CN1123266A - Liquid plant-foliage fertilizer and preparation method thereof - Google Patents

Liquid plant-foliage fertilizer and preparation method thereof Download PDF

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Publication number
CN1123266A
CN1123266A CN94117725A CN94117725A CN1123266A CN 1123266 A CN1123266 A CN 1123266A CN 94117725 A CN94117725 A CN 94117725A CN 94117725 A CN94117725 A CN 94117725A CN 1123266 A CN1123266 A CN 1123266A
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weight
amino acid
mother liquor
plant
acid mother
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CN94117725A
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张克旭
毛宗祺
葛树丰
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    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00—Fertilisers characterised by their form
    • C05G5/20—Liquid fertilisers
    • C05G5/23—Solutions

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  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Fertilizers (AREA)

Abstract

The fertilizer consists of (wt%) 80-85% of compound amino acid mother liquor, 3-8% of CuSO4.5H2O, 1-3% of ZnSO4.7H2O, 2-5% of Na2B4O7.10H2O, 2-4% of MnSO4.5H2O, 1-3% of plant-growth regulator and 0.5-1% of foliage penetrating-moistening agent. The preparation method is mainly characterized by adopting such processes of hydrochloric acid hydrolytic decomposition and ammonia liquor neutralization to prepare thin compound amino acid mother liquor from cleaned human hair and/or pig hair and/or waste leather and/or animal blood, then using pressure-reducing process to concentrate it into concentrated compound amino acid mother liquor.

