CN107476080A - A kind of ribbon low-temperature dyeing method - Google Patents
A kind of ribbon low-temperature dyeing method Download PDFInfo
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- CN107476080A CN107476080A CN201710918326.6A CN201710918326A CN107476080A CN 107476080 A CN107476080 A CN 107476080A CN 201710918326 A CN201710918326 A CN 201710918326A CN 107476080 A CN107476080 A CN 107476080A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/445—Use of auxiliary substances before, during or after dyeing or printing
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/642—Compounds containing nitrogen
- D06P1/647—Nitrogen-containing carboxylic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65125—Compounds containing ester groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/667—Organo-phosphorus compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
- D06P1/67375—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341 with sulfur-containing anions
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/002—Locally enhancing dye affinity of a textile material by chemical means
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/10—After-treatment with compounds containing metal
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Coloring (AREA)
Abstract
The present invention discloses a kind of ribbon low-temperature dyeing method, including following operating procedure：（1）After ribbon is cleaned, the 160min of immersion treatment 140 in modification liquid is put into；（2）To by step（1）The ribbon of processing carries out two leachings two and rolled, and the temperature of dyeing is 112 118 DEG C, bath raio 1:15 18, pick-up rate is 60 75%；（3）After the ribbon drying after dyeing, it is put into reduction cleaning liquid, after the 40min of immersion treatment 30, takes out, after being cleaned with clear water, dries finished product.Ribbon low-temperature dyeing method provided by the invention, simple to operate, energy consumption is low, and dyeing is stable, safety and environmental protection, can effectively reduce temperature when padding, and Color is notable, uniform color, and color fastness is high, greatly improves the quality of ribbon.
Description
Technical field
The invention belongs to ribbon staining technique field, and in particular to a kind of ribbon low-temperature dyeing method.
Background technology
Colored ribbon is widely used because of its good decorating effect and every excellent in mechanical performance in all trades and professions.
In the preparation process of colored ribbon, dyeing has strong influence to its quality.In the prior art, to the dyeing of ribbon
Method is pad-dry-cure dyeing method, and it is that dyestuff is uniformly rolled into terylene ribbon in ribbon to by way of padding dye liquor, through padding,
Preliminary drying, bake, the dyestuff of fiber surface by fibers adsorption, diffuse into a kind of decoration method of fibrous inside and set.It is but such a
Method, in padding process, the temperature of dye liquor is higher, it is necessary to up to 200 DEG C or so, can be only achieved preferable Color, the energy
Consumption is big, adds the cost of ribbon preparation.
The content of the invention
In order to solve the above-mentioned technical problem, the present invention provides a kind of ribbon low-temperature dyeing method.
The present invention is achieved by the following technical solutions.
A kind of ribbon low-temperature dyeing method, including following operating procedure：
（1）After ribbon is cleaned, be put into immersion treatment 140-160min in modification liquid, wherein modification liquid by following parts by weight group
Divide and be made：1,2- 1,2-diaminocyclohexane tetraacetic acid 18-26 parts, sodium hexafluoro phosphate 10-14 parts, D-ALPHA-Hydroxypropionic acid methyl esters 36-45 parts, the second of methyl three
Acyloxy silane 32-40 parts, ethanol 150-200 parts, water 750-820 parts；
（2）To by step（1）The ribbon of processing carries out two leachings two and rolled, and wherein dyeing liquor is made up of the component of following parts by weight：
Dyestuff 36-42 parts, bleeding agent 12-14 parts, dispersant 10-13 parts, sodium vanadate 2-5 parts, sodium phytate 4-7 parts, sodium polysulfide 2-4
Part, water 640-700 parts, the temperature of dyeing is 112-118 DEG C, bath raio 1:15-18, pick-up rate 60-75%；
（3）After the ribbon drying after dyeing, it is put into reduction cleaning liquid, after immersion treatment 30-40min, takes out, washed with clear water
After net, finished product is dried.
Specifically, above-mentioned steps（1）Middle modification liquid is made of following methods：Will：1,2- 1,2-diaminocyclohexane tetraacetic acids, hexafluoro
Sodium phosphate is added to the water, and stirs 10min using 300r/min rotating speed, D-ALPHA-Hydroxypropionic acid methyl esters, methyl triacetoxysilane add
Into ethanol, 20min is stirred using 300r/min rotating speed, after then two mixed liquors of gained are well mixed, is made and changes
Property liquid.
