the details. Approximating language, as used herein in the following examples, may be applied to identify quantitative representations that could permissibly vary in number without resulting in a change in the basic function. Unless defined otherwise, technical and scientific terms used in the following examples have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs.
Example 1
The method comprises the steps of feeding raw sorghum stalks into a crusher by a conveyor belt to be crushed into 3-5 cm, carrying out dust removal (water or wind power), then screening by a diamond vibrating screen (removing part of impurities firstly), then feeding into a digester by a screw or the conveyor belt (connecting pipe cooking or vertical pot), steaming for 8 hours at the temperature of 85-105 ℃, then feeding into a high-concentration mill by a feeder to carry out coarse grinding, then adding water to dilute for 2.0%, feeding into an ultrasonic reactor by a pump (the ultrasonic reactor consists of three parts which are respectively a generator, a heat exchanger and a reaction container), passing through the ultrasonic reactor, then pumping into a slag remover to remove heavy slag (the heavy slag is sent into the digester and is cooked again), pumping good pulp into a cylinder thickener to wash and concentrate for 2.5-3.0%, and pumping into a coarse pulp tank for later use.
The method is utilized to prepare the paper pulp for three times respectively, and the finished paper is prepared by adopting the conventional paper making method, and then the performance of the paper is detected as follows:
TABLE 1 paper Property test results
Name (R) Concentration% Degree of percussion SR Wet weight Whiteness degree
Test 1 3.0 31 3.5 40
Test 2 2.6 29 3.0 42
Test 3 2.3 26.5 3.1 40.5
The test data show that the method for preparing the pulp for the packaging paper by using the sorghum stalks is completely feasible.
Example 2
The method for manufacturing the sorghum stalk fiber pulp for the packaging paper by ultrasonic waves comprises the following steps: the method comprises the following steps of feeding raw sorghum stalks into a crusher by a conveying belt to be crushed to 3-5 cm, removing dust, screening by a diamond vibrating screen, feeding into a digester, steaming for 8 hours at the water temperature of 85-105 ℃, feeding into a high-concentration mill by a feeder to perform coarse grinding, adding water to dilute to the concentration of 2.0%, feeding into an ultrasonic reactor by a pump, performing ultrasonic treatment, pumping into a slag remover to remove heavy slag, pumping good pulp into a cylinder thickener to be washed and concentrated to the concentration of 2.5-3.0%, and pumping into a coarse pulp tank for later use.
Wherein, the dust removal is realized by utilizing a fan or water washing equipment. After the rhombus vibrating screen is screened, the material is sent into a digester by a screw conveyer or a conveyer belt. The digester is a vertical pot or a connecting pipe for cooking. The ultrasonic reactor comprises a generator, a heat exchanger and a reaction container. And (5) before the heavy slag is sent to the digester, the heavy slag is steamed again.
Example 3
The method for manufacturing the sorghum stalk fiber pulp for the packaging paper by ultrasonic waves comprises the following steps: the method comprises the following steps of feeding raw sorghum stalks into a crusher by a conveying belt to be crushed to 3-5 cm, removing dust, screening by a diamond vibrating screen, feeding into a digester, steaming for 8 hours at the water temperature of 85-105 ℃, feeding into a high-concentration mill by a feeder to perform coarse grinding, adding water to dilute to the concentration of 2.0%, feeding into an ultrasonic reactor by a pump, performing ultrasonic treatment, pumping into a slag remover to remove heavy slag, pumping good pulp into a cylinder thickener to be washed and concentrated to the concentration of 2.5-3.0%, and pumping into a coarse pulp tank for later use.
The embodiments of the present invention have been described in detail, but the description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention. Any modification, equivalent replacement, and improvement made within the scope of the application of the present invention should be included in the protection scope of the present invention.

