CN112174523A - Ceramic clay titanium series ultra-white crystal glaze and preparation method thereof - Google Patents
Ceramic clay titanium series ultra-white crystal glaze and preparation method thereof Download PDFInfo
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- CN112174523A CN112174523A CN202010946277.9A CN202010946277A CN112174523A CN 112174523 A CN112174523 A CN 112174523A CN 202010946277 A CN202010946277 A CN 202010946277A CN 112174523 A CN112174523 A CN 112174523A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
Abstract
The invention discloses a ceramic mud titanium system ultra-white crystal glaze and a preparation method thereof, wherein the ceramic mud titanium system ultra-white crystal glaze comprises a ground glaze and a surface glaze; the ground glaze comprises the following components in parts by mass: 40-50 parts of potassium feldspar; 8-13 parts of dolomite; 5-10 parts of calcite; 10-15 parts of spodumene; 10-12 parts of rutile; the overglaze comprises the following components in parts by mass: 30 to 35 parts of potash feldspar, 10 to 15 parts of calcite, 10 to 15 parts of talcum, 15 to 20 parts of zinc oxide and 10 to 15 parts of titanium oxide. The product of the invention is integrally snow white, wherein blue crystals are generated, the product is natural and elegant, and the whiteness of blue light can reach 93%.
Description
Technical Field
The invention relates to a ceramic clay titanium series ultra-white crystal glaze and a preparation method thereof.
Background
At present, as early as the period of business weeks, the phase splitting phenomenon has been observed in the original celadon glaze, and the south-ward Liang Huaian kiln 1400 years ago has produced the phase splitting glazed porcelain; the successfully-sintered crystallized glaze in Song Dynasty is famous and precious microcrystalline glaze such as Tianmu, tea dust, iron rust flower, grape dot, sesame and the like, and the main body of the glaze is a product which is subject to iron element and has a yellow color tone.
The crystallization was studied abroad beginning in about the 19 th century, mostly to study the zinc-silicon-zinc ore crystallized glaze series products.
The crystal glaze series products present various research types, and different crystal series products gather the experience and intelligence of countless artists.
Disclosure of Invention
The technical problem to be solved by the invention is to overcome the defects of the prior art and provide the clay titanium system ultra-white crystal glaze, the whole product of the ceramic clay titanium system ultra-white crystal glaze is snow white, blue crystals are generated, the ceramic clay titanium system ultra-white crystal glaze is natural and elegant, and the whiteness of blue light can reach 93%.
In order to solve the technical problems, the technical scheme of the invention is as follows: a kind of ceramic clay titanium series ultra-white crystal glaze, it includes ground glaze and overglaze; wherein the content of the first and second substances,
the ground coat comprises the following components in parts by mass:
40-50 parts of potassium feldspar; 8-13 parts of dolomite; 5-10 parts of calcite; 10-15 parts of spodumene; 10-12 parts of rutile;
the overglaze comprises the following components in parts by mass:
30 to 35 parts of potash feldspar, 10 to 15 parts of calcite, 10 to 15 parts of talcum, 15 to 20 parts of zinc oxide and 10 to 15 parts of titanium oxide.
The invention provides a preparation method of a clay titanium series ultra-white crystal glaze, which comprises the following steps:
preparing a ground glaze slip and a surface glaze slip;
taking a clean clay body, applying a ground glaze by using ground glaze slurry, drying, and spraying a surface glaze by using surface glaze slurry;
then sintering in a drawer kiln at 1290 ℃; the preparation process of the ground glaze slurry and the surface glaze slurry comprises the following steps:
and (3) after the material is prepared, performing wet ball milling for 12-14 hours according to the mass ratio of glaze to ball to water of 1 to 1.6 to 0.7, and after the ball milled glaze is sieved by a 160-mesh sieve, modulating the glaze into 51-53 Baume concentration for later use.
After the technical scheme is adopted, the product is integrally snow white, wherein blue crystals are generated, the product is natural and elegant, and the whiteness of blue light can reach 93%.
Detailed Description
The invention provides a ceramic clay titanium series ultra-white crystal glaze and a preparation method thereof, and a person skilled in the art can use the contents for reference and appropriately improve the process parameters for realization. It is expressly intended that all such similar substitutes and modifications apparent to those skilled in the art are deemed to be within the scope of the invention. While the methods and applications of this invention have been described in terms of preferred embodiments, it will be apparent to those of ordinary skill in the art that variations and modifications in the methods and applications described herein, as well as other suitable variations and combinations, may be made to implement and use the techniques of this invention without departing from the spirit and scope of the invention.
