CN105105327B - A kind of champignon cigarette and preparation method thereof containing full constituent tobacco extract - Google Patents
A kind of champignon cigarette and preparation method thereof containing full constituent tobacco extract Download PDFInfo
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- CN105105327B CN105105327B CN201510429376.9A CN201510429376A CN105105327B CN 105105327 B CN105105327 B CN 105105327B CN 201510429376 A CN201510429376 A CN 201510429376A CN 105105327 B CN105105327 B CN 105105327B
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Abstract
The invention belongs to tobacco product fields, disclose a kind of champignon cigarette and preparation method thereof containing full constituent tobacco extract.A kind of champignon cigarette containing full constituent tobacco extract includes functional components, carbonaceous powder, plant fiber, adhesive；The functional components are tobacco extract and tobacco extract particle；The tobacco extract particle includes at least two substrate layers with different tobacco extract contents；The substrate layer successively coats, and the surface of substrate layer is coated with coatings, contains excipient in the substrate layer；The tobacco extract particle is gradually reduced by tobacco extract content in interior substrate layer outward.Tobacco component in champignon cigarette containing full constituent tobacco extract is provided by both tobacco extract and tobacco extract particle, the release process of the two forms complementation, the tobacco component content in the champignon cigarette containing full constituent tobacco extract is maintained, provides lasting and uniform taste for consumer.
Description
Technical field
The invention belongs to tobacco product fields, more particularly, to a kind of champignon cigarette containing full constituent tobacco extract
And preparation method thereof.
Background technique
The smokeless tobacco articles on overseas market are mostly tobacco powder product at present, mostly with packed buccal cigarette, bulk form
The forms such as buccal cigarette, snuff exist.A kind of important supplement form of the tobacco chewing gum as smokeless tobacco articles, meets tobacco
The psychological need of consumer, but the absorption mode of traditional tobacco ingredient is changed, consumer is difficult to adapt to this smoking habit.
Summary of the invention
The technical problem to be solved in the present invention is that overcoming the deficiencies of existing technologies, one kind is provided and is mentioned containing full constituent tobacco
The champignon cigarette of object is taken, the champignon cigarette containing full constituent tobacco extract can effectively control nicotine and contain full constituent tobacco
Rate of release in the champignon cigarette combustion process of extract increases the course that the ingredients such as nicotine at the uniform velocity discharge.
Another object of the present invention is to provide the preparation sides of the champignon cigarette described in one kind containing full constituent tobacco extract
Method.
The invention is realized by the following technical scheme:
A kind of champignon cigarette containing full constituent tobacco extract, including it is functional components, carbonaceous powder, plant fiber, viscous
Mixture；The functional components are tobacco extract and tobacco extract particle；
The tobacco extract accounts for the 3%~15% of champignon cigarette quality；Tobacco extract particle account for champignon cigarette quality 5%~
30%；
The tobacco extract particle includes at least two substrate layers with different tobacco extract contents；The substrate
Layer successively coats, and the surface of substrate layer is coated with coatings, contains excipient in the substrate layer；The tobacco extract particle
It is gradually reduced by tobacco extract content in interior substrate layer outward.
Tobacco component in champignon cigarette of the present invention containing full constituent tobacco extract is by tobacco extract and tobacco
Both extract particles provide, and the tobacco extract is dispersed in champignon cigarette, and tobacco extract particle is in granular form
It is uniformly distributed in champignon cigarette.In combustion, while gradually decreasing with initial tobacco extract content, tobacco is extracted
Tobacco extract in object particle gradually discharges, and then maintains the tobacco of the champignon cigarette release containing full constituent tobacco extract
Component content provides lasting and uniform smoking effect for consumer.
The coatings can avoid tobacco in the process of manufacture of the champignon cigarette containing full constituent tobacco extract
The volatilization loss of effective component in extract particle, convenient for the preservation of tobacco extract；The nicotine in particle etc. is prevented to be dissolved into
Ensure the flavor of tobacco product in champignon cigarette containing full constituent tobacco extract in turn；In addition coatings also play sustained release
Effect, can improve the release uniformity of tobacco extract particle in use.
The content of tobacco extract is gradually reduced outward by interior in the tobacco extract particle, can effectively have been controlled
The release for imitating ingredient provides uniform flavor in the combustion process of the champignon cigarette containing full constituent tobacco extract and holds perfume (or spice)
Property.For example, the content of the tobacco extract particle is gradually reduced outward by interior, can overcome containing full constituent tobacco extract
Champignon cigarette combustion process middle and later periods effective smoke components burst size deficiency, the smoking effect of continuous and effective is provided.
The tobacco that the present invention uses is one or more of burley tobaccos, flue-cured tobacco, Turkish tobaccos.
