CN112175691A - Functional lubricating oil with good comprehensive performance and processing technology - Google Patents

Functional lubricating oil with good comprehensive performance and processing technology Download PDF

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Publication number
CN112175691A
CN112175691A CN202011209320.XA CN202011209320A CN112175691A CN 112175691 A CN112175691 A CN 112175691A CN 202011209320 A CN202011209320 A CN 202011209320A CN 112175691 A CN112175691 A CN 112175691A
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agent
lubricating oil
semi
finished product
stirring
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梁大伟
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Dongguan Huitong Energy Co ltd
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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M167/00Lubricating compositions characterised by the additive being a mixture of a macromolecular compound, a non-macromolecular compound and a compound of unknown or incompletely defined constitution, each of these compounds being essential
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/04Elements
    • C10M2201/041Carbon; Graphite; Carbon black
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/04Elements
    • C10M2201/05Metals; Alloys
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/06Metal compounds
    • C10M2201/062Oxides; Hydroxides; Carbonates or bicarbonates
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/06Metal compounds
    • C10M2201/065Sulfides; Selenides; Tellurides
    • C10M2201/066Molybdenum sulfide
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/08Inorganic acids or salts thereof
    • C10M2201/084Inorganic acids or salts thereof containing sulfur, selenium or tellurium
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/087Boron oxides, acids or salts
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/02Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/08Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing monomers having an unsaturated radical bound to a carboxyl radical, e.g. acrylate type
    • C10M2209/084Acrylate; Methacrylate
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2213/00Organic macromolecular compounds containing halogen as ingredients in lubricant compositions
    • C10M2213/06Perfluoro polymers
    • C10M2213/062Polytetrafluoroethylene [PTFE]
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04Siloxanes with specific structure
    • C10M2229/041Siloxanes with specific structure containing aliphatic substituents

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
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  • Lubricants (AREA)

Abstract

The invention discloses a functional lubricating oil with good comprehensive performance and a processing technology thereof, and the formula comprises: the anti-corrosion and anti-wear lubricating oil comprises base oil, a composite pour point depressant, an anti-foaming machine, a solid filler, a dispersing agent, a boron anti-wear agent, a detergent and a sodium carbonate antirust agent, wherein the components in parts by weight are as follows: 85-95 parts of base oil, 0.2-0.4 part of composite pour point depressant, 0.1-0.2 part of antifoaming agent, 0.1-0.2 part of solid filler, 0.5-0.8 part of dispersing agent, 0.1-0.3 part of boron antiwear agent, 0.4-0.8 part of detergent and 0.2-0.4 part of sodium carbonate antirust agent.

Description

Functional lubricating oil with good comprehensive performance and processing technology
Technical Field
The invention relates to the technical field of lubricating oil, in particular to functional lubricating oil with good comprehensive performance and a processing technology.
Background
The lubricating oil is a liquid or semisolid lubricating agent used on various types of automobiles and mechanical equipment to reduce friction and protect machines and workpieces, generally consists of base oil and additives, the lubricating oil is a technically intensive product and is a complex hydrocarbon mixture and mainly plays roles of lubrication, cooling, rust prevention, cleaning, sealing, buffering and the like, so the lubricating oil is visible everywhere in the mechanical production process, but the traditional lubricating oil is easy to generate bubbles in the preparation process, so the contact area of the lubricating oil and gas is increased, the oxidation reaction rate is increased, the quality of the lubricating oil is reduced, meanwhile, in the preparation process, solid fillers are usually added to increase the anti-wear property of the lubricating oil, but in the adding process, the solid fillers are easily aggregated together, the diameter of powder particles is increased, so the mechanical structure is easily damaged, meanwhile, the phenomenon of solidification is easily caused when the lubricating oil is used in a low-temperature environment, and the comprehensive performance of the lubricating oil is reduced.
Disclosure of Invention
The invention aims to provide functional lubricating oil with good comprehensive performance and a processing technology, so as to solve the problems in the background technology.
