CN112374756A - Method for preparing Longquan porcelain by combining Guizhou kiln wooden leaf cup and Longquan kiln thick glaze - Google Patents
Method for preparing Longquan porcelain by combining Guizhou kiln wooden leaf cup and Longquan kiln thick glaze Download PDFInfo
- Publication number
- CN112374756A CN112374756A CN202011109837.1A CN202011109837A CN112374756A CN 112374756 A CN112374756 A CN 112374756A CN 202011109837 A CN202011109837 A CN 202011109837A CN 112374756 A CN112374756 A CN 112374756A
- Authority
- CN
- China
- Prior art keywords
- kiln
- parts
- glaze
- longquan
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/24—Manufacture of porcelain or white ware
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/32—Burning methods
- C04B33/34—Burning methods combined with glazing
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6567—Treatment time
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/66—Specific sintering techniques, e.g. centrifugal sintering
- C04B2235/661—Multi-step sintering
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Structural Engineering (AREA)
- Inorganic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacturing & Machinery (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Glass Compositions (AREA)
Abstract
The invention discloses a preparation method for manufacturing Longquan porcelain by combining a Jizhou kiln marigold and Longquan kiln thick glaze, which comprises the following steps: preparing plum green glaze; preparing black glaze material; preparing a blank; repairing a groove at a required green glaze applying position, and dipping plum green glaze slurry on the groove by a writing brush to form arc bulges layer by layer; firing the green body in a kiln to form Longquan kiln thick glaze; naturally cooling the fired blank in a kiln to room temperature, and taking out of the kiln; spraying black glaze on the part without the primary glaze by using a spray gun; picking up autumn mature mulberry leaves, putting the mulberry leaves into boiled saline water for cooking, taking the mulberry leaves out of a pot, and airing and flattening the mulberry leaves; naturally placing mulberry leaves on the blank body coated with the black glaze; firing in three stages after entering the kiln; naturally cooling to normal temperature after stopping fire and taking out of the kiln. The porcelain fired by the invention has the beneficial effects of strong jade sense of thick glaze, difficult falling and cracking, clear veins, elegance and simple and plain art combination.
Description
Technical Field
The invention relates to a preparation method for manufacturing Longquan porcelain by combining a Jizhou kiln marigold and Longquan kiln thick glaze.
Background
The Jizhou kiln marigold is a great characteristic of the Jizhou kiln, mulberry leaves are added into porcelain for firing, not only ash and fume are not eliminated, but also beautiful lines, shapes and veins are kept on the tea marigold completely and completely in a dark state, the marigold has high requirements on fire control due to the complex process, the firing success ratio is extremely low, the Longquan porcelain is more precious, celadon is taken as the main material, the Longquan material taking and firing process is obviously different from that of the Jizhou kiln, in the prior art, a precedent for preparing the Longquan porcelain by combining the Jizhou kiln marigold and the Longquan kiln is not used, and the technical disclosure for preparing the Longquan porcelain by combining the Jizhou kiln marigold and the Longquan kiln thick glaze is not used.
Disclosure of Invention
The invention provides a preparation method for manufacturing Longquan porcelain by combining the Jizhou kiln marigold and Longquan kiln thick glaze according to the defects.