Description

A kind of liquid plant-foliage fertilizer and preparation method thereof
The present invention relates to fertilizer, specifically, the present invention relates to a kind of liquid plant-foliage fertilizer.
CN1061770A discloses a kind of fertilizer used only for cotton leaf surface material, and it contains a large amount of potassium primary phosphates and borax and a spot of mepiquat chloride and acetyl salicylic acid.Some effect of increasing production of this fertilizer and resistance against diseases, its weak point are the wherein contained easy and micro-Cu of a large amount of potassium primary phosphates 2+, Zn 2+, Fe 2+Deng generating water-fast precipitation, be difficult for by plant absorbing, wherein contained a large amount of borax and a spot of acetyl salicylic acid price height rise the cost of this fertilizer significantly.
CN1052654 discloses a kind of plant leaf surface compound manure, contain the amino acid solution that useful animal waste is made in this fertilizer, but being easy to decompose, sodium bisulfite wherein emits the sulfurous gas toxic gas, amino acid solution does not concentrate, aminoacids content in the fertilizer is low, and fertilizer efficiency is had bigger influence.
Therefore, an object of the present invention is to provide a kind of liquid plant-foliage fertilizer that multiple nutritional components can be provided plant-growth with growth regulating effect and resistant effect.
Another object of the present invention provides a kind of method for preparing described liquid plant-foliage fertilizer.
Liquid plant-foliage fertilizer of the present invention comprises;
The compounded amino acid mother liquor of 80-85% (weight), the weight concentration of this compounded amino acid mother liquor are 8-12%;
The CuSO of 3-8% (weight) 45H 2O, the ZnSO of 1-3% (weight) 47H 2O, the Na of 2-5% (weight) 2B 4O 710H 2O, the MnSO of 2-4% (weight) 45H 2O;
The plant of 1-3% (weight) generates conditioning agent, and it is paclobutrazol, choline dichloride, mepiquat chloride or brassinolide that this plant generates conditioning agent;
0.5 the blade face of-1% (weight) infiltration wetting agent, this blade face infiltration wetting agent is Fatty Alcohol(C12-C14 and C12-C18) ethylene oxide condensate (JFC) or polyoxyethylenated alcohol sodium sulfate salt (AES).
The method for preparing aforesaid liquid plant-foliage fertilizer of the present invention comprises the following steps: successively
(1) people who cleans is sent out and/or pig hair and/or waste leather and/or animal blood add and fills in the hydrolysis kettle of hydrochloric acid that concentration is 10N, hydrolysis is 8-10 hours under 105-110 ℃ temperature, filter hydrolyzed solution for the first time with common whizzer, hydrolyzed solution after filtering is put into and still, adding concentration and be 20% ammoniacal liquor neutralizes, the pH value of the hydrolyzed solution that is neutralized is transferred to 4.8, Gelucystine is precipitated out, obtain rare compounded amino acid mother liquor after filtering for the second time with generic centrifuge;
As a kind of selection, or above-mentioned hydrolyzed solution after filtering for the first time put into and still, add concentration and be 20% ammoniacal liquor and neutralize, the pH value of the hydrolyzed solution that is neutralized is transferred to 2-3, do not make the Gelucystine precipitation, thereby obtain containing rare compounded amino acid mother liquor of Gelucystine;
Select as another kind, or in hydrolysis kettle, with the aqueous solution of the useless gelatin of enzymic hydrolysis, hydrolysis temperature is 40-50 ℃ that the time is 4 hours, obtains rare compounded amino acid mother liquor;
(2) rare compounded amino acid mother liquor is put into the decompression still, under the pressure of 85-95 ℃ temperature and 80KPa, be condensed into weight concentration and be 8-12% dense compounded amino acid mother liquor;
(3) dense compounded amino acid mother liquor is put into subsider, be cooled to room temperature, make NH wherein 4Cl precipitation, then with generic centrifuge with NH 4Cl precipitates filtering, obtains pure compounded amino acid mother liquor;
(4) pure compounded amino acid mother liquor is put into stirring tank, be heated to 80 ℃, add CuSO while stirring successively 45H 2O, ZnSO 47H 2O, Na 2B 4O 710H 2O and MnSO 45H 2O is so that their whole dissolvings are cooled to room temperature with this solution then;
(5) adding concentration in being cooled to the solution of room temperature is 10% ammoniacal liquor, and the pH value of solution is transferred to about 6;
(6) in stirring tank, add blade face infiltration wetting agent while stirring, make itself and solution uniform mixing;
(7) in stirring tank, add plant-growth regulator while stirring, itself and solution uniform mixing are dissolved;
(8) adding concentration is 10% ammoniacal liquor, and the pH value of finished product liquid plant-foliage fertilizer is transferred to 6.8.
Not as existing foliar nutrient, or only contain amino acid and trace element, or only contain amino acid and plant-growth regulator, liquid plant-foliage fertilizer of the present invention had both contained aminoacids complex and trace element, contain plant-growth regulator and blade face infiltration wetting agent again, it is a kind of being easy to by the plant biochemistry nutrient substance of the comprehensive type of plant absorbing, plant is had adjust nutrition, regulate special efficacy such as grow, prevent and cure diseases, and can increase substantially the output of farm crop or vegetables.
Adopt liquid plant-foliage fertilizer, low cost of manufacture, the steady quality, safe in utilization of method preparation of the present invention.
