CN112315854A - Rose compound essential oil - Google Patents

Rose compound essential oil Download PDF

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Publication number
CN112315854A
CN112315854A CN202011443734.9A CN202011443734A CN112315854A CN 112315854 A CN112315854 A CN 112315854A CN 202011443734 A CN202011443734 A CN 202011443734A CN 112315854 A CN112315854 A CN 112315854A
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parts
oil
rose
essential oil
essential
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CN202011443734.9A
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陈祎
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Individual
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Priority to CN202011443734.9A priority Critical patent/CN112315854A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • A61K8/988Honey; Royal jelly, Propolis
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/025Recovery by solvent extraction
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Chemical & Material Sciences (AREA)
  • Emergency Medicine (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Zoology (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Dermatology (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses rose compound essential oil which comprises the following raw materials in parts by weight: 60-80 parts of rose essential oil, 5-8 parts of bergamot essential oil, 3-6 parts of avocado oil, 3-5 parts of grape seed oil, 2-4 parts of evening primrose oil, 6-8 parts of coconut oil, 1-3 parts of honey, 4-8 parts of perilla oil, 4-8 parts of parsley seed oil, 1-3 parts of rosemary essential oil, 6-9 parts of lemon oil, 2-6 parts of calendula oil, 3-6 parts of walnut oil, 6-8 parts of clove oil, 1-3 parts of shaddock oil and 1-3 parts of asafetida oil. The essential oil has scientific formula, environmental protection, safety, comprehensive functions and high efficiency, and is beneficial to moistening and maintaining skin.