The technical scheme of the invention is as follows:
a preparation method for manufacturing Longquan porcelain by combining Guizhou kiln marigold and Longquan kiln thick glaze comprises the following steps:
s1, preparing plum green glaze, which comprises the following components in parts by weight: 50-70 parts of albite, 15-25 parts of quartz stone, 8-12 parts of limestone, 2-4 parts of kaolin, 2-4 parts of amethyst and 2-4 parts of talc, performing ball milling on the mixture for 20 hours by using a ball mill according to a water ball ratio, and filtering the mixture through a 120-mesh sieve to obtain plum green glaze slurry, wherein the concentration of the plum green glaze slurry is measured to be 55 ℃ by using a hydrometer;
s2, preparing a black glaze material, which comprises the following components in parts by weight: 25-35 parts of Xiyuan glaze soil, 20-30 parts of LingGen glaze soil, 4-6 parts of Fujian black soil, 20-30 parts of quartz stone, 2-4 parts of manganese dioxide and 10-15 parts of Baozi violet gold soil are subjected to ball milling by a ball mill according to a water ball ratio for 20 hours, and then filtered by a 120-mesh sieve to obtain black glaze slurry;
s3, making a blank, wherein the blank body is made of Longquan cinnabar, and the blank is naturally dried after being formed by drawing;
s4, trimming a groove at the position where the green glaze needs to be applied after trimming the blank;
s5, glazing, namely dipping plum green glaze slurry on the grooves by a writing brush, and coating the plum green glaze slurry on the grooves layer by layer to form circular arc bulges;
s6, putting the blank into a kiln to be fired in a strong reducing atmosphere for the first time to form the Longquan kiln thick glaze;
s7, naturally cooling the fired blank in a kiln to room temperature, and taking out of the kiln;
s8, spraying black glaze on the part without the primary glaze by using a spray gun, and adjusting the particle size of the spray gun to be coarse;
s9 picking up autumn mature folium Mori, cooking in boiled saline water, taking out, air drying, and flattening;
s10, naturally placing mulberry leaves on the blank body coated with the black glaze;
s11 firing in three stages after entering the kiln: the first stage, the kiln temperature is raised to be close to 500 ℃ within 4 hours, the kiln door is not closed tightly in the process, a gap of close to 10 cm is reserved, and the kiln door is closed tightly when the kiln temperature is raised to be close to 500 ℃; then, in the second stage, when the temperature is between 500 and 1000 ℃, the temperature is stably raised to 1000 ℃ according to the temperature rise speed of one degree per minute, and then the temperature is kept for half an hour; in the third stage, when the temperature is increased from 1000 ℃ to 1280 ℃, the temperature is increased to 1280 ℃ according to the temperature increasing speed of one degree per two minutes, and then the temperature is kept for half an hour to stop fire;
and S12, naturally cooling to normal temperature after stopping fire, and taking out of the kiln.
Further, the plum green glaze comprises the following components in parts by weight: 60 parts of albite, 20 parts of quartz stone, 10 parts of limestone, 3 parts of kaolin, 3 parts of gilt clay and 4 parts of talc.
Further, the black glaze material comprises the following components in parts by weight: 30 parts of Xiyuan glaze soil, 25 parts of Ling root glaze soil, 5 parts of Fujian black soil, 25 parts of quartz stone, 3 parts of manganese dioxide and 12 parts of Baoxi purple golden soil.
Further, in step S6, the first firing in a strongly reducing atmosphere includes the steps of: in the first stage, the furnace door of the kiln is kept at 10 cm and is not tightly closed, and the time is 500 minutes from normal temperature to 495 ℃; in the second stage, the furnace door of the kiln is closed, the time is 2 hours from 495 ℃ to 950 ℃, and the temperature is kept for 1 hour when the temperature reaches 950 ℃; in the third stage, the temperature is raised from 950 ℃ to 1290 ℃ every minute, and after reaching 1290 ℃, the temperature is maintained for half an hour and then the fire is stopped.
Further, in the step S9, when picking up autumn-ripe mulberry leaves, the leaves are lightly picked up by hand, and the leaves easily cut off from the branches are ideal leaves.
In step S9, the saline water is added by ten jin of water.
Further, in step S9, the book is flatly laid in a book and flatly pressed.
Further, in the step S3, when the tire is naturally dried, the drying degree is that the tire body is not sticky when touched by a hand and is not deformed when held by a hand.
Further, in step S4, the shape of the groove is circular arc, and the depth of the circular arc bottom of the circular arc is close to the width of the circular arc.
Further, in the step S6, the longquan kiln thick glaze is in one or more of a spherical shape, an egg shape, and a circular shape.
The manufacturing of the Jizhou kiln marigold is originally one of the most difficult-to-fire kilns, and a lot of uncertain factors exist, so that the Jizhou kiln marigold works fired by the Longquan green ware are more difficult to add; the Longquan kiln thick glaze is also a very difficult firing process, in the prior art, the thin glaze is a common preparation method, and is not easy to crack, but the thin glaze cannot embody specific artistic works such as jades, when the thick glaze is fired, because the expansion coefficient of the common glaze is different from that of the body matrix and the two are easy to fall off, and meanwhile, the thick glaze fired by the common glaze is easy to crack.
