CN112335932A - Solid aromatic bead for heating non-combustible cigarette bullet and preparation method thereof - Google Patents
Solid aromatic bead for heating non-combustible cigarette bullet and preparation method thereof Download PDFInfo
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- CN112335932A CN112335932A CN202011252646.0A CN202011252646A CN112335932A CN 112335932 A CN112335932 A CN 112335932A CN 202011252646 A CN202011252646 A CN 202011252646A CN 112335932 A CN112335932 A CN 112335932A
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- 239000011324 bead Substances 0.000 title claims abstract description 168
- 125000003118 aryl group Chemical group 0.000 title claims abstract description 61
- 239000007787 solid Substances 0.000 title claims abstract description 53
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 37
- 238000010438 heat treatment Methods 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title abstract description 14
- 239000000126 substance Substances 0.000 claims abstract description 156
- 238000000576 coating method Methods 0.000 claims abstract description 87
- 239000011248 coating agent Substances 0.000 claims abstract description 86
- 239000000919 ceramic Substances 0.000 claims abstract description 69
- 238000002791 soaking Methods 0.000 claims abstract description 40
- 238000001816 cooling Methods 0.000 claims abstract description 7
- 239000011148 porous material Substances 0.000 claims abstract description 7
- 239000007788 liquid Substances 0.000 claims description 25
- 238000003756 stirring Methods 0.000 claims description 24
- 239000000796 flavoring agent Substances 0.000 claims description 21
- 235000019634 flavors Nutrition 0.000 claims description 21
- 241000207199 Citrus Species 0.000 claims description 16
- 235000020971 citrus fruits Nutrition 0.000 claims description 16
- 239000000443 aerosol Substances 0.000 claims description 14
- 239000003795 chemical substances by application Substances 0.000 claims description 14
- 239000002245 particle Substances 0.000 claims description 12
- 235000013871 bee wax Nutrition 0.000 claims description 11
- 239000012166 beeswax Substances 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 11
- 235000006679 Mentha X verticillata Nutrition 0.000 claims description 9
- 235000002899 Mentha suaveolens Nutrition 0.000 claims description 9
- 235000001636 Mentha x rotundifolia Nutrition 0.000 claims description 9
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 8
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 claims description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 6
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 238000011049 filling Methods 0.000 claims description 6
- 235000012907 honey Nutrition 0.000 claims description 6
- 238000007789 sealing Methods 0.000 claims description 6
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- HPEUJPJOZXNMSJ-UHFFFAOYSA-N Methyl stearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC HPEUJPJOZXNMSJ-UHFFFAOYSA-N 0.000 claims description 4
- ZDJFDFNNEAPGOP-UHFFFAOYSA-N dimethyl tetradecanedioate Chemical compound COC(=O)CCCCCCCCCCCCC(=O)OC ZDJFDFNNEAPGOP-UHFFFAOYSA-N 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 4
- MMKRHZKQPFCLLS-UHFFFAOYSA-N ethyl myristate Chemical compound CCCCCCCCCCCCCC(=O)OCC MMKRHZKQPFCLLS-UHFFFAOYSA-N 0.000 claims description 4
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 4
- URAYPUMNDPQOKB-UHFFFAOYSA-N triacetin Chemical compound CC(=O)OCC(OC(C)=O)COC(C)=O URAYPUMNDPQOKB-UHFFFAOYSA-N 0.000 claims description 4
- 229960000541 cetyl alcohol Drugs 0.000 claims description 3
- OVOUKWFJRHALDD-UHFFFAOYSA-N 2-[2-(2-acetyloxyethoxy)ethoxy]ethyl acetate Chemical compound CC(=O)OCCOCCOCCOC(C)=O OVOUKWFJRHALDD-UHFFFAOYSA-N 0.000 claims description 2
- HIQIXEFWDLTDED-UHFFFAOYSA-N 4-hydroxy-1-piperidin-4-ylpyrrolidin-2-one Chemical compound O=C1CC(O)CN1C1CCNCC1 HIQIXEFWDLTDED-UHFFFAOYSA-N 0.000 claims description 2
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 2
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims description 2
- 239000004348 Glyceryl diacetate Substances 0.000 claims description 2
- DOOTYTYQINUNNV-UHFFFAOYSA-N Triethyl citrate Chemical compound CCOC(=O)CC(O)(C(=O)OCC)CC(=O)OCC DOOTYTYQINUNNV-UHFFFAOYSA-N 0.000 claims description 2
