CN112370398A - 一种红参中药洗发水及其制备工艺 - Google Patents
一种红参中药洗发水及其制备工艺 Download PDFInfo
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- CN112370398A CN112370398A CN202011539350.7A CN202011539350A CN112370398A CN 112370398 A CN112370398 A CN 112370398A CN 202011539350 A CN202011539350 A CN 202011539350A CN 112370398 A CN112370398 A CN 112370398A
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- red ginseng
- ammonium chloride
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Abstract
本发明公开了一种红参中药洗发水及其制备工艺，其中，一种红参中药洗发水，包括如下重量份数的组分：纯水；表面活性剂；中药提取物混合物；发用调理剂；保湿剂；pH调节剂；乳化剂；增稠剂；其他组分；表面活性剂包括月桂醇聚醚硫酸酯铵、月桂醇硫酸酯铵、硬脂酰胺丙基二甲胺、椰子油脂肪酸二乙醇酰胺、椰油酰胺丙基甜菜碱；红参提取物；发用调理剂包括聚季铵盐‑10、瓜儿胶羟丙基三甲基氯化铵、EFA亚油酰胺丙基丙二醇单磷酸酯基二甲基氯化铵。本发明的洗发水对人的刺激更低，对人体更安全，具有优异的止痒、去屑、去油控油、防护效果。
Description
技术领域
本发明涉及护肤品技术领域，具体为一种红参中药洗发水及其制备工艺。
背景技术
随着城市中人们的生活节奏的加快，也带来了作息不规律、精神压力大、经常性失眠等诸如此类的问题，加上各类化学物质在日常生活中的广泛应用，头发的健康问题越来越多。其中，头发油、头皮屑增多、头皮发痒、脱发是几种常见的头发问题。红参是人参的熟制品，除具有补元气、补脾肺、生津安神的作用外，其药性更温，具有火大、劲足、功效强的特点，有改善贫血促进血液流动的作用，能够抑制全身炎症反应，有很好的抗炎效果。传统的洗发水为追求较好的去油效果，通常采用去油能力较强的表面活性剂。虽然达到了去油效果，但也会对头皮和头发造成损伤，导致出现更多的头发干枯、头皮发痒、头屑增多、脱发等现象。因此，一种具有较好的去油、止痒、去屑、固发等作用的洗发水具有较好的商业价值。
发明内容
针对现有技术存在的不足，本发明的目的之一在于提供一种红参中药洗发水，洗发水对人的刺激更低，对人体更安全具有优异的止痒、抗炎、去屑、去油、防护等效果。
为实现上述目的，本发明提供如下技术方案：