Detailed Description
The invention will now be further illustrated with reference to the following examples:
example 1: a preparation method for manufacturing Longquan porcelain by combining Guizhou kiln marigold and Longquan kiln thick glaze comprises the following steps:
s1, preparing plum green glaze, which comprises the following components in parts by weight: 50 parts of albite, 15 parts of quartz stone, 8 parts of limestone, 2 parts of kaolin, 2 parts of gilt clay and 2 parts of talcum are subjected to ball milling for 20 hours by a ball mill according to a water ball ratio, and then are filtered by a 120-mesh sieve to obtain plum green glaze slurry, wherein the concentration of the plum green glaze slurry is measured by a hydrometer to be 55 ℃;
s2, preparing a black glaze material, which comprises the following components in parts by weight: 25 parts of Xiyuan glaze soil, 20 parts of Ling root glaze soil, 4 parts of Fujian black soil, 20 parts of quartz stone, 2 parts of manganese dioxide and 10 parts of Baozi violet gold soil are subjected to ball milling for 20 hours by a ball mill according to a water ball ratio, and then filtered by a 120-mesh sieve to obtain black glaze slurry;
s3, making a blank, wherein the blank body is made of Longquan cinnabar, and the blank is naturally dried after being formed by drawing; the drying degree is that the tyre body is not sticky when touched by hands and is not deformed when held by hands;
s4, trimming a groove at the position where the green glaze needs to be applied after trimming the blank; the shape of the groove is arc-shaped; the glaze slurry filling and firing process has the advantages that the wall of the common glaze slurry filling and firing process is thin, the grooves are formed along the top surfaces of the bowl opening and the cup opening, the grooves are connected to be approximate to a circular ring shape, when the glaze slurry is filled and fired successfully, the thick glaze part is embedded into the top surfaces of the bowl opening and the cup opening like a circular ring shape, the cross section of the circular ring shape is approximate to an ellipse, the process can be used for obtaining the thicker glaze works, due to the thick glaze shape, the jade feeling is very strong, if the glaze slurry is a handheld part at the top of the cup cover, and the bowl bottom or the cup bottom is provided with the grooves, at the moment, if the spherical or egg-shaped works are required to be embodied, the grooves are approximate to the local shape of the spherical or egg shape, and when the glaze slurry is filled and fired successfully, the spherical or egg-shaped works; obviously, the works with strong jade quality can embody the quality of high price; the arrangement of the grooves can improve the adhesive force and can also obviously improve the thickness of the thick glaze;
it should be noted that if the concentration of the glaze slip is very high, the smoothness of the surface cannot be obtained under the condition of lacking fluidity, and the glaze slip is also easy to break, if the concentration is low, the fluidity is too good, the effect of thick glaze cannot be achieved, and only if the proper concentration is matched with the design of the groove, the thick glaze can be obtained, and the condition that the thickness is relatively thick and the brightness of the surface reaches the ideal condition can be achieved.
S5, glazing, namely dipping plum green glaze slurry on the grooves by a writing brush to form arc bulges layer by layer, and slightly vibrating when necessary to enable the surface of the thick glaze to be smoother;
s6, putting the blank into a kiln for firing, wherein in the first stage, the kiln door is not tightly closed after being kept at 10 cm, and the blank takes 500 minutes from normal temperature to 495 ℃; in the second stage, the furnace door of the kiln is closed, the time is 2 hours from 495 ℃ to 950 ℃, and the temperature is kept for 1 hour when the temperature reaches 950 ℃; in the third stage, the temperature is raised once per minute from 950 ℃ to 1290 ℃, the temperature is maintained for half an hour after the temperature is raised to 1290 ℃, and then the fire is stopped, so that the Longquan kiln thick glaze is formed; the Longquan kiln thick glaze is more than one of spherical, egg-shaped or annular;
s7, naturally cooling the fired blank in a kiln to room temperature, and taking out of the kiln;
s8, spraying black glaze on the part without the primary glaze by using a spray gun, and adjusting the particle size of the spray gun to be coarse;
s9 picking mature mulberry leaves in autumn, lightly picking the leaves by hands, easily breaking the leaves from branches to be ideal leaves, and it needs to be explained that old and tender mulberry leaves can affect the quality of the product, and bad mulberry leaves can be mapped to the phenomena of cracking and winding of mulberry leaf patterns in porcelain, and can affect the embodiment of the product. Putting the mixture into boiled saline water for cooking, wherein the saline water is prepared by adding one kilogram of salt into ten kilograms of water, taking the mixture out of a pot, drying the mixture, spreading the mixture in a book, and flattening the mixture.
