CN112358798A - Manufacturing method of floor waterproof material - Google Patents

Manufacturing method of floor waterproof material Download PDF

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Publication number
CN112358798A
CN112358798A CN202011185126.2A CN202011185126A CN112358798A CN 112358798 A CN112358798 A CN 112358798A CN 202011185126 A CN202011185126 A CN 202011185126A CN 112358798 A CN112358798 A CN 112358798A
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waterproof
emulsion
stirring
mixing
parts
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刘华
郑宪明
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Anhui Dayu Waterproof Technology Development Co ltd
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Anhui Dayu Waterproof Technology Development Co ltd
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Priority to CN202011185126.2A priority Critical patent/CN112358798A/en
Publication of CN112358798A publication Critical patent/CN112358798A/en
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D175/00Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
    • C09D175/04Polyurethanes
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D191/00Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
    • C09D191/06Waxes
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18Fireproof paints including high temperature resistant paints
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/61Additives non-macromolecular inorganic
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/18Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20Oxides; Hydroxides
    • C08K3/22Oxides; Hydroxides of metals
    • C08K2003/2217Oxides; Hydroxides of metals of magnesium
    • C08K2003/222Magnesia, i.e. magnesium oxide
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/18Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20Oxides; Hydroxides
    • C08K3/22Oxides; Hydroxides of metals
    • C08K2003/2227Oxides; Hydroxides of metals of aluminium
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/32Phosphorus-containing compounds
    • C08K2003/321Phosphates
    • C08K2003/324Alkali metal phosphate
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00Properties
    • C08L2201/02Flame or fire retardant/resistant
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical And Physical Treatments For Wood And The Like (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

The invention discloses a manufacturing method of a floor waterproof material, which comprises the steps of preparing mixed resin emulsion, preparing mixed liquid, preparing dipping suspension emulsion, and preparing waterproof dipping emulsion, wherein the waterproof dipping emulsion is prepared from water-soluble phenolic resin, water-soluble polyurethane resin emulsion, hydrophobic silicon dioxide, talcum powder, flame retardant, nano magnesium oxide, aluminum oxide, sodium pyrophosphate, melamine and nano paraffin emulsion; according to the invention, the wood floor has a waterproof effect by preparing the waterproof material into the impregnating emulsion for waterproof impregnation, complex attaching or coating processing is not required, the construction is convenient and rapid, the waterproof effect is obvious, the formed waterproof layer has good wear resistance by adding the aluminum oxide powder, the wood floor is protected while the waterproof layer is protected, and the flame retardant can enable the waterproof layer to have a flame retardant effect, so that the flame retardant effect of the wood floor is better.