A kind of ceramic clay titanium series ultra-white crystal glaze, it includes ground glaze and overglaze; wherein the content of the first and second substances,
the ground coat comprises the following components in parts by mass:
40-50 parts of potassium feldspar; 8-13 parts of dolomite; 5-10 parts of calcite; 10-15 parts of spodumene; 10-12 parts of rutile;
the overglaze comprises the following components in parts by mass:
30 to 35 parts of potash feldspar, 10 to 15 parts of calcite, 10 to 15 parts of talcum, 15 to 20 parts of zinc oxide and 10 to 15 parts of titanium oxide.
The invention provides a preparation method of a clay titanium series ultra-white crystal glaze, which comprises the following steps:
preparing a ground glaze slip and a surface glaze slip;
taking a clean clay body, applying a ground glaze by using ground glaze slurry, drying, and spraying a surface glaze by using surface glaze slurry;
then sintering in a drawer kiln at 1290 ℃; the preparation process of the ground glaze slurry and the surface glaze slurry comprises the following steps:
and (3) after the material is prepared, performing wet ball milling for 12-14 hours according to the mass ratio of glaze to ball to water of 1 to 1.6 to 0.7, and after the ball milled glaze is sieved by a 160-mesh sieve, modulating the glaze into 51-53 Baume concentration for later use.
The product is integrally represented as snow white, wherein blue crystals are generated, the product is natural and elegant, and the whiteness of blue light can reach 93%.
In order that the present invention may be more clearly understood, the following detailed description of the present invention is given with reference to specific examples.
Comparative example 1
A kind of ceramic clay titanium series ultra-white crystal glaze, it includes ground glaze and overglaze; wherein the content of the first and second substances,
the ground coat comprises the following components in parts by mass:
40 parts of potassium feldspar; 8 parts of dolomite; 5 parts of calcite; 10 parts of spodumene; 10 parts of rutile;
the overglaze comprises the following components in parts by mass:
30 parts of potassium feldspar, 10 parts of calcite, 10 parts of talcum, 15 parts of zinc oxide and 5 parts of titanium oxide.
The preparation method of the ceramic clay titanium series ultra-white crystal glaze comprises the following steps:
preparing a ground glaze slip and a surface glaze slip;
taking a clean clay body, applying a ground glaze by using ground glaze slurry, drying, and spraying a surface glaze by using surface glaze slurry;
then sintering in a drawer kiln at 1290 ℃; the preparation process of the ground glaze slurry and the surface glaze slurry comprises the following steps:
and (3) after the material is prepared, performing wet ball milling for 12-14 hours according to the mass ratio of glaze to ball to water of 1 to 1.6 to 0.7, and after the ball milled glaze is sieved by a 160-mesh sieve, modulating the glaze into 51-53 Baume concentration for later use.
The whiteness of the product manufactured by adopting the white mud blank according to the operation is 80% of the whiteness of blue light, the crystal diameter is about 1mm approximately, and the product does not meet the design requirement.
Comparative example No. two
A kind of ceramic clay titanium series ultra-white crystal glaze, it includes ground glaze and overglaze; wherein the content of the first and second substances,
the ground coat comprises the following components in parts by mass:
50 parts of potassium feldspar; 13 parts of dolomite; 10 parts of calcite; 15 parts of spodumene; 12 parts of rutile;
the overglaze comprises the following components in parts by mass:
35 parts of potassium feldspar, 15 parts of calcite, 15 parts of talcum, 20 parts of zinc oxide and 8 parts of titanium oxide.
The preparation method of the ceramic clay titanium series ultra-white crystal glaze comprises the following steps:
preparing a ground glaze slip and a surface glaze slip;
taking a clean clay body, applying a ground glaze by using ground glaze slurry, drying, and spraying a surface glaze by using surface glaze slurry;
then sintering in a drawer kiln at 1290 ℃; the preparation process of the ground glaze slurry and the surface glaze slurry comprises the following steps:
and (3) after the material is prepared, performing wet ball milling for 12-14 hours according to the mass ratio of glaze to ball to water of 1 to 1.6 to 0.7, and after the ball milled glaze is sieved by a 160-mesh sieve, modulating the glaze into 51-53 Baume concentration for later use.
