CN112400914A - Archival repository insecticide - Google Patents
Archival repository insecticide Download PDFInfo
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- CN112400914A CN112400914A CN202011144837.5A CN202011144837A CN112400914A CN 112400914 A CN112400914 A CN 112400914A CN 202011144837 A CN202011144837 A CN 202011144837A CN 112400914 A CN112400914 A CN 112400914A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/06—Oxygen or sulfur directly attached to a cycloaliphatic ring system
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N49/00—Biocides, pest repellants or attractants, or plant growth regulators, containing compounds containing the group, wherein m+n>=1, both X together may also mean —Y— or a direct carbon-to-carbon bond, and the carbon atoms marked with an asterisk are not part of any ring system other than that which may be formed by the atoms X, the carbon atoms in square brackets being part of any acyclic or cyclic structure, or the group, wherein A means a carbon atom or Y, n>=0, and not more than one of these carbon atoms being a member of the same ring system, e.g. juvenile insect hormones or mimics thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/06—Coniferophyta [gymnosperms], e.g. cypress
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/24—Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/44—Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention discloses an archival repository insecticide in the technical field of archival repository insecticides, which comprises the following specific steps: mixing rhizome of herba Setariae viridis, fruit of Carpesium fructus, Chenopodium album, folium Artemisiae Argyi, herba Taraxaci and herba Menthae, stirring, and decocting in water; adding water into the rutabaga and the mint in corresponding parts for distillation, and collecting distillate; mixing the decoction residues in the step two and the distillation residues in the step three, decocting again for 40-60 minutes, and mixing the decocted supernatant with the solutions in the container A and the container B to obtain a solution C; the preparation method comprises the steps of adding ethanol into the solution C, filtering by using a 800-mesh sieve, and taking supernatant, so as to finish the preparation of main medicine components, so as to be convenient for the preparation of tablets and gel.
Description
Technical Field
The invention relates to the technical field of medium-grade storehouse pesticides, in particular to a file storehouse pesticide.
Background
The file storehouse belongs to a relatively special public place, and insect expelling and sterilization of the file storehouse are necessary to a certain extent. The file storehouse is relatively closed, air flowability is poor, moisture is easy to occur, microbes such as bacteria, insects and mites are easy to breed, and the file data stacked for years can emit paper stain smell and mildew smell. In addition, some newly-warehoused files can also generate various microorganisms in the processing process, ink, dye, type and adhesive used in the file binding process in the paper are volatilized to generate pungent smell, and after the files are returned by borrowing, the hidden danger of bacteria is also existed, so that the health of workers or follow-up borrowers can be possibly damaged. Above will certainly cause the interior environment of file storehouse dirty, the easy cross infection of various communicable diseases, the camphor ball disinfection that present file storehouse adopted more, disinfect, but the volatile gas that the camphor ball produced has the stimulation effect to human retina, respiratory track, influences staff or borrower's healthy, for this reason, we propose a file storehouse insecticide.
Disclosure of Invention
The invention aims to provide an archival repository insecticide to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme: an archival repository insecticide comprises the following components:
the main medicine components are as follows: 5-11 parts of Pilocarpus japonicas, 5-11 parts of rhizome of green bristlegrass, 5-11 parts of fruit of common carpesium fruit, 5-11 parts of chenopodium album linn, 3-5 parts of Artemisia argyi, 2-5 parts of mint, 2-5 parts of dandelion and 2-4 parts of ethanol;
auxiliary additive for tablet preparation: 5-10 parts of borneol, 5-10 parts of cedrol, 2-3 parts of cedar oil, 1-2 parts of pine needle oil, 2-4 parts of lavender oil, 1-3 parts of rosemary oil, 1-2 parts of anise, 1-2 parts of geraniol and 1 part of cinnamyl cinnamate;
gel preparation auxiliary additive: 5-10 parts of litsea cubeba oil, 5-8 parts of methoprene, 4-7 parts of pyrethrin, 2-4 parts of sodium silicate solution, 1-3 parts of diluted hydrochloric acid and 1-2 parts of insect attractant.