Description

Manufacturing method of floor waterproof material
Technical Field
The invention relates to the technical field of waterproof materials, in particular to a manufacturing method of a floor waterproof material.
Background
The floor, i.e. the surface layer of the floor or floor of a house, is made of wood or other materials, and the floor is classified into a plurality of categories, including: solid wood floors, laminate wood floors, three-layer solid wood laminate floors, bamboo and wood floors, anti-corrosion floors, cork floors, and the most popular multilayer solid wood laminate floors; classified by use are: household, commercial, antistatic floors, outdoor floors, floors dedicated to stage dancing, floors dedicated to sports stadiums, floors dedicated to track and field, etc.;
after being laid, the wood floor is often stained with water or eroded by damp air, so the wood floor generally has a certain waterproof function, and the traditional waterproof method is to attach or plate a layer of waterproof film on the surface of the wood floor, the traditional waterproof film has poor wear resistance, is easy to wear, and the construction method is troublesome, so the construction period is influenced, therefore, the invention provides a manufacturing method of the floor waterproof material to solve the problems in the prior art.
Disclosure of Invention
In view of the above problems, an object of the present invention is to provide a method for manufacturing a floor waterproof material, in which a wood floor has a waterproof effect by preparing a waterproof material into an impregnation emulsion for waterproof impregnation, and no complicated adhesion or coating process is required, the construction is convenient and fast, the waterproof effect is significant, the waterproof layer formed by adding aluminum oxide powder has good wear resistance, the wood floor is protected while the waterproof layer is protected, and the flame retardant enables the waterproof layer to have a flame retardant effect, so that the flame retardant effect of the wood floor is better.
In order to realize the purpose of the invention, the invention is realized by the following technical scheme: a manufacturing method of a floor waterproof material comprises the following steps:
step one, mixing water-soluble phenolic resin and water-soluble polyurethane resin emulsion according to the required parts, adding the mixture into a reaction kettle, mixing and stirring at the stirring speed of 120-140 r/min to prepare mixed resin emulsion;
step two, mixing hydrophobic silicon dioxide, talcum powder, flame retardant, nano-magnesia and aluminum oxide according to the required parts to obtain mixed powder, adding the mixed powder into the mixed resin emulsion prepared in the step one, continuously mixing and stirring by using a reaction kettle, and reducing the stirring speed to 80-100 revolutions per minute to prepare a mixed solution;
step three, mixing the sodium pyrophosphate and the melamine according to the required parts, adding the mixture into the mixed solution prepared in the step two, mixing and stirring the mixture, and increasing the stirring speed to 150-170 revolutions per minute to prepare the dipping suspension emulsion;
and step four, adding the nano paraffin emulsion before the dipping suspension emulsion is used, and mixing and stirring by using a mixing and stirring tool, wherein the stirring speed is controlled at 60-70 r/min, so as to prepare the waterproof dipping emulsion.
The further improvement lies in that: in the first step, the water-soluble phenolic resin and the water-soluble polyurethane resin emulsion account for 30-35 parts to 45-50 parts of the total weight of the waterproof impregnating solution, and when a reaction kettle is used for mixing and stirring, the reaction kettle is heated to 50-70 ℃, and the temperature is kept and the stirring is continued for 5-8 min.
The further improvement lies in that: in the second step, the hydrophobic silicon dioxide, the talcum powder, the flame retardant, the nano magnesium oxide and the aluminum oxide account for 5-8 parts, 3-5 parts, 7-10 parts and 20-25 parts of the waterproof dipping solution in the total weight ratio, the temperature of the reaction kettle is reduced to 30-35 ℃ during mixing and stirring, and the reaction kettle is kept warm and is continuously stirred for 10-15 min.
The further improvement lies in that: and in the second step, the flame retardant is one of phosphoric acid triester, pentabromoethyl benzene and tetrabromobisphenol A.
The further improvement lies in that: in the third step, the total weight ratio of the sodium pyrophosphate to the melamine in the waterproof impregnating solution is 3-5 parts to 4-6 parts, and the temperature is kept at 30-35 ℃ during mixing and stirring for 7-10 minutes.
The further improvement lies in that: the preparation of the micro-nano paraffin emulsion in the fourth step is to use the sliced paraffin as a raw material, add an emulsifier compounded by span 80 and OP-15 emulsifier, and prepare the micro-nano paraffin emulsion by combining an O-D emulsification method and a PIT steering emulsification method.
The further improvement lies in that: the application method of the waterproof dipping emulsion prepared in the fourth step is that before the floor is laid, the floor is placed into the waterproof dipping emulsion to be dipped for 60-80 min, then the floor is taken out to be dried, and the laying construction can be carried out when a layer of smooth protective film is formed on the surface.
