CN112274466A - 一种冰沙喷雾及其制备方法 - Google Patents
一种冰沙喷雾及其制备方法 Download PDFInfo
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Abstract
本发明公开了一种冰沙喷雾，主要是通过0.01%‑1%琼脂糖和0.05%‑0.5%丙烯酰二甲基牛磺酸铵/VP共聚物按照一定比例的复配，能够提升成膜性，使得形成的薄膜具有均匀、丝滑、清爽、保湿效果好的优点。
Description
技术领域
本发明涉及化妆品技术领域，特别是涉及一种冰沙喷雾及其制备方法。
背景技术
目前市售的喷雾类化妆品物理形态都为液体形态，通过泵头雾化，能使产品均匀吸附在皮肤上且被快速吸收，但一般化妆品中添加物可能会含有金属离子和有机物，当有这些物质存在的时候，液体形态配方悬浮力度不好体系不容易稳定，容易产生絮状物或者沉淀。如果做成固体冰沙形态，则不会出现上述问题。
中国专利申请201810762512X公开了一种可水洗面膜，其说明书摘要记载了“以N-乙烯基吡咯烷酮、甲基丙烯酰胺丙基二甲基胺等为原料聚合得到弹性成膜剂的描述”。但是，实际上该专利说明书和权利要求书都没有描述上述两种物质，本领域技术人员无法从该专利中得知乙烯基吡咯烷酮的用量等参数，乙烯基吡咯烷酮是否能够形成薄膜也是未知的。
发明内容
本发明的目的在于，提供一种冰沙喷雾，形成的薄膜具有均匀、丝滑、清爽、保湿效果好的优点。
本发明是通过以下技术方案实现的
一种冰沙喷雾，按重量百分比计，包括以下组分：
琼脂糖 0.1-1%；
丙烯酰二甲基牛磺酸铵/VP 共聚物 0.05-0.5%；
填充剂 70.5-98%；
保湿剂 1-15%；
防腐剂 0.01-4%；
皮肤调理剂 0.01-5%；
抗敏剂 0.01-3%；
香精 0.001-0.5%；
增溶剂 0.001-1%；
琼脂糖与丙烯酰二甲基牛磺酸铵/VP 共聚物的重量比为10:1-2:1。
优选的，琼脂糖与丙烯酰二甲基牛磺酸铵/VP 共聚物的重量比为5:1-3:1。
所述的填充剂选自去离子水。
所述保湿剂包括甘油、丁二醇、丙二醇和山梨醇中的至少一种。
所述防腐剂包括宣称为无添加的防腐剂和传统防腐剂，包括对羟基苯乙酮，1,2-己二醇，1,2-戊二醇，咪唑烷基脲、甲基异噻唑啉酮、苯氧乙醇、苯氯甘醚、对羟基苯甲酸甲酯中的一种或多种的复配物。
例：
对羟基苯乙酮：1,2-己二醇的重量比为1:1-1:3
苯氯甘醚：苯氧乙醇的重量比为1:1-1:3
1,2-己二醇，1,2-戊二醇的重量比为1:1-1:4
所述皮肤调理剂为聚乙二醇-8、甲基葡糖醇聚醚-20，甘油聚醚-26，聚季铵盐-7和甲基丙二醇中的至少一种。
所述抗敏剂为甘草酸二钾、马齿苋提取物、金盏花提取物、芦荟提取物、尿囊素和金缕梅提取物中的至少一种。
所述香精包括花香、果香中的至少一种。
所述增溶剂为化妆品领域常用原料，包括吐温-20、聚氧乙烯氢化蓖麻油中的至少一种。
上述的冰沙喷雾的制备方法，包括以下步骤：
（1）用保湿剂分散琼脂糖、丙烯酰二甲基牛磺酸铵/VP 共聚物，成浆状后加入填充剂，缓慢搅拌加热至85±2℃，保温条件下300~400r/min搅拌5-10分钟后，缓慢降温至50±2℃；
（2）加入防腐剂，皮肤调理剂和抗敏剂，搅拌溶解；
（3）将香精和增溶剂混合加入，搅拌溶解；
（4）保持料体50±2℃温度，灌装入透明PET瓶，即刻旋喷雾泵头完成小包装工序，然后静置固化完全后大力摇匀即可。
本发明就有如下有益效果
本发明创造性的采用琼脂糖协同丙烯酰二甲基牛磺酸铵/VP 共聚物作为成膜剂，使得冰沙喷雾实现喷雾后成膜均匀的效果，并且成膜稳定性性强，使成膜后具有均匀、丝滑、清爽、保湿效果好的优点。
附图说明
图1：成膜性测试示意图，中间白色部分为膜。
具体实施方式