The preparation method of the pesticide comprises the following specific steps:
the method comprises the following steps: selecting and removing impurities of the components, weighing the components according to the parts ratio of the components, and independently placing the components for later use;
step two: mixing and stirring rhizome of green bristlegrass herb, fruit of carpesium abrotanoides, chenopodium glaucum, artemisia argyi, dandelion and mint together, adding water for decocting, continuously stirring in the decocting process, boiling, decocting with slow fire for 30-60 minutes, filtering to obtain filtrate, and storing by a container as A;
step three: adding water into the rutabaga and the mint in corresponding parts for distillation, collecting distillate, and storing the distilled water solution as B through a container;
step four: mixing the decoction residues in the step two and the distillation residues in the step three, decocting again for 40-60 minutes, and mixing the decocted supernatant with the solutions in the container A and the container B to obtain a solution C;
step five: adding ethanol into the solution C, stirring while adding ethanol, detecting the alcohol content in the solution C in real time by an alcohol content detector to ensure that the alcohol content reaches more than 40%, filtering by using a 800-mesh sieve to obtain a supernatant, thereby completing the preparation of the main drug component, and then equally dividing the supernatant into two parts and subpackaging the two parts in two groups of reagent bottles for later use;
step six: preparing tablets: taking out one part of the reagent bottle in the fifth step, putting the solution into a sealed heating kettle, putting borneol, cedrol, cedar oil, pine needle oil, lavender oil, rosemary oil, anise, geraniol and lauryl cinnamate into the sealed heating kettle, heating to 200 +/-10 ℃, mixing and melting, on one hand, preparing medicament tablets by pouring a mold while hot, and on the other hand, cooling, crystallizing and processing into tablets after melting;
step seven: preparing gel: and taking out the other part of the reagent bottle in the fifth step, adding the litsea cubeba oil, the methoprene and the pyrethrin, stirring until a uniform and transparent liquid is formed, supplementing water into the liquid, weighing the sodium silicate solution, adding the sodium silicate solution into the water, stirring and diluting uniformly, strongly stirring at normal temperature, slowly adding the dilute hydrochloric acid until the pH value is adjusted to 7-8, rapidly adding the insect attractant under strong stirring, uniformly stirring, pouring into four glass vessels in equal parts, and standing to form the transparent gel.
And seventhly, selecting the water-based microemulsion and 10-15% of water-soluble solvent as the insect attractant, diluting the water-based microemulsion with water at room temperature, dissolving the rest components in the water-soluble solvent, uniformly mixing the two solutions, and preparing into transparent uniform liquid.
Compared with the prior art, the invention has the beneficial effects that:
1. the invention takes the Ruta graveolens, the rhizome of Setaria viridis, the fruit of Carpesium, the Chenopodium album linn, the Artemisia argyi and the dandelion as main medicine components, the supernatant fluid is taken by decoction, the gas volatilized from the liquid has the functions of expelling parasite, killing parasite, sterilizing and inhibiting the reproduction of worm eggs, and the Ruta graveolens and the mint also have the function of eliminating the bitter smell, the dandelion is taken as an adjuvant drug to further harmonize the property of the main drug, the effects of sterilization and air freshening are further enhanced, the ethanol content is lower, the invention has good effect on human body, no irritation and no corrosion to surrounding articles, the plant components extracted in the invention can enhance the immunity of human body, and the like, is especially suitable for being used in a relatively closed file room with unsmooth air circulation, equally divides the main drug components into two groups, different auxiliary materials are respectively added into the two groups for tablet preparation and gel preparation, and the finished products have the environment-friendly insecticidal property of the main drug;