一种红参中药洗发水，包括如下重量份数的组分：红参提取物2-6份，香榧提取物0.1-0.3份，侧柏提取物0.1-0.3份，牛蒡提取物0.1-0.3份，黑豆提取物0.1-0.3份，鱼腥草提取物0.1-0.3份，紫苏叶提取物0.1-0.3份，何首乌提取物0.1-0.3份，月桂醇聚醚硫酸酯铵11-13份，月桂醇硫酸酯铵3-5份，硬脂酰胺丙基二甲胺0.2-0.4份，椰子油脂肪酸二乙醇酰胺0.8-1.2份，椰油酰胺丙基甜菜碱5-7份，聚季铵盐-10 0.08-0.12份，瓜儿胶羟丙基三甲基氯化铵0.18-0.22份，EFA 亚油酰胺丙基丙二醇单磷酸酯基二甲基氯化铵0.18-0.22份，羟乙基脲2-4份，发酵马油0.08-0.12份，乙基己基甘油0.04-0.06份，柠檬酸0.185-0.205份，PEG -7椰油甘油酸酯1-3份，油醇聚醚-5磷酸酯0.2-0.4份，SCP 二聚亚油酰胺丙基 PG-二甲基氯化铵磷酸酯0.4-0.6份，对羟基苯乙酮0.1-0.3份，食盐2.5-4.5份，己脒定0.02-0.04份，香水0.05-0.15份，余量用水补充至100份。
另外，一种红参中药洗发水的制备工艺，其特征在于，按照所述的重量分配比，包括如下步骤：
S1，将水抽入水相锅中，搅拌并慢慢加入聚季铵盐-10、瓜儿胶羟丙基三甲基氯化铵升温至80-85℃形成A相混合物；
S2，A相完全溶解呈透明状后，依次加入月桂醇聚醚硫酸酯铵、月桂醇硫酸酯铵硬脂酰胺丙基二甲胺搅拌溶解，完全溶解后温度降至60℃以下；
S3，新容器中依次加入CDEA-椰子油脂肪酸二乙醇酰胺、羟乙基脲、红参提取物、香榧提取物、侧柏提取物、牛蒡提取物、黑豆提取物、鱼腥草提取物、紫苏叶提取物、何首乌提取物、发酵马油、PEG -7椰油甘油酸酯、油醇聚醚-5磷酸酯、EFA 亚油酰胺丙基丙二醇单磷酸酯基二甲基氯化铵、SCP 二聚亚油酰胺丙基 PG-二甲基氯化铵磷酸酯、椰油酰胺丙基甜菜碱、柠檬酸形成B相；新容器中依次加入对羟基苯乙酮、乙基己基甘油、苯甲酸钠形成C相；将对羟基苯乙酮、乙基己基甘油、苯甲酸钠混合形成D相。
S4，将C相、D相依次加入A相中搅拌溶解，取样观察，检测pH，完全溶解后温度降至45℃以下时，依次加入己脒定和香水搅拌溶解10min后，加入食盐水调整粘度，必要时，需要打循环；合成锅中，混合均匀，加热至75-80℃，保温混合30-35min，形成第二混合物；
S5，将步骤S4中获得的混合物送检、出料、包装。
通过上述技术方案，表面活性剂中，月桂醇聚醚硫酸酯铵、月桂醇硫酸酯铵、硬脂酰胺丙基二甲胺、椰子油脂肪酸二乙醇酰胺、椰油酰胺丙基甜菜碱，具有较好的去油效果，使头皮和头发保持清洁。有助于提高止痒、去屑、固发的效果。且中药提取物混合物为纯天然植物提取物提取混合获得，刺激性非常小，且具有较好的滋养效果，在清洗头发和头皮的过程中，可达到较好的保护头皮和头发的作用。中药提取物混合物中，红参提取物、香榧提取物、侧柏提取物、牛蒡提取物、黑豆提取物、鱼腥草提取物、紫苏叶提取物、何首乌提取物相互配合有助于提高止痒、去屑、固发的效果。且中药提取物混合物为纯天然植物提取物提取混合获得，刺激性非常小，且具有较好的滋养效果，在清洗头发和头皮的过程中，可达到较好的保护头皮和头发的作用。发用调理剂中，将季铵盐-10、瓜儿胶羟丙基三甲基氯化铵、EFA 亚油酰胺丙基丙二醇单磷酸酯基二甲基氯化铵相互配合使用，有助于使头发柔软、顺滑，并可改善湿发、干发梳理性，减少头发打结的现象出现。发用调理剂与红参中药提取进行复配使用，使本申请中的洗发水对头皮具有较好的防护效果以及控油效果。
具体实施方式
为了让本领域技术人员更清楚地了解本发明相对现有技术的改进之处，下面结合实施例对本发明作进一步的说明，实施例提及的内容并非对本发明的限定。