S10, naturally placing mulberry leaves on the blank body coated with the black glaze;
s11 firing in three stages after entering the kiln: the first stage, the kiln temperature is raised to be close to 500 ℃ within 4 hours, the kiln door is not closed tightly in the process, a gap of close to 10 cm is reserved, and the kiln door is closed tightly when the kiln temperature is raised to be close to 500 ℃; then, in the second stage, when the temperature is between 500 and 1000 ℃, the temperature is stably raised to 1000 ℃ according to the temperature rise speed of one degree per minute, and then the temperature is kept for half an hour; in the third stage, when the temperature is increased from 1000 ℃ to 1280 ℃, the temperature is increased to 1280 ℃ according to the temperature increasing speed of one degree per two minutes, and then the temperature is kept for half an hour to stop fire;
and S12, naturally cooling to normal temperature after stopping fire, and taking out of the kiln.
Example 2: preparing plum green glaze, wherein the components in parts by weight are as follows: 70 parts of albite, 25 parts of quartz stone, 12 parts of limestone, 4 parts of kaolin, 4 parts of gilt clay and 4 parts of talcum are subjected to ball milling by a ball mill according to a water ball ratio for 20 hours, and then are filtered by a 120-mesh sieve to obtain plum green glaze slurry, wherein the concentration of the plum green glaze slurry is measured by a hydrometer to be 55 ℃;
preparing black glaze material, taking the following components in parts by weight: 35 parts of Xiyuan glaze soil, 30 parts of Ling root glaze soil, 6 parts of Fujian black soil, 30 parts of quartz stone, 4 parts of manganese dioxide and 15 parts of Baozi violet gold soil are subjected to ball milling for 20 hours by a ball mill according to a water ball ratio, and then filtered by a 120-mesh sieve to obtain black glaze slurry;
the other steps were the same as in example 1.
Example 3: preparing plum green glaze, wherein the components in parts by weight are as follows: the plum green glaze consists of the following components in parts by weight: 60 parts of albite, 20 parts of quartz stone, 10 parts of limestone, 3 parts of kaolin, 3 parts of gilt clay and 4 parts of talc. Ball-milling with a ball mill according to a water ball ratio for 20 hours, and filtering with a 120-mesh sieve to obtain plum green glaze slurry, wherein the concentration of the plum green glaze slurry is measured by a hydrometer to be 55 ℃;
preparing black glaze material, taking the following components in parts by weight: 30 parts of Xiyuan glaze soil, 25 parts of Ling root glaze soil, 5 parts of Fujian black soil, 25 parts of quartz stone, 3 parts of manganese dioxide and 12 parts of Baoxi purple golden soil. Ball-milling the mixture for 20 hours by a ball mill according to the water ball ratio, and filtering the mixture by a 120-mesh sieve to obtain black glaze slurry;
the other steps were the same as in example 1.
Claims (10)
1. A preparation method for manufacturing Longquan porcelain by combining Guizhou kiln marigold and Longquan kiln thick glaze is characterized by comprising the following steps:
s1, preparing plum green glaze, which comprises the following components in parts by weight: 50-70 parts of albite, 15-25 parts of quartz stone, 8-12 parts of limestone, 2-4 parts of kaolin, 2-4 parts of amethyst and 2-4 parts of talc, performing ball milling on the mixture for 20 hours by using a ball mill according to a water ball ratio, and filtering the mixture through a 120-mesh sieve to obtain plum green glaze slurry, wherein the concentration of the plum green glaze slurry is measured to be 55 ℃ by using a hydrometer;
s2, preparing a black glaze material, which comprises the following components in parts by weight: 25-35 parts of Xiyuan glaze soil, 20-30 parts of LingGen glaze soil, 4-6 parts of Fujian black soil, 20-30 parts of quartz stone, 2-4 parts of manganese dioxide and 10-15 parts of Baozi violet gold soil are subjected to ball milling by a ball mill according to a water ball ratio for 20 hours, and then filtered by a 120-mesh sieve to obtain black glaze slurry;
s3, making a blank, wherein the blank body is made of Longquan cinnabar, and the blank is naturally dried after being formed by drawing;
s4, trimming a groove at the position where the green glaze needs to be applied after trimming the blank;
s5, glazing, namely dipping plum green glaze slurry on the grooves by a writing brush, and coating the plum green glaze slurry on the grooves layer by layer to form circular arc bulges;
s6, putting the blank into a kiln to be fired in a strong reducing atmosphere for the first time to form the Longquan kiln thick glaze;
s7, naturally cooling the fired blank in a kiln to room temperature, and taking out of the kiln;
s8, spraying black glaze on the part without the primary glaze by using a spray gun, and adjusting the particle size of the spray gun to be coarse;
s9 picking up autumn mature folium Mori, cooking in boiled saline water, taking out, air drying, and flattening;
s10, naturally placing mulberry leaves on the blank body coated with the black glaze;
s11 firing in three stages after entering the kiln: the first stage, the kiln temperature is raised to be close to 500 ℃ within 4 hours, the kiln door is not closed tightly in the process, a gap of close to 10 cm is reserved, and the kiln door is closed tightly when the kiln temperature is raised to be close to 500 ℃; then, in the second stage, when the temperature is between 500 and 1000 ℃, the temperature is stably raised to 1000 ℃ according to the temperature rise speed of one degree per minute, and then the temperature is kept for half an hour; in the third stage, when the temperature is increased from 1000 ℃ to 1280 ℃, the temperature is increased to 1280 ℃ according to the temperature increasing speed of one degree per two minutes, and then the temperature is kept for half an hour to stop fire;
and S12, naturally cooling to normal temperature after stopping fire, and taking out of the kiln.