The whiteness of the product manufactured by adopting the white mud blank according to the operation is 86% of the whiteness of blue light, the crystal diameter is about 1mm approximately, and the product does not meet the design requirement.
Example one
A kind of ceramic clay titanium series ultra-white crystal glaze, it includes ground glaze and overglaze; wherein the content of the first and second substances,
the ground coat comprises the following components in parts by mass:
40 parts of potassium feldspar; 8 parts of dolomite; 5 parts of calcite; 10 parts of spodumene; 10 parts of rutile;
the overglaze comprises the following components in parts by mass:
35 parts of potassium feldspar, 15 parts of calcite, 15 parts of talcum, 20 parts of zinc oxide and 15 parts of titanium oxide.
The preparation method of the ceramic clay titanium series ultra-white crystal glaze comprises the following steps:
preparing a ground glaze slip and a surface glaze slip;
taking a clean clay body, applying a ground glaze by using ground glaze slurry, drying, and spraying a surface glaze by using surface glaze slurry;
then sintering in a drawer kiln at 1290 ℃; the preparation process of the ground glaze slurry and the surface glaze slurry comprises the following steps:
and (3) after the material is prepared, performing wet ball milling for 12-14 hours according to the mass ratio of glaze to ball to water of 1 to 1.6 to 0.7, and after the ball milled glaze is sieved by a 160-mesh sieve, modulating the glaze into 51-53 Baume concentration for later use.
Example two
A kind of ceramic clay titanium series ultra-white crystal glaze, it includes ground glaze and overglaze; wherein the content of the first and second substances,
the ground coat comprises the following components in parts by mass:
50 parts of potassium feldspar; 13 parts of dolomite; 10 parts of calcite; 15 parts of spodumene; 12 parts of rutile;
the overglaze comprises the following components in parts by mass:
35 parts of potassium feldspar, 15 parts of calcite, 15 parts of talcum, 20 parts of zinc oxide and 15 parts of titanium oxide.
The preparation method of the ceramic clay titanium series ultra-white crystal glaze comprises the following steps:
preparing a ground glaze slip and a surface glaze slip;
taking a clean clay body, applying a ground glaze by using ground glaze slurry, drying, and spraying a surface glaze by using surface glaze slurry;
then sintering in a drawer kiln at 1290 ℃; the preparation process of the ground glaze slurry and the surface glaze slurry comprises the following steps:
and (3) after the material is prepared, performing wet ball milling for 12-14 hours according to the mass ratio of glaze to ball to water of 1 to 1.6 to 0.7, and after the ball milled glaze is sieved by a 160-mesh sieve, modulating the glaze into 51-53 Baume concentration for later use.
EXAMPLE III
A kind of ceramic clay titanium series ultra-white crystal glaze, it includes ground glaze and overglaze; wherein the content of the first and second substances,
the ground coat comprises the following components in parts by mass:
45 parts of potassium feldspar; 10 parts of dolomite; 7 parts of calcite; 12 parts of spodumene; 11 parts of rutile;
the overglaze comprises the following components in parts by mass:
32 parts of potash feldspar, 12 parts of calcite, 12 parts of talcum, 17 parts of zinc oxide and 12 parts of titanium oxide.
The preparation method of the ceramic clay titanium series ultra-white crystal glaze comprises the following steps:
preparing a ground glaze slip and a surface glaze slip;
taking a clean clay body, applying a ground glaze by using ground glaze slurry, drying, and spraying a surface glaze by using surface glaze slurry;
then sintering in a drawer kiln at 1290 ℃; the preparation process of the ground glaze slurry and the surface glaze slurry comprises the following steps:
and (3) after the material is prepared, performing wet ball milling for 12-14 hours according to the mass ratio of glaze to ball to water of 1 to 1.6 to 0.7, and after the ball milled glaze is sieved by a 160-mesh sieve, modulating the glaze into 51-53 Baume concentration for later use.
The products prepared in the first to third examples are snow white in whole, wherein blue crystals are generated, and the whiteness of blue light can reach 93 percent.