- IZMOTZDBVPMOFE-UHFFFAOYSA-N dimethyl dodecanedioate Chemical compound COC(=O)CCCCCCCCCCC(=O)OC IZMOTZDBVPMOFE-UHFFFAOYSA-N 0.000 claims description 2
- CAMHHLOGFDZBBG-UHFFFAOYSA-N epoxidized methyl oleate Natural products CCCCCCCCC1OC1CCCCCCCC(=O)OC CAMHHLOGFDZBBG-UHFFFAOYSA-N 0.000 claims description 2
- 235000019443 glyceryl diacetate Nutrition 0.000 claims description 2
- 239000001087 glyceryl triacetate Substances 0.000 claims description 2
- 235000013773 glyceryl triacetate Nutrition 0.000 claims description 2
- 239000004310 lactic acid Substances 0.000 claims description 2
- 235000014655 lactic acid Nutrition 0.000 claims description 2
- 239000000600 sorbitol Substances 0.000 claims description 2
- 239000000758 substrate Substances 0.000 claims description 2
- 229960002622 triacetin Drugs 0.000 claims description 2
- 239000001069 triethyl citrate Substances 0.000 claims description 2
- VMYFZRTXGLUXMZ-UHFFFAOYSA-N triethyl citrate Natural products CCOC(=O)C(O)(C(=O)OCC)C(=O)OCC VMYFZRTXGLUXMZ-UHFFFAOYSA-N 0.000 claims description 2
- 235000013769 triethyl citrate Nutrition 0.000 claims description 2
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 claims description 2
- 244000241257 Cucumis melo Species 0.000 claims 3
- 235000009847 Cucumis melo var cantalupensis Nutrition 0.000 claims 2
- 239000007967 peppermint flavor Substances 0.000 claims 2
- 235000011187 glycerol Nutrition 0.000 claims 1
- 230000000391 smoking effect Effects 0.000 abstract description 10
- 239000011159 matrix material Substances 0.000 abstract description 7
- 239000000843 powder Substances 0.000 description 8
- 235000013599 spices Nutrition 0.000 description 8
- 229920002472 Starch Polymers 0.000 description 7
- 238000005422 blasting Methods 0.000 description 7
- 235000019698 starch Nutrition 0.000 description 7
- 239000008107 starch Substances 0.000 description 7
- 239000006187 pill Substances 0.000 description 6
- 241000219112 Cucumis Species 0.000 description 5
- 241000209094 Oryza Species 0.000 description 5
- 235000007164 Oryza sativa Nutrition 0.000 description 5
- 244000062793 Sorghum vulgare Species 0.000 description 5
- 235000019713 millet Nutrition 0.000 description 5
- 235000009566 rice Nutrition 0.000 description 5
- OXQOBQJCDNLAPO-UHFFFAOYSA-N 2,3-Dimethylpyrazine Chemical compound CC1=NC=CN=C1C OXQOBQJCDNLAPO-UHFFFAOYSA-N 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 4
- 229940119429 cocoa extract Drugs 0.000 description 4
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 4
- 229930014626 natural product Natural products 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- YIKYNHJUKRTCJL-UHFFFAOYSA-N Ethyl maltol Chemical compound CCC=1OC=CC(=O)C=1O YIKYNHJUKRTCJL-UHFFFAOYSA-N 0.000 description 2
- 239000011258 core-shell material Substances 0.000 description 2
- 229940093503 ethyl maltol Drugs 0.000 description 2
- 239000002304 perfume Substances 0.000 description 2
- 239000000779 smoke Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000011247 coating layer Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 235000015073 liquid stocks Nutrition 0.000 description 1
- 239000011550 stock solution Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/17—Filters specially adapted for simulated smoking devices
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Bakery Products And Manufacturing Methods Therefor (AREA)
Abstract
A solid aromatic bead for heating non-combustible cigarette bullet and its preparation method are provided. The invention aims to solve the problem that in the prior art, the solid aromatic bead is heated to release the aromatic substances more quickly, so that the aromatic substances in the solid aromatic bead are basically released in the later period of smoking, and comfortable experience cannot be obtained. The technical points are as follows: the solid fragrant bead includes kernel and coating, and features that the kernel has porous ceramic bead body as matrix and the porous ceramic bead body has kernel fragrant matter permeating through its pores and the coating has fragrant matter coating. The preparation method comprises the steps of preparing the fragrant substance of the inner core → soaking the porous ceramic bead body → preparing the fragrant bead → preparing the fragrant substance of the coating → coating the fragrant bead → guiding and cooling to obtain the solid fragrant bead.