Specifically, the volume fraction of above-mentioned ethanol is 95%.
Specifically, above-mentioned steps（2）In, above-mentioned bleeding agent is AEO, and above-mentioned dispersant is dispersant
NNO, its chemical composition are naphthalene sulfonate salt formaldehyde condensation products.
Specifically, above-mentioned steps（3）In, reduction cleaning liquid is made up of the component of following parts by weight：Sodium hydroxide 4-7 parts,
Sodium dithionite 3-6 parts, water 850-900 parts.
Technical scheme more than, the beneficial effects of the invention are as follows：
Ribbon low-temperature dyeing method provided by the invention, simple to operate, energy consumption is low, and dyeing is stable, and safety and environmental protection can be effective
Temperature of reduction when padding, and Color is notable, uniform color, and color fastness is high, greatly improves the quality of ribbon.
Above-mentioned steps（1）In modification liquid, CDTA, sodium hexafluoro phosphate can effectively lift the permeability of ribbon,
Lift the uniformity of permeability and distribution of the dye liquor in ribbon；D-ALPHA-Hydroxypropionic acid methyl esters and methyl triacetoxysilane synergy
Afterwards, the surface-active of ribbon can be effectively lifted, lifts adhesion of the dye molecule on ribbon surface, and then improves color jail
Degree；After sodium vanadate, sodium phytate, sodium polysulfide synergy, the activity of dye molecule can be effectively lifted, may be such that dyestuff point
Son can be just effectively combined in the environment of compared with low temperature with ribbon, and wherein sodium phytate can be with the surface of dye molecule and ribbon point
Chemical bond is formed between son, dye molecule is may be such that and is attached in the environment of low temperature on ribbon.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, following examples are carried out to the present invention
It is further described.It should be appreciated that specific embodiment party example described herein is not used to limit only to explain the present invention
The fixed present invention.
Embodiment 1
A kind of ribbon low-temperature dyeing method, including following operating procedure：
（1）After ribbon is cleaned, be put into immersion treatment 140min in modification liquid, wherein modification liquid by following parts by weight component system
Into：18 parts of 1,2- 1,2-diaminocyclohexane tetraacetic acids, 10 parts of sodium hexafluoro phosphate, 36 parts of D-ALPHA-Hydroxypropionic acid methyl esters, methyl triacetoxysilane 32
Part, 150 parts of ethanol, 750 parts of water；
（2）To by step（1）The ribbon of processing carries out two leachings two and rolled, and wherein dyeing liquor is made up of the component of following parts by weight：
36 parts of dyestuff, 12 parts of bleeding agent, 10 parts of dispersant, 2 parts of sodium vanadate, 4 parts of sodium phytate, 2 parts of sodium polysulfide, 640 parts of water, dyeing
Temperature be 112 DEG C, bath raio 1:15, pick-up rate 60%；
（3）After the ribbon drying after dyeing, it is put into reduction cleaning liquid, after immersion treatment 30min, takes out, cleaned with clear water
Afterwards, finished product is dried.
Specifically, above-mentioned steps（1）Middle modification liquid is made of following methods：Will：1,2- 1,2-diaminocyclohexane tetraacetic acids, hexafluoro
Sodium phosphate is added to the water, and stirs 10min using 300r/min rotating speed, D-ALPHA-Hydroxypropionic acid methyl esters, methyl triacetoxysilane add
Into ethanol, 20min is stirred using 300r/min rotating speed, after then two mixed liquors of gained are well mixed, is made and changes
Property liquid.
Specifically, the volume fraction of above-mentioned ethanol is 95%.
Specifically, above-mentioned steps（2）In, above-mentioned bleeding agent is AEO, and above-mentioned dispersant is dispersant
NNO, its chemical composition are naphthalene sulfonate salt formaldehyde condensation products.
Specifically, above-mentioned steps（3）In, reduction cleaning liquid is made up of the component of following parts by weight：4 parts of sodium hydroxide, connect
3 parts of sodium sulfite, 850 parts of water.