Embodiment 1
The compounded amino acid mother liquor of 80% (weight), the CuSO of 4% (weight) 45H 2O, the ZnSO of 3% (weight) 47H 2O, the Na of 5% (weight) 2B 4O 710H 2O, the MnSO of 4% (weight) 45H 2O, the choline dichloride of the JFC of 1% (weight) and 3% (weight).
By 200000 milliliters of above-mentioned formulation cotton foliar nutrients, 8 experimental points in Yanjin County, Henan Province spray 400 mu of cotton fields, every mu sprays 500 milliliters, divide and spray for three times, spray 100 milliliters in the Sheng flower bud phase, spray 200 milliliters at initial bloom stage, spray 200 milliliters at full-bloom stage, water was by 1: 300 dilution proportion foliar nutrient before spraying.The same cotton field that sprays foliar nutrient with nothing compares, spray the every mu of volume increase in the cotton field gined cotton 38.36Kg of foliar nutrient, stimulation ratio is 49.4%, produce to throw than being 29: 1, the ginning outturn that sprays the cotton of foliar nutrient increases by 9.9%, and fineness increases by 2.3%, powerful increase by 5.41%, mature coefficient increases by 7.36%, and the quality of cotton improves a grade.
Embodiment 2
The CuSO of the compounded amino acid mother liquor .8% (weight) of 85% (weight) 45H 2O, the ZnSO of 1% (weight) 47H 2O, the Na of 2% (weight) 2B 4O 710H 2O, the MnSO of 2% (weight) 45H 2O, the mepiquat chloride of the AES of 0.5% (weight) and 1.5% (weight).
By 100000 milliliters of above-mentioned formulation cotton foliar nutrients, 200 mu of cotton fields in Yanjin County, Henan Province spray, every mu sprays 500 milliliters, divide and spray for three times, spray 100 milliliters in the Sheng flower bud phase, spray 200 milliliters at initial bloom stage, spray 200 milliliters at full-bloom stage, water was by 1: 300 dilution proportion foliar nutrient before spraying.Compare with the same cotton field that only sprays paclobutrazol, the stimulation ratio that sprays the cotton field of foliar nutrient is 42.7%, the ginning outturn of cotton increases by 2.94%, the verticillium sickness rate reduces by 93%, angular leaf spot reduces by 99%, and cotton boll blight reduces by 90%, and the cotton field disease of using paclobutrazol is serious, early ageing, cotton plant is withered at the beginning of 10 months.
Embodiment 3
The compounded amino acid mother liquor of 80% (weight), the CuSO of 4% (weight) 45H 2O, the ZnSO of 3% (weight) 47H 2O, the Na of 5% (weight) 2B 4O 710H 2O, the MnSO of 4% (weight) 45H 2O, the JFC of 1% (weight), the paclobutrazol of 1.7% (weight), the FeSO of 1% (weight) 47H 2(the NH of O and 0.3% (weight) 4) 6Mo 7O 24
By 25000 milliliters of above-mentioned formulation peanut foliar nutrients, spray 50 mu of peanut fields in Yanjin County, Henan Province, every mu sprays 500 milliliters, spray at twice, spray 300 milliliters at initial bloom stage, spray 200 milliliters at full-bloom stage, water was by 1: 300 dilution proportion foliar nutrient before spraying.Spray 740 jin of the average every per mu yield peanuts in peanut field of foliar nutrient, do not spray 560 jin of the average every per mu yield peanuts in same peanut field of foliar nutrient, stimulation ratio is 30.7%, check a station to detect through Beijing's food quality supervision, the lipid content of peanut is 47.1 %, the content of heavy metal Pb does not detect, and meets request of national standard.
Embodiment 4
The compounded amino acid mother liquor of 80% (weight), the CuSO of 3% (weight) 45H 2O, the ZnSO of 2% (weight) 47H 2O, the Na of 3% (weight) 2B 4O 710H 2O, the Na of 2 (weight) 2B 4O 710H 2O, the MnSO of 1% (weight) 45H 2O, the AEC of 0.5 (weight), the brassinolide of 1.5% (weight), the FeSO of 1% (weight) 47H 2The MgSO of O and 0.3% (weight) 45H 2O and the K that amounts to into 3% (weight) 2The KCl of O.
By 2500 milliliters of above-mentioned formulation soybean foliar nutrients, spray 50 mu of soybean fields in Ke Nan province Yanjin County, every mu sprays 500 milliliters, sprays at twice, spraying 200 milliliters at initial bloom stage, spray 300 milliliters at full-bloom stage. water was by 1: 300 dilution proportion foliar nutrient before spraying.Spray 480 jin of the average every per mu yield soybean in soybean field of foliar nutrient, thousand seed weight 257 grams, do not spray 300 jin of the average every per mu yield soybean in same soybean field of foliar nutrient, thousand seed weight 169.9 grams, per mu yield soybean yield-increasing rate is 60%, thousand weightening finish 50.86%, checks a station to detect through Beijing's food quality supervision, soy-protein increases by 4.17%, the residual reduction of heavy metal Pb.
As mentioned above, liquid plant-foliage fertilizer of the present invention removes to comprise and has Cu 2+, Zn 2+, Na 2+And Mn 2+Vitriol and borate with crystal water outside, can also comprise the FeSO of 1-3% (weight) according to the production needs of different plants 47H 2(the NH of O and/or 0.1-0.5% (weight) 4) 6Mo 7O 24And/or the MgSO of 2-4% (weight) 45H 2O and/or amount to into the K of 2-8% (weight) 2The KCl of O.
In the total material that liquid plant-foliage fertilizer of the present invention contained, except that the compounded amino acid mother liquor need prepare by the step 1 in the method for above-mentioned this foliar nutrient of preparation and 2, other material all can have been bought from the market easily.
Use liquid plant-foliage fertilizer of the present invention will note following item:
1, can not use with alkaline matter such as alkaline agricultural chemicals;
2, spray other plant-growth regulator no longer in addition;
3, must cooperate liquid manure and other field management.