The invention has the beneficial effects that: according to the invention, the wood floor has a waterproof effect by preparing the waterproof material into the impregnating emulsion for waterproof impregnation, complex attaching or coating processing is not required, the construction is convenient and rapid, the waterproof effect is obvious, the formed waterproof layer has good wear resistance by adding the aluminum oxide powder, the wood floor is protected while the waterproof layer is protected, and the flame retardant can enable the waterproof layer to have a flame retardant effect, so that the flame retardant effect of the wood floor is better.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to these drawings without creative efforts.
FIG. 1 is a flow chart of the present invention.
Detailed Description
In order to further understand the present invention, the following detailed description will be made with reference to the following examples, which are only used for explaining the present invention and are not to be construed as limiting the scope of the present invention.
Example 1
According to fig. 1, the embodiment provides a method for manufacturing a floor waterproof material, which comprises the following steps:
step one, mixing water-soluble phenolic resin and water-soluble polyurethane resin emulsion according to the required parts, adding the mixture into a reaction kettle, mixing and stirring at the stirring speed of 120-140 r/min to prepare mixed resin emulsion;
step two, mixing hydrophobic silicon dioxide, talcum powder, flame retardant, nano-magnesia and aluminum oxide according to the required parts to obtain mixed powder, adding the mixed powder into the mixed resin emulsion prepared in the step one, continuously mixing and stirring by using a reaction kettle, and reducing the stirring speed to 80-100 revolutions per minute to prepare a mixed solution;
step three, mixing the sodium pyrophosphate and the melamine according to the required parts, adding the mixture into the mixed solution prepared in the step two, mixing and stirring the mixture, and increasing the stirring speed to 150-170 revolutions per minute to prepare the dipping suspension emulsion;
and step four, adding the nano paraffin emulsion before the dipping suspension emulsion is used, and mixing and stirring by using a mixing and stirring tool, wherein the stirring speed is controlled at 60-70 r/min, so as to prepare the waterproof dipping emulsion.
In the first step, the water-soluble phenolic resin and the water-soluble polyurethane resin emulsion account for 30-35 parts to 45-50 parts of the total weight of the waterproof impregnating solution, and when a reaction kettle is used for mixing and stirring, the reaction kettle is heated to 50-70 ℃, and the temperature is kept and the stirring is continued for 5-8 min.
In the second step, the hydrophobic silicon dioxide, the talcum powder, the flame retardant, the nano magnesium oxide and the aluminum oxide account for 5-8 parts, 3-5 parts, 7-10 parts and 20-25 parts of the waterproof dipping solution in the total weight ratio, the temperature of the reaction kettle is reduced to 30-35 ℃ during mixing and stirring, the temperature is kept and the stirring is continued for 10-15 min, and the flame retardant is phosphotriester in the second step.
In the third step, the total weight ratio of the sodium pyrophosphate to the melamine in the waterproof impregnating solution is 3-5 parts to 4-6 parts, and the temperature is kept at 30-35 ℃ during mixing and stirring for 7-10 minutes.
The preparation of the micro-nano paraffin emulsion in the fourth step is to use the sliced paraffin as a raw material, add an emulsifier compounded by span 80 and OP-15 emulsifier, and prepare the micro-nano paraffin emulsion by combining an O-D emulsification method and a PIT steering emulsification method.
The application method of the waterproof dipping emulsion prepared in the fourth step is that before the floor is laid, the floor is placed into the waterproof dipping emulsion to be dipped for 60-80 min, then the floor is taken out to be dried, and the laying construction can be carried out when a layer of smooth protective film is formed on the surface.
Example 2
According to fig. 1, the embodiment provides a method for manufacturing a floor waterproof material, which comprises the following steps:
step one, mixing water-soluble phenolic resin and water-soluble polyurethane resin emulsion according to the required parts, adding the mixture into a reaction kettle, mixing and stirring at the stirring speed of 120-140 r/min to prepare mixed resin emulsion;
step two, mixing hydrophobic silicon dioxide, talcum powder, flame retardant, nano-magnesia and aluminum oxide according to the required parts to obtain mixed powder, adding the mixed powder into the mixed resin emulsion prepared in the step one, continuously mixing and stirring by using a reaction kettle, and reducing the stirring speed to 80-100 revolutions per minute to prepare a mixed solution;
step three, mixing the sodium pyrophosphate and the melamine according to the required parts, adding the mixture into the mixed solution prepared in the step two, mixing and stirring the mixture, and increasing the stirring speed to 150-170 revolutions per minute to prepare the dipping suspension emulsion;
and step four, adding the nano paraffin emulsion before the dipping suspension emulsion is used, and mixing and stirring by using a mixing and stirring tool, wherein the stirring speed is controlled at 60-70 r/min, so as to prepare the waterproof dipping emulsion.