Description

Rose compound essential oil
Technical Field
The invention relates to the technical field of cosmetics, in particular to rose compound essential oil.
Background
The rose essential oil is a high-grade concentrated essence which is famous and precious in the world, is a fine product in the essential oil, is an important and expensive raw material for manufacturing high-grade famous and precious perfume, is not only used for manufacturing cosmetics such as beauty, skin care, hair care and the like, but also widely used in the fields of medicine, food and the like, and is known as 'after essential oil'. The rose essential oil can adjust female endocrine, nourish uterus, relieve dysmenorrhea, and improve sexual indifference and climacteric discomfort; especially has good effects of beautifying and protecting skin, can nourish the interior and the exterior, lighten spots, promote the decomposition of melanin, improve the dryness of the skin and restore the elasticity of the skin, so that women have white and elastic healthy skin.
The rose essential oil is extracted from natural rose, and the extraction method mainly comprises a squeezing method, a steam distillation method, a solvent extraction method and the like. The common rose essential oil in the market at present has single component, and is doped with a large amount of substances harmful to human bodies in order to reduce the cost, so that the skin is easily damaged.
Therefore, how to provide the rose compound essential oil with scientific formulation, environmental protection, safety, comprehensive functions and high efficiency becomes a technical problem to be urgently solved by technical personnel in the field.
Disclosure of Invention
In order to solve the technical problems, the invention provides the rose compound essential oil which is scientific in formula, environment-friendly, safe, comprehensive in function, efficient and beneficial to skin moistening and maintenance.
The invention discloses rose compound essential oil which comprises the following raw materials in parts by weight: 60-80 parts of rose essential oil, 5-8 parts of bergamot essential oil, 3-6 parts of avocado oil, 3-5 parts of grape seed oil, 2-4 parts of evening primrose oil, 6-8 parts of coconut oil, 1-3 parts of honey, 4-8 parts of perilla oil, 4-8 parts of parsley seed oil, 1-3 parts of rosemary essential oil, 6-9 parts of lemon oil, 2-6 parts of calendula oil, 3-6 parts of walnut oil, 6-8 parts of clove oil, 1-3 parts of shaddock oil and 1-3 parts of asafetida oil.
Preferably, the feed comprises the following raw materials in parts by weight: 70-80 parts of rose essential oil, 5-6 parts of bergamot essential oil, 3-5 parts of avocado oil, 3-5 parts of grape seed oil, 2-3 parts of evening primrose oil, 6-8 parts of coconut oil, 1-3 parts of honey, 6-8 parts of perilla oil, 4-6 parts of parsley seed oil, 1-3 parts of rosemary essential oil, 6-8 parts of lemon oil, 2-4 parts of calendula oil, 3-5 parts of walnut oil, 6-8 parts of clove oil, 1-3 parts of shaddock oil and 1-3 parts of asafetida oil.
Preferably, the feed comprises the following raw materials in parts by weight: 75 parts of rose essential oil, 5 parts of bergamot essential oil, 4 parts of avocado oil, 4 parts of grape seed oil, 3 parts of evening primrose oil, 6 parts of coconut oil, 2 parts of honey, 7 parts of perilla oil, 5 parts of parsley seed oil, 2 parts of rosemary essential oil, 7 parts of lemon oil, 3 parts of calendula officinalis oil, 4 parts of walnut oil, 6 parts of clove oil, 2 parts of grapefruit oil and 3 parts of asafetida oil.
Preferably, the composition also comprises one or more of Peru resin, benzoin ester, vetiver oil, vanillin, acetyl eugenol, benzyl benzoate and linalyl phenylacetate.
Preferably, the extraction method of the rose essential oil comprises the following steps:
cleaning: picking fresh rose petals, removing impurities, and cleaning;
drying: drying the washed rose petals at 80-95 ℃;
and (3) extraction: mixing the dried rose petals with an extracting agent, performing microwave extraction at 25-40 ℃ for 40-55min to obtain a microwave extraction mixture, centrifuging the microwave extraction mixture, and collecting an extraction liquid;
and (3) purification: and purifying the extract to obtain the rose essential oil.
Preferably, the extractant is a mixed solution of ethanol and ethyl acetate.
Preferably, the volume ratio of the rose petals to the extracting agent is 1: 2.
preferably, the purification process comprises the following steps:
and (3) distillation and purification: vacuum distilling the extractive solution at 28-35 deg.C and 3000-4500Pa for 8-15s to obtain oil-water mixture;
oil-water separation: and putting the oil-water mixture into an oil-water separator, and separating and removing the water phase to obtain the rose essential oil.
Preferably, the temperature of the oil-water separation process is 23-27 ℃.
Detailed Description
In order to make those skilled in the art better understand the technical solutions in the present application, the technical solutions in the embodiments of the present application will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present application, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present application.
Example 1
The rose compound essential oil comprises the following raw materials in parts by weight: 80 parts of rose essential oil, 5 parts of bergamot essential oil, 3 parts of avocado oil, 3 parts of grape seed oil, 2 parts of evening primrose oil, 6 parts of coconut oil, 1 part of honey, 4 parts of perilla oil, 4 parts of parsley seed oil, 1 part of rosemary essential oil, 6 parts of lemon oil, 2 parts of calendula officinalis oil, 3 parts of walnut oil, 6 parts of clove oil, 1 part of grapefruit oil and 1 part of asafetida oil.