实施例1
一种红参中药洗发水，包括如下重量份数的组分：红参提取物2份，香榧提取物0.1份，侧柏提取物0.1份，牛蒡提取物0.1份，黑豆提取物0.1份，鱼腥草提取物0.1份，紫苏叶提取物0.1份，何首乌提取物0.1份，月桂醇聚醚硫酸酯铵11份，月桂醇硫酸酯铵3份，硬脂酰胺丙基二甲胺0.2份，椰子油脂肪酸二乙醇酰胺0.8份，椰油酰胺丙基甜菜碱5份，聚季铵盐-100.08份，瓜儿胶羟丙基三甲基氯化铵0.18份，EFA 亚油酰胺丙基丙二醇单磷酸酯基二甲基氯化铵0.18份，羟乙基脲2份，发酵马油0.08份，乙基己基甘油0.04份，柠檬酸0.185份，PEG-7椰油甘油酸酯1份，油醇聚醚-5磷酸酯0.2份，SCP 二聚亚油酰胺丙基 PG-二甲基氯化铵磷酸酯0.4份，对羟基苯乙酮0.1份，食盐2.5份，己脒定0.02份，香水0.05份，余量用水补充至100份。
制备过程：
S1，将水抽入水相锅中，搅拌并慢慢加入聚季铵盐-10、瓜儿胶羟丙基三甲基氯化铵升温至85℃形成A相混合物；
S2，A相完全溶解呈透明状后，依次加入月桂醇聚醚硫酸酯铵、月桂醇硫酸酯铵硬脂酰胺丙基二甲胺搅拌溶解，完全溶解后温度降至60℃；
S3，新容器中依次加入CDEA-椰子油脂肪酸二乙醇酰胺、羟乙基脲、红参提取物、香榧提取物、侧柏提取物、牛蒡提取物、黑豆提取物、鱼腥草提取物、紫苏叶提取物、何首乌提取物、发酵马油、PEG -7椰油甘油酸酯、油醇聚醚-5磷酸酯、EFA 亚油酰胺丙基丙二醇单磷酸酯基二甲基氯化铵、SCP 二聚亚油酰胺丙基 PG-二甲基氯化铵磷酸酯、椰油酰胺丙基甜菜碱、柠檬酸形成B相；新容器中依次加入对羟基苯乙酮、乙基己基甘油、苯甲酸钠形成C相；将对羟基苯乙酮、乙基己基甘油、苯甲酸钠混合形成D相。
S4，将C相、D相依次加入A相中搅拌溶解，取样观察，检测pH，完全溶解后温度降至45℃时，依次加入己脒定和香水搅拌溶解10min后，加入食盐水调整粘度，必要时，需要打循环；
合成锅中，混合均匀，加热至80℃，保温混合35min，形成第二混合物；
S5，将步骤S4中获得的混合物送检、出料、包装。
实施例2
一种红参中药洗发水，包括如下重量份数的组分：红参提取物6份，香榧提取物0.1份，侧柏提取物0.1份，牛蒡提取物0.1份，黑豆提取物0.1份，鱼腥草提取物0.1份，紫苏叶提取物0.1份，何首乌提取物0.1份，月桂醇聚醚硫酸酯铵13份，月桂醇硫酸酯铵5份，硬脂酰胺丙基二甲胺0.4份，椰子油脂肪酸二乙醇酰胺1.2份，椰油酰胺丙基甜菜碱7份，聚季铵盐-100.12份，瓜儿胶羟丙基三甲基氯化铵0.22份，EFA 亚油酰胺丙基丙二醇单磷酸酯基二甲基氯化铵0.22份，羟乙基脲4份，发酵马油0.12份，乙基己基甘油0.06份，柠檬酸0.205份，PEG-7椰油甘油酸酯3份，油醇聚醚-5磷酸酯0.4份，SCP 二聚亚油酰胺丙基 PG-二甲基氯化铵磷酸酯0.6份，对羟基苯乙酮0.3份，食盐4.5份，己脒定0.04份，香水0.15份，余量用水补充至100份。
制备过程：
S1，将水抽入水相锅中，搅拌并慢慢加入聚季铵盐-10、瓜儿胶羟丙基三甲基氯化铵升温至80℃形成A相混合物；
S2，A相完全溶解呈透明状后，依次加入月桂醇聚醚硫酸酯铵、月桂醇硫酸酯铵硬脂酰胺丙基二甲胺搅拌溶解，完全溶解后温度降至45℃；
