CN112281514A - Method for dyeing chemical fiber textile fabric by using complex enzyme - Google Patents
Method for dyeing chemical fiber textile fabric by using complex enzyme Download PDFInfo
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- CN112281514A CN112281514A CN202011020532.3A CN202011020532A CN112281514A CN 112281514 A CN112281514 A CN 112281514A CN 202011020532 A CN202011020532 A CN 202011020532A CN 112281514 A CN112281514 A CN 112281514A
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- dyeing
- chemical fiber
- complex enzyme
- deionized water
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- 238000004043 dyeing Methods 0.000 title claims abstract description 76
- 239000004744 fabric Substances 0.000 title claims abstract description 48
- 239000004753 textile Substances 0.000 title claims abstract description 30
- 239000000126 substance Substances 0.000 title claims abstract description 27
- 239000000835 fiber Substances 0.000 title claims abstract description 26
- 238000000034 method Methods 0.000 title claims abstract description 26
- 102000004190 Enzymes Human genes 0.000 title claims abstract description 13
- 108090000790 Enzymes Proteins 0.000 title claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 42
- 239000007788 liquid Substances 0.000 claims abstract description 23
- 238000005406 washing Methods 0.000 claims abstract description 14
- 229940088598 enzyme Drugs 0.000 claims abstract description 12
- 239000004382 Amylase Substances 0.000 claims abstract description 9
- 102000013142 Amylases Human genes 0.000 claims abstract description 9
- 108010065511 Amylases Proteins 0.000 claims abstract description 9
- 108010059892 Cellulase Proteins 0.000 claims abstract description 9
- 102000004882 Lipase Human genes 0.000 claims abstract description 9
- 108090001060 Lipase Proteins 0.000 claims abstract description 9
- 239000004367 Lipase Substances 0.000 claims abstract description 9
- 235000019418 amylase Nutrition 0.000 claims abstract description 9
- 229940106157 cellulase Drugs 0.000 claims abstract description 9
- 238000001035 drying Methods 0.000 claims abstract description 9
- 235000019421 lipase Nutrition 0.000 claims abstract description 9
- VFLDPWHFBUODDF-FCXRPNKRSA-N curcumin Chemical compound C1=C(O)C(OC)=CC(\C=C\C(=O)CC(=O)\C=C\C=2C=C(OC)C(O)=CC=2)=C1 VFLDPWHFBUODDF-FCXRPNKRSA-N 0.000 claims description 24
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 18
- 229940109262 curcumin Drugs 0.000 claims description 12
- 235000012754 curcumin Nutrition 0.000 claims description 12
- 239000004148 curcumin Substances 0.000 claims description 12
- VFLDPWHFBUODDF-UHFFFAOYSA-N diferuloylmethane Natural products C1=C(O)C(OC)=CC(C=CC(=O)CC(=O)C=CC=2C=C(OC)C(O)=CC=2)=C1 VFLDPWHFBUODDF-UHFFFAOYSA-N 0.000 claims description 12
- 102000019197 Superoxide Dismutase Human genes 0.000 claims description 10
- 108010012715 Superoxide dismutase Proteins 0.000 claims description 10
- KSEBMYQBYZTDHS-HWKANZROSA-M (E)-Ferulic acid Natural products COC1=CC(\C=C\C([O-])=O)=CC=C1O KSEBMYQBYZTDHS-HWKANZROSA-M 0.000 claims description 9
- 229960000583 acetic acid Drugs 0.000 claims description 9
- KSEBMYQBYZTDHS-HWKANZROSA-N ferulic acid Chemical compound COC1=CC(\C=C\C(O)=O)=CC=C1O KSEBMYQBYZTDHS-HWKANZROSA-N 0.000 claims description 9
- 229940114124 ferulic acid Drugs 0.000 claims description 9
- KSEBMYQBYZTDHS-UHFFFAOYSA-N ferulic acid Natural products COC1=CC(C=CC(O)=O)=CC=C1O KSEBMYQBYZTDHS-UHFFFAOYSA-N 0.000 claims description 9
- 235000001785 ferulic acid Nutrition 0.000 claims description 9
- 239000012362 glacial acetic acid Substances 0.000 claims description 9
- 238000009210 therapy by ultrasound Methods 0.000 claims description 9
- QURCVMIEKCOAJU-UHFFFAOYSA-N trans-isoferulic acid Natural products COC1=CC=C(C=CC(O)=O)C=C1O QURCVMIEKCOAJU-UHFFFAOYSA-N 0.000 claims description 9
- 230000000694 effects Effects 0.000 abstract description 6
- 239000003795 chemical substances by application Substances 0.000 abstract description 2
- 239000012535 impurity Substances 0.000 abstract description 2
- 238000004513 sizing Methods 0.000 abstract description 2
- 238000002360 preparation method Methods 0.000 abstract 1
- 239000008367 deionised water Substances 0.000 description 36
- 229910021641 deionized water Inorganic materials 0.000 description 36
- 229920004933 Terylene® Polymers 0.000 description 14
- 239000005020 polyethylene terephthalate Substances 0.000 description 14
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 12
- 238000010438 heat treatment Methods 0.000 description 12
- 229920000728 polyester Polymers 0.000 description 8
- 238000004321 preservation Methods 0.000 description 7
- 239000008399 tap water Substances 0.000 description 5
- 235000020679 tap water Nutrition 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 3
- 239000000975 dye Substances 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000009987 spinning Methods 0.000 description 2
- 229930182559 Natural dye Natural products 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000978 natural dye Substances 0.000 description 1
- 231100000956 nontoxicity Toxicity 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/445—Use of auxiliary substances before, during or after dyeing or printing
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6536—Aromatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/20—Physical treatments affecting dyeing, e.g. ultrasonic or electric
- D06P5/2011—Application of vibrations, pulses or waves for non-thermic purposes
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Coloring (AREA)
Abstract
The invention belongs to the field of chemical dyeing, and particularly relates to a method for dyeing chemical fiber textile fabrics by using complex enzyme. The method comprises the steps of placing the chemical fiber textile to be dyed in pretreatment liquid compounded with an enzyme preparation, placing the textile in dyeing liquid for dyeing, fixing the color of the textile, washing with water and then drying. The invention utilizes the pretreatment liquid composed of cellulase, amylase and lipase to remove impurities such as residual sizing agent, oil stain and the like in the process of chemical fiber textile fabrics, thereby improving the subsequent dyeing effect.
Description
Technical Field
The invention belongs to the field of chemical dyeing, and particularly relates to a method for dyeing chemical fiber textile fabrics by using complex enzyme.
Background
The chemical fiber is prepared by using natural high molecular compound or artificially synthesized high molecular compound as raw material and through the processes of preparing spinning solution, spinning, post-treatment and the like. Has the advantages of wear resistance, easy washing, easy drying, no mildew and rot, no worm damage and the like. Is widely used for manufacturing clothing fabrics, filter cloth, conveyor belts, medical sutures and the like. In order to meet the market requirements, chemical fiber products also need to be dyed and finished, and the added value of the chemical fiber products is improved.
But the existing chemical fiber textile fabric dyeing process is complex and has great environmental pollution; the dyeing condition is high, parameters such as pH value, temperature and the like need to be strictly controlled, the water consumption and energy consumption are high, and the dyeing wastewater is difficult to treat. The common dye has low molecular weight, poor rubbing fastness of a dyeing product, low tinting strength, low dye utilization rate, different degrees of light resistance and heat resistance, poor fiber applicability and the like. Therefore, the discovery of new dyeing methods is clearly of great practical importance.
Disclosure of Invention
In order to solve the defects of the prior art, the method for dyeing the chemical fiber textile by using the complex enzyme is provided, has low dyeing cost, wide raw material source and simple dyeing process, and is suitable for industrial large-scale production.
The purpose of the invention is realized by the following technical scheme:
a method for dyeing textiles by chemical fibers by using a complex enzyme comprises the following steps:
1) placing a chemical fiber textile to be dyed in a pretreatment liquid, wherein the pretreatment liquid comprises the following components in parts by weight: 1-2 parts of cellulase, 2-3 parts of amylase, 3-6 parts of lipase and 90-94 parts of water;
2) placing the textile obtained in the step 1) in a dyeing solution for dyeing, wherein the dyeing solution comprises the following components in parts by weight: 3-5 parts of superoxide dismutase, 8-10 parts of curcumin, 1-2 parts of ferulic acid, 5-7 parts of glacial acetic acid and 76-83 parts of water;
3) fixing the color of the textile fabric obtained in the step 2), and drying after washing.
Preferably, the chemical fiber textile to be dyed in the step 1) is placed in the pretreatment liquid, heated to 50-60 ℃, and kept warm for 10-20 min.
Preferably, the dyeing temperature in the step 2) is 80-100 ℃, and the dyeing time is 30-40 min.
Preferably, the dyeing process in step 2) further comprises an ultrasonic treatment step.
Preferably, the ultrasonic treatment is carried out for 10-20 min under the conditions that the ultrasonic power is 100-200W and the frequency is 200-300 kHz.
Preferably, the color fixation is high-temperature color fixation, the color fixation temperature is 120-130 ℃, and the color fixation time is 10-20 s.
The invention utilizes the pretreatment liquid composed of cellulase, amylase and lipase to remove impurities such as residual sizing agent, oil stain and the like in the process of chemical fiber textile fabrics, thereby improving the subsequent dyeing effect.
Curcumin in the dyeing liquid is a natural dye, and the dyeing effect of green and environmental protection can be realized by using the curcumin. In addition, curcumin can improve the activity of superoxide dismutase, ensure the dyeing effect and simultaneously increase the oxidation resistance of chemical fiber textiles.
The ultrasonic treatment can effectively promote dye molecules to enter the textile, and the dyeing performance and the dyeing effect of the textile are improved.
The method has the advantages of uniform dyeing, high color fastness, greenness, no toxicity, increased chemical fiber oxidation resistance, good light stability and durability, effectively prolonged service life and improved service performance.
Detailed Description
The present invention will be described in further detail with reference to specific examples, but the embodiments of the present invention are not limited to the scope of the examples. These examples are intended to illustrate the invention only and are not intended to limit the scope of the invention. In addition, various modifications may occur to those skilled in the art upon reading the present disclosure, and such equivalent variations are within the scope of the present invention as defined in the appended claims.
Example 1
(1) 1 part of cellulase, 2 parts of amylase, 3 parts of lipase and 94 parts of deionized water are taken according to the parts by weight and uniformly mixed to prepare a pretreatment liquid. Placing the terylene cloth to be dyed in a pretreatment solution, and controlling the bath ratio to be 1: 10, namely the weight ratio of the polyester fabric to be dyed to the deionized water in the pretreatment liquid is 1: 10, heating to 50 ℃, and preserving the heat for 10 min. Taking out the terylene cloth, and washing the terylene cloth once by using deionized water.
(2) Taking 3 parts of superoxide dismutase, 8 parts of curcumin, 1 part of ferulic acid, 5 parts of glacial acetic acid and 83 parts of deionized water according to parts by weight, uniformly mixing to prepare a dyeing solution, adjusting the pH value of the dyeing solution to 4, placing the polyester fabric washed by the deionized water into the dyeing solution after the pH value is adjusted, and controlling the bath ratio to be 1: 20, namely the weight ratio of the terylene fabric to the deionized water in the dyeing solution is 1: 20, heating to 80 ℃, and preserving the heat for 30 min.
(3) And (4) taking out after heat preservation is finished, carrying out high-temperature color fixing treatment at 120 ℃ for 10s, washing with tap water, and drying at 65 ℃.
Example 2
(1) 1.5 parts of cellulase, 2.5 parts of amylase, 4 parts of lipase and 92 parts of deionized water are uniformly mixed according to the parts by weight to prepare a pretreatment liquid. Placing the terylene cloth to be dyed in a pretreatment solution, and controlling the bath ratio to be 1: 20, namely the weight ratio of the polyester fabric to be dyed to the deionized water in the pretreatment liquid is 1: 20, heating to 55 ℃, and keeping the temperature for 15 min. Taking out the terylene cloth, and washing the terylene cloth once by using deionized water.
(2) Taking 4 parts of superoxide dismutase, 9 parts of curcumin, 1.5 parts of ferulic acid, 6 parts of glacial acetic acid and 79.5 parts of deionized water according to parts by weight, uniformly mixing to prepare a dyeing solution, adjusting the pH value of the dyeing solution to 5, placing polyester fabric washed by the deionized water into the dyeing solution after the pH value is adjusted, and controlling the bath ratio to be 1: 25, namely the weight ratio of the terylene fabric to the deionized water in the dyeing solution is 1: and 25, heating to 90 ℃, and keeping the temperature for 35 min.
(3) And (4) taking out after heat preservation is finished, carrying out high-temperature color fixing treatment at 125 ℃ for 15s, washing with tap water, and drying at 70 ℃.
Example 3
(1) Taking 2 parts of cellulase, 2 parts of amylase, 6 parts of lipase and 90 parts of deionized water according to parts by weight, and uniformly mixing to prepare a pretreatment liquid. Placing the terylene cloth to be dyed in a pretreatment solution, and controlling the bath ratio to be 1: 25, namely the weight ratio of the polyester fabric to be dyed to the deionized water in the pretreatment liquid is 1: and 25, heating to 60 ℃, and keeping the temperature for 20 min. Taking out the terylene cloth, and washing the terylene cloth once by using deionized water.
(2) Taking 5 parts of superoxide dismutase, 10 parts of curcumin, 2 parts of ferulic acid, 7 parts of glacial acetic acid and 76 parts of deionized water according to parts by weight, uniformly mixing to prepare a dyeing solution, adjusting the pH value of the dyeing solution to 6.5, placing the polyester fabric washed by the deionized water into the dyeing solution after the pH value is adjusted, and controlling the bath ratio to be 1: 30, namely the weight ratio of the terylene fabric to the deionized water in the dyeing solution is 1: 30, heating to 100 ℃, and preserving the heat for 40 min.
(3) And (4) taking out after the heat preservation is finished, carrying out high-temperature color fixing treatment at 130 ℃ for 20s, washing with tap water, and drying at 80 ℃.
Example 4
(1) 1 part of cellulase, 3 parts of amylase, 3 parts of lipase and 93 parts of deionized water are taken according to the parts by weight and uniformly mixed to prepare a pretreatment liquid. Placing the acrylic fabric to be dyed in pretreatment liquid, and controlling the bath ratio to be 1: 10, namely the weight ratio of the acrylic fabric to be dyed to the deionized water in the pretreatment liquid is 1: 10, heating to 50 ℃, and preserving the heat for 10 min. And taking out the acrylic fabric, and washing the acrylic fabric once by using deionized water.
(2) Taking 3 parts of superoxide dismutase, 8 parts of curcumin, 1 part of ferulic acid, 5 parts of glacial acetic acid and 83 parts of deionized water according to parts by weight, uniformly mixing to prepare a dyeing solution, adjusting the pH value of the dyeing solution to 4, placing the acrylic fabric cleaned by the deionized water into the dyeing solution after the pH value is adjusted, and controlling the bath ratio to be 1: 20, namely the weight ratio of the deionized water in the acrylic fabric to the dyeing liquor is 1: 20, heating to 80 ℃, preserving heat for 30min, starting to perform ultrasonic treatment by introducing ultrasonic waves at the same time of heat preservation, and performing ultrasonic treatment for 10min under the conditions of ultrasonic power of 100W and frequency of 200 kHz.
(3) And (4) taking out after heat preservation is finished, carrying out high-temperature color fixing treatment at 120 ℃ for 10s, washing with tap water, and drying at 65 ℃.
Example 5
(1) Taking 2 parts of cellulase, 2 parts of amylase, 6 parts of lipase and 90 parts of deionized water according to parts by weight, and uniformly mixing to prepare a pretreatment liquid. Arranging the acrylic fabric to be dyed in pretreatment liquid, controlling the bath ratio to be 1: 25, namely the weight ratio of the acrylic fabric to be dyed to the deionized water in the pretreatment liquid is 1: and 25, heating to 60 ℃, and keeping the temperature for 20 min. And taking out the acrylic fabric, and washing the acrylic fabric once by using deionized water.
(2) Taking 5 parts of superoxide dismutase, 10 parts of curcumin, 2 parts of ferulic acid, 7 parts of glacial acetic acid and 76 parts of deionized water according to parts by weight, uniformly mixing to prepare a dyeing solution, adjusting the pH value of the dyeing solution to 6.5, placing the acrylic fabric cleaned by the deionized water into the dyeing solution after the pH value is adjusted, and controlling the bath ratio to be 1: 30, namely the weight ratio of the deionized water in the acrylic fabric to the dyeing liquor is 1: 30, heating to 100 ℃, preserving the heat for 40min, introducing ultrasonic waves for ultrasonic treatment at the same time when the heat preservation is started, and performing ultrasonic treatment for 20min under the conditions that the ultrasonic power is 200W and the frequency is 300 kHz.
(3) And (4) taking out after the heat preservation is finished, carrying out high-temperature color fixing treatment at 130 ℃ for 20s, washing with tap water, and drying at 80 ℃.
Comparative example 1
The same dyeing method as in example 1 was used, except that the dyeing solution used in step (2) was different and no superoxide dismutase was contained, and step (2) was specifically as follows:
taking 8 parts of curcumin, 1 part of ferulic acid, 5 parts of glacial acetic acid and 86 parts of deionized water according to parts by weight, uniformly mixing to prepare a dyeing solution, adjusting the pH value of the dyeing solution to 4, placing the polyester fabric washed by the deionized water into the dyeing solution after the pH value is adjusted, and controlling the bath ratio to be 1: 20, namely the weight ratio of the terylene fabric to the deionized water in the dyeing solution is 1: 20, heating to 80 ℃, and preserving the heat for 30 min.
Comparative example 2
The same dyeing method as in example 1 was used, except that the dyeing solution used in step (2) was different and ferulic acid was not contained, and step (2) was specifically as follows:
taking 3 parts of superoxide dismutase, 8 parts of curcumin, 5 parts of glacial acetic acid and 84 parts of deionized water according to parts by weight, uniformly mixing to prepare a dyeing solution, adjusting the pH value of the dyeing solution to 4, placing the polyester fabric washed by the deionized water into the dyeing solution after the pH value is adjusted, and controlling the bath ratio to be 1: 20, namely the weight ratio of the terylene fabric to the deionized water in the dyeing solution is 1: 20, heating to 80 ℃, and preserving the heat for 30 min.
The color fastness to sunlight of the finished products obtained in examples 1-5 and comparative examples 1-2 is determined according to GB/T8427-2019, and is detailed in Table 1.
TABLE 1 detection of color fastness to sunlight
As can be seen from Table 1, the invention has the advantages of sun-proof property, high oxidation resistance, simple process, environmental protection, energy saving, clean dyeing process, higher application value in the textile industry and wide market prospect.
Claims (6)
1. A method for dyeing textiles by chemical fibers by using a complex enzyme is characterized by comprising the following steps:
1) placing a chemical fiber textile to be dyed in a pretreatment liquid, wherein the pretreatment liquid comprises the following components in parts by weight: 1-2 parts of cellulase, 2-3 parts of amylase, 3-6 parts of lipase and 90-94 parts of water;
2) placing the textile obtained in the step 1) in a dyeing solution for dyeing, wherein the dyeing solution comprises the following components in parts by weight: 3-5 parts of superoxide dismutase, 8-10 parts of curcumin, 1-2 parts of ferulic acid, 5-7 parts of glacial acetic acid and 76-83 parts of water;
3) fixing the color of the textile fabric obtained in the step 2), and drying after washing.