Preferably, the champignon cigarette containing full constituent tobacco extract by following mass percent material composition:
Tobacco extract 3%~15%；Tobacco extract particle 5%~30%；Carbonaceous powder 10%~50%；Plant fiber 10%
~35%；Adhesive 1%~10%；
The tobacco extract particle includes at least two substrate layers with different tobacco extract contents；The substrate
Layer successively coats, and the surface of substrate layer is coated with coatings, contains excipient in the substrate layer；The tobacco extract particle
It is gradually reduced by tobacco extract content in interior substrate layer outward.
It is further preferred that tobacco extract 6%~12%；Tobacco extract particle 9%~23%；Carbonaceous powder 18%~
42%；Plant fiber 15%~30%；Adhesive 4%~7%；The tobacco extract particle includes that there are different tobacco extracts to contain
The substrate layer of amount；The substrate layer successively coats, and the surface of substrate layer is coated with coatings, contains figuration in the substrate layer
Agent；The tobacco extract particle is gradually reduced by tobacco extract content in interior substrate layer outward.
Preferably, the partial size of the tobacco extract particle is 100um~1000um.Further preferably, the cigarette
The partial size of careless extract particle is 400um~600um.
Preferably, the tobacco extract is medicinal extract shape, amorphous powder, solution etc..
Preferably, the mass fraction of nicotine is 8% in the tobacco extract；Nicotine in the tobacco extract particle
Mass fraction is 6%.
Preferably, the carbonaceous powder be charcoal powder or bamboo charcoal powder, granularity be 80~150 mesh, ash be 8%~
12%, moisture≤10%.
Preferably, the plant fiber is or mixtures thereof wood-fibred through defibrination, bamboo fibre, secondary stock, certainly
It can also be according to raw material state using other plant fibers.
Preferably, described adhesive is elm bark powder, bakelite powder, alphalise starch, methylcellulose.
Due to different extracting method and extraction process, can be obtained extract component have it is dramatically different.Due to containing
The use of the champignon cigarette of full constituent tobacco extract is different from traditional cigarette, therefore meets suction as traditional cigarette to obtain
The demand (main component is nicotine) of cigarette person, while the generation of other miscellaneous tastes is avoided, mouthfeel is destroyed, and be unfavorable for containing full constituent
The subsequent seasoning and adjusting incense of the champignon cigarette of tobacco extract.It is extracted in the present invention using two steps, and two extraction steps
In the high water of nicotine solubility and ethyl alcohol (being polar solvent) is respectively adopted as extractant, ensuring abundant extraction nicotine
Meanwhile, it is capable to efficiently reduce the dissolution of the nonessential oil components of other in tobacco.
Preferably, tobacco extract extracting method the following steps are included:
S11. nonpolar solvent is added into tobacco after 60 DEG C~70 DEG C are impregnated, it is cooling, in not higher than 30 DEG C of items
It is filtered after ultrasonic extraction under part, obtains filter residue a and filtrate a；
S12. it after polar solvent being added into the filter residue a of S11, filters, obtains after ultrasonic extraction under the conditions of not higher than 30 DEG C
To filter residue b and filtrate b；
S13. filtrate a and filtrate b is mixed, concentration obtains the tobacco extract.
According to the principle that balances each other that substance is spread, the present invention uses two step abstraction techniques, more can effectively extract in tobacco
The effective components such as nicotine.Impregnate using 60 DEG C~70 DEG C of nonpolar solvent and can quickly moisten tobacco of rising, and can subtract
Reaction between few tobacco component；Furthermore the volatility of nonpolar solvent is weaker, effective component in tobacco can be effectively avoided
Volatilization.Tobacco structure after ultrasonic extraction is more loose, enables polar solvent to reach the inside of tobacco rapidly, is not required to
To impregnate again, can the effective components such as nicotine to tobacco internal further extract, improve extraction yield.
Preferably, the nonpolar solvent is in petroleum ether, acetone, chloroform, hexane, ethyl acetate, methylene chloride etc.
One or more.
Preferably, the polar solvent is selected from one or more of water, ethyl alcohol etc..
In order to prevent during ultrasonic extraction, improves extraction efficiency and prevent the loss of effective component, it is preferably ultrasonic
Extraction temperature is not higher than 30 DEG C.
Preferably, the excipient be selected from starch, Icing Sugar, dextrin, lactose, modified starch, microcrystalline cellulose, mannitol,
The one or more of sorbierite and erythrose.
Preferably, the material of the coating is microcrystalline cellulose, Arabic gum, sodium alginate, carragheen, dextrin, modification
Any one in starch, gelatin, casein, polyvinyl alcohol, sodium carboxymethylcellulose, ethyl cellulose or methylcellulose is several
Kind.
In order to control the rate of release of tobacco extract, in the use process of the champignon cigarette containing full constituent tobacco extract
In, so that being extracted in the substrate of the release of extract and the champignon cigarette containing full constituent tobacco extract in tobacco extract particle
The release of object has gentle transition, it is preferable that also contains pore-foaming agent in the material of the coating；So that coatings have centainly
Hole, conducive to the release of tobacco extract.