2. borneol, cedrol, cedar oil, pine needle oil, lavender oil, rosemary oil, anise, geraniol and cinnamic acid ester are adopted in the preparation of the tablets, the components can play a role in synergism and synergy, are favorable for preventing pests from generating drug resistance, and have high-efficiency insect repelling, killing and bacteriostasis effects;
3. the invention adopts litsea cubeba oil, methoprene and pyrethrin to prepare water-soluble sol in the preparation process of the gel, can be directly coated on the inner wall of a file cabinet, has the advantages of wide insecticidal spectrum, high efficiency, ovicidal effect, insect growth inhibition, small dosage, convenient application, difficult pest drug resistance generation, fumigating and killing effect, has the double functions of bacteriostasis, mildew prevention and insect killing, low residue, safety to human and livestock, can eliminate pollution caused by unbalanced application, and is beneficial to the improvement of ecological environment.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
An archival repository insecticide comprises the following components:
the main medicine components are as follows: 6 parts of herba Pileae Scriptae, 6 parts of rhizome of herba Setariae viridis, 6 parts of fruit of Carpesium fructus, 7 parts of Chenopodium album, 3 parts of folium Artemisiae Argyi, 3 parts of herba Menthae, 3 parts of herba Taraxaci and 3 parts of ethanol;
auxiliary additive for tablet preparation: 7 parts of borneol, 7 parts of cedrol, 2 parts of cedar oil, 1 part of pine needle oil, 3 parts of lavender oil, 2 parts of rosemary oil, 1 part of anise, 1 part of geraniol and 1 part of cinnamic acid ester;
gel preparation auxiliary additive: 8 parts of litsea cubeba oil, 6 parts of methoprene, 5 parts of pyrethrin, 3 parts of sodium silicate solution, 2 parts of dilute hydrochloric acid and 1 part of insect attractant.
The preparation method of the pesticide comprises the following specific steps:
the method comprises the following steps: selecting and removing impurities of the components, weighing the components according to the parts ratio of the components, and independently placing the components for later use;
step two: mixing and stirring rhizome of green bristlegrass herb, fruit of carpesium abrotanoides, chenopodium glaucum, artemisia argyi, dandelion and mint together, then adding water for decocting, continuously stirring the materials in the decocting process, boiling the materials firstly, then decocting the materials for 40 minutes by soft fire, filtering the materials to obtain filtrate, and storing the filtrate by a container to obtain A;
step three: adding water into the rutabaga and the mint in corresponding parts for distillation, collecting distillate, and storing the distilled water solution as B through a container;
step four: mixing the decoction residues in the step two and the distillation residues in the step three, decocting again for 40 minutes, and mixing the decocted supernatant with the solutions in the container A and the container B to obtain a solution C;
step five: adding ethanol into the solution C, stirring while adding ethanol, detecting the alcohol content in the solution C in real time by an alcohol content detector to ensure that the alcohol content reaches more than 40%, filtering by using a 800-mesh sieve to obtain a supernatant, thereby completing the preparation of the main drug component, and then equally dividing the supernatant into two parts and subpackaging the two parts in two groups of reagent bottles for later use;
step six: preparing tablets: taking out one part of the reagent bottle in the fifth step, putting the solution into a sealed heating kettle, putting borneol, cedrol, cedar oil, pine needle oil, lavender oil, rosemary oil, anise, geraniol and lauryl cinnamate into the sealed heating kettle, heating to 200 +/-10 ℃, mixing and melting, on one hand, preparing medicament tablets by pouring a mold while hot, and on the other hand, cooling, crystallizing and processing into tablets after melting;
step seven: preparing gel: and taking out the other part of the reagent bottle in the fifth step, adding the litsea cubeba oil, the methoprene and the pyrethrin, stirring until a uniform and transparent liquid is formed, supplementing water into the liquid, weighing the sodium silicate solution, adding the sodium silicate solution into the water, stirring and diluting uniformly, strongly stirring at normal temperature, slowly adding the dilute hydrochloric acid until the pH value is adjusted to 7-8, rapidly adding the insect attractant under strong stirring, uniformly stirring, pouring into four glass vessels in equal parts, and standing to form the transparent gel.