S3，新容器中依次加入CDEA-椰子油脂肪酸二乙醇酰胺、羟乙基脲、红参提取物、香榧提取物、侧柏提取物、牛蒡提取物、黑豆提取物、鱼腥草提取物、紫苏叶提取物、何首乌提取物、发酵马油、PEG -7椰油甘油酸酯、油醇聚醚-5磷酸酯、EFA 亚油酰胺丙基丙二醇单磷酸酯基二甲基氯化铵、SCP 二聚亚油酰胺丙基 PG-二甲基氯化铵磷酸酯、椰油酰胺丙基甜菜碱、柠檬酸形成B相；新容器中依次加入对羟基苯乙酮、乙基己基甘油、苯甲酸钠形成C相；将对羟基苯乙酮、乙基己基甘油、苯甲酸钠混合形成D相。
S4，将C相、D相依次加入A相中搅拌溶解，取样观察，检测pH，完全溶解后温度降至35℃时，依次加入己脒定和香水搅拌溶解10min后，加入食盐水调整粘度，必要时，需要打循环；
合成锅中，混合均匀，加热至75℃，保温混合30min，形成第二混合物；
S5，将步骤S4中获得的混合物送检、出料、包装。
实施例3
一种红参中药洗发水，包括如下重量份数的组分：红参提取物4份，香榧提取物0.15份，侧柏提取物0.2份，牛蒡提取物0.15份，黑豆提取物0.18份，鱼腥草提取物0.25份，紫苏叶提取物0.15份，何首乌提取物0.3份，月桂醇聚醚硫酸酯铵12份，月桂醇硫酸酯铵4份，硬脂酰胺丙基二甲胺0.3份，椰子油脂肪酸二乙醇酰胺1份，椰油酰胺丙基甜菜碱6份，聚季铵盐-100.1份，瓜儿胶羟丙基三甲基氯化铵0.2份，EFA 亚油酰胺丙基丙二醇单磷酸酯基二甲基氯化铵0.2份，羟乙基脲3份，发酵马油0.1份，乙基己基甘油0.05份，柠檬酸0.1955份，PEG -7椰油甘油酸酯2份，油醇聚醚-5磷酸酯0.3份，SCP 二聚亚油酰胺丙基 PG-二甲基氯化铵磷酸酯0.5份，对羟基苯乙酮0.2份，食盐3.5份，己脒定0.03份，香水0.1份，余量用水补充至100份。
制备过程：
S1，将水抽入水相锅中，搅拌并慢慢加入聚季铵盐-10、瓜儿胶羟丙基三甲基氯化铵升温至83℃形成A相混合物；
S2，A相完全溶解呈透明状后，依次加入月桂醇聚醚硫酸酯铵、月桂醇硫酸酯铵硬脂酰胺丙基二甲胺搅拌溶解，完全溶解后温度降至55℃；
S3，新容器中依次加入CDEA-椰子油脂肪酸二乙醇酰胺、羟乙基脲、红参提取物、香榧提取物、侧柏提取物、牛蒡提取物、黑豆提取物、鱼腥草提取物、紫苏叶提取物、何首乌提取物、发酵马油、PEG -7椰油甘油酸酯、油醇聚醚-5磷酸酯、EFA 亚油酰胺丙基丙二醇单磷酸酯基二甲基氯化铵、SCP 二聚亚油酰胺丙基 PG-二甲基氯化铵磷酸酯、椰油酰胺丙基甜菜碱、柠檬酸形成B相；新容器中依次加入对羟基苯乙酮、乙基己基甘油、苯甲酸钠形成C相；将对羟基苯乙酮、乙基己基甘油、苯甲酸钠混合形成D相。
S4，将C相、D相依次加入A相中搅拌溶解，取样观察，检测pH，完全溶解后温度降至40℃时，依次加入己脒定和香水搅拌溶解10min后，加入食盐水调整粘度，必要时，需要打循环；
合成锅中，混合均匀，加热至78℃，保温混合33min，形成第二混合物；
S5，将步骤S4中获得的混合物送检、出料、包装。
实施例4