Preferably, the pore-foaming agent is sucrose, sorbierite, mannitol, polyethylene glycol, hydroxypropyl methyl cellulose, hydroxyl
One or more of propyl cellulose.
Preferably, the mass ratio of the absolute dry mass and nonpolar solvent of tobacco is 1:13~15 in S11；Filter residue a in S12
The mass ratio of absolute dry mass and polar solvent is 1:6~8；The power of ultrasonic wave is 250W~350W in S11 and S12, ultrasonic
Time is 30min~70min；Ultrasonic temperature is 20 DEG C~30 DEG C.
It is further preferred that the absolute dry mass of tobacco described in S11 and the mass ratio of nonpolar solvent are 1:14；In S12
The absolute dry mass of filter residue a and the mass ratio of polar solvent are 1:7；The power of ultrasonic wave is 300W, ultrasonic temperature in S11 and S12
It is 25 DEG C；The time of the S11 ultrasound is 60min；The time of the S12 ultrasound is 30min.The ratio energy of the tobacco and water
It is enough sufficiently to moisten tobacco of rising, and the concentration difference of the effective components such as nicotine two-phase in water and tobacco can be made larger, improve ultrasound extraction
Take efficiency.Loss of effective components caused by a large amount of extract liquors of subsequent concentration is also avoided simultaneously, and can be reduced energy consumption.
A kind of preparation method of the tobacco extract particle, comprising the following steps:
S21. the tobacco extract is uniformly mixed with excipient, adds water that softwood is made；
S22. softwood made from S21 is put into extrusion-round as a ball pelletizer and is pelletized, then obtain core material through drying, sieving；
S23. the first-class dynamic mixtures of tobacco extract and excipient are prepared；
Core material made from S22 is put into fluidized bed pelletizer, each parameter of fluidized bed pelletizer is adjusted, is in core material
Fluidized state sprays into first-class dynamic mixtures, forms first base material layer in core surfaces after drying, it is micro- that sieving obtains first
Grain；
S24. the N flowable state mixture of tobacco extract and excipient, N >=2 are prepared；
First particle made from S23 is put into fluidized bed pelletizer, each parameter of fluidized bed pelletizer is adjusted, makes first
Particle is in fluidized state, sprays into N flowable state mixture, forms N substrate layer in the first microparticle surfaces after drying, is sieved
To N particle；
S25. coating solution is prepared；
N particle made from S24 is put into fluidized bed pelletizer, each parameter of fluidized bed pelletizer is adjusted, keeps N micro-
Grain is in fluidized state, sprays into coating solution, forms coatings in N microparticle surfaces after drying, sieving obtains the tobacco and extracts
Object particle；
Wherein, tobacco extract content > first base material layer tobacco extract content > N substrate layer of the core material
Tobacco extract content.
The core material of tobacco extract particle of the present invention is granulated by extrusion-round as a ball pelletizer, so that the more cause of core material
Close and tobacco extract content is maximum, is conducive to extend the release duration of tobacco extract and provides burst size, it is ensured that is new
Type tobacco product uses the taste and flavor in latter stage.
The core material has coated multiple substrate layers by bed spray more than once, on the surface of core material, and by
The interior tobacco extract concentration to outer different substrate materials layer is gradually reduced, so that can in the use process of new tobacco products
There are uniform taste and fragrance.More uniform covered effect can be obtained using fluidized bed pelletizer.
Preferably, the partial size of the first particle and N particle incrementally increases in S23, S24, it is further preferred that the difference
It is 100um~110um that the partial size of particle, which increases amplitude,.In order to ensure the variation of taste is uniform, and ensure with a batch of particle
The uniformity of quality, it is preferable that the first particle, N particle respective partial size range be no more than 100um.Preferably, described
The partial size of one particle is 400 um~500um, and the partial size of the second particle is 500 um~600um.
Preferably, core material passes through 3 cladding substrate layers, i.e. N is 3.
Since in synchronization, the dissolution of different tobacco extract particles or releasing degree are different, uniform in order to obtain
Taste, this requires the concentration differences between core material, different substrate materials layer in a reasonable range.Based on technical solution of the present invention,
Preferably, the tobacco extract content difference of core material, first base material layer, N substrate layer is 10%~15%.
Preferably, extrusion-round as a ball pelletizer extrusion hole diameter of sieve (perforated) plate is 0.2~0.4mm in S22；Extrusion revolving speed is 80r/
The r/min of min~150；Round as a ball revolving speed is the r/min of 250r/min~350；The round as a ball time is 3min~6min；Drying temperature is
40~45 DEG C；The partial size of the core material is 300 um~500um.