The extraction method of the rose essential oil comprises the following steps:
cleaning: picking fresh rose petals, removing impurities, and cleaning;
drying: drying the washed rose petals at 80 ℃;
and (3) extraction: mixing the dried rose petals with an extracting agent (a mixed solution of ethanol and ethyl acetate), performing microwave extraction at 25 ℃ for 55min to obtain a microwave extraction mixture, centrifuging the microwave extraction mixture, and collecting an extract;
and (3) purification: and (3) distillation and purification: vacuum distilling the extractive solution at 28 deg.C and 4500Pa for 15s to obtain oil-water mixture;
oil-water separation: and (3) putting the oil-water mixture into an oil-water separator, and separating and removing the water phase at the temperature of 23 ℃ to obtain the rose essential oil.
Example 2
The rose compound essential oil comprises the following raw materials in parts by weight: 60 parts of rose essential oil, 8 parts of bergamot essential oil, 6 parts of avocado oil, 5 parts of grape seed oil, 4 parts of evening primrose oil, 8 parts of coconut oil, 3 parts of honey, 8 parts of perilla oil, 8 parts of parsley seed oil, 3 parts of rosemary essential oil, 9 parts of lemon oil, 6 parts of calendula oil, 6 parts of walnut oil, 8 parts of clove oil, 3 parts of grapefruit oil and 3 parts of asafetida oil.
The extraction method of the rose essential oil comprises the following steps:
cleaning: picking fresh rose petals, removing impurities, and cleaning;
drying: drying the washed rose petals at 95 ℃;
and (3) extraction: mixing the dried rose petals with an extracting agent (a mixed solution of ethanol and ethyl acetate), performing microwave extraction at 40 ℃ for 40min to obtain a microwave extraction mixture, centrifuging the microwave extraction mixture, and collecting an extract;
and (3) purification: and (3) distillation and purification: vacuum distilling the extractive solution at 35 deg.C and 3000Pa for 8s to obtain oil-water mixture;
oil-water separation: and (3) putting the oil-water mixture into an oil-water separator, and separating and removing the water phase at the temperature of 23-27 ℃ to obtain the rose essential oil.
Example 3
The rose compound essential oil comprises the following raw materials in parts by weight: the formula comprises, by weight, 65 parts of rose essential oil, 5.5 parts of bergamot essential oil, 4 parts of avocado oil, 3 parts of grape seed oil, 2 parts of evening primrose oil, 6 parts of coconut oil, 1 part of honey, 8 parts of perilla oil, 4 parts of parsley seed oil, 2 parts of rosemary essential oil, 7 parts of lemon oil, 2 parts of calendula oil, 5 parts of walnut oil, 6 parts of clove oil, 1 part of grapefruit oil and 1 part of asafetida oil.
The extraction method of the rose essential oil comprises the following steps:
cleaning: picking fresh rose petals, removing impurities, and cleaning;
drying: drying the washed rose petals at 90 ℃;
and (3) extraction: mixing the dried rose petals with an extracting agent (a mixed solution of ethanol and ethyl acetate), performing microwave extraction at 30 ℃ for 50min to obtain a microwave extraction mixture, centrifuging the microwave extraction mixture, and collecting an extract;
and (3) purification: and (3) distillation and purification: vacuum distilling the extractive solution at 32 deg.C and 3500Pa for 10s to obtain oil-water mixture;
oil-water separation: and (3) putting the oil-water mixture into an oil-water separator, and separating and removing the water phase at the temperature of 25 ℃ to obtain the rose essential oil.
Example 4
The rose compound essential oil comprises the following raw materials in parts by weight: 70 parts of rose essential oil, 6 parts of bergamot essential oil, 5 parts of avocado oil, 5 parts of grape seed oil, 3 parts of evening primrose oil, 8 parts of coconut oil, 3 parts of honey, 8 parts of perilla oil, 6 parts of parsley seed oil, 3 parts of rosemary essential oil, 8 parts of lemon oil, 4 parts of calendula officinalis oil, 5 parts of walnut oil, 8 parts of clove oil, 3 parts of grapefruit oil and 3 parts of asafetida oil.
Example 5
The rose compound essential oil comprises the following raw materials in parts by weight: 75 parts of rose essential oil, 5 parts of bergamot essential oil, 4 parts of avocado oil, 4 parts of grape seed oil, 3 parts of evening primrose oil, 6 parts of coconut oil, 2 parts of honey, 7 parts of perilla oil, 5 parts of parsley seed oil, 2 parts of rosemary essential oil, 7 parts of lemon oil, 3 parts of calendula officinalis oil, 4 parts of walnut oil, 6 parts of clove oil, 2 parts of grapefruit oil and 3 parts of asafetida oil.
Example 6
The rose compound essential oil comprises the following raw materials in parts by weight: 75 parts of rose essential oil, 5 parts of bergamot essential oil, 4 parts of avocado oil, 4 parts of grape seed oil, 3 parts of evening primrose oil, 6 parts of coconut oil, 2 parts of honey, 7 parts of perilla oil, 5 parts of parsley seed oil, 2 parts of rosemary essential oil, 7 parts of lemon oil, 3 parts of calendula officinalis oil, 4 parts of walnut oil, 6 parts of clove oil, 2 parts of grapefruit oil, 3 parts of asafetida oil, 1 part of benzoin ester, 3 parts of vetiver oil, 2 parts of vanillin and 1 part of acetyl eugenol.
The embodiments in the present specification are described in a progressive manner, each embodiment focuses on differences from other embodiments, and the same or similar parts in the embodiments are referred to each other.
The previous description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.