Claims (10)

1, a kind of liquid plant-foliage fertilizer is characterized in that, it comprises:
The compounded amino acid mother liquor of 80-85% (weight), the weight concentration of this compounded amino acid mother liquor are 8-12%;
The CuSO of 3-8% (weight) 45H 2O, the ZnSO of 1-3% (weight) 47H 2O, the NaB of 2-5% (weight) 4O 710H 2O, the MnSO of 2-4 (weight) 45H 2O;
The plant-growth regulator of 1-3% (weight), it is paclobutrazol, choline dichloride, mepiquat chloride or brassinolide that this plant generates conditioning agent;
0.5 the blade face of-1% (weight) infiltration wetting agent, this plant leaf surface infiltration wetting agent is Fatty Alcohol(C12-C14 and C12-C18) ethylene oxide condensate (JFC) or AES (AES).
2, by the described liquid plant-foliage fertilizer of claim 1, it is characterized in that: the FeSO that also contains 1-3% (weight) 47H 2O.
3, by claim 1 or 2 described liquid plant-foliage fertilizers, it is characterized in that, also contain (the NH of 0.1-0.5% (weight) 4) 6Mo 7O 24
4, by claim 1 or 2 described liquid plant-foliage fertilizers, it is characterized in that, also contain the MgSO of 2-4% (weight) 45H 2O.
5, by the described liquid plant-foliage fertilizer of claim 3, it is characterized in that, also contain the MgSO of 2-4% (weight) 45H 2O.
6, by claim 1 or 2 described liquid plant-foliage fertilizers, it is characterized in that also contain potash fertilizer, said potash fertilizer is amounted to into K 2O, content are 2-8% (weight).
7, by the described liquid plant-foliage fertilizer of claim 3, it is characterized in that also contain potash fertilizer, said potash fertilizer is amounted to into K 2O, content are 2-8% (weight).
8, by the described liquid plant-foliage fertilizer of claim 4, it is characterized in that also contain potash fertilizer, said potash fertilizer is amounted to into K 2O, content are 2-8% (weight).
9, by the described liquid plant-foliage fertilizer of claim 5, it is characterized in that also contain potash fertilizer, said potash fertilizer is amounted to into K 2O, content are 2-8% (weight).
10, a kind of method of making liquid plant-foliage fertilizer as claimed in claim 1 is characterized in that, this method comprises the following steps: successively
(1) people who cleans is sent out and/or pig hair and/or waste leather and/or animal blood add and fills in the hydrolysis kettle of hydrochloric acid that concentration is 10N, hydrolysis is 8-10 hours under 105-110 ℃ temperature, filter hydrolyzed solution for the first time with common whizzer, hydrolyzed solution after filtering is put into and still, adding concentration and be 20% ammoniacal liquor neutralizes, the pH value of the hydrolyzed solution that is neutralized is transferred to 4.8, Gelucystine is precipitated out, obtain rare compounded amino acid mother liquor after filtering for the second time with generic centrifuge;
Or above-mentioned hydrolyzed solution after filtering for the first time put into and still, add concentration and be 20% ammoniacal liquor and neutralize, the pH value of the hydrolyzed solution that is neutralized is transferred to 2-3, do not make the Gelucystine precipitation, thereby obtain containing rare compounded amino acid mother liquor of Gelucystine;
Or in hydrolysis kettle, with the aqueous solution of the useless gelatin of enzymic hydrolysis, hydrolysis temperature is 40-50 ℃, and the time is 4 hours, obtains rare compounded amino acid mother liquor;
(2) rare compounded amino acid mother liquor is put into the decompression still, under the pressure of 85-95 ℃ temperature and 80KPa, be condensed into weight concentration and be 8-12% dense compounded amino acid mother liquor;
(3) dense compounded amino acid mother liquor is put into subsider, be cooled to room temperature, make NH wherein 4Cl precipitation, then with generic centrifuge with NH 4Cl precipitates filtering, obtains pure compounded amino acid mother liquor;
(4) pure compounded amino acid mother liquor is put into stirring tank, be heated to 80 ℃, add CuSO while stirring successively 45H 2O, ZnSO 47H 2O, Na 2B 4O 710H 2O and MnSO 45H 2O is so that their whole dissolvings are cooled to room temperature with this solution then;
(5) adding concentration in being cooled to the solution of room temperature is 10% ammoniacal liquor, and the pH value of solution is transferred to about 6;
(6) in stirring tank, add blade face infiltration wetting agent while stirring, make itself and solution uniform mixing;
(7) in stirring tank, add plant-growth regulator while stirring, itself and solution uniform mixing are dissolved;
(8) adding concentration is 10% ammoniacal liquor, and the pH value of finished product liquid plant-foliage fertilizer is transferred to 6.8.
CN94117725A 1994-11-14 1994-11-14 Liquid plant-foliage fertilizer and preparation method thereof Pending CN1123266A (en)