Claims (6)

1. The method for manufacturing the sorghum stalk fiber pulp for the packaging paper by ultrasonic waves is characterized by comprising the following steps: the method comprises the following steps of feeding raw sorghum stalks into a crusher by a conveying belt to be crushed to 3-5 cm, removing dust, screening by a diamond vibrating screen, feeding into a digester, steaming for 8 hours at the water temperature of 85-105 ℃, feeding into a high-concentration mill by a feeder to perform coarse grinding, adding water to dilute to the concentration of 2.0%, feeding into an ultrasonic reactor by a pump, performing ultrasonic treatment, pumping into a slag remover to remove heavy slag, pumping good pulp into a cylinder thickener to be washed and concentrated to the concentration of 2.5-3.0%, and pumping into a coarse pulp tank for later use.
2. The method of ultrasonically manufacturing sorghum stalk fiber pulp for wrapping paper according to claim 1, wherein the dust removal is performed by using a blower or a water washing apparatus.
3. The ultrasonic method for manufacturing sorghum stalk fiber slurry for wrapping paper according to claim 1, wherein after the screen of the diamond-shaped vibrating screen, the material is fed into a digester by a screw conveyor or a conveyer belt.
4. The method of ultrasonically manufacturing sorghum stalk fiber pulp for wrapping paper according to claim 1, wherein the digester is a vertical pot or a pipe-connected digester.
5. The method of ultrasonically manufacturing sorghum stalk fiber pulp for wrapping paper according to claim 1, wherein the ultrasonic reactor comprises a generator, a heat exchanger and a reaction vessel.
6. The method of ultrasonically manufacturing sorghum stalk fiber slurry for wrapping paper according to claim 1, wherein the heavy residues are re-cooked before being fed to the digester.
CN202011220436.3A 2020-11-05 2020-11-05 Method for manufacturing sorghum stalk fiber pulp for packaging paper by ultrasonic wave Pending CN112411229A (en)

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WO2009018469A1 (en) * 2007-07-31 2009-02-05 Hoffman Richard B System and method of preparing pre-treated biorefinery feedstock from raw and recycled waste cellulosic biomass
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CN105239199A (en) * 2015-10-20 2016-01-13 湖州申祥丝织有限责任公司 Novel composite fiber based on sweet sorghum skin fiber and preparation method thereof
CN105906398A (en) * 2016-04-13 2016-08-31 齐鲁工业大学 Method for preparing organic fertilizer through processing agriculture and forestry wastes by using organic solvent
CN106400560A (en) * 2016-08-19 2017-02-15 陈淑华 Process for producing paper pulp through enzymolysis
CN106636218A (en) * 2017-03-16 2017-05-10 福建农林大学 Method for preparing biogas and paper pulp from energy grass
CN107747246A (en) * 2017-10-28 2018-03-02 李鑫 A kind of ultrasonic wave extraction string production technology and equipments
CN110002445A (en) * 2019-04-10 2019-07-12 浙江清风源环保科技有限公司 The method for preparing high absorption property active carbon and activation using broomcorn straw
CN111712597A (en) * 2018-02-13 2020-09-25 日本制纸株式会社 Flame-retardant composite fiber and method for producing same

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WO2009018469A1 (en) * 2007-07-31 2009-02-05 Hoffman Richard B System and method of preparing pre-treated biorefinery feedstock from raw and recycled waste cellulosic biomass
CN101362596A (en) * 2008-06-18 2009-02-11 梁知维 Systematization method for ecological carbon emission reduction
CN105239199A (en) * 2015-10-20 2016-01-13 湖州申祥丝织有限责任公司 Novel composite fiber based on sweet sorghum skin fiber and preparation method thereof
CN105906398A (en) * 2016-04-13 2016-08-31 齐鲁工业大学 Method for preparing organic fertilizer through processing agriculture and forestry wastes by using organic solvent
CN106400560A (en) * 2016-08-19 2017-02-15 陈淑华 Process for producing paper pulp through enzymolysis
CN106636218A (en) * 2017-03-16 2017-05-10 福建农林大学 Method for preparing biogas and paper pulp from energy grass
CN107747246A (en) * 2017-10-28 2018-03-02 李鑫 A kind of ultrasonic wave extraction string production technology and equipments
CN111712597A (en) * 2018-02-13 2020-09-25 日本制纸株式会社 Flame-retardant composite fiber and method for producing same
CN110002445A (en) * 2019-04-10 2019-07-12 浙江清风源环保科技有限公司 The method for preparing high absorption property active carbon and activation using broomcorn straw

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Application publication date: 20210226