It is further preferred that extrusion-round as a ball pelletizer extrusion hole diameter of sieve (perforated) plate is 0.3mm in S22；Squeezing out revolving speed is 120
r/min；Round as a ball revolving speed is 300 r/min；The round as a ball time is 5min；Drying temperature is 42 DEG C；The partial size of the core material is 300
Um~400um.
Preferably, in S23, S24 and S25 fluidized bed pelletizer process conditions are as follows: intake be 500 m3/ h~800m3/
H, stream temperature are 40~45 DEG C, and atomization gas pressure is 0.2Mpa~0.4Mpa；First-class dynamic mixtures, N flowable state are mixed
Close object, coating solution concentration be 6%~10%, mist flow be 0.6ml/min~0.9ml/min.
It is further preferred that in S23, S24 and S25 fluidized bed pelletizer process conditions are as follows: intake 600m3/ h,
Stream temperature is 43 DEG C, and atomization gas pressure is 0.3Mpa；First-class dynamic mixtures, N flowable state mixture, coating solution it is dense
Degree is 7%, mist flow 0.8ml/min.
Preferably, the solvent that coating solution uses is water or ethyl alcohol, is also added with surfactant.
In order to obtain optimal slow release effect and the variation of uniform mouthfeel, it is preferable that core material, first base material layer and N substrate
The mass fraction that layer accounts for the tobacco extract particle is equal.
A kind of preparation method of the champignon cigarette containing full constituent tobacco extract, comprising the following steps:
S31. plant fiber is taken to be discongested, be beaten by weight percent, adjust concentration after obtain vegetable-fibre slurry；
S32. it after vegetable-fibre slurry and tobacco extract particle, carbonaceous powder, adhesive being mixed, copies
Make, be dehydrated, punch forming, low temperature drying remove water, obtain champignon cigarette substrate；
S33. the upper tobacco extract is sprayed on above-mentioned champignon cigarette substrate, obtains described mentioning containing full constituent tobacco
Take the champignon cigarette of object.
The present invention is mentioned with the tobacco that reduces that tobacco extract particle and vegetable-fibre slurry etc. mix high degree
Take object manufacture paper with pulp, be dehydrated and drying course in loss.In champignon cigarette substrate it is added to tobacco extract particle simultaneously, it can be with
Increase the preservation form of tobacco component and holding time in the champignon cigarette containing full constituent tobacco extract, also can increase tobacco
The mode of extract release.The tobacco extract being sprayed on champignon cigarette substrate is that the uniformity of tobacco component release plays pass
Key effect.
Tobacco extract and tobacco extract particle are successively added in two steps and extract containing full constituent tobacco by the present invention
In the champignon cigarette of object, is on the one hand conducive to tobacco extract and is uniformly distributed；On the other hand, prevent tobacco extract from largely covering
After tobacco extract particle, cause to be unevenly distributed, it is agglomerating the disadvantages of.
Compared with prior art, the invention has the following advantages:
Tobacco component in champignon cigarette of the present invention containing full constituent tobacco extract is by tobacco extract and tobacco
Both extract particles provide, and the release process of the two forms complementation, maintains the champignon cigarette containing full constituent tobacco extract
In tobacco component content, provide and continue and uniform taste for consumer.
Tobacco extract particle in champignon cigarette containing full constituent tobacco extract has substrate layer and coatings, and base
The concentration of the tobacco extract of material layer is gradually reduced from inside to outside so that in particle tobacco extract burst size and rate of release
Uniformly, it ensure that the uniformity of new tobacco products taste and fragrance.
Pore-foaming agent in the coatings makes the release of extract and new tobacco products in tobacco extract particle
The release of extract has gentle transition in substrate.
The effective components such as Extraction solvent and the method energy sufficiently extraction nicotine of the tobacco extract, while avoiding other miscellaneous
The generation of taste improves mouthfeel and is conducive to being used cooperatively for tobacco extract and other flavor additives usefuls, and sterile no residue product, defends
Raw safety.
The particle of the prilling process for the substep that the present invention uses, preparation has multilayered structure, and can effectively control difference
The tobacco extract content of substrate layer and the thickness of substrate layer etc., it is ensured that the tobacco extract particle of preparation has well
Even property, and then ensure that the taste and flavor for being added to the new tobacco products of the tobacco extract particle.
Specific embodiment
The present invention is further illustrated combined with specific embodiments below.Unless stated otherwise, it is used in the embodiment of the present invention
Raw material, device and method are the raw material of this field regular market purchase, conventional use of device and method.