下面结合具体实施例对本发明进行详细说明。以下实施例将有助于本领域的技术人员进一步理解本发明，但不以任何形式限制本发明。应当指出的是，对本领域的普通技术人员来说，在不脱离本发明构思的前提下，还可以做出若干变形和改进。这些都属于本发明的保护范围。
本发明采用的主要原料来源于市售：
琼脂糖（SeaPureTM Agarose，龙沙）：
丙烯酰二甲基牛磺酸铵/VP 共聚物（Aristoflex AVC，科莱恩）：
聚乙二醇-8（Macrogol 400，陶氏化学）
甘草酸二钾（GLYTINON K2，常磐制药）
对羟基苯乙酮（SymSave® H，Symrise）
丙二醇（Propylene glycol USP，陶氏化学）
聚氧乙烯氢化蓖麻油（NIKKOL HCO-60，NIHON SURFACTANT）
玫瑰香精（GF-833539，上海爱普）
实施例和对比例冰沙喷雾的制备方法：
（1）用保湿剂分散琼脂糖、丙烯酰二甲基牛磺酸铵/VP 共聚物，成浆状后加入填充剂，缓慢搅拌加热至85±2℃，保温条件下300~400r/min搅拌5-10分钟后，缓慢降温至50±2℃；
（2）加入防腐剂，皮肤调理剂和抗敏剂，搅拌溶解；
（3）将香精和增溶剂混合加入，搅拌溶解；
（4）保持料体50±2℃温度，灌装入透明PET瓶，即刻旋喷雾泵头完成小包装工序，然后静置固化完全后大力摇匀即可。
各项性能测试方法：
（1）保湿测试方法：
产品涂抹区和空白对照区应随机分布于左右手臂标定区域，确保所有产品和空白区域位置在统计学上达到平衡。测试样品按(2.0±0.1) mg/cm2的用量进行单次涂布，使用乳胶指套将试样均匀涂布于试验区内，并记录实际涂样量。按电容法皮肤水分测定仪使用说明书调整仪器后，进行产品区域和对照区域的测量，每个区域平行测定至少3次。先测量各测试区域的初始值（样品使用前） ，然后在设定时间后测定受试区域和对照区域的皮肤水分含量。设定时间应大于1h，可根据产品评价需要设定2h、3h等多个测定点，通常不超过24h。同一个受试者的测试必须使用同一仪器由同一个测量人员完成，两次测量之间应清洁测量探头。产品使用期间如志愿者皮肤出现不良反应，应立即终止测试 并对志愿者进行适当医治。对不良反应应予以记录。
（2）成膜测试方法：将产品喷在备好的（5cm*5cm）纸板上，放置于（105±1）恒温烘箱内烘3h后取出，置干燥器内冷却至室温。用裁纸刀将含有产品的纸板裁成细丝状，再利用全功能研究级生物显微镜（型号：BX53）观察细丝的横截面。如膜状平滑、厚度均匀则说明成膜效果好，反正则不好，主观评分1-5分，分数越高成膜性越好。
表1：实施例沙冰喷雾各组分配比（重量百分比）
| 实施例1 | 实施例2 | 实施例3 | 实施例4 | 实施例5 | 实施例6 | |
| 琼脂糖 | 0.5 | 0.49 | 0.46 | 0.42 | 0.37 | 0.4 |
| 丙烯酰二甲基牛磺酸铵/VP 共聚物 | 0.05 | 0.06 | 0.09 | 0.13 | 0.18 | 0.1 |
| 丙二醇 | 6 | 6 | 6 | 6 | 6 | 8 |
| 防腐剂 | 0.9 | 0.9 | 0.9 | 0.9 | 0.9 | 0.9 |
| 聚乙二醇-8 | 0.6 | 0.6 | 0.6 | 0.6 | 0.6 | 0.8 |
| 甘草酸二钾 | 0.3 | 0.3 | 0.3 | 0.3 | 0.3 | 0.1 |
| 香精 | 0.02 | 0.02 | 0.02 | 0.02 | 0.02 | 0.018 |
| 聚氧乙烯氢化蓖麻油 | 0.04 | 0.04 | 0.04 | 0.04 | 0.04 | 0.036 |
| 去离子水 | 余量 | 余量 | 余量 | 余量 | 余量 | 余量 |
| 涂抹1小时后含水量% | 45.6 | 47.4 | 49.6 | 50.9 | 48.7 | 49.4 |
| 涂抹2小时后含水量% | 16.7 | 19.7 | 20.2 | 20.0 | 18.6 | 19.0 |
| 成膜性 | 3 | 4 | 5 | 5 | 4 | 3 |
续表1：
| 对比例1 | 对比例2 | 对比例3 | 对比例4 | |
| 琼脂糖 | 0.55 | 0.54 | 0.01 | |
| 丙烯酰二甲基牛磺酸铵/VP 共聚物 | 0.55 | 0.01 | 0.54 | |
| 丙二醇 | 6 | 6 | 6 | 6 |
| 聚乙二醇-8 | 0.6 | 0.6 | 0.6 | 0.6 |
| 甘草酸二钾 | 0.3 | 0.3 | 0.3 | 0.3 |
| 香精 | 0.02 | 0.02 | 0.02 | 0.02 |
| 聚氧乙烯氢化蓖麻油 | 0.04 | 0.04 | 0.04 | 0.04 |
| 去离子水 | 余量 | 余量 | 余量 | 余量 |
| 涂抹1小时后含水量% | 40.7 | 42.5 | 39.6 | 43.1 |
| 涂抹2小时后含水量% | 11.6 | 12.7 | 12.3 | 13.6 |
| 成膜性 | 1 | 2 | 1 | 2 |
上表中，防腐剂采用：对羟基苯乙酮：0.4%，1,2-己二醇：0.5%；
香精采用：花香（玫瑰香精）：0.02%。
对比例2虽然采用0.55份丙烯酰二甲基牛磺酸铵/VP 共聚物，成膜厚度较厚，但是膜的厚度均匀性不好，导致一部分水分会通过较薄的膜出挥发掉，导致保湿性下降。
Claims (10)
1.一种冰沙喷雾，其特征在于，按重量百分比计，包括以下组分：
琼脂糖 0.1-1%；
丙烯酰二甲基牛磺酸铵/VP 共聚物 0.05-0.5%；
填充剂 70.5-98%；
保湿剂 1-15%；
防腐剂 0.01-4%；
皮肤调理剂 0.01-5%；
抗敏剂 0.01-3%；
香精 0.001-0.5%；
增溶剂 0.001-1%；
琼脂糖与丙烯酰二甲基牛磺酸铵/VP 共聚物的重量比为10:1-2:1。
2.根据权利要求1所述的冰沙喷雾，其特征在于，琼脂糖与丙烯酰二甲基牛磺酸铵/VP共聚物的重量比为5:1-3:1。
3.根据权利要求1所述的冰沙喷雾，其特征在于，所述的填充剂选自去离子水。
4.根据权利要求1所述的冰沙喷雾，其特征在于，所述保湿剂包括甘油、丁二醇、丙二醇和山梨醇中的至少一种。
5.根据权利要求1所述的冰沙喷雾，其特征在于，所述防腐剂包括宣称为无添加的防腐剂和传统防腐剂，包括对羟基苯乙酮，1,2-己二醇，1,2-戊二醇，咪唑烷基脲、甲基异噻唑啉酮、苯氧乙醇、苯氯甘醚和对羟基苯甲酸甲酯中的一种或多种的复配物。
6.根据权利要求1所述的冰沙喷雾，其特征在于，所述皮肤调理剂选自聚乙二醇-8、甲基葡糖醇聚醚-20，甘油聚醚-26，聚季铵盐-7、甲基丙二醇中的至少一种。
7.根据权利要求1所述的冰沙喷雾，其特征在于，所述抗敏剂选自甘草酸二钾、马齿苋提取物、金盏花提取物、芦荟提取物、尿囊素、金缕梅提取物中的至少一种。
8.根据权利要求1所述的冰沙喷雾，其特征在于，所述香精包括花香、果香中的至少一种。
9.根据权利要求1所述的冰沙喷雾，其特征在于，所述增溶剂为化妆品领域常用原料，包括吐温-20、聚氧乙烯氢化蓖麻油中的至少一种。
10.权利要求1-9任一项所述的冰沙喷雾的制备方法，其特征在于，包括以下步骤：
（1）用保湿剂分散琼脂糖、丙烯酰二甲基牛磺酸铵/VP 共聚物，成浆状后加入填充剂，缓慢搅拌加热至85±2℃，保温条件下300~400r/min搅拌5-10分钟后，缓慢降温至50±2℃；
（2）加入防腐剂，皮肤调理剂和抗敏剂，搅拌溶解；
（3）将香精和增溶剂混合加入，搅拌溶解；
（4）保持料体50±2℃温度，灌装入透明PET瓶，即刻旋喷雾泵头完成小包装工序，然后静置固化完全后大力摇匀即可。
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