And seventhly, selecting the water-based microemulsion and a 10% water-soluble solvent as the insect attractant, diluting the water-based microemulsion with water at room temperature, dissolving the rest components in the water-soluble solvent, uniformly mixing the two solutions to prepare a transparent uniform liquid, wherein the water-based microemulsion does not contain benzene solvents and solvent oil compared with the missible oil, does not have print when being sprayed on a storage object, does not pollute the storage object, reduces the dosage of effective components while keeping the same control effect, greatly reduces the dosage of organic solvents, and ensures that the preparation meets the requirement of environmental protection better.
Example 2
An archival repository insecticide comprises the following components:
the main medicine components are as follows: 10 parts of herba Pileae Scriptae, 10 parts of rhizome of herba Setariae viridis, 10 parts of fructus Carpesii fruit, 9 parts of Chenopodium album, 5 parts of folium Artemisiae Argyi, 4 parts of herba Menthae, 4 parts of herba Taraxaci and 4 parts of ethanol;
auxiliary additive for tablet preparation: 9 parts of borneol, 9 parts of cedrol, 3 parts of cedar oil, 2 parts of pine needle oil, 4 parts of lavender oil, 3 parts of rosemary oil, 2 parts of anise, 2 parts of geraniol and 1 part of cinnamic acid ester;
gel preparation auxiliary additive: 10 parts of litsea cubeba oil, 8 parts of methoprene, 6 parts of pyrethrin, 4 parts of sodium silicate solution, 3 parts of dilute hydrochloric acid and 2 parts of insect attractant.
The preparation method of the pesticide comprises the following specific steps:
the method comprises the following steps: selecting and removing impurities of the components, weighing the components according to the parts ratio of the components, and independently placing the components for later use;
step two: mixing and stirring rhizome of green bristlegrass herb, fruit of carpesium abrotanoides, chenopodium glaucum, artemisia argyi, dandelion and mint together, then adding water for decocting, continuously stirring the materials in the decocting process, boiling the materials firstly, then decocting the materials with soft fire for 60 minutes, filtering the materials to obtain filtrate, and storing the filtrate by a container to obtain A;
step three: adding water into the rutabaga and the mint in corresponding parts for distillation, collecting distillate, and storing the distilled water solution as B through a container;
step four: mixing the decoction residues in the step two and the distillation residues in the step three, decocting again for 60 minutes, and mixing the decocted supernatant with the solutions in the container A and the container B to obtain a solution C;
step five: adding ethanol into the solution C, stirring while adding ethanol, detecting the alcohol content in the solution C in real time by an alcohol content detector to ensure that the alcohol content reaches more than 40%, filtering by using a 800-mesh sieve to obtain a supernatant, thereby completing the preparation of the main drug component, and then equally dividing the supernatant into two parts and subpackaging the two parts in two groups of reagent bottles for later use;
step six: preparing tablets: taking out one part of the reagent bottle in the fifth step, putting the solution into a sealed heating kettle, putting borneol, cedrol, cedar oil, pine needle oil, lavender oil, rosemary oil, anise, geraniol and lauryl cinnamate into the sealed heating kettle, heating to 200 +/-10 ℃, mixing and melting, on one hand, preparing medicament tablets by pouring a mold while hot, and on the other hand, cooling, crystallizing and processing into tablets after melting;
step seven: preparing gel: and taking out the other part of the reagent bottle in the fifth step, adding the litsea cubeba oil, the methoprene and the pyrethrin, stirring until a uniform and transparent liquid is formed, supplementing water into the liquid, weighing the sodium silicate solution, adding the sodium silicate solution into the water, stirring and diluting uniformly, strongly stirring at normal temperature, slowly adding the dilute hydrochloric acid until the pH value is adjusted to 7-8, rapidly adding the insect attractant under strong stirring, uniformly stirring, pouring into four glass vessels in equal parts, and standing to form the transparent gel.
And seventhly, selecting the water-based microemulsion and a 15% water-soluble solvent as the insect attractant, diluting the water-based microemulsion with water at room temperature, dissolving the rest components in the water-soluble solvent, uniformly mixing the two solutions to prepare a transparent uniform liquid, wherein the water-based microemulsion does not contain benzene solvents and solvent oil compared with the missible oil, does not have print when being sprayed on a storage object, does not pollute the storage object, reduces the dosage of effective components while keeping the same control effect, greatly reduces the dosage of organic solvents, and ensures that the preparation meets the requirement of environmental protection better.