Description
Technical Field
The invention relates to the technical field of compensating or increasing aroma on cigarettes, in particular to a solid aromatic bead for heating a non-combustible cigarette bomb and a preparation method thereof.
Background
The aromatic beads are used for compensating or increasing the aroma of the cigarettes by smokers, so that the cigarettes have richer and more fragrant mouthfeel, and the smokers can obtain more comfortable experience. The first fragrant bead is named as "bead blasting", and is small glue bead with different types of perfume liquid packed inside and set inside the cigarette filter tow for smoker to burst and make the liquid inside the bead flow out. Because fingers, teeth or bead blasting pliers are often required to be used for blasting during blasting, the use is troublesome, and the types of the perfume liquid which can be wrapped by the small rubber beads are limited, solid fragrant beads capable of slowly releasing fragrance appear in the field of cigarettes to replace 'bead blasting'.
The Chinese patent No. 202010130324.2 discloses a solid aromatic bead with a core-shell structure and an application thereof in cigarette filter sticks, which is characterized in that the solid aromatic bead with the core-shell structure is prepared by taking millet or yellow rice as an inner core and externally wrapping natural product powder, plant powder and the like through a coating technology, namely, the millet or yellow rice is taken as the core and the natural product powder or plant powder is taken as a shell, and then essence and spice for cigarettes are added in the coating process. The raw materials and the weight portions thereof are as follows: the total parts are 100 parts, wherein 10-40 parts of millet or yellow rice, 50-80 parts of natural product powder or plant powder and 5-10 parts of essence spice for cigarettes are included. The preparation method comprises the following steps: soaking millet or yellow rice, placing the millet or yellow rice into a shot blasting machine or a coating machine for rotation, slowly spraying natural product powder or plant powder into the shot blasting machine or the coating machine to obtain solid flavor bead pills, placing the solid flavor bead pills into a hot air oven for drying to remove water, spraying tobacco flavor and spice for flavor coating, and placing the solid flavor bead pills into the hot air oven for drying to obtain the solid flavor beads. The disadvantages of this solution are: the solid aromatic bead is heated to release the aromatic substances in the coating in the former stage of smoking, so that a smoker can have more comfortable experience, but the aromatic substances in the solid aromatic bead are basically released in the later stage of smoking, so that the smoker cannot have comfortable experience.
Chinese patent No. 201910439499.9 discloses a cigarette filter stick containing novel solid aromatic beads and a preparation method thereof, which is characterized in that the solid aromatic beads are prepared by taking porous starch as a main raw material and adsorbing one or more mixed spices of cocoa extract, 2, 3-dimethyl pyrazine, furfural and ethyl maltol. The raw materials and the weight percentage thereof are as follows: the cocoa extract comprises one to five percent of porous starch; the 2, 3-dimethyl pyrazine accounts for five to ten parts per million of the porous starch; the proportion of the furfural in the porous starch is five to ten parts per million; the proportion of the ethyl maltol in the porous starch is three hundred and six hundred thousand. The preparation method comprises the following steps: preparing cocoa extract, mixing the cocoa extract with other raw materials to prepare solid flavor bead young pills, and performing microwave treatment on the flavor bead young pills to improve the strength of the flavor bead young pills and generate flavor substances to form solid flavor beads. The disadvantages of this solution are: the solid aromatic bead takes the porous starch as a matrix for storing the aromatic substances, and the porous starch can be thermally degraded under the baking of hot smoke and can damage the performance of the stored aromatic substances, so that the solid aromatic bead is heated to release the aromatic substances more quickly, and the aromatic substances in the solid aromatic bead can be basically released in the later period of smoking by a smoker, so that the comfortable experience cannot be obtained.