Claims (9)

1. The rose compound essential oil is characterized by comprising the following raw materials in parts by weight: 60-80 parts of rose essential oil, 5-8 parts of bergamot essential oil, 3-6 parts of avocado oil, 3-5 parts of grape seed oil, 2-4 parts of evening primrose oil, 6-8 parts of coconut oil, 1-3 parts of honey, 4-8 parts of perilla oil, 4-8 parts of parsley seed oil, 1-3 parts of rosemary essential oil, 6-9 parts of lemon oil, 2-6 parts of calendula oil, 3-6 parts of walnut oil, 6-8 parts of clove oil, 1-3 parts of shaddock oil and 1-3 parts of asafetida oil.
2. The rose complex essential oil according to claim 1, which is characterized by comprising the following raw materials in parts by weight: 70-80 parts of rose essential oil, 5-6 parts of bergamot essential oil, 3-5 parts of avocado oil, 3-5 parts of grape seed oil, 2-3 parts of evening primrose oil, 6-8 parts of coconut oil, 1-3 parts of honey, 6-8 parts of perilla oil, 4-6 parts of parsley seed oil, 1-3 parts of rosemary essential oil, 6-8 parts of lemon oil, 2-4 parts of calendula oil, 3-5 parts of walnut oil, 6-8 parts of clove oil, 1-3 parts of shaddock oil and 1-3 parts of asafetida oil.
3. The rose composite essential oil according to claim 2, which is characterized by comprising the following raw materials in parts by weight: 75 parts of rose essential oil, 5 parts of bergamot essential oil, 4 parts of avocado oil, 4 parts of grape seed oil, 3 parts of evening primrose oil, 6 parts of coconut oil, 2 parts of honey, 7 parts of perilla oil, 5 parts of parsley seed oil, 2 parts of rosemary essential oil, 7 parts of lemon oil, 3 parts of calendula officinalis oil, 4 parts of walnut oil, 6 parts of clove oil, 2 parts of grapefruit oil and 3 parts of asafetida oil.
4. The rose complex essential oil of claim 1, further comprising one or more of peru resin, benzoin ester, vetiver oil, vanillin, acetyl eugenol, benzyl benzoate and linalyl phenylacetate.
5. The rose essential oil composition according to any one of claims 1 to 4, wherein the extraction method of the rose essential oil comprises the following steps:
cleaning: picking fresh rose petals, removing impurities, and cleaning;
drying: drying the washed rose petals at 80-95 ℃;
and (3) extraction: mixing the dried rose petals with an extracting agent, performing microwave extraction at 25-40 ℃ for 40-55min to obtain a microwave extraction mixture, centrifuging the microwave extraction mixture, and collecting an extraction liquid;
and (3) purification: and purifying the extract to obtain the rose essential oil.
6. The rose complex essential oil of claim 5, wherein the extractant is a mixed solution of ethanol and ethyl acetate.
7. The rose complex essential oil of claim 5, wherein the volume ratio of the rose petals to the extractant is 1: 2.
8. the rose complex essential oil according to claim 5, wherein the purification process comprises the following steps:
and (3) distillation and purification: vacuum distilling the extractive solution at 28-35 deg.C and 3000-4500Pa for 8-15s to obtain oil-water mixture;
oil-water separation: and putting the oil-water mixture into an oil-water separator, and separating and removing the water phase to obtain the rose essential oil.
9. The rose complex essential oil according to claim 8, wherein the temperature of the oil-water separation process is 23-27 ℃.
CN202011443734.9A 2020-12-11 2020-12-11 Rose compound essential oil Pending CN112315854A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202011443734.9A CN112315854A (en) 2020-12-11 2020-12-11 Rose compound essential oil

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202011443734.9A CN112315854A (en) 2020-12-11 2020-12-11 Rose compound essential oil

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CN112315854A true CN112315854A (en) 2021-02-05

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109330971A (en) * 2018-12-04 2019-02-15 贵州鼎立生物科技香料有限公司 A kind of compound Rosa Damascana
CN109576054A (en) * 2017-09-28 2019-04-05 王少平 A kind of extracting method of Rosa Damascana
CN111821224A (en) * 2020-09-08 2020-10-27 谭燕妮 Essential oil formula

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109576054A (en) * 2017-09-28 2019-04-05 王少平 A kind of extracting method of Rosa Damascana
CN109330971A (en) * 2018-12-04 2019-02-15 贵州鼎立生物科技香料有限公司 A kind of compound Rosa Damascana
CN111821224A (en) * 2020-09-08 2020-10-27 谭燕妮 Essential oil formula

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Application publication date: 20210205