The invention takes the main drug components of the northern ruta, the rhizome of the green bristlegrass herb, the fruit of the carpesium arvense, the chenopodium glaucum, the mugwort and the dandelion as main drug components, the supernatant fluid is taken by decoction, the gas volatilized by the liquid has the functions of expelling parasites, killing insects, disinfecting, sterilizing and inhibiting the propagation of worm eggs, the northern ruta and the mint also have the function of eliminating bitter odor, the dandelion is taken as an adjuvant drug to further regulate the drug properties of the main drug components, the functions of sterilizing and refreshing air are further enhanced, the ethanol content is lower, the main drug components have good and non-irritant properties to human bodies, and have no corrosivity to surrounding articles, the plant components extracted in the invention can enhance the immunity of human bodies and the like, and are particularly suitable for being used in a file room which is relatively closed and has unsmooth air circulation, the main drug components are equally divided into two groups, and different auxiliary materials, borneol, cedrol, cedar oil, pine needle oil, lavender oil, rosemary oil, anise, geraniol and cinnamic acid ester are adopted in the preparation of the tablet, the components can play a role in synergism and synergism, are favorable for preventing pests from generating drug resistance, have high-efficiency insect repelling, killing and bacteriostasis effects, have no toxic or side effect in each component in the formula, are harmless to the health, have stable chemical properties, do not generate chemical reaction and color change on preserved articles, adopt litsea cubeba oil, methoprene and pyrethrin in the preparation process of gel to prepare water-soluble sol, can be directly coated on the inner wall of a file cabinet, have wide insecticidal spectrum, high efficiency, egg killing, insect growth inhibition, small dosage, convenient application, and difficult pest drug resistance generation, and have the effect of fumigating and killing.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (2)
1. An archival repository insecticide, which is characterized in that: the insecticide comprises the following components:
the main medicine components are as follows: 5-11 parts of Pilocarpus japonicas, 5-11 parts of rhizome of green bristlegrass, 5-11 parts of fruit of common carpesium fruit, 5-11 parts of chenopodium album linn, 3-5 parts of Artemisia argyi, 2-5 parts of mint, 2-5 parts of dandelion and 2-4 parts of ethanol;
auxiliary additive for tablet preparation: 5-10 parts of borneol, 5-10 parts of cedrol, 2-3 parts of cedar oil, 1-2 parts of pine needle oil, 2-4 parts of lavender oil, 1-3 parts of rosemary oil, 1-2 parts of anise, 1-2 parts of geraniol and 1 part of cinnamyl cinnamate;
gel preparation auxiliary additive: 5-10 parts of litsea cubeba oil, 5-8 parts of methoprene, 4-7 parts of pyrethrin, 2-4 parts of sodium silicate solution, 1-3 parts of diluted hydrochloric acid and 1-2 parts of insect attractant;
the preparation method of the pesticide comprises the following specific steps:
the method comprises the following steps: selecting and removing impurities of the components, weighing the components according to the parts ratio of the components, and independently placing the components for later use;
step two: mixing and stirring rhizome of green bristlegrass herb, fruit of carpesium abrotanoides, chenopodium glaucum, artemisia argyi, dandelion and mint together, adding water for decocting, continuously stirring in the decocting process, boiling, decocting with slow fire for 30-60 minutes, filtering to obtain filtrate, and storing by a container as A;
step three: adding water into the rutabaga and the mint in corresponding parts for distillation, collecting distillate, and storing the distilled water solution as B through a container;
step four: mixing the decoction residues in the step two and the distillation residues in the step three, decocting again for 40-60 minutes, and mixing the decocted supernatant with the solutions in the container A and the container B to obtain a solution C;