Embodiment 1
(1) preparation of tobacco extract
S11. taking absolute dry mass is the flue-cured tobacco of 100g, and 1400g acetone is added after 60 DEG C carry out immersion 25min, is cooled to
20 DEG C or so, the ultrasonic extraction 60min under the conditions of 25 ± 2 DEG C, the power of ultrasonic wave is 300W, and then vacuum suction filtering, obtains
To filter residue a and filtrate a；
S12. it is ultrasonic under the conditions of 25 ± 2 DEG C after the ethyl alcohol of 7 times of absolute dry mass of filter residue a is added into the filter residue a of S11
30min is extracted, the power of ultrasonic wave is 300W, and then vacuum suction filtering, obtains filter residue b and filtrate b；
S13. filtrate a and filtrate b is mixed, it is 15% that solid content is concentrated in vacuo under the conditions of 25 DEG C, obtains the cigarette
Careless extract.
(2) preparation of tobacco extract particle
S21. the tobacco extract prepared in (1) is uniformly mixed with starch, adds suitable water that softwood is made；
S22. softwood made from S21 is put into extrusion-round as a ball pelletizer and is pelletized, extrusion-round as a ball pelletizer squeezes in S2
Hole diameter of sieve (perforated) plate is 0.3mm out；Extrusion revolving speed is 120 r/min；Round as a ball revolving speed is 300 r/min；The round as a ball time is 5min；Then at
Drying temperature at 42 DEG C；It is 300 um~400um core material that sieving, which obtains partial size, and the content of tobacco extract is 50% in core material.
S23. the first-class dynamic mixtures of tobacco extract and starch are prepared；
Core material made from S22 is put into fluidized bed pelletizer, each parameter of fluidized bed pelletizer is adjusted, is in core material
Fluidized state sprays into first-class dynamic mixtures.The technological condition of fluidized bed pelletizer are as follows: intake 500m3/ h, stream
Changing temperature is 40 DEG C, and atomization gas pressure is 0.2Mpa；The concentration of first-class dynamic mixtures is 8%, mist flow 0.9ml/
min.First base material layer is formed in core surfaces after drying, it is the first particle of 400 um~500um, the first base that sieving, which obtains partial size,
The content of tobacco extract is 40% in material layer.
S24. the second dynamic mixtures of tobacco extract and excipient are prepared；
First particle made from S23 is put into fluidized bed pelletizer, each parameter of fluidized bed pelletizer is adjusted, makes first
Particle is in fluidized state, sprays into second dynamic mixtures.The technological condition of fluidized bed pelletizer are as follows: intake is
600m3/ h, stream temperature are 43 DEG C, and atomization gas pressure is 0.3Mpa；The concentration of second dynamic mixtures is 7%, mist flow
For 0.8ml/min.The second substrate layer is formed in the first microparticle surfaces after drying, it is 600 um~700um that sieving, which obtains partial size,
Two particles, the content of tobacco extract is 30% in the second substrate layer.
S25. the third flowable state mixture of tobacco extract and excipient is prepared；
Second particle made from S24 is put into fluidized bed pelletizer, each parameter of fluidized bed pelletizer is adjusted, makes second
Particle is in fluidized state, sprays into third flowable state mixture.The technological condition of fluidized bed pelletizer are as follows: intake is
800m3/ h, stream temperature are 45 DEG C, and atomization gas pressure is 0.4Mpa；The concentration of third flowable state mixture is 9%, mist flow
For 0.6ml/min.Third substrate layer is formed in the second microparticle surfaces after drying, it is 700 um~800um that sieving, which obtains partial size,
Three particles, the content of tobacco extract is 20% in third substrate layer.
S26. coating solution is prepared；Coating solution is made of microcrystalline cellulose, polyvinyl alcohol and suitable water, microcrystalline cellulose
Mass ratio with polyvinyl alcohol is 9:1, and the concentration of coating solution is 9%.
Third particle made from S25 is put into fluidized bed pelletizer, each parameter of fluidized bed pelletizer is adjusted, makes third
Particle is in fluidized state, sprays into coating solution.The technological condition of fluidized bed pelletizer are as follows: intake 800m3/ h, fluidisation
Temperature is 45 DEG C, and atomization gas pressure is 0.4Mpa；Mist flow is 0.6ml/min.It is formed and is wrapped in third microparticle surfaces after drying
Clothing layer, it is 800um~900um tobacco extract particle that sieving, which obtains partial size,.
Core material, first base material layer, the second substrate layer, third substrate layer account for the mass fraction phase of the tobacco extract particle
Deng.
(3) preparation of the champignon cigarette containing full constituent tobacco extract
S31. 30g wood-fibred is taken to be discongested, be beaten, adjust concentration after obtain 8% vegetable-fibre slurry；
S32. by the vegetable-fibre slurry of S31 and 23g tobacco extract particle, 25g bamboo charcoal powder, 7g methylcellulose into
After row is mixed, manufactures paper with pulp, be dehydrated, punch forming, low temperature drying remove water, obtain champignon cigarette substrate；
S33. upper 12g tobacco extract is sprayed on the champignon cigarette substrate of above-mentioned S32, obtains mentioning containing full constituent tobacco
Take the champignon cigarette of object.