Disclosure of Invention
In order to solve the problem that in the prior art, the solid aromatic bead is heated to release aromatic substances quickly, so that a smoker can not obtain comfortable experience because the aromatic substances in the solid aromatic bead are basically released in the later period of smoking, the invention aims to provide the solid aromatic bead for heating a non-combustible cigarette bullet and the preparation method thereof, and the defects in the prior art can be overcome.
The technical scheme adopted by the invention for solving the technical problems is as follows: a solid aromatic bead for heating a non-combustible cigarette cartridge, comprising an inner core and a coating on the outer surface of the inner core, characterized in that: the inner core takes a porous ceramic bead body as a matrix, the porous ceramic bead body is infiltrated with an inner core aroma substance in the body through micropores of the porous ceramic bead body, and the coating contains a coating aroma substance.
According to the technical scheme, the porous ceramic beads can be a ceramic body with a large number of open micro pores on the surface, the pore size of the micro pores is micron-sized or submicron-sized, and the particle size of the porous ceramic beads can be 3.1-3.6 mm. The porous ceramic beads may be porous ceramic beads or porous ceramic beads.
According to the technical scheme, the inner core aroma substance can be formed by mixing a spice and an aerosol generating agent, the spice can adopt a mint essence and a Hami melon essence, and the components and the weight percentages of the inner core aroma substance adopting the mint essence and the Hami melon essence can adopt: 42-48% of mint essence; 16-23% of Hami melon essence; 30-40% of aerosol generating agent.
The inner core aromatic substance in the technical scheme can be formed by mixing a spice and an aerosol generating agent, wherein the spice can adopt a citrus essence and a citrus extract, and the inner core aromatic substance adopting the citrus essence and the citrus extract comprises the following components in percentage by weight: 28-35% of citrus essence; 16-22% of citrus extract; 45-55% of aerosol generating agent.
In the above technical scheme, the aerosol generating agent may be a liquid stock solution of a mixture of one or more of sorbitol, glycerol, propylene glycol, triethylene glycol, lactic acid, diacetin, triacetin, triethylene glycol diacetate, triethyl citrate, ethyl myristate, isopropyl myristate, methyl stearate, dimethyl dodecanedioate, and dimethyl tetradecanedioate.
The coating aroma substance in the technical scheme comprises the following components in percentage by weight: 15-25% of honey; 13-18% of beeswax; 52-60% of conversion sugar; 8-14% of cetyl alcohol.
The preparation method of the solid aromatic bead for heating the non-combustible cigarette bullet in the technical scheme is characterized by comprising the following process steps of:
firstly, taking the weight percentage of each component substance for composing the kernel fragrant substance, putting the components substances into a stirrer, mixing and stirring the components to be fully dissolved together, then modulating the components to be 10-30% in concentration to form the kernel fragrant substance, and then filling the kernel fragrant substance into a sealed container for standby;
putting the porous ceramic beads with the particle size of 3.1-3.6 mm into a soaking container, then pouring the inner core aroma substance into the soaking container, enabling the liquid level to be higher than that of the porous ceramic beads in the soaking container, and soaking the porous ceramic beads in the inner core aroma substance for 70-74 hours;
thirdly, taking the porous ceramic beads out of the soaking container, drying liquid substances on the surfaces of the porous ceramic beads to form fragrant beads, and putting the fragrant beads into a light-resistant bottle for sealing for later use;
taking the weight percentage of each component substance for forming the coating aroma substance, and fully stirring and dissolving the components substance at the temperature of 60-80 ℃ to form liquid to obtain the coating aroma substance;
taking coating aroma substances accounting for 5-20% of the weight of the fragrant beads to be coated, uniformly stirring the coating aroma substances and the fragrant beads to be coated in a coating stirrer, and coating the fragrant beads, wherein the coating temperature is controlled to be 60-80 ℃, and the stirring time is controlled to be 5-10 minutes;
sixthly, guiding out the coated incense beads, and cooling to obtain the finished solid incense beads.
When the porous ceramic beads are taken out from the soaking container, the kernel aromatic substances for soaking can be filtered by adopting a 60-mesh filter screen, and liquid substances on the surfaces of the porous ceramic beads can be sucked by adopting vacuum equipment.
The component substance of the kernel fragrant substance in the technical scheme can adopt mint essence, the temperature of the kernel fragrant substance adopting the mint essence is kept above 25 ℃ when the kernel fragrant substance is prepared or soaked, and the heating temperature is controlled below 60 ℃ when the kernel fragrant substance is heated below 25 ℃.