2. The method for preparing Longquan porcelain by combining Guizhou kiln marigold and Longquan kiln thick glaze according to claim 1, wherein the plum green glaze comprises the following components in parts by weight: 60 parts of albite, 20 parts of quartz stone, 10 parts of limestone, 3 parts of kaolin, 3 parts of gilt clay and 4 parts of talc.
3. The method for preparing Longquan porcelain by combining the mugwort cup in Guizhou kiln and the Longquan kiln thick glaze according to claim 1, wherein the black glaze material comprises the following components in parts by weight: 30 parts of Xiyuan glaze soil, 25 parts of Ling root glaze soil, 5 parts of Fujian black soil, 25 parts of quartz stone, 3 parts of manganese dioxide and 12 parts of Baoxi purple golden soil.
4. The method as claimed in claim 1, wherein the step of firing in the first strong reducing atmosphere in step S6 comprises the steps of: in the first stage, the furnace door of the kiln is kept at 10 cm and is not tightly closed, and the time is 500 minutes from normal temperature to 495 ℃; in the second stage, the furnace door of the kiln is closed, the time is 2 hours from 495 ℃ to 950 ℃, and the temperature is kept for 1 hour when the temperature reaches 950 ℃; in the third stage, the temperature is raised from 950 ℃ to 1290 ℃ every minute, and after reaching 1290 ℃, the temperature is maintained for half an hour and then the fire is stopped.
5. The method as claimed in claim 1, wherein the step S9 of picking mature mulberry leaves in autumn by picking the leaves gently by hand, the leaves easily broken from the branches are ideal leaves.
6. The method as claimed in claim 1, wherein in step S9, the salt water is added in a ratio of ten jin of water to one jin of salt.
7. The method of claim 1, wherein in step S9, the porcelain is laid flat in a book and pressed flat.
8. The method of claim 1, wherein in step S3, the drying is performed by hand, without sticking to the carcass and without deformation when being held by hand.
9. The method as claimed in claim 1, wherein in step S4, the shape of the recess is circular arc, and the depth of the circular arc bottom is close to the width of the circular arc.