一种红参中药洗发水，包括如下重量份数的组分：红参提取物5份，香榧提取物0.3份，侧柏提取物0.3份，牛蒡提取物0.3份，黑豆提取物0.3份，鱼腥草提取物0.3份，紫苏叶提取物0.3份，何首乌提取物0.3份，月桂醇聚醚硫酸酯铵12.5份，月桂醇硫酸酯铵4.5份，硬脂酰胺丙基二甲胺0.35份，椰子油脂肪酸二乙醇酰胺1.1份，椰油酰胺丙基甜菜碱6.5份，聚季铵盐-10 0.11份，瓜儿胶羟丙基三甲基氯化铵0.195份，EFA 亚油酰胺丙基丙二醇单磷酸酯基二甲基氯化铵0.195份，羟乙基脲3.5份，发酵马油0.095份，乙基己基甘油0.055份，柠檬酸0.2份，PEG -7椰油甘油酸酯2.5份，油醇聚醚-5磷酸酯0.35份，SCP 二聚亚油酰胺丙基 PG-二甲基氯化铵磷酸酯0.55份，对羟基苯乙酮0.25份，食盐4份，己脒定0.035份，香水0.15份，余量用水补充至100份。
制备过程：
S1，将水抽入水相锅中，搅拌并慢慢加入聚季铵盐-10、瓜儿胶羟丙基三甲基氯化铵升温至80℃形成A相混合物；
S2，A相完全溶解呈透明状后，依次加入月桂醇聚醚硫酸酯铵、月桂醇硫酸酯铵硬脂酰胺丙基二甲胺搅拌溶解，完全溶解后温度降至58℃；
S3，新容器中依次加入CDEA-椰子油脂肪酸二乙醇酰胺、羟乙基脲、红参提取物、香榧提取物、侧柏提取物、牛蒡提取物、黑豆提取物、鱼腥草提取物、紫苏叶提取物、何首乌提取物、发酵马油、PEG -7椰油甘油酸酯、油醇聚醚-5磷酸酯、EFA 亚油酰胺丙基丙二醇单磷酸酯基二甲基氯化铵、SCP 二聚亚油酰胺丙基 PG-二甲基氯化铵磷酸酯、椰油酰胺丙基甜菜碱、柠檬酸形成B相；新容器中依次加入对羟基苯乙酮、乙基己基甘油、苯甲酸钠形成C相；将对羟基苯乙酮、乙基己基甘油、苯甲酸钠混合形成D相。
S4，将C相、D相依次加入A相中搅拌溶解，取样观察，检测pH，完全溶解后温度降至42℃时，依次加入己脒定和香水搅拌溶解10min后，加入食盐水调整粘度，必要时，需要打循环；
合成锅中，混合均匀，加热至77℃，保温混合32min，形成第二混合物；
S5，将步骤S4中获得的混合物送检、出料、包装。
对比例1
本对比例采用在实施例1的基础上去掉月桂醇聚醚硫酸酯铵，其余组分同实施例1。
对比例2
本对比例采用在实施例1的基础上去掉红参提取物，其余组分同实施例1。
对比例3
本对比例采用市售的无中药成分的某品牌洗发水。
试验：使用者体验感试验
（一）试验方法：选取同一地区、年龄段为20-55岁、具有脱发、头皮痒、头发疏密性类似且长短类似的受试者700名，平均分成7组，各组在年龄以及头皮对洗发水刺激性敏感程度、发质等方面均无显著性差异，第1-7组分别使用实施例1-4制备得到的洗发水以及对比例1-3的洗发水。
（二）测试结果：采用调查评分法进行综合评分。每组人群每两天洗头一次，连续洗头2个月，填写试用评分表。评分表中各项使用效果总分为10分，9-10分表示效果最优；6-8分表示效果较好；4-5分表示效果一般；3分以下表示效果较差，各项使用效果平均得分情况如表1所示。
表1
| 降低刺激程度 | 清洁程度 | 发质改善程度 | 止痒效果 | |
| 实施例1 | 9.4 | 9.1 | 8.7 | 9.1 |
| 实施例2 | 9.3 | 9.0 | 8.6 | 9.4 |
| 实施例3 | 9.7 | 9.3 | 9.0 | 9.3 |
| 实施例4 | 9.5 | 9.2 | 8.8 | 9.2 |
| 对比例1 | 9.0 | 8.7 | 8.1 | 9.0 |
| 对比例2 | 8.7 | 8.5 | 8.0 | 8.6 |
| 对比例3 | 8.3 | 8.2 | 7.6 | 8.5 |
测试结果如上表所示，在清洁程度和降低刺激程度指标的评分中，实施例第1-4组受试者在使用相应的试验样后，可达到较好的去油能力、去屑能力、头发柔顺程度、止痒效果，并且在24h内具有较好的控油效果，长期时候后，可改善脱发掉发的现象，达到固发的效果。实施例1-4均略高于对比例1-3，尤其在降低刺激程度指标的评分中，实施例1-4提供的洗发水的效果要明显优于对比例3提供的市售的不含中药取物成分的某品牌洗发水，说明本发明的洗发水对人的刺激更低，对人体更安全。实施例1-4提供的洗发水的效果与对比例2相比由于缺少红参提取物造成难以达到较好的止痒效果、控油效果、固发效果。
Claims (2)
1.一种红参中药洗发水，其特征在于，包括如下重量份数的组分：
红参提取物2-6份，香榧提取物0.1-0.3份，侧柏提取物0.1-0.3份，牛蒡提取物0.1-0.3份，黑豆提取物0.1-0.3份，鱼腥草提取物0.1-0.3份，紫苏叶提取物0.1-0.3份，何首乌提取物0.1-0.3份，月桂醇聚醚硫酸酯铵11-13份，月桂醇硫酸酯铵3-5份，硬脂酰胺丙基二甲胺0.2-0.4份，椰子油脂肪酸二乙醇酰胺0.8-1.2份，椰油酰胺丙基甜菜碱5-7份，聚季铵盐-100.08-0.12份，瓜儿胶羟丙基三甲基氯化铵0.18-0.22份，EFA 亚油酰胺丙基丙二醇单磷酸酯基二甲基氯化铵0.18-0.22份，羟乙基脲2-4份，发酵马油0.08-0.12份，乙基己基甘油0.04-0.06份，柠檬酸0.185-0.205份，PEG -7椰油甘油酸酯1-3份，油醇聚醚-5磷酸酯0.2-0.4份，SCP 二聚亚油酰胺丙基 PG-二甲基氯化铵磷酸酯0.4-0.6份，对羟基苯乙酮0.1-0.3份，食盐2.5-4.5份，己脒定0.02-0.04份，香水0.05-0.15份，余量用水补充至100份。
2.一种红参中药洗发水的制备工艺，其特征在于，按照所述的重量分配比，包括如下步骤：
S1，将水抽入水相锅中，搅拌并慢慢加入聚季铵盐-10、瓜儿胶羟丙基三甲基氯化铵升温至80-85℃形成A相混合物；
S2，A相完全溶解呈透明状后，依次加入月桂醇聚醚硫酸酯铵、月桂醇硫酸酯铵硬脂酰胺丙基二甲胺搅拌溶解，完全溶解后温度降至60℃以下；
S3，新容器中依次加入CDEA-椰子油脂肪酸二乙醇酰胺、羟乙基脲、红参提取物、香榧提取物、侧柏提取物、牛蒡提取物、黑豆提取物、鱼腥草提取物、紫苏叶提取物、何首乌提取物、发酵马油、PEG -7椰油甘油酸酯、油醇聚醚-5磷酸酯、EFA 亚油酰胺丙基丙二醇单磷酸酯基二甲基氯化铵、SCP 二聚亚油酰胺丙基 PG-二甲基氯化铵磷酸酯、椰油酰胺丙基甜菜碱、柠檬酸形成B相；新容器中依次加入对羟基苯乙酮、乙基己基甘油、苯甲酸钠形成C相；将对羟基苯乙酮、乙基己基甘油、苯甲酸钠混合形成D相；
S4，将C相、D相依次加入A相中搅拌溶解，取样观察，检测pH，完全溶解后温度降至45℃以下时，依次加入己脒定和香水搅拌溶解10min后，加入食盐水调整粘度，必要时，需要打循环；
合成锅中，混合均匀，加热至75-80℃，保温混合30-35min，形成第二混合物；
S5，将步骤S4中获得的混合物送检、出料、包装。
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