The coating aroma substance can be beeswax, and when the coating is carried out, the coating aroma substance adopting beeswax is heated at 64-70 ℃ until the beeswax is molten, and then the coating is carried out.
The solid aromatic bead finished by the technical scheme is suitable for being arranged inside a cigarette bullet which is not combusted by heating, and can also be arranged in a filter tow of a cigarette.
The invention has the beneficial effects that: the porous ceramic beads are used as a core substrate, core aroma substances are infiltrated into the porous ceramic beads, and the porous ceramic beads are coated by the coating aroma substances to form two different aroma substance storage structures which are integrated into a whole, so that a smoker can release the coating aroma substances from the coating layer in the front stage of smoking, and the smoker can obtain more comfortable experience; in the later period of smoking, because the porous ceramic beads are used for depositing the inner core aroma substances, the porous ceramic beads are not thermally degraded under the baking of hot smoke in the former period of smoking, and the structure and the performance of the deposited aroma substances cannot be damaged, the inner core aroma substances deposited in the inner core can be continuously released enough in the later period of smoking, so that a smoker can obtain more comfortable experience; therefore, the cigarette can be compensated or added in the whole process of smoking a cigarette which is not burnt after being heated once, and the cigarette has richer and more fragrant mouthfeel and more comfortable experience.
The present invention will be further described with reference to the following examples.
Detailed Description
The first embodiment is as follows: the solid aromatic bead for heating the non-combustible cigarette bullet comprises an inner core and a coating coated on the outer surface of the inner core, and is characterized in that: the inner core takes a porous ceramic bead body with the particle size of 3.1-3.3 mm as a matrix, the porous ceramic bead body is infiltrated with an inner core aroma substance in the body through micropores of the porous ceramic bead body, and the coating contains a coating aroma substance. The kernel aroma substance comprises the following components in percentage by weight: 42-45% of mint essence; 16-21% of Hami melon essence; 34-40% of aerosol generating agent. The coating aroma substance comprises the following components in percentage by weight: 15-18% of honey; 17-18% of beeswax; 52-55% of conversion sugar; 12-14% of hexadecanol.
The preparation method of the solid aromatic bead for heating the non-combustible cigarette bullet comprises the following process steps:
firstly, taking the weight percentage of each component substance for composing the kernel fragrant substance, putting the components substances into a stirrer for mixing and stirring under the condition of 25-60 ℃, fully dissolving the components together, then modulating the mixture into the kernel fragrant substance with the concentration of 10 percent, and then filling the kernel fragrant substance into a sealed container for standby;
placing the porous ceramic beads with the particle size of 3.1-3.3 mm into a soaking container, then pouring the inner core aroma substance into the soaking container at the temperature of 25-60 ℃, enabling the liquid level to be higher than that of the porous ceramic beads in the soaking container, and soaking the porous ceramic beads in the inner core aroma substance for 70-74 hours;
thirdly, taking the porous ceramic beads out of the soaking container, filtering out the kernel aroma substances for soaking by adopting a 60-mesh filter screen when taking out, sucking the liquid substances on the surfaces of the porous ceramic beads by using vacuum equipment to form aroma beads, and putting the aroma beads into a light-resistant bottle for sealing for later use;
taking the weight percentage of each component substance for forming the coating aroma substance, and fully stirring and dissolving the components substance at the temperature of 64-70 ℃ to form liquid to obtain the coating aroma substance;
taking coating aroma substances accounting for 5-10% of the weight of the fragrant beads to be coated, uniformly stirring the coating aroma substances and the fragrant beads to be coated in a coating stirrer, and coating the fragrant beads, wherein the coating temperature is controlled to be constant at 64-70 ℃, and the stirring time is controlled to be 5-7 minutes;
sixthly, guiding out the coated incense beads, and cooling to obtain the finished solid incense beads.
Example two: the solid aromatic bead for heating the non-combustible cigarette bullet comprises an inner core and a coating coated on the outer surface of the inner core, and is characterized in that: the inner core takes a porous ceramic bead body with the particle size of 3.3-3.6 mm as a matrix, the porous ceramic bead body is infiltrated with an inner core aroma substance in the body through micropores of the porous ceramic bead body, and the coating contains a coating aroma substance. The kernel aroma substance comprises the following components in percentage by weight: 45-48% of mint essence; 21-23% of Hami melon essence; 30-34% of aerosol generating agent. The coating aroma substance comprises the following components in percentage by weight: 18-25% of honey; 13-17% of beeswax; 54-60% of conversion sugar; 8-12% of cetyl alcohol.