10. The method as claimed in claim 1, wherein the step S6 is performed by using a combination of muzzle and Longquan kiln thick glaze to make Longquan porcelain.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011109837.1A CN112374756B (en) | 2020-10-16 | 2020-10-16 | Method for preparing Longquan porcelain by combining Guizhou kiln wooden leaf cup and Longquan kiln thick glaze |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011109837.1A CN112374756B (en) | 2020-10-16 | 2020-10-16 | Method for preparing Longquan porcelain by combining Guizhou kiln wooden leaf cup and Longquan kiln thick glaze |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN112374756A true CN112374756A (en) | 2021-02-19 |
| CN112374756B CN112374756B (en) | 2022-05-10 |
Family
ID=74579926
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202011109837.1A Active CN112374756B (en) | 2020-10-16 | 2020-10-16 | Method for preparing Longquan porcelain by combining Guizhou kiln wooden leaf cup and Longquan kiln thick glaze |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN112374756B (en) |
Citations (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2000264759A (en) * | 1999-03-15 | 2000-09-26 | Saga Prefecture | Copper green glaze free from lead for low temperature firing |
| CN1715229A (en) * | 2004-07-03 | 2006-01-04 | 陈根 | Longquan celadon frostwork glaze and its producing method for product |
| CN101734948A (en) * | 2008-11-04 | 2010-06-16 | 李邦强 | Longquan official ware celadon glaze of the Ming Dynasty and method for manufacturing Longquan official ware celadon product of the Ming Dynasty by using glaze |
| CN102060571A (en) * | 2010-10-29 | 2011-05-18 | 南京工业大学 | Green glaze for daily porcelain |
| CN104030733A (en) * | 2014-06-25 | 2014-09-10 | 龙泉市建春青瓷厂 | Moon-white Song-dynasty official and brother kiln glaze material, moon-white Song-dynasty official and brother kiln porcelain and preparation method of porcelain |
| CN104605699A (en) * | 2014-11-18 | 2015-05-13 | 陈伟群 | Cup with flickering function |
| CN105217957A (en) * | 2015-09-18 | 2016-01-06 | 丽水学院 | A kind of Longquan celadon is without tire glaze ancient piece of jade, round, flat and with a hole in its centre and preparation method thereof and application |
| CN105541407A (en) * | 2015-12-08 | 2016-05-04 | 丽水学院 | Making technology for celadon glaze color generation through combination of clay and petuntse |
| CN105753322A (en) * | 2016-03-13 | 2016-07-13 | 浙江天丰陶瓷有限公司 | Medium-temperature plum green glaze and medium-temperature plum green Longquan celadon |
| CN105776866A (en) * | 2016-02-02 | 2016-07-20 | 丽水学院 | Longquan celadon jasper green glaze, jasper green Longquan celadon and preparation method thereof |
| CN106082671A (en) * | 2016-06-22 | 2016-11-09 | 丽水学院 | Longquan celadon green grass or young crops glaze, Longquan celadon and preparation method thereof |
| CN108752050A (en) * | 2018-06-19 | 2018-11-06 | 张玉凤 | Your porcelain tea-dust glaze of one kind and preparation method thereof |
| CN109721249A (en) * | 2019-01-31 | 2019-05-07 | 齐鲁工业大学 | A kind of preparation method of the ceramic glaze based on leaf |
| CN110066190A (en) * | 2019-06-12 | 2019-07-30 | 景德镇陶瓷大学 | A kind of preparation method, black glazed ware product and its method for cooking of high temperature ice blue lima-wood leaf black glazed ware |
| CN110204305A (en) * | 2019-05-17 | 2019-09-06 | 龙泉市群力瓷业有限公司 | A kind of brother's kiln celadon and its method for cooking |
| CN111302627A (en) * | 2020-02-18 | 2020-06-19 | 龙泉瓯江青瓷有限公司 | Firing process and firing equipment for medium-temperature Longquan green glaze |
-
2020
- 2020-10-16 CN CN202011109837.1A patent/CN112374756B/en active Active
Patent Citations (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2000264759A (en) * | 1999-03-15 | 2000-09-26 | Saga Prefecture | Copper green glaze free from lead for low temperature firing |
| CN1715229A (en) * | 2004-07-03 | 2006-01-04 | 陈根 | Longquan celadon frostwork glaze and its producing method for product |
| CN101734948A (en) * | 2008-11-04 | 2010-06-16 | 李邦强 | Longquan official ware celadon glaze of the Ming Dynasty and method for manufacturing Longquan official ware celadon product of the Ming Dynasty by using glaze |
| CN102060571A (en) * | 2010-10-29 | 2011-05-18 | 南京工业大学 | Green glaze for daily porcelain |
| CN104030733A (en) * | 2014-06-25 | 2014-09-10 | 龙泉市建春青瓷厂 | Moon-white Song-dynasty official and brother kiln glaze material, moon-white Song-dynasty official and brother kiln porcelain and preparation method of porcelain |