Embodiment 2
A kind of ribbon low-temperature dyeing method, including following operating procedure：
（1）After ribbon is cleaned, be put into immersion treatment 150min in modification liquid, wherein modification liquid by following parts by weight component system
Into：22 parts of 1,2- 1,2-diaminocyclohexane tetraacetic acids, 12 parts of sodium hexafluoro phosphate, 40 parts of D-ALPHA-Hydroxypropionic acid methyl esters, methyl triacetoxysilane 34
Part, 180 parts of ethanol, 780 parts of water；
（2）To by step（1）The ribbon of processing carries out two leachings two and rolled, and wherein dyeing liquor is made up of the component of following parts by weight：
40 parts of dyestuff, 13 parts of bleeding agent, 12 parts of dispersant, 3 parts of sodium vanadate, 5 parts of sodium phytate, 3 parts of sodium polysulfide, 660 parts of water, dyeing
Temperature be 114 DEG C, bath raio 1:17, pick-up rate 70%；
（3）After the ribbon drying after dyeing, it is put into reduction cleaning liquid, after immersion treatment 35min, takes out, cleaned with clear water
Afterwards, finished product is dried.
Specifically, above-mentioned steps（1）Middle modification liquid is made of following methods：Will：1,2- 1,2-diaminocyclohexane tetraacetic acids, hexafluoro
Sodium phosphate is added to the water, and stirs 10min using 300r/min rotating speed, D-ALPHA-Hydroxypropionic acid methyl esters, methyl triacetoxysilane add
Into ethanol, 20min is stirred using 300r/min rotating speed, after then two mixed liquors of gained are well mixed, is made and changes
Property liquid.
Specifically, the volume fraction of above-mentioned ethanol is 95%.
Specifically, above-mentioned steps（2）In, above-mentioned bleeding agent is AEO, and above-mentioned dispersant is dispersant
NNO, its chemical composition are naphthalene sulfonate salt formaldehyde condensation products.
Specifically, above-mentioned steps（3）In, reduction cleaning liquid is made up of the component of following parts by weight：5 parts of sodium hydroxide, connect
5 parts of sodium sulfite, 880 parts of water.
Embodiment 3
A kind of ribbon low-temperature dyeing method, including following operating procedure：
（1）After ribbon is cleaned, be put into immersion treatment 160min in modification liquid, wherein modification liquid by following parts by weight component system
Into：26 parts of 1,2- 1,2-diaminocyclohexane tetraacetic acids, 14 parts of sodium hexafluoro phosphate, 45 parts of D-ALPHA-Hydroxypropionic acid methyl esters, methyl triacetoxysilane 40
Part, 200 parts of ethanol, 820 parts of water；
（2）To by step（1）The ribbon of processing carries out two leachings two and rolled, and wherein dyeing liquor is made up of the component of following parts by weight：
42 parts of dyestuff, 14 parts of bleeding agent, 13 parts of dispersant, 5 parts of sodium vanadate, 7 parts of sodium phytate, 4 parts of sodium polysulfide, 700 parts of water, dyeing
Temperature be 118 DEG C, bath raio 1:18, pick-up rate 75%；
（3）After the ribbon drying after dyeing, it is put into reduction cleaning liquid, after immersion treatment 40min, takes out, cleaned with clear water
Afterwards, finished product is dried.
Specifically, above-mentioned steps（1）Middle modification liquid is made of following methods：Will：1,2- 1,2-diaminocyclohexane tetraacetic acids, hexafluoro
Sodium phosphate is added to the water, and stirs 10min using 300r/min rotating speed, D-ALPHA-Hydroxypropionic acid methyl esters, methyl triacetoxysilane add
Into ethanol, 20min is stirred using 300r/min rotating speed, after then two mixed liquors of gained are well mixed, is made and changes
Property liquid.
Specifically, the volume fraction of above-mentioned ethanol is 95%.
Specifically, above-mentioned steps（2）In, above-mentioned bleeding agent is AEO, and above-mentioned dispersant is dispersant
NNO, its chemical composition are naphthalene sulfonate salt formaldehyde condensation products.
Specifically, above-mentioned steps（3）In, reduction cleaning liquid is made up of the component of following parts by weight：7 parts of sodium hydroxide, connect
6 parts of sodium sulfite, 900 parts of water.
Comparative example 1
Without step（1）Processing, remaining operating procedure are identical with embodiment 1.
Comparative example 2
Step（2）In do not contain sodium vanadate, sodium phytate, sodium polysulfide composition, remaining operating procedure and 2 complete phase of embodiment
Together.
Dyeing processing is carried out to terylene ribbon with the method for each embodiment and comparative example respectively, coloration result is as shown in table 1：
The Color of the terylene ribbon of table 1
| Project | Colour fastness to rubbing | Washing color fastness | Dye-uptake, % |
| Embodiment 1 | 4 | 5 | 95.2 |
| Comparative example 1 | 2 | 2 | 85.1 |
| Embodiment 2 | 5 | 5 | 96.3 |
| Comparative example 2 | 2 | 2 | 87.3 |
| Embodiment 3 | 5 | 5 | 97.1 |
As shown in Table 1, a kind of ribbon low-temperature dyeing method provided by the invention, the Color of ribbon can effectively be lifted.
Certainly, it is limitation of the present invention that described above, which is not, and the present invention is also not limited to the example above, the art
Those of ordinary skill, the present invention essential scope in, change, change, addition or the replacement made, should all belong to the present invention
Protection domain.
Claims (5)
1. a kind of ribbon low-temperature dyeing method, it is characterised in that including following operating procedure：
（1）After ribbon is cleaned, be put into immersion treatment 140-160min in modification liquid, wherein modification liquid by following parts by weight group
Divide and be made：1,2- 1,2-diaminocyclohexane tetraacetic acid 18-26 parts, sodium hexafluoro phosphate 10-14 parts, D-ALPHA-Hydroxypropionic acid methyl esters 36-45 parts, the second of methyl three
Acyloxy silane 32-40 parts, ethanol 150-200 parts, water 750-820 parts；
（2）To by step（1）The ribbon of processing carries out two leachings two and rolled, and wherein dyeing liquor is made up of the component of following parts by weight：
Dyestuff 36-42 parts, bleeding agent 12-14 parts, dispersant 10-13 parts, sodium vanadate 2-5 parts, sodium phytate 4-7 parts, sodium polysulfide 2-4
Part, water 640-700 parts, the temperature of dyeing is 112-118 DEG C, bath raio 1:15-18, pick-up rate 60-75%；
（3）After the ribbon drying after dyeing, it is put into reduction cleaning liquid, after immersion treatment 30-40min, takes out, washed with clear water
After net, finished product is dried.
2. according to a kind of ribbon low-temperature dyeing method described in claim 1, it is characterised in that above-mentioned steps（1）Middle modification
Liquid is made of following methods：Will：CDTA, sodium hexafluoro phosphate are added to the water, using turning for 300r/min
Speed stirring 10min, D-ALPHA-Hydroxypropionic acid methyl esters, methyl triacetoxysilane are added into ethanol, are stirred using 300r/min rotating speed
20min, after then two mixed liquors of gained are well mixed, modification liquid is made.
3. according to a kind of ribbon low-temperature dyeing method described in claim 2, it is characterised in that the volume fraction of above-mentioned ethanol
For 95%.
4. according to a kind of ribbon low-temperature dyeing method described in claim 1, it is characterised in that above-mentioned steps（2）In, it is above-mentioned
Bleeding agent is AEO, and above-mentioned dispersant is dispersant NNO, and its chemical composition is naphthalene sulfonate salt formaldehyde condensation
Thing.
5. according to a kind of ribbon low-temperature dyeing method described in claim 1, it is characterised in that above-mentioned steps（3）In, reduction
Cleaning fluid is made up of the component of following parts by weight：Sodium hydroxide 4-7 parts, sodium dithionite 3-6 parts, water 850-900 parts.
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| CN201710918326.6A CN107476080A (en) | 2017-09-30 | 2017-09-30 | A kind of ribbon low-temperature dyeing method |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109322172A (en) * | 2018-09-28 | 2019-02-12 | 安徽省永欣织带有限公司 | A kind of colouring method of ribbon terylene net-thread |
| CN112281525A (en) * | 2020-11-15 | 2021-01-29 | 广州众缘纺织科技有限公司 | Tie-dyeing method and silver bright yarn knitted fabric prepared by tie-dyeing method |
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