In order to solve the technical problems, the invention provides the following technical scheme: a functional lubricating oil with good comprehensive performance comprises the following components in percentage by weight: the anti-corrosion and anti-wear lubricating oil comprises base oil, a composite pour point depressant, an anti-foaming machine, a solid filler, a dispersing agent, a boron anti-wear agent, a detergent and a sodium carbonate antirust agent, wherein the components in parts by weight are as follows: 85-95 parts of base oil, 0.2-0.4 part of composite pour point depressant, 0.1-0.2 part of anti-foaming agent, 0.1-0.2 part of solid filler, 0.5-0.8 part of dispersant, 0.1-0.3 part of boron anti-wear agent, 0.4-0.8 part of detergent and 0.2-0.4 part of sodium carbonate antirust agent.
A processing technology of functional lubricating oil with good comprehensive performance comprises the following steps of firstly, selecting raw materials; step two, heating and preserving heat; step three, mixing and stirring; step four, dispersing and stirring; step five, stopping heat preservation; step six, cooling and standing;
in the first step, 85-95 parts of base oil, 0.2-0.4 part of composite pour point depressant, 0.1-0.2 part of anti-foaming agent, 0.1-0.2 part of solid filler, 0.5-0.8 part of dispersant, 0.1-0.3 part of boron anti-wear agent, 0.4-0.8 part of detergent and 0.2-0.4 part of sodium carbonate antirust agent are respectively selected according to the weight parts of the components for later use;
in the second step, firstly, the base oil and the antifoaming agent selected in the first step are placed in a magnetic heating stirrer together to be subjected to variable heating and variable stirring for 20-30min to obtain a mixed material for later use, and the heating is stopped to carry out heat preservation treatment when the heating temperature reaches 80-90 ℃, wherein the stirring speed is 200-;
in the third step, the composite anticoagulant, the boron antiwear agent, the detergent and the sodium carbonate antirust agent selected in the first step are placed in a stirrer together and stirred for 10-15min to obtain an additive for later use, wherein the stirring speed is 100-120 r/min;
in the fourth step, the solid filler selected in the first step is subjected to ultrasonic high-speed dispersion treatment, then the dispersed solid filler is placed in the rotating dispersing agent in the first step to be stirred and mixed to obtain dispersed filler, and then the dispersed filler is subjected to ultrasonic high-speed dispersion treatment again;
in the fifth step, the additive obtained in the third step and the dispersed filler obtained in the fourth step are placed in the mixture obtained in the second step together to be stirred to obtain a semi-finished product, and the heat preservation can be stopped after the stirring is finished;
and in the sixth step, naturally cooling the semi-finished product obtained in the fifth step, cooling the semi-finished product by using dry ice or liquid nitrogen when the semi-finished product is cooled to normal temperature, stirring the semi-finished product in the cooling process so as to uniformly cool the semi-finished product, removing the dry ice or the liquid nitrogen when the temperature of the semi-finished product is cooled to 10-15 ℃, filtering the semi-finished product by using a vacuum oil filter, and standing the obtained filtrate for 60-80min to obtain the lubricating oil.
According to the technical scheme, the composite pour point depressant is prepared by mixing a polyacrylic acid higher alcohol ester pour point depressant and a polyolefin pour point depressant according to the weight ratio of 3: 2.
According to the technical scheme, the anti-foaming agent is prepared by mixing dimethyl silicone oil and a non-organic silicon polymer anti-foaming agent according to the weight ratio of 1: 1.
According to the technical scheme, the solid filler is prepared by mixing graphite, molybdenum disulfide, polytetrafluoroethylene and nano metal powder according to the weight ratio of 2: 1.
According to the technical scheme, the detergent is high-base-number synthetic calcium sulfate T106.
According to the technical scheme, in the fourth step, the ultrasonic frequency is 20-30KHz, the dispersion speed is 4000-4500r/min, and the dispersion time is 20-30 min.
According to the above technical scheme, in the fifth step, the stirring time is 60-90min, and the stirring speed is 400-500 r/min.
Compared with the prior art, the invention has the following beneficial effects: according to the invention, the added anti-foaming agent is prepared by mixing two anti-foaming substances, so that the anti-foaming effect of the lubricating oil is improved, the residual quantity of bubbles in the lubricating oil is reduced, the contact quantity of the lubricating oil and gas is further reduced, and the quality of the lubricating oil is improved; meanwhile, the solid filler is subjected to dispersion treatment in the preparation process, so that the aggregation phenomenon of particles in the solid filler is avoided, the damage to a mechanical structure is reduced, and the required lubricating mechanical structure is protected; and the semi-finished product is cooled and filtered to obtain easily solidified substances, so that the lubricating oil can be normally used in a low-temperature environment, and the comprehensive performance of the lubricating oil is improved.
Drawings
The accompanying drawings, which are included to provide a further understanding of the invention and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention and together with the description serve to explain the principles of the invention and not to limit the invention. In the drawings:
FIG. 1 is a process flow diagram of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1, the present invention provides a technical solution:
example 1:
a functional lubricating oil with good comprehensive performance comprises the following components in percentage by weight: the anti-corrosion and anti-wear lubricating oil comprises base oil, a composite pour point depressant, an anti-foaming machine, a solid filler, a dispersing agent, a boron anti-wear agent, a detergent and a sodium carbonate antirust agent, wherein the components in parts by weight are as follows: 85-95 parts of base oil, 0.2-0.4 part of composite pour point depressant, 0.1-0.2 part of anti-foaming agent, 0.1-0.2 part of solid filler, 0.5-0.8 part of dispersing agent, 0.1-0.3 part of boron anti-wear agent, 0.4-0.8 part of detergent and 0.2-0.4 part of sodium carbonate antirust agent, wherein the composite pour point depressant is prepared by mixing polyacrylic acid higher alcohol ester pour point depressant and polyolefin pour point depressant according to the weight ratio of 3: 2, the anti-foaming agent is prepared by mixing dimethyl silicone oil and non-organosilicon polymer anti-foaming agent according to the weight ratio of 1: 1, the solid filler is prepared by mixing graphite, molybdenum disulfide, polytetrafluoroethylene and nano metal powder according to the weight ratio of 2: 1, and the detergent is high-base-number synthetic calcium sulfate T106.
A processing technology of functional lubricating oil with good comprehensive performance comprises the following steps of firstly, selecting raw materials; step two, heating and preserving heat; step three, mixing and stirring; step four, dispersing and stirring; step five, stopping heat preservation; step six, cooling and standing;
in the first step, 85 parts of base oil, 0.2 part of composite pour point depressant, 0.1 part of anti-foaming agent, 0.1 part of solid filler, 0.5 part of dispersant, 0.1 part of boron anti-wear agent, 0.4 part of detergent and 0.2 part of sodium carbonate antirust agent are respectively selected according to the weight parts of the components for standby;
in the second step, firstly, the base oil and the antifoaming agent selected in the first step are placed in a magnetic heating stirrer together to be subjected to variable heating and variable stirring for 20-30min to obtain a mixed material for later use, and the heating is stopped to carry out heat preservation treatment when the heating temperature reaches 80-90 ℃, wherein the stirring speed is 200-;
in the third step, the composite anticoagulant, the boron antiwear agent, the detergent and the sodium carbonate antirust agent selected in the first step are placed in a stirrer together and stirred for 10-15min to obtain an additive for later use, wherein the stirring speed is 100-120 r/min;
in the fourth step, the solid filler selected in the first step is subjected to ultrasonic high-speed dispersion treatment, the ultrasonic frequency is 20-30KHz, the dispersion speed is 4000-4500r/min, and the dispersion time is 20-30min, then the dispersed solid filler is placed in the rotating dispersing agent in the first step to be stirred and mixed to obtain the dispersed filler, and then the dispersed filler is subjected to ultrasonic high-speed dispersion treatment again;
in the fifth step, the additive obtained in the third step and the dispersed filler obtained in the fourth step are placed in the mixture obtained in the second step together and stirred to obtain a semi-finished product, the stirring time is 60-90min, the stirring speed is 400-500r/min, and the heat preservation can be stopped after the stirring is finished;
and in the sixth step, naturally cooling the semi-finished product obtained in the fifth step, cooling the semi-finished product by using dry ice or liquid nitrogen when the semi-finished product is cooled to normal temperature, stirring the semi-finished product in the cooling process so as to uniformly cool the semi-finished product, removing the dry ice or the liquid nitrogen when the temperature of the semi-finished product is cooled to 10-15 ℃, filtering the semi-finished product by using a vacuum oil filter, and standing the obtained filtrate for 60-80min to obtain the lubricating oil.
Example 2:
a functional lubricating oil with good comprehensive performance comprises the following components in percentage by weight: the anti-corrosion and anti-wear lubricating oil comprises base oil, a composite pour point depressant, an anti-foaming machine, a solid filler, a dispersing agent, a boron anti-wear agent, a detergent and a sodium carbonate antirust agent, wherein the components in parts by weight are as follows: 85-95 parts of base oil, 0.2-0.4 part of composite pour point depressant, 0.1-0.2 part of anti-foaming agent, 0.1-0.2 part of solid filler, 0.5-0.8 part of dispersing agent, 0.1-0.3 part of boron anti-wear agent, 0.4-0.8 part of detergent and 0.2-0.4 part of sodium carbonate antirust agent, wherein the composite pour point depressant is prepared by mixing polyacrylic acid higher alcohol ester pour point depressant and polyolefin pour point depressant according to the weight ratio of 3: 2, the anti-foaming agent is prepared by mixing dimethyl silicone oil and non-organosilicon polymer anti-foaming agent according to the weight ratio of 1: 1, the solid filler is prepared by mixing graphite, molybdenum disulfide, polytetrafluoroethylene and nano metal powder according to the weight ratio of 2: 1, and the detergent is high-base-number synthetic calcium sulfate T106.
A processing technology of functional lubricating oil with good comprehensive performance comprises the following steps of firstly, selecting raw materials; step two, heating and preserving heat; step three, mixing and stirring; step four, dispersing and stirring; step five, stopping heat preservation; step six, cooling and standing;
in the first step, 95 parts of base oil, 0.4 part of composite pour point depressant, 0.2 part of anti-foaming agent, 0.2 part of solid filler, 0.8 part of dispersant, 0.3 part of boron anti-wear agent, 0.8 part of detergent and 0.4 part of sodium carbonate antirust agent are respectively selected according to the weight parts of the components for later use;
in the second step, firstly, the base oil and the antifoaming agent selected in the first step are placed in a magnetic heating stirrer together to be subjected to variable heating and variable stirring for 20-30min to obtain a mixed material for later use, and the heating is stopped to carry out heat preservation treatment when the heating temperature reaches 80-90 ℃, wherein the stirring speed is 200-;
in the third step, the composite anticoagulant, the boron antiwear agent, the detergent and the sodium carbonate antirust agent selected in the first step are placed in a stirrer together and stirred for 10-15min to obtain an additive for later use, wherein the stirring speed is 100-120 r/min;
in the fourth step, the solid filler selected in the first step is subjected to ultrasonic high-speed dispersion treatment, the ultrasonic frequency is 20-30KHz, the dispersion speed is 4000-4500r/min, and the dispersion time is 20-30min, then the dispersed solid filler is placed in the rotating dispersing agent in the first step to be stirred and mixed to obtain the dispersed filler, and then the dispersed filler is subjected to ultrasonic high-speed dispersion treatment again;
in the fifth step, the additive obtained in the third step and the dispersed filler obtained in the fourth step are placed in the mixture obtained in the second step together and stirred to obtain a semi-finished product, the stirring time is 60-90min, the stirring speed is 400-500r/min, and the heat preservation can be stopped after the stirring is finished;
and in the sixth step, naturally cooling the semi-finished product obtained in the fifth step, cooling the semi-finished product by using dry ice or liquid nitrogen when the semi-finished product is cooled to normal temperature, stirring the semi-finished product in the cooling process so as to uniformly cool the semi-finished product, removing the dry ice or the liquid nitrogen when the temperature of the semi-finished product is cooled to 10-15 ℃, filtering the semi-finished product by using a vacuum oil filter, and standing the obtained filtrate for 60-80min to obtain the lubricating oil.
Example 3:
a functional lubricating oil with good comprehensive performance comprises the following components in percentage by weight: the anti-corrosion and anti-wear lubricating oil comprises base oil, a composite pour point depressant, an anti-foaming machine, a solid filler, a dispersing agent, a boron anti-wear agent, a detergent and a sodium carbonate antirust agent, wherein the components in parts by weight are as follows: 85-95 parts of base oil, 0.2-0.4 part of composite pour point depressant, 0.1-0.2 part of anti-foaming agent, 0.1-0.2 part of solid filler, 0.5-0.8 part of dispersing agent, 0.1-0.3 part of boron anti-wear agent, 0.4-0.8 part of detergent and 0.2-0.4 part of sodium carbonate antirust agent, wherein the composite pour point depressant is prepared by mixing polyacrylic acid higher alcohol ester pour point depressant and polyolefin pour point depressant according to the weight ratio of 3: 2, the anti-foaming agent is prepared by mixing dimethyl silicone oil and non-organosilicon polymer anti-foaming agent according to the weight ratio of 1: 1, the solid filler is prepared by mixing graphite, molybdenum disulfide, polytetrafluoroethylene and nano metal powder according to the weight ratio of 2: 1, and the detergent is high-base-number synthetic calcium sulfate T106.
A processing technology of functional lubricating oil with good comprehensive performance comprises the following steps of firstly, selecting raw materials; step two, heating and preserving heat; step three, mixing and stirring; step four, dispersing and stirring; step five, stopping heat preservation; step six, cooling and standing;
in the first step, 90 parts of base oil, 0.3 part of composite pour point depressant, 0.2 part of anti-foaming agent, 0.1 part of solid filler, 0.7 part of dispersant, 0.2 part of boron anti-wear agent, 0.6 part of detergent and 0.3 part of sodium carbonate antirust agent are respectively selected according to the weight parts of the components for standby;
in the second step, firstly, the base oil and the antifoaming agent selected in the first step are placed in a magnetic heating stirrer together to be subjected to variable heating and variable stirring for 20-30min to obtain a mixed material for later use, and the heating is stopped to carry out heat preservation treatment when the heating temperature reaches 80-90 ℃, wherein the stirring speed is 200-;
in the third step, the composite anticoagulant, the boron antiwear agent, the detergent and the sodium carbonate antirust agent selected in the first step are placed in a stirrer together and stirred for 10-15min to obtain an additive for later use, wherein the stirring speed is 100-120 r/min;
in the fourth step, the solid filler selected in the first step is subjected to ultrasonic high-speed dispersion treatment, the ultrasonic frequency is 20-30KHz, the dispersion speed is 4000-4500r/min, and the dispersion time is 20-30min, then the dispersed solid filler is placed in the rotating dispersing agent in the first step to be stirred and mixed to obtain the dispersed filler, and then the dispersed filler is subjected to ultrasonic high-speed dispersion treatment again;
in the fifth step, the additive obtained in the third step and the dispersed filler obtained in the fourth step are placed in the mixture obtained in the second step together and stirred to obtain a semi-finished product, the stirring time is 60-90min, the stirring speed is 400-500r/min, and the heat preservation can be stopped after the stirring is finished;
and in the sixth step, naturally cooling the semi-finished product obtained in the fifth step, cooling the semi-finished product by using dry ice or liquid nitrogen when the semi-finished product is cooled to normal temperature, stirring the semi-finished product in the cooling process so as to uniformly cool the semi-finished product, removing the dry ice or the liquid nitrogen when the temperature of the semi-finished product is cooled to 10-15 ℃, filtering the semi-finished product by using a vacuum oil filter, and standing the obtained filtrate for 60-80min to obtain the lubricating oil.
The lubricating oils obtained in the above examples were tested separately and the data obtained are shown in the following table:
viscosity index
Example 1 165
Example 2 167
Example 3 170
Based on the above, the lubricating oil has the advantages that the lubricating oil is prepared by mixing two different anti-foaming substances with the added anti-foaming agent, so that the anti-foaming effect of the lubricating oil is improved, the bubble residue in the lubricating oil is reduced, the quality of the lubricating oil is improved, meanwhile, the solid filler is subjected to ultrasonic dispersion treatment in the preparation process, the components in the solid filler are prevented from being mixed and gathered together to increase the diameter of particles, the required lubricating mechanical structure is abraded, the mechanical structure is protected, the lubricating oil is subjected to cooling and filtering treatment in the production process, substances which are easy to solidify in a low-temperature environment are filtered, the lubricating oil is used normally in the low-temperature environment, and the comprehensive performance of the lubricating oil is improved.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (8)

1. A functional lubricating oil with good comprehensive performance comprises the following components in percentage by weight: the anti-corrosion and anti-wear lubricating oil comprises base oil, a composite pour point depressant, an anti-foaming machine, a solid filler, a dispersing agent, a boron anti-wear agent, a detergent and a sodium carbonate antirust agent, and is characterized in that: the weight parts of the components are respectively as follows: 85-95 parts of base oil, 0.2-0.4 part of composite pour point depressant, 0.1-0.2 part of anti-foaming agent, 0.1-0.2 part of solid filler, 0.5-0.8 part of dispersant, 0.1-0.3 part of boron anti-wear agent, 0.4-0.8 part of detergent and 0.2-0.4 part of sodium carbonate antirust agent.
2. A processing technology of functional lubricating oil with good comprehensive performance comprises the following steps of firstly, selecting raw materials; step two, heating and preserving heat; step three, mixing and stirring; step four, dispersing and stirring; step five, stopping heat preservation; step six, cooling and standing; the method is characterized in that:
in the first step, 85-95 parts of base oil, 0.2-0.4 part of composite pour point depressant, 0.1-0.2 part of anti-foaming agent, 0.1-0.2 part of solid filler, 0.5-0.8 part of dispersant, 0.1-0.3 part of boron anti-wear agent, 0.4-0.8 part of detergent and 0.2-0.4 part of sodium carbonate antirust agent are respectively selected according to the weight parts of the components for later use;
in the second step, firstly, the base oil and the antifoaming agent selected in the first step are placed in a magnetic heating stirrer together to be subjected to variable heating and variable stirring for 20-30min to obtain a mixed material for later use, and the heating is stopped to carry out heat preservation treatment when the heating temperature reaches 80-90 ℃, wherein the stirring speed is 200-;
in the third step, the composite anticoagulant, the boron antiwear agent, the detergent and the sodium carbonate antirust agent selected in the first step are placed in a stirrer together and stirred for 10-15min to obtain an additive for later use, wherein the stirring speed is 100-120 r/min;
in the fourth step, the solid filler selected in the first step is subjected to ultrasonic high-speed dispersion treatment, then the dispersed solid filler is placed in the rotating dispersing agent in the first step to be stirred and mixed to obtain dispersed filler, and then the dispersed filler is subjected to ultrasonic high-speed dispersion treatment again;
in the fifth step, the additive obtained in the third step and the dispersed filler obtained in the fourth step are placed in the mixture obtained in the second step together to be stirred to obtain a semi-finished product, and the heat preservation can be stopped after the stirring is finished;
and in the sixth step, naturally cooling the semi-finished product obtained in the fifth step, cooling the semi-finished product by using dry ice or liquid nitrogen when the semi-finished product is cooled to normal temperature, stirring the semi-finished product in the cooling process so as to uniformly cool the semi-finished product, removing the dry ice or the liquid nitrogen when the temperature of the semi-finished product is cooled to 10-15 ℃, filtering the semi-finished product by using a vacuum oil filter, and standing the obtained filtrate for 60-80min to obtain the lubricating oil.
3. The functional lubricating oil with good comprehensive performance as claimed in claim 1, wherein: the composite pour point depressant is prepared by mixing a polyacrylic acid higher alcohol ester pour point depressant and a polyolefin pour point depressant according to the weight ratio of 3: 2.
4. The functional lubricating oil with good comprehensive performance as claimed in claim 1, wherein: the anti-foaming agent is prepared by mixing dimethyl silicone oil and a non-organic silicon polymer anti-foaming agent according to the weight ratio of 1: 1.
5. The functional lubricating oil with good comprehensive performance as claimed in claim 1, wherein: the solid filler is prepared by mixing graphite, molybdenum disulfide, polytetrafluoroethylene and nano metal powder according to the weight ratio of 2: 1.
6. The functional lubricating oil with good comprehensive performance as claimed in claim 1, wherein: the detergent is high-base number synthetic calcium sulfate T106.
7. The process for processing the functional lubricating oil with good comprehensive performance as claimed in claim 2, wherein the process comprises the following steps: in the fourth step, the ultrasonic frequency is 20-30KHz, the dispersion speed is 4000-4500r/min, and the dispersion time is 20-30 min.
8. The process for processing the functional lubricating oil with good comprehensive performance as claimed in claim 2, wherein the process comprises the following steps: in the fifth step, the stirring time is 60-90min, and the stirring speed is 400-500 r/min.
CN202011209320.XA 2020-11-03 2020-11-03 Functional lubricating oil with good comprehensive performance and processing technology Pending CN112175691A (en)

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