| CN104605699A (en) * | 2014-11-18 | 2015-05-13 | 陈伟群 | Cup with flickering function |
| CN105217957A (en) * | 2015-09-18 | 2016-01-06 | 丽水学院 | A kind of Longquan celadon is without tire glaze ancient piece of jade, round, flat and with a hole in its centre and preparation method thereof and application |
| CN105541407A (en) * | 2015-12-08 | 2016-05-04 | 丽水学院 | Making technology for celadon glaze color generation through combination of clay and petuntse |
| CN105776866A (en) * | 2016-02-02 | 2016-07-20 | 丽水学院 | Longquan celadon jasper green glaze, jasper green Longquan celadon and preparation method thereof |
| CN105753322A (en) * | 2016-03-13 | 2016-07-13 | 浙江天丰陶瓷有限公司 | Medium-temperature plum green glaze and medium-temperature plum green Longquan celadon |
| CN106082671A (en) * | 2016-06-22 | 2016-11-09 | 丽水学院 | Longquan celadon green grass or young crops glaze, Longquan celadon and preparation method thereof |
| CN108752050A (en) * | 2018-06-19 | 2018-11-06 | 张玉凤 | Your porcelain tea-dust glaze of one kind and preparation method thereof |
| CN109721249A (en) * | 2019-01-31 | 2019-05-07 | 齐鲁工业大学 | A kind of preparation method of the ceramic glaze based on leaf |
| CN110204305A (en) * | 2019-05-17 | 2019-09-06 | 龙泉市群力瓷业有限公司 | A kind of brother's kiln celadon and its method for cooking |
| CN110066190A (en) * | 2019-06-12 | 2019-07-30 | 景德镇陶瓷大学 | A kind of preparation method, black glazed ware product and its method for cooking of high temperature ice blue lima-wood leaf black glazed ware |
| CN111302627A (en) * | 2020-02-18 | 2020-06-19 | 龙泉瓯江青瓷有限公司 | Firing process and firing equipment for medium-temperature Longquan green glaze |
Non-Patent Citations (1)
| Title |
|---|
| 吴艳芳等: "中温原矿梅子青釉的研制", 《佛山陶瓷》 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN112374756B (en) | 2022-05-10 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109721249B (en) | Preparation method of leaf-based ceramic glaze | |
| CN106673437B (en) | A kind of preparation method of high rigidity hacking glaze porcelain | |
| CN111087253B (en) | Decoration process on low-water-absorption ceramic surface | |
| CN110228993B (en) | Processing technology of crackle celadon cosmetic bottle with inner non-crackle glaze | |
| CN104193417A (en) | Elder brother glaze and younger brother glaze combined celadon ware calcining process and glaze formulas | |
| CN110615616A (en) | Green glaze and application method thereof | |
| CN106490901A (en) | The manufacture method of colorful ceramic vase and colorful ceramic vase | |
| CN112374762A (en) | Moon white glaze for jun porcelain and preparation method thereof | |
| CN110627360A (en) | Dark green glaze and application method thereof | |
| CN107573017A (en) | A kind of technique for manufacturing stealthy decorative pattern ceramic | |
| CN110963786B (en) | Colored artistic porcelain based on De-white porcelain body and preparation process thereof | |
| CN112374756B (en) | Method for preparing Longquan porcelain by combining Guizhou kiln wooden leaf cup and Longquan kiln thick glaze | |
| CN106083200B (en) | Dragon's fountain Song Dynasty brother's kiln celadon glaze and the method for making dragon's fountain Song Dynasty brother's kiln celadon product with the glaze | |
| CN112028606A (en) | Longquan Ge kiln garbage broken glaze and firing process thereof | |
| CN108129028B (en) | Glittering and translucent thick-glaze ceramic product and manufacturing process thereof | |
| CN113213888B (en) | Combined transmutation glaze, combined transmutation glaze porcelain and preparation method thereof | |
| CN107663022B (en) | Celeste jun porcelain glaze and preparation method thereof | |
| CN115991573A (en) | Double-layer kiln red glaze, porcelain adopting double-layer kiln red glaze and preparation method of double-layer kiln red glaze | |
| CN115385661A (en) | Production process of painted pottery large plate | |
| CN111517652B (en) | Yellow ground glaze for marigold and method for manufacturing marigold by adopting yellow ground glaze | |
| CN111533533A (en) | Pearl porcelain and preparation method thereof | |
| CN110655324A (en) | Light green glaze and application method thereof | |
| CN110950536A (en) | Bronze-imitating artistic ceramic and preparation method thereof | |
| CN108373265A (en) | A kind of shrinkproof glaze handicraft of celadon and method | |
| CN112374860B (en) | Porcelain underglaze decoration material and preparation and application method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |