CN112159199A - Hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent and preparation method thereof - Google Patents
Hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent and preparation method thereof Download PDFInfo
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- CN112159199A CN112159199A CN201910589880.3A CN201910589880A CN112159199A CN 112159199 A CN112159199 A CN 112159199A CN 201910589880 A CN201910589880 A CN 201910589880A CN 112159199 A CN112159199 A CN 112159199A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/24—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing alkyl, ammonium or metal silicates; containing silica sols
- C04B28/26—Silicates of the alkali metals
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/27—Water resistance, i.e. waterproof or water-repellent materials
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
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Abstract
The invention relates to a hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent, a preparation method and application thereof, wherein the multifunctional waterproof agent comprises the following raw materials: the component A comprises: purified water, sodium silicate, a catalyst, a pure acrylic emulsion, a dispersing agent, a defoaming agent, a pigment filler, hydroxyethyl cellulose, hydroxyl-terminated polysiloxane and fluorine-containing polyether polyol; the component B comprises: inorganic thixotropic thickener, surfactant, mildew preventive, film forming additive, plasticizer, ammonia water, kaolin, coarse whiting powder and titanium pigment. The hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent has extremely high adhesive force, can generate a hydrophobic chemical bond and generate esterification reaction to enable emulsion to be crosslinked into a film, greatly improves the waterproof and hot water-proof performances of the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent, has excellent heat insulation and light reflection performances, is environment-friendly and safe, has flexible coating, is not easy to crack, has strong adhesive force and covering power, is low in cost and long in service life, and has wide application prospect.
Description
Technical Field
The invention belongs to the technical field of coatings, and particularly relates to a hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent, and a preparation method and application thereof.
Background
The waterproof material is as follows: the material adopted by the living structure of the building to meet the functions of moisture prevention, seepage prevention and leakage prevention becomes the building waterproof material. In the house decoration process, waterproof treatment is carried out on the use places such as kitchens, toilets and the like as long as water environments exist frequently. The use of the multifunctional waterproof agent of hexagonal matrix self-repairing infiltration crystallization not only relates to the integral effect of house decoration, but also is closely related to the health of residents. The waterproof treatment is a 'hidden project' in decoration, and the effect of the waterproof treatment can be presented after a long service life. If the multifunctional waterproof agent of the hexagonal matrix self-repairing permeable crystallization contains toxicity and is not waterproof completely, the multifunctional waterproof agent becomes an invisible killer in the house. Therefore, the choice of waterproof material is not negligible. The main objects of waterproofing in construction engineering are: more than 90 percent of the concrete structure is formed. The sealing and waterproof effects of common materials and concrete are difficult to achieve under the complex characteristics.
Disclosure of Invention
The invention aims to provide a hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent.
The invention relates to a hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent which comprises the following raw materials in parts by weight: the component A comprises: 0.8 to 1.2 portions of purified water, 0.2 to 0.3 portion of sodium silicate, 0.08 to 0.09 portion of catalyst, 1.5 to 6.8 portions of pure acrylic emulsion, 1 to 5 portions of dispersant, 2 to 4 portions of defoaming agent, 0.5 to 3 portions of pigment and filler, 1 to 8 portions of hydroxyethyl cellulose, 4 to 15 portions of hydroxyl-terminated polysiloxane and 1 to 10 portions of fluorine-containing polyether polyol; the component B comprises: 1 to 8 portions of inorganic thixotropic thickener, 2 to 10 portions of surfactant, 1 to 5 portions of mildew inhibitor, 3 to 7 portions of film-forming assistant, 1 to 10 portions of plasticizer, 0.1 to 1 portion of ammonia water, 5 to 10 portions of kaolin, 20 to 30 portions of heavy calcium powder and 2 to 5 portions of titanium pigment.
The hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent has high adhesive force, can generate a hydrophobic chemical bond and generate esterification reaction to enable emulsion to be crosslinked into a film, greatly improves the waterproof and hot water-proof performances of the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent, is stable in component, convenient to store, excellent in heat insulation and light reflection performance, environment-friendly and safe, flexible in coating, not easy to crack, strong in adhesive force and covering power, low in cost, long in service life and wide in application prospect.
In addition, the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent disclosed by the invention can also have the following additional technical characteristics:
as a preferred embodiment of the invention, the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent comprises the following raw materials in parts by weight: the component A comprises: 0.8 part of purified water, 0.3 part of sodium silicate, 0.08 part of catalyst, 6.8 parts of pure acrylic emulsion, 1 part of dispersant, 4 parts of defoaming agent, 0.5 part of pigment and filler, 8 parts of hydroxyethyl cellulose, 4 parts of hydroxyl-terminated polysiloxane and 10 parts of fluorine-containing polyether polyol; the component B comprises: 1 part of inorganic thixotropic thickener, 10 parts of surfactant, 1 part of mildew inhibitor, 7 parts of film-forming assistant, 1 part of plasticizer, 1 part of ammonia water, 5 parts of kaolin, 30 parts of heavy calcium powder and 2 parts of titanium dioxide.
As a preferred embodiment of the invention, the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent comprises the following raw materials in parts by weight: the component A comprises: 1.2 parts of purified water, 0.2 part of sodium silicate, 0.09 part of catalyst, 1.5 parts of pure acrylic emulsion, 5 parts of dispersant, 2 parts of defoaming agent, 3 parts of pigment and filler, 1 part of hydroxyethyl cellulose, 15 parts of hydroxyl-terminated polysiloxane and 1 part of fluorine-containing polyether polyol; the component B comprises: 8 parts of inorganic thixotropic thickener, 2 parts of surfactant, 5 parts of mildew preventive, 3 parts of film-forming additive, 10 parts of plasticizer, 0.1 part of ammonia water, 10 parts of kaolin, 20 parts of heavy calcium powder and 5 parts of titanium dioxide.
As a preferred embodiment of the invention, the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent comprises the following raw materials in parts by weight: the component A comprises: 1 part of purified water, 0.25 part of sodium silicate, 0.085 part of catalyst, 4 parts of pure acrylic emulsion, 2.5 parts of dispersing agent, 3 parts of defoaming agent, 1.75 parts of pigment and filler, 4 parts of hydroxyethyl cellulose, 9 parts of hydroxyl-terminated polysiloxane and 5 parts of fluorine-containing polyether polyol; the component B comprises: 4 parts of inorganic thixotropic thickener, 6 parts of surfactant, 2.5 parts of mildew preventive, 5 parts of film-forming additive, 5 parts of plasticizer, 0.5 part of ammonia water, 7.5 parts of kaolin, 25 parts of heavy calcium powder and 3.5 parts of titanium dioxide.
The invention also aims to provide a preparation method of the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent.
The preparation method of the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent comprises the following steps: s101: mixing and stirring the raw materials of the component A, heating to 40-60 ℃, stirring for 15-30 min, filtering and collecting filtrate; s102: and mixing the inorganic thixotropic thickener, the surfactant, the mildew preventive, the film forming aid and the plasticizer in the component B, adding the mixture into the product obtained in the step S101, stirring for 10-20 min, then reducing the temperature to room temperature, and adding the rest raw material components to obtain the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent.
Furthermore, the rotating speed during stirring is 500r/min to 3000 r/min.
Furthermore, the aperture of the filter screen adopted during the filtration is 1 nm-100 nm.
The invention further aims to provide application of the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent in the field of buildings.
Additional aspects and advantages of the invention will be set forth in part in the description which follows and, in part, will be obvious from the description, or may be learned by practice of the invention.
Detailed Description
The following detailed description of embodiments of the invention is intended to be illustrative, and not to be construed as limiting the invention.
Example 1
Embodiment 1 provides a hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent, which comprises the following raw materials in parts by weight: the component A comprises: 0.8 part of purified water, 0.3 part of sodium silicate, 0.08 part of catalyst, 6.8 parts of pure acrylic emulsion, 1 part of dispersant, 4 parts of defoaming agent, 0.5 part of pigment and filler, 8 parts of hydroxyethyl cellulose, 4 parts of hydroxyl-terminated polysiloxane and 10 parts of fluorine-containing polyether polyol; the component B comprises: 1 part of inorganic thixotropic thickener, 10 parts of surfactant, 1 part of mildew inhibitor, 7 parts of film-forming assistant, 1 part of plasticizer, 1 part of ammonia water, 5 parts of kaolin, 30 parts of heavy calcium powder and 2 parts of titanium dioxide.
The preparation method of the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent of the embodiment 1 comprises the following steps:
(1) mixing and stirring the raw materials of the component A, heating to 40 ℃, stirring for 15min at the rotating speed of 3000r/min, filtering by using a filter screen with the aperture of 100nm, and collecting filtrate.
(2) And (2) mixing and adding the inorganic thixotropic thickener, the surfactant, the mildew preventive, the film forming aid and the plasticizer in the component B into the product obtained in the