2. The method for dyeing the textile fabric by using the chemical fiber with the complex enzyme according to claim 1, wherein the chemical fiber textile fabric to be dyed in the step 1) is placed in the pretreatment liquid, heated to 50-60 ℃, and kept warm for 10-20 min.
3. The method for dyeing the textile fabric by using the chemical fiber by using the complex enzyme according to claim 1, wherein the dyeing temperature in the step 2) is 80-100 ℃, and the dyeing time is 30-40 min.
4. The method for dyeing textiles with chemical fibers by using the complex enzyme according to claim 1, characterized in that the dyeing process of step 2) further comprises an ultrasonic treatment step.
5. The method for dyeing textiles with chemical fibers by using the complex enzyme as claimed in claim 1, wherein the ultrasonic treatment is performed for 10-20 min under the conditions of 100-200W of ultrasonic power and 200-300 kHz of frequency.
6. The method for dyeing textiles by using chemical fibers by using the complex enzyme as claimed in claim 1, wherein the color fixation is high-temperature color fixation, the color fixation temperature is 120-130 ℃, and the color fixation time is 10-20 s.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011020532.3A CN112281514A (en) | 2020-09-25 | 2020-09-25 | Method for dyeing chemical fiber textile fabric by using complex enzyme |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202011020532.3A CN112281514A (en) | 2020-09-25 | 2020-09-25 | Method for dyeing chemical fiber textile fabric by using complex enzyme |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JPH06257074A (en) * | 1993-03-03 | 1994-09-13 | Kondo Toshio | Method for processing textile product by microorganism and apparatus for processing the same |
| CN101476248A (en) * | 2009-01-20 | 2009-07-08 | 西安际华三五一一家纺有限公司 | Method for using natural grape seed dyeing extract in textile dyeing |
| CN103717072A (en) * | 2011-08-04 | 2014-04-09 | 克拉里安特国际有限公司 | Compositions comprising isosorbide monoesters and halogenated antimicrobial active substances |
| CN105671955A (en) * | 2016-01-21 | 2016-06-15 | 苏州印丝特纺织数码科技有限公司 | Fabric antioxidant with seaweed extract and method for preparing fabric antioxidant |
| CN105780542A (en) * | 2016-03-17 | 2016-07-20 | 金华知产婺源信息技术有限公司 | High-efficiency short-process dyeing process |
| CN108642911A (en) * | 2018-03-27 | 2018-10-12 | 武汉纺织大学 | Improve the ecological antioxidant of natural dye dying fibre photooxidation resistant performance |
-
2020
- 2020-09-25 CN CN202011020532.3A patent/CN112281514A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06257074A (en) * | 1993-03-03 | 1994-09-13 | Kondo Toshio | Method for processing textile product by microorganism and apparatus for processing the same |
| CN101476248A (en) * | 2009-01-20 | 2009-07-08 | 西安际华三五一一家纺有限公司 | Method for using natural grape seed dyeing extract in textile dyeing |
| CN103717072A (en) * | 2011-08-04 | 2014-04-09 | 克拉里安特国际有限公司 | Compositions comprising isosorbide monoesters and halogenated antimicrobial active substances |
| CN105671955A (en) * | 2016-01-21 | 2016-06-15 | 苏州印丝特纺织数码科技有限公司 | Fabric antioxidant with seaweed extract and method for preparing fabric antioxidant |
| CN105780542A (en) * | 2016-03-17 | 2016-07-20 | 金华知产婺源信息技术有限公司 | High-efficiency short-process dyeing process |
| CN108642911A (en) * | 2018-03-27 | 2018-10-12 | 武汉纺织大学 | Improve the ecological antioxidant of natural dye dying fibre photooxidation resistant performance |
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