Embodiment 2~3 and comparative example 1~3
The preparation step of the tobacco extract of the embodiment of the present invention 2~3 and comparative example 1~3 and tobacco extract particle with
Embodiment 1 is similar, the difference is that as shown in the table:
| Technological parameter | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 |
| S11 nonpolar solvent, additional amount, g | Hexane, 1300 | Ethyl acetate, 1500 | Acetone, 1200 | Hexane, 1600 | Ethyl acetate, 1500 |
| S12 polar solvent, additional amount, times | Water, 6 | Ethyl alcohol, 8 | Ethyl alcohol, 5 | Water, 9 | Ethyl alcohol, 8 |
| S11/S12 ultrasonic temperature, DEG C | 20±2 | 25±2 | 20±2 | 35±2 | 25±2 |
| S11/S12 ultrasonic power, W | 250 | 350 | 300 | 250 | 300 |
| S21 excipient | Dextrin | Microcrystalline cellulose | Dextrin | Microcrystalline cellulose | Microcrystalline cellulose |
| S22 squeezes out revolving speed, r/min | 80 | 150 | 70 | 160 | 150 |
| The round as a ball revolving speed of S22, r/min | 250 | 350 | 240 | 360 | 350 |
| S23/ S24/ S25 stream temperature, DEG C | 40 | 45 | 35 | 50 | 45 |
| S23/ S24/ S25 mist flow ml/min | 0.6 | 0.9 | 0.5 | 1.0 | 0.9 |
| S23/ S24/ S25 atomization gas pressure, Mpa | 0.2 | 0.4 | 0.1 | 05 | 0.4 |
| S26 coating material/pore-foaming agent | Arabic gum/sorbierite | Polyvinyl alcohol/methylcellulose | Arabic gum/sorbierite | Polyvinyl alcohol/nothing | Polyvinyl alcohol/methylcellulose |
| Whether S22~S26 is sieved respectively | It is | It is | It is | It is | It is no |
The preparation process of champignon cigarette containing full constituent tobacco extract is as follows:
| Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 |
| Tobacco extract 3g | Tobacco extract 15g | Tobacco extract 10g | Tobacco extract 3g | Tobacco extract 15g |
| Charcoal powder 50g | Bamboo charcoal powder 10g | Bamboo charcoal powder 25g | Charcoal powder 50g | Bamboo charcoal powder 10g |
| Secondary stock 35g | Bamboo fibre 35g | Wood-fibred 30g | Secondary stock 35g | Bamboo fibre 35g |
| Elm bark powder 5g | Bakelite powder 1g | Methylcellulose 7g | Elm bark powder 5g | Bakelite powder 1g |
| Tobacco extract particle 5g | Tobacco extract particle 30g | Tobacco extract particle 17g | Tobacco extract particle 5g | Tobacco extract particle 30g |
Comparative example 4
(1) preparation of tobacco extract
S11. taking absolute dry mass is the flue-cured tobacco of 100g, and 1400g water is added after 60 DEG C carry out immersion 25min, is cooled to 20
DEG C or so, the ethanol solution of 700g is added, the ultrasonic extraction 90min under the conditions of 25 ± 2 DEG C, the power of ultrasonic wave is 300W,
Then vacuum suction filtering, obtains filter residue a and filtrate a；
S12., it is 15% that filtrate a is concentrated in vacuo to solid content under the conditions of 25 DEG C, obtains tobacco extract.
(2) it the preparation of tobacco extract particle: is carried out referring to the step of embodiment 1 with method, it is micro- that tobacco extract is made
Grain.
(3) it the preparation of the champignon cigarette containing full constituent tobacco extract: is carried out referring to the step of embodiment 1 with method, system
Obtain the champignon cigarette containing full constituent tobacco extract.
Comparative example 5
(1) it the preparation of tobacco extract: is carried out referring to the step of embodiment 1 with method, tobacco extract is made.
(2) preparation of tobacco extract particle
S21. the tobacco extract prepared in (1) is uniformly mixed with starch, the mixture that concentration is 8% is made；
S22. mixture made from S21 is granulated in fluidized bed pelletizer.The technological condition of fluidized bed pelletizer
Are as follows: intake 500m3/ h, stream temperature are 40 DEG C, and atomization gas pressure is 0.2Mpa；The concentration of first-class dynamic mixtures is
8%, mist flow 0.9ml/min.After drying, it is 700 um~800um particle that sieving, which obtains partial size, and tobacco mentions in particle
The content for taking object is average value that 35%(is each layer tobacco extract content in tobacco extract particle described in embodiment 1).
S23. coating solution is prepared；Coating solution is made of microcrystalline cellulose, polyvinyl alcohol and suitable water, microcrystalline cellulose
Mass ratio with polyvinyl alcohol is 9:1, and the concentration of coating solution is 9%.
Particle made from S22 is put into fluidized bed pelletizer, each parameter of fluidized bed pelletizer is adjusted, is in particle
Fluidized state sprays into coating solution.The technological condition of fluidized bed pelletizer are as follows: intake 800m3/ h, stream temperature 45
DEG C, atomization gas pressure is 0.4Mpa；Mist flow is 0.6ml/min.Coatings, sieving are formed in third microparticle surfaces after drying
Obtaining partial size is 800um~900um tobacco extract particle.
(3) it the preparation of the champignon cigarette containing full constituent tobacco extract: is carried out referring to the step of embodiment 1 with method, system
Obtain the champignon cigarette containing full constituent tobacco extract.
Comparative example 6
(1) it the preparation of tobacco extract: is carried out referring to the step of embodiment 1 with method, tobacco extract is made.
(2) it the preparation of tobacco extract particle: is carried out referring to the step of embodiment 1 with method, it is micro- that tobacco extract is made
Grain.
(3) preparation of the champignon cigarette containing full constituent tobacco extract
S31. 30g wood-fibred is taken to be discongested, be beaten, adjust concentration after obtain 8% vegetable-fibre slurry；
S32. it after the vegetable-fibre slurry of S31,25g bamboo charcoal powder, 7g methylcellulose being mixed, manufactures paper with pulp, take off
Water, punch forming, low temperature drying remove water, obtain champignon cigarette substrate；
S33. upper 12g tobacco extract is sprayed on the champignon cigarette substrate of above-mentioned S32, obtains mentioning containing full constituent tobacco
Take the champignon cigarette of object.
The evaluation of effect
15 criticism persons for having smoking habit usually are chosen, are lighted in a room containing full constituent tobacco extract
Champignon cigarette is judged, and according to the mouthfeel of the champignon cigarette containing full constituent tobacco extract, is held the indexs such as fragrance, quality and is beaten
Point, and acquire average value record in the following table, evaluation criterion:
Fragrance: fragrance dense (10~8 points), fragrance moderate (6~4 points), fragrance are light (2~1 points)
Strength: strength moderate (10~8 points), strength big (2~1 points), strength are small (2~1 points)
It holds fragrance (the release persistence for referring to tobacco extract in the champignon cigarette containing full constituent tobacco extract): release
Time 8~10min(10~8 point), less than 6 minutes release time (6~4 points), 4 minutes release time (2~1 points)
Taste uniformity (i.e. the release uniformity of tobacco extract particle is evaluated in the fluctuation of taste, situation of change): taste
Uniformly (10~8 points), taste more uniform (6~4 points), taste fluctuate big (2~1 points)
Irritation: small (10~8 points), in (6~4 points), big (2~1 points)
Miscellaneous taste: micro- to have (10~8 points), heavier (6~4 points), serious (2~1 points)
Evaluation result is as follows:
| Sample/index | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 | Comparative example 5 | Comparative example 6 |
| Fragrance | 10 | 9 | 10 | 4 | 2 | 2 | 1 | 1 | 5 |
| Strength | 10 | 10 | 8 | 4 | 4 | 1 | 1 | 1 | 1 |
| Hold fragrance | 10 | 8 | 9 | 6 | 2 | 2 | 4 | 1 | 4 |
| Taste uniformity | 10 | 9 | 10 | 4 | 5 | 1 | 5 | 2 | 1 |
| Irritation | 10 | 10 | 9 | 5 | 5 | 2 | 1 | 1 | 4 |
| Miscellaneous taste | 10 | 9 | 10 | 4 | 3 | 1 | 1 | 1 | 1 |
| It is total | 60 | 51 | 56 | 27 | 21 | 9 | 13 | 7 | 16 |
According to above-mentioned assay it is found that the champignon containing full constituent tobacco extract prepared by the embodiment of the present invention 1~3
Tobacco extract particle is with burst size and rate of release are uniform, slow release effect is lasting, fragrance is lasting and no impurity taste in cigarette.Comparison
Tobacco extract particle is since manufacturing condition cannot in champignon cigarette containing full constituent tobacco extract prepared by example 1 and 2
Collaboration, keeps its tobacco extract particle many index poor, and the coating of comparative example 2 is useless to use pore-foaming agent, and release is uniform
Worse, the tobacco extract in the release and particle of the tobacco extract in the champignon cigarette containing full constituent tobacco extract of property
Release can not gently excessively, and irritation is larger；The extraction temperature of comparative example 2 to have lost in extraction process more higher than 30 DEG C
Volatile tobacco effective component so that its fragrance level is poor.Due to not existing in particle preparation process in comparative example 3
Links screen particle, so that the content of tobacco extract is irregular in final tobacco extract particle, it is micro-
Also difference is larger for the density of grain, so that strength, taste uniformity and miscellaneous taste and quality etc. are poor.Comparative example 4 is due to tobacco
Only onestep extraction, the active constituent content in tobacco extract is lower, and impurity is more, so that its fragrance level, strength, miscellaneous taste
It is very poor Deng evaluating.The technique that comparative example 5 is granulated using Direct spraying, the strength of tobacco extract particle is larger, slow release effect,
The evaluation of taste uniformity and quality etc. is all very poor.Comparative example 6 prepare the champignon cigarette containing full constituent tobacco extract by
In no addition tobacco extract particle, so that the strength of the champignon cigarette containing full constituent tobacco extract, taste uniformity etc.