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Application Number Priority Date Filing Date Title
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Cited By (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0940380A1 (en) * 1998-03-02 1999-09-08 Hidekatsu Kawamato Organic liquid nutrition source for plants and manufacturing method for same
CN100411514C (en) * 2005-07-22 2008-08-20 浙江大学 Preparation in use for prolonging activate period of brassin lactone
CN101274864B (en) * 2008-05-19 2010-11-03 翟丙年 Efficient fruits nutrition physiology hyperchromic fertilizer and preparation thereof
CN101953337A (en) * 2010-09-21 2011-01-26 中国科学院植物研究所 Plant growth regulator composition and application thereof
CN102219610A (en) * 2011-05-19 2011-10-19 湖南省中科农业有限公司 Amino acid compound leaf fertilizer and preparation method thereof
CN101320023B (en) * 2007-06-05 2011-12-07 中华人民共和国北京出入境检验检疫局 Method for measuring residual quantity of cycocel and mepiquat chloride
CN102344318A (en) * 2011-07-06 2012-02-08 山东宝源生物有限公司 Liquid nutrition fertilizer for applying on cherry tomato
CN102432381A (en) * 2011-09-21 2012-05-02 常州润海花木有限公司 Foliar fertilizer for flowers
CN101648835B (en) * 2009-07-17 2012-07-04 郭徐澄 Jujube growth conditioning nutrient solution for preventing and suppressing fruit shrink disease and preparation method thereof
CN101768021B (en) * 2008-12-31 2014-02-05 罗波 Organic material composting promoter and preparation method and application thereof
WO2014108099A1 (en) * 2013-01-14 2014-07-17 佛山市新新叶面肥料有限公司 Organic liquid suitable for being used as raw material for foliar fertilizers
CN104844388A (en) * 2015-05-06 2015-08-19 肥西县农业技术推广中心 Rice heading period foliar fertilizer and preparation method thereof
CN104920027A (en) * 2015-06-09 2015-09-23 张国停 Medicinal castor planting method
CN105010346A (en) * 2015-07-15 2015-11-04 四川国光农化股份有限公司 Plant growth regulating composition and preparation and application thereof
CN105294310A (en) * 2015-11-30 2016-02-03 四川惠丰天然药物发展有限公司 Composite leaf fertilizer comprising houttuynia cordata, and preparation method thereof
CN105523821A (en) * 2014-09-29 2016-04-27 安庆华辉生物科技有限公司 Compound amino acid water-soluble fertilizer for fructus trichosanthis and preparation method thereof
CN105523820A (en) * 2014-09-29 2016-04-27 安庆华辉生物科技有限公司 Foliage amino acid water-soluble fertilizer for muskmelon and preparation method thereof
CN106032337A (en) * 2015-03-17 2016-10-19 安徽云峰农业发展有限公司 Water-soluble fertilizer containing amino acids and trace elements such as manganese and copper
CN106588457A (en) * 2016-12-04 2017-04-26 钦州市星火计划办公室 Liquid foliar fertilizer and preparation method thereof