step five: adding ethanol into the solution C, stirring while adding ethanol, detecting the alcohol content in the solution C in real time by an alcohol content detector to ensure that the alcohol content reaches more than 40%, filtering by using a 800-mesh sieve to obtain a supernatant, thereby completing the preparation of the main drug component, and then equally dividing the supernatant into two parts and subpackaging the two parts in two groups of reagent bottles for later use;
step six: preparing tablets: taking out one part of the reagent bottle in the fifth step, putting the solution into a sealed heating kettle, putting borneol, cedrol, cedar oil, pine needle oil, lavender oil, rosemary oil, anise, geraniol and lauryl cinnamate into the sealed heating kettle, heating to 200 +/-10 ℃, mixing and melting, on one hand, preparing medicament tablets by pouring a mold while hot, and on the other hand, cooling, crystallizing and processing into tablets after melting;
step seven: preparing gel: and taking out the other part of the reagent bottle in the fifth step, adding the litsea cubeba oil, the methoprene and the pyrethrin, stirring until a uniform and transparent liquid is formed, supplementing water into the liquid, weighing the sodium silicate solution, adding the sodium silicate solution into the water, stirring and diluting uniformly, strongly stirring at normal temperature, slowly adding the dilute hydrochloric acid until the pH value is adjusted to 7-8, rapidly adding the insect attractant under strong stirring, uniformly stirring, pouring into four glass vessels in equal parts, and standing to form the transparent gel.
2. The archival repository insecticide of claim 1, wherein: and seventhly, selecting the water-based microemulsion and 10-15% of water-soluble solvent as the insect attractant, diluting the water-based microemulsion with water at room temperature, dissolving the rest components in the water-soluble solvent, uniformly mixing the two solutions, and preparing into transparent uniform liquid.
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CN202011144837.5A CN112400914A (en) | 2020-10-23 | 2020-10-23 | Archival repository insecticide |
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CN202011144837.5A CN112400914A (en) | 2020-10-23 | 2020-10-23 | Archival repository insecticide |
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CN1086960A (en) * | 1992-11-17 | 1994-05-25 | 白瑛 | A kind of efficient safety moth preventing agent |
CN101999345A (en) * | 2010-10-20 | 2011-04-06 | 周端午 | Environmentally-friendly, long-acting, bacteriostatic, mildewproof and pesticidal sol preparation |
CN102450250A (en) * | 2010-10-20 | 2012-05-16 | 周端午 | Bacteriostatic mildew-resistant insecticidal sustained release agent prepared from sol/gel also used as insect attractant |
CN102450252A (en) * | 2010-10-20 | 2012-05-16 | 周端午 | Green, long-lasting antibacterial, mildew-resistant and insecticidal water-based micro-emulsifier |
CN104888260A (en) * | 2015-06-06 | 2015-09-09 | 青岛科维源环保技术有限公司 | Traditional Mongolian and Chinese medicine air freshener for realizing insect expelling and sterilization of muniment room |
WO2017136544A1 (en) * | 2016-02-05 | 2017-08-10 | Genviro Inc. | Insect control formulations |
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2020
- 2020-10-23 CN CN202011144837.5A patent/CN112400914A/en active Pending
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1086960A (en) * | 1992-11-17 | 1994-05-25 | 白瑛 | A kind of efficient safety moth preventing agent |
CN101999345A (en) * | 2010-10-20 | 2011-04-06 | 周端午 | Environmentally-friendly, long-acting, bacteriostatic, mildewproof and pesticidal sol preparation |
CN102450250A (en) * | 2010-10-20 | 2012-05-16 | 周端午 | Bacteriostatic mildew-resistant insecticidal sustained release agent prepared from sol/gel also used as insect attractant |
CN102450252A (en) * | 2010-10-20 | 2012-05-16 | 周端午 | Green, long-lasting antibacterial, mildew-resistant and insecticidal water-based micro-emulsifier |
CN104888260A (en) * | 2015-06-06 | 2015-09-09 | 青岛科维源环保技术有限公司 | Traditional Mongolian and Chinese medicine air freshener for realizing insect expelling and sterilization of muniment room |
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