The above embodiments are described in further detail to solve the technical problems, technical solutions and advantages of the present invention, and it should be understood that the above embodiments are only examples of the present invention and are not intended to limit the present invention, and any modifications, equivalent substitutions, improvements and the like made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (2)
1. A kind of ceramic clay titanium series ultra-white crystal glaze, characterized by that it includes ground coat and overglaze; wherein the content of the first and second substances,
the ground coat comprises the following components in parts by mass:
40-50 parts of potassium feldspar; 8-13 parts of dolomite; 5-10 parts of calcite; 10-15 parts of spodumene; 10-12 parts of rutile;
the overglaze comprises the following components in parts by mass:
30 to 35 parts of potash feldspar, 10 to 15 parts of calcite, 10 to 15 parts of talcum, 15 to 20 parts of zinc oxide and 10 to 15 parts of titanium oxide.
2. The method for preparing the ceramic clay titanium-based ultra-white crystalline glaze according to claim 1, which is characterized by comprising the following steps:
preparing a ground glaze slip and a surface glaze slip;
taking a clean clay body, applying a ground glaze by using ground glaze slurry, drying, and spraying a surface glaze by using surface glaze slurry;
then sintering in a drawer kiln at 1290 ℃; the preparation process of the ground glaze slurry and the surface glaze slurry comprises the following steps:
and (3) after the material is prepared, performing wet ball milling for 12-14 hours according to the mass ratio of glaze to ball to water of 1 to 1.6 to 0.7, and after the ball milled glaze is sieved by a 160-mesh sieve, modulating the glaze into 51-53 Baume concentration for later use.
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| CN101306958A (en) * | 2008-07-03 | 2008-11-19 | 湖南省醴陵市楚华陶瓷实业有限公司 | Method of making crystal fancy glaze |
| CN104016719A (en) * | 2014-05-13 | 2014-09-03 | 醴陵陶润实业发展有限公司 | Reactive crystalline glaze with sagging effect and preparation method of reactive crystalline glaze |
| CN104609899A (en) * | 2014-12-25 | 2015-05-13 | 醴陵陶润实业发展有限公司 | Gathering and flowing diffusion glaze with crystals and preparation method of gathering and flowing diffusion glaze |
| CN108706875A (en) * | 2018-07-14 | 2018-10-26 | 醴陵陶润实业发展有限公司 | Double-deck brilliant glaze of blue stream and preparation method thereof |
| CN109265004A (en) * | 2018-12-15 | 2019-01-25 | 醴陵陶润实业发展有限公司 | Sea blue double-deck reaction glaze and preparation method thereof |
| CN109912215A (en) * | 2017-12-13 | 2019-06-21 | 程莉 | Gold-decorated furnace transmutation glaze of black matrix and preparation method thereof |
| CN110790506A (en) * | 2019-12-18 | 2020-02-14 | 湖南华联瓷业股份有限公司 | Granular double-layer reaction glaze and preparation method thereof |
-
2020
- 2020-09-10 CN CN202010946277.9A patent/CN112174523A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101306958A (en) * | 2008-07-03 | 2008-11-19 | 湖南省醴陵市楚华陶瓷实业有限公司 | Method of making crystal fancy glaze |
| CN104016719A (en) * | 2014-05-13 | 2014-09-03 | 醴陵陶润实业发展有限公司 | Reactive crystalline glaze with sagging effect and preparation method of reactive crystalline glaze |
| CN104609899A (en) * | 2014-12-25 | 2015-05-13 | 醴陵陶润实业发展有限公司 | Gathering and flowing diffusion glaze with crystals and preparation method of gathering and flowing diffusion glaze |
| CN109912215A (en) * | 2017-12-13 | 2019-06-21 | 程莉 | Gold-decorated furnace transmutation glaze of black matrix and preparation method thereof |
| CN108706875A (en) * | 2018-07-14 | 2018-10-26 | 醴陵陶润实业发展有限公司 | Double-deck brilliant glaze of blue stream and preparation method thereof |
| CN109265004A (en) * | 2018-12-15 | 2019-01-25 | 醴陵陶润实业发展有限公司 | Sea blue double-deck reaction glaze and preparation method thereof |
| CN110790506A (en) * | 2019-12-18 | 2020-02-14 | 湖南华联瓷业股份有限公司 | Granular double-layer reaction glaze and preparation method thereof |
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