Cited By (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0940380A1 (en) * 1998-03-02 1999-09-08 Hidekatsu Kawamato Organic liquid nutrition source for plants and manufacturing method for same
CN100411514C (en) * 2005-07-22 2008-08-20 浙江大学 Preparation in use for prolonging activate period of brassin lactone
CN101320023B (en) * 2007-06-05 2011-12-07 中华人民共和国北京出入境检验检疫局 Method for measuring residual quantity of cycocel and mepiquat chloride
CN101274864B (en) * 2008-05-19 2010-11-03 翟丙年 Efficient fruits nutrition physiology hyperchromic fertilizer and preparation thereof
CN101768021B (en) * 2008-12-31 2014-02-05 罗波 Organic material composting promoter and preparation method and application thereof
CN101648835B (en) * 2009-07-17 2012-07-04 郭徐澄 Jujube growth conditioning nutrient solution for preventing and suppressing fruit shrink disease and preparation method thereof
CN101953337B (en) * 2010-09-21 2013-06-26 中国科学院植物研究所 Plant growth regulator composition and application thereof
CN101953337A (en) * 2010-09-21 2011-01-26 中国科学院植物研究所 Plant growth regulator composition and application thereof
CN102219610A (en) * 2011-05-19 2011-10-19 湖南省中科农业有限公司 Amino acid compound leaf fertilizer and preparation method thereof
CN102344318A (en) * 2011-07-06 2012-02-08 山东宝源生物有限公司 Liquid nutrition fertilizer for applying on cherry tomato
CN102432381A (en) * 2011-09-21 2012-05-02 常州润海花木有限公司 Foliar fertilizer for flowers
WO2014108099A1 (en) * 2013-01-14 2014-07-17 佛山市新新叶面肥料有限公司 Organic liquid suitable for being used as raw material for foliar fertilizers
CN105523821A (en) * 2014-09-29 2016-04-27 安庆华辉生物科技有限公司 Compound amino acid water-soluble fertilizer for fructus trichosanthis and preparation method thereof
CN105523820A (en) * 2014-09-29 2016-04-27 安庆华辉生物科技有限公司 Foliage amino acid water-soluble fertilizer for muskmelon and preparation method thereof
CN106032337A (en) * 2015-03-17 2016-10-19 安徽云峰农业发展有限公司 Water-soluble fertilizer containing amino acids and trace elements such as manganese and copper
CN104844388A (en) * 2015-05-06 2015-08-19 肥西县农业技术推广中心 Rice heading period foliar fertilizer and preparation method thereof
CN104920027A (en) * 2015-06-09 2015-09-23 张国停 Medicinal castor planting method
CN105010346A (en) * 2015-07-15 2015-11-04 四川国光农化股份有限公司 Plant growth regulating composition and preparation and application thereof
CN105294310A (en) * 2015-11-30 2016-02-03 四川惠丰天然药物发展有限公司 Composite leaf fertilizer comprising houttuynia cordata, and preparation method thereof
CN106588457A (en) * 2016-12-04 2017-04-26 钦州市星火计划办公室 Liquid foliar fertilizer and preparation method thereof

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