The preparation method of the solid aromatic bead for heating the non-combustible cigarette bullet comprises the following process steps:
firstly, taking the proportioning of the weight percentage of each component substance for composing the kernel fragrant substance, putting the components substances into a stirrer for mixing and stirring under the condition of 25-60 ℃, fully dissolving the components together, then modulating the mixture into a concentration of 20 percent to become the kernel fragrant substance, and then filling the kernel fragrant substance into a sealed container for standby;
placing the porous ceramic beads with the particle size of 3.3-3.6 mm into a soaking container, then pouring the kernel aroma-causing substance into the soaking container at the temperature of 25-60 ℃, enabling the liquid level to be higher than that of the porous ceramic beads in the soaking container, and soaking the porous ceramic beads in the kernel aroma-causing substance for 70-74 hours;
thirdly, taking the porous ceramic beads out of the soaking container, filtering out the kernel aroma substances for soaking by adopting a 60-mesh filter screen when taking out, sucking the liquid substances on the surfaces of the porous ceramic beads by using vacuum equipment to form aroma beads, and putting the aroma beads into a light-resistant bottle for sealing for later use;
taking the weight percentage of each component substance for forming the coating aroma substance, and fully stirring and dissolving the components substance at the temperature of 64-70 ℃ to form liquid to obtain the coating aroma substance;
taking coating aroma substances accounting for 5-15% of the weight of the fragrant beads to be coated, uniformly stirring the coating aroma substances and the fragrant beads to be coated in a coating stirrer, and coating the fragrant beads, wherein the coating temperature is controlled to be constant at 64-70 ℃, and the stirring time is controlled to be 7-10 minutes;
sixthly, guiding out the coated incense beads, and cooling to obtain the finished solid incense beads.
Example three: the solid aromatic bead for heating the non-combustible cigarette bullet comprises an inner core and a coating coated on the outer surface of the inner core, and is characterized in that: the inner core takes a porous ceramic bead body with the particle size of 3.1-3.3 mm as a matrix, the porous ceramic bead body is infiltrated with an inner core aroma substance in the body through micropores of the porous ceramic bead body, and the coating contains a coating aroma substance. The kernel aroma substance comprises the following components in percentage by weight: 28-32% of citrus essence; 16-19% of citrus extract; 50-55% of aerosol generating agent. The coating aroma substance comprises the following components in percentage by weight: 15-18% of honey; 17-18% of beeswax; 52-55% of conversion sugar; 12-14% of hexadecanol.
The preparation method of the solid aromatic bead for heating the non-combustible cigarette bullet comprises the following process steps:
taking the proportioning of the weight percentage of each component substance for composing the kernel fragrant substance, putting the components in a stirrer for mixing and stirring under the normal temperature condition to fully dissolve the components together, then modulating the components into the kernel fragrant substance with the concentration of 20 percent to form the kernel fragrant substance, and then filling the kernel fragrant substance into a sealed container for standby;
placing the porous ceramic beads with the particle size of 3.1-3.3 mm into a soaking container, then pouring the kernel aroma-causing substance into the soaking container under the condition of normal temperature, enabling the liquid level to be higher than that of the porous ceramic beads in the soaking container, and soaking the porous ceramic beads in the kernel aroma-causing substance for 70-74 hours;
thirdly, taking the porous ceramic beads out of the soaking container, filtering out the kernel aroma substances for soaking by adopting a 60-mesh filter screen when taking out, sucking the liquid substances on the surfaces of the porous ceramic beads by using vacuum equipment to form aroma beads, and putting the aroma beads into a light-resistant bottle for sealing for later use;
taking the weight percentage of each component substance for forming the coating aroma substance, and fully stirring and dissolving the components substance at the temperature of 64-70 ℃ to form liquid to obtain the coating aroma substance;
taking coating aroma substances accounting for 5-10% of the weight of the fragrant beads to be coated, uniformly stirring the coating aroma substances and the fragrant beads to be coated in a coating stirrer, and coating the fragrant beads, wherein the coating temperature is controlled to be constant at 64-70 ℃, and the stirring time is controlled to be 5-7 minutes;
sixthly, guiding out the coated incense beads, and cooling to obtain the finished solid incense beads.