Index is deteriorated.
Claims (7)
1. a kind of champignon cigarette containing full constituent tobacco extract, which is characterized in that including functional components, carbonaceous powder, plant
Fibres, adhesive；The functional components are tobacco extract and tobacco extract particle；
The tobacco extract accounts for the 3%~15% of champignon cigarette quality；Tobacco extract particle accounts for the 5%~30% of champignon cigarette quality；
The tobacco extract particle includes at least two substrate layers with different tobacco extract contents；The substrate layer by
Layer cladding, the surface of substrate layer is coated with coatings, contains excipient in the substrate layer；The tobacco extract particle is by interior
Tobacco extract content is gradually reduced in substrate layer outward；
The tobacco extract is mixture of the tobacco through polar solvent and non-polar solvent extract.
2. the champignon cigarette containing full constituent tobacco extract according to claim 1, which is characterized in that described to contain full constituent
The champignon cigarette of tobacco extract by following mass percent material composition:
Tobacco extract 3%~15%；Tobacco extract particle 5%~30%；Carbonaceous powder 10%~50%；Plant fiber 10%~
35%；Adhesive 1%~10%；
The tobacco extract particle includes at least two substrate layers with different tobacco extract contents；The substrate layer by
Layer cladding, the surface of substrate layer is coated with coatings, contains excipient in the substrate layer；The tobacco extract particle is by interior
Tobacco extract content is gradually reduced in substrate layer outward.
3. the champignon cigarette containing full constituent tobacco extract according to claim 1, which is characterized in that the tobacco extract
Extracting method the following steps are included:
S11. add nonpolar solvent water after 60 DEG C~70 DEG C are impregnated into tobacco, it is cooling, under the conditions of not higher than 30 DEG C
It is filtered after ultrasonic extraction, obtains filter residue a and filtrate a；
S12. it after polar solvent being added into the filter residue a of S11, filters, is filtered after ultrasonic extraction under the conditions of not higher than 30 DEG C
Slag b and filtrate b；
S13. filtrate a and filtrate b is mixed, concentration obtains the tobacco extract.
4. the champignon cigarette containing full constituent tobacco extract according to claim 1, which is characterized in that the tobacco extract
The partial size of particle is 100um~1000um.
5. the champignon cigarette containing full constituent tobacco extract according to claim 1, which is characterized in that the material of the coating
In also contain pore-foaming agent；The pore-foaming agent is sucrose, sorbierite, mannitol, polyethylene glycol, hydroxypropyl methyl cellulose, hydroxyl
One or more of propyl cellulose.
6. the champignon cigarette containing full constituent tobacco extract according to claim 2, which is characterized in that tobacco is exhausted in S11
The mass ratio of dry mass and water is 1:13~15；The mass ratio of the absolute dry mass of filter residue a and ethyl alcohol is 1:6~8 in S12；S11 and
The power of ultrasonic wave is 250W~350W in S12, and the ultrasonic time is 30min~70min, and ultrasonic temperature is 20 DEG C~30 DEG C.
7. a kind of preparation method of the champignon cigarette described in claim 1~6 any one containing full constituent tobacco extract, special
Sign is, comprising the following steps:
S31. tobacco extract, filler, flavoring agent, adhesive are taken by weight percent after mixing, be added water and/or
After ethyl alcohol stirring, soft material is made；
S32. after mixing by soft material made from S31 and tobacco extract particle, it is granulated, is mixed lubricant is added, pressure
Piece is dried to obtain the champignon cigarette containing full constituent tobacco extract.
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| CN107319641A (en) * | 2017-07-21 | 2017-11-07 | 上海烟草集团有限责任公司 | A kind of tobacco fuming liquids for heating the tobacco product that do not burn and its production and use |
| CN111436648A (en) * | 2019-01-16 | 2020-07-24 | 深圳波顿香料有限公司 | Preparation method of pellet for cigarette and application of pellet in cigarette filter |
| CN110537723A (en) * | 2019-07-22 | 2019-12-06 | 中国农业科学院烟草研究所 | Method for preparing incense from tobacco powder |
| CN113455700B (en) * | 2021-07-12 | 2023-08-18 | 河南中烟工业有限责任公司 | Heated cigarette with uniform release of esters |
| CN114209084A (en) * | 2021-12-11 | 2022-03-22 | 梅尔斯特(广东)生物科技有限公司 | Anti-seepage treatment method for surface of plant particles |
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