In the first step, the water-soluble phenolic resin and the water-soluble polyurethane resin emulsion account for 30-35 parts to 45-50 parts of the total weight of the waterproof impregnating solution, and when a reaction kettle is used for mixing and stirring, the reaction kettle is heated to 50-70 ℃, and the temperature is kept and the stirring is continued for 5-8 min.
In the second step, the hydrophobic silicon dioxide, the talcum powder, the flame retardant, the nano magnesium oxide and the aluminum oxide account for 5-8 parts, 3-5 parts, 7-10 parts and 20-25 parts of the waterproof dipping solution in the total weight ratio, the temperature of the reaction kettle is reduced to 30-35 ℃ during mixing and stirring, the temperature is kept and the stirring is continued for 10-15 min, and the flame retardant is pentabromoethylbenzene in the second step.
In the third step, the total weight ratio of the sodium pyrophosphate to the melamine in the waterproof impregnating solution is 3-5 parts to 4-6 parts, and the temperature is kept at 30-35 ℃ during mixing and stirring for 7-10 minutes.
The preparation of the micro-nano paraffin emulsion in the fourth step is to use the sliced paraffin as a raw material, add an emulsifier compounded by span 80 and OP-15 emulsifier, and prepare the micro-nano paraffin emulsion by combining an O-D emulsification method and a PIT steering emulsification method.
The application method of the waterproof dipping emulsion prepared in the fourth step is that before the floor is laid, the floor is placed into the waterproof dipping emulsion to be dipped for 60-80 min, then the floor is taken out to be dried, and the laying construction can be carried out when a layer of smooth protective film is formed on the surface.
Example 3
According to fig. 1, the embodiment provides a method for manufacturing a floor waterproof material, which comprises the following steps:
step one, mixing water-soluble phenolic resin and water-soluble polyurethane resin emulsion according to the required parts, adding the mixture into a reaction kettle, mixing and stirring at the stirring speed of 120-140 r/min to prepare mixed resin emulsion;
step two, mixing hydrophobic silicon dioxide, talcum powder, flame retardant, nano-magnesia and aluminum oxide according to the required parts to obtain mixed powder, adding the mixed powder into the mixed resin emulsion prepared in the step one, continuously mixing and stirring by using a reaction kettle, and reducing the stirring speed to 80-100 revolutions per minute to prepare a mixed solution;
step three, mixing the sodium pyrophosphate and the melamine according to the required parts, adding the mixture into the mixed solution prepared in the step two, mixing and stirring the mixture, and increasing the stirring speed to 150-170 revolutions per minute to prepare the dipping suspension emulsion;
and step four, adding the nano paraffin emulsion before the dipping suspension emulsion is used, and mixing and stirring by using a mixing and stirring tool, wherein the stirring speed is controlled at 60-70 r/min, so as to prepare the waterproof dipping emulsion.
In the first step, the water-soluble phenolic resin and the water-soluble polyurethane resin emulsion account for 30-35 parts to 45-50 parts of the total weight of the waterproof impregnating solution, and when a reaction kettle is used for mixing and stirring, the reaction kettle is heated to 50-70 ℃, and the temperature is kept and the stirring is continued for 5-8 min.
In the second step, the hydrophobic silica, the talcum powder, the flame retardant, the nano magnesium oxide and the aluminum oxide account for 5-8 parts, 3-5 parts, 7-10 parts and 20-25 parts of the waterproof dipping liquid in the total weight ratio, the temperature of the reaction kettle is reduced to 30-35 ℃ during mixing and stirring, the temperature is kept and the stirring is continued for 10-15 min, and the flame retardant is tetrabromobisphenol A in the second step.
In the third step, the total weight ratio of the sodium pyrophosphate to the melamine in the waterproof impregnating solution is 3-5 parts to 4-6 parts, and the temperature is kept at 30-35 ℃ during mixing and stirring for 7-10 minutes.
The preparation of the micro-nano paraffin emulsion in the fourth step is to use the sliced paraffin as a raw material, add an emulsifier compounded by span 80 and OP-15 emulsifier, and prepare the micro-nano paraffin emulsion by combining an O-D emulsification method and a PIT steering emulsification method.
The application method of the waterproof dipping emulsion prepared in the fourth step is that before the floor is laid, the floor is placed into the waterproof dipping emulsion to be dipped for 60-80 min, then the floor is taken out to be dried, and the laying construction can be carried out when a layer of smooth protective film is formed on the surface.
According to the manufacturing method of the floor waterproof material, the wood floor has the waterproof effect by the method of manufacturing the waterproof material into the dipping emulsion for waterproof dipping, complex attaching or coating processing is not needed, construction is convenient and fast, the waterproof effect is obvious, the formed waterproof layer has good wear resistance by adding the aluminum oxide powder, the wood floor is protected while the waterproof layer is protected, and the flame retardant can enable the waterproof layer to have the flame-retardant effect, so that the flame-retardant effect of the wood floor is better.
The foregoing illustrates and describes the principles, general features, and advantages of the present invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the invention as claimed. The scope of the invention is defined by the appended claims and equivalents thereof.

Claims (7)

1. A manufacturing method of a floor waterproof material is characterized by comprising the following steps:
step one, mixing water-soluble phenolic resin and water-soluble polyurethane resin emulsion according to the required parts, adding the mixture into a reaction kettle, mixing and stirring at the stirring speed of 120-140 r/min to prepare mixed resin emulsion;
step two, mixing hydrophobic silicon dioxide, talcum powder, flame retardant, nano-magnesia and aluminum oxide according to the required parts to obtain mixed powder, adding the mixed powder into the mixed resin emulsion prepared in the step one, continuously mixing and stirring by using a reaction kettle, and reducing the stirring speed to 80-100 revolutions per minute to prepare a mixed solution;
step three, mixing the sodium pyrophosphate and the melamine according to the required parts, adding the mixture into the mixed solution prepared in the step two, mixing and stirring the mixture, and increasing the stirring speed to 150-170 revolutions per minute to prepare the dipping suspension emulsion;
and step four, adding the nano paraffin emulsion before the dipping suspension emulsion is used, and mixing and stirring by using a mixing and stirring tool, wherein the stirring speed is controlled at 60-70 r/min, so as to prepare the waterproof dipping emulsion.
2. The manufacturing method of the floor waterproof material as claimed in claim 1, wherein: in the first step, the water-soluble phenolic resin and the water-soluble polyurethane resin emulsion account for 30-35 parts to 45-50 parts of the total weight of the waterproof impregnating solution, and when a reaction kettle is used for mixing and stirring, the reaction kettle is heated to 50-70 ℃, and the temperature is kept and the stirring is continued for 5-8 min.
3. The manufacturing method of the floor waterproof material as claimed in claim 1, wherein: in the second step, the hydrophobic silicon dioxide, the talcum powder, the flame retardant, the nano magnesium oxide and the aluminum oxide account for 5-8 parts, 3-5 parts, 7-10 parts and 20-25 parts of the waterproof dipping solution in the total weight ratio, the temperature of the reaction kettle is reduced to 30-35 ℃ during mixing and stirring, and the reaction kettle is kept warm and is continuously stirred for 10-15 min.
4. The manufacturing method of the floor waterproof material as claimed in claim 1, wherein: and in the second step, the flame retardant is one of phosphoric acid triester, pentabromoethyl benzene and tetrabromobisphenol A.
5. The manufacturing method of the floor waterproof material as claimed in claim 1, wherein: in the third step, the total weight ratio of the sodium pyrophosphate to the melamine in the waterproof impregnating solution is 3-5 parts to 4-6 parts, and the temperature is kept at 30-35 ℃ during mixing and stirring for 7-10 minutes.
6. The manufacturing method of the floor waterproof material as claimed in claim 1, wherein: the preparation of the micro-nano paraffin emulsion in the fourth step is to use the sliced paraffin as a raw material, add an emulsifier compounded by span 80 and OP-15 emulsifier, and prepare the micro-nano paraffin emulsion by combining an O-D emulsification method and a PIT steering emulsification method.
7. The manufacturing method of the floor waterproof material as claimed in claim 1, wherein: the application method of the waterproof dipping emulsion prepared in the fourth step is that before the floor is laid, the floor is placed into the waterproof dipping emulsion to be dipped for 60-80 min, then the floor is taken out to be dried, and the laying construction can be carried out when a layer of smooth protective film is formed on the surface.
CN202011185126.2A 2020-10-30 2020-10-30 Manufacturing method of floor waterproof material Pending CN112358798A (en)

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Publication number Priority date Publication date Assignee Title
CN114939910A (en) * 2022-05-31 2022-08-26 南京林业大学 Waterproof agent for wood composite board and application method thereof

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CN106280959A (en) * 2016-09-07 2017-01-04 广西大学 Water-in-water type sound insulation multi-color and preparation method thereof
CN107903758A (en) * 2017-10-30 2018-04-13 合肥林邦门业有限公司 A kind of preparation method of the water-fast timber coating of aqueous, environmental protective
CN109295801A (en) * 2018-09-30 2019-02-01 兰溪泛仕达新材料科技有限公司 A kind of water-based hydrophobic water-proof emulsion
CN111205757A (en) * 2020-02-18 2020-05-29 关怡 Waterborne polyurethane coating

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114939910A (en) * 2022-05-31 2022-08-26 南京林业大学 Waterproof agent for wood composite board and application method thereof

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Application publication date: 20210212