Example four: the solid aromatic bead for heating the non-combustible cigarette bullet comprises an inner core and a coating coated on the outer surface of the inner core, and is characterized in that: the inner core takes a porous ceramic bead body with the particle size of 3.3-3.6 mm as a matrix, the porous ceramic bead body is infiltrated with an inner core aroma substance in the body through micropores of the porous ceramic bead body, and the coating contains a coating aroma substance. The kernel aroma substance comprises the following components in percentage by weight: 32-35% of citrus essence; 18-22% of citrus extract; 45-50% of aerosol generating agent. The coating aroma substance comprises the following components in percentage by weight: 15-18% of honey; 17-18% of beeswax; 52-55% of conversion sugar; 12-14% of hexadecanol.
The preparation method of the solid aromatic bead for heating the non-combustible cigarette bullet comprises the following process steps:
taking the weight percentage of each component substance for composing the kernel aroma substance, putting the components substances into a stirrer for mixing and stirring under the condition of normal temperature, fully dissolving the components together, then modulating the mixture into a concentration of 30 percent to form the kernel aroma substance, and then filling the kernel aroma substance into a sealed container for standby;
placing the porous ceramic beads with the particle size of 3.3-3.6 mm into a soaking container, then pouring the kernel aroma-causing substance into the soaking container under the condition of normal temperature, enabling the liquid level to be higher than that of the porous ceramic beads in the soaking container, and soaking the porous ceramic beads in the kernel aroma-causing substance for 70-74 hours;
thirdly, taking the porous ceramic beads out of the soaking container, filtering out the kernel aroma substances for soaking by adopting a 60-mesh filter screen when taking out, sucking the liquid substances on the surfaces of the porous ceramic beads by using vacuum equipment to form aroma beads, and putting the aroma beads into a light-resistant bottle for sealing for later use;
taking the weight percentage of each component substance for forming the coating aroma substance, and fully stirring and dissolving the components substance at the temperature of 60-80 ℃ to form liquid to obtain the coating aroma substance;
taking coating aroma substances accounting for 5-10% of the weight of the fragrant beads to be coated, uniformly stirring the coating aroma substances and the fragrant beads to be coated in a coating stirrer, and coating the fragrant beads, wherein the coating temperature is controlled to be constant at 60-80 ℃, and the stirring time is controlled to be 5-7 minutes;
sixthly, guiding out the coated incense beads, and cooling to obtain the finished solid incense beads.
Claims (10)
1. A solid aromatic bead for heating a non-combustible cigarette cartridge, comprising an inner core and a coating on the outer surface of the inner core, characterized in that: the inner core uses a microporous ceramic bead body as a substrate, the microporous ceramic bead body is infiltrated with an inner core aroma substance in the body through micropores of the microporous ceramic bead body, and the coating contains a coating aroma substance.
2. The solid flavor bead for heating a non-combustible cigarette bomb according to claim 1, wherein the porous ceramic bead body is a ceramic body having fine open pores densely distributed on the surface, the pore size of the fine pores is in the micron or submicron order, and the particle size of the porous ceramic bead body is 3.1-3.6 mm.
3. The solid aromatic bead for heating a non-combustible cigarette bullet of claim 1, wherein said inner core aromatic substance is composed of a mixture of a flavor and an aerosol generating agent, said flavor is selected from the group consisting of peppermint flavor and cantaloupe flavor, and the components of the inner core aromatic substance selected from the group consisting of said peppermint flavor and cantaloupe flavor and the weight percentages thereof are as follows: 42-48% of mint essence; 16-23% of Hami melon essence; 30-40% of aerosol generating agent.
4. The solid aromatic bead for heating a non-combustible cigarette bomb according to claim 1, wherein said inner core aromatic substance is composed of a mixture of a flavor and an aerosol generating agent, said flavor is citrus flavor and citrus extract, and the components and weight percentages of the inner core aromatic substance using said citrus flavor and citrus extract are: 28-35% of citrus essence; 16-22% of citrus extract; 45-55% of aerosol generating agent.
5. The solid flavor bead for heating a non-combustible cigarette bullet of claim 3 or 4, wherein said aerosol generating agent is a liquid raw liquid of one or a mixture of two or more of sorbitol, glycerin, propylene glycol, triethylene glycol, lactic acid, diacetin, triacetin, triethylene glycol diacetate, triethyl citrate, ethyl myristate, isopropyl myristate, methyl stearate, dimethyl dodecanedioate and dimethyl tetradecanedioate.
6. Solid aromatic bead for heating non-combustible cartridges according to claim 1, characterised in that the composition and the percentages by weight of the coating aromatic substance are: 15-25% of honey; 13-18% of beeswax; 52-60% of conversion sugar; 8-14% of cetyl alcohol.
7. The method for preparing solid beads for heating a non-combustible cigarette bomb according to claim 1, 2, 3, 4 or 6, characterized by the following process steps:
firstly, taking the weight percentage of each component substance for composing the kernel fragrant substance, putting the components substances into a stirrer, mixing and stirring the components to be fully dissolved together, then modulating the components to be 10-30% in concentration to form the kernel fragrant substance, and then filling the kernel fragrant substance into a sealed container for standby;
putting the porous ceramic beads with the particle size of 3.1-3.6 mm into a soaking container, then pouring the inner core aroma substance into the soaking container, enabling the liquid level to be higher than that of the porous ceramic beads in the soaking container, and soaking the porous ceramic beads in the inner core aroma substance for 70-74 hours;
thirdly, taking the porous ceramic beads out of the soaking container, drying liquid substances on the surfaces of the porous ceramic beads to form fragrant beads, and putting the fragrant beads into a light-resistant bottle for sealing for later use;
taking the weight percentage of each component substance for forming the coating aroma substance, and fully stirring and dissolving the components substance at the temperature of 60-80 ℃ to form liquid to obtain the coating aroma substance;
taking coating aroma substances accounting for 5-20% of the weight of the fragrant beads to be coated, uniformly stirring the coating aroma substances and the fragrant beads to be coated in a coating stirrer, and coating the fragrant beads, wherein the coating temperature is controlled to be 60-80 ℃, and the stirring time is controlled to be 5-10 minutes;
sixthly, guiding out the coated incense beads, and cooling to obtain the finished solid incense beads.
8. The method of claim 7, wherein the porous ceramic beads are removed from the soaking container by filtering out the core aromatic substance for soaking with a 60 mesh sieve and sucking out the liquid substance on the surface of the porous ceramic beads with a vacuum device.
9. The method for preparing solid aromatic beads for heating a non-combustible cigarette bullet according to claim 7, wherein the component substances of the inner core aromatic substance are mint essence, the temperature of the inner core aromatic substance is kept above 25 ℃ when the inner core aromatic substance is prepared or soaked, and the heating temperature is controlled below 60 ℃ when the inner core aromatic substance is heated below 25 ℃.
10. The method for preparing solid aromatic beads for heating a non-combustible cigarette bullet according to claim 1 or 2, characterized in that the coating aromatic substance is composed of beeswax, and the coating aromatic substance is heated at 64-70 ℃ until the beeswax is melted when the coating is performed, and then the coating is performed.
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| CN108851214A (en) * | 2018-08-06 | 2018-11-23 | 江西中烟工业有限责任公司 | A kind of ramuscule cigarette holder stick and preparation method thereof containing single solid-state perfume (or spice) pearl particle |
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| WO2019135618A1 (en) * | 2018-01-03 | 2019-07-11 | 주식회사 케이티앤지 | Aerosol-generating article and apparatus |
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| CN213881751U (en) * | 2020-11-11 | 2021-08-06 | 上海德明生物科技有限公司 | Solid aromatic bead for heating non-combustible cigarette bullet |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2019135618A1 (en) * | 2018-01-03 | 2019-07-11 | 주식회사 케이티앤지 | Aerosol-generating article and apparatus |
| CN108851214A (en) * | 2018-08-06 | 2018-11-23 | 江西中烟工业有限责任公司 | A kind of ramuscule cigarette holder stick and preparation method thereof containing single solid-state perfume (or spice) pearl particle |
| CN109907368A (en) * | 2019-03-01 | 2019-06-21 | 江西中烟工业有限责任公司 | The preparation method of active nano solid ceramic perfume (or spice) pearl and its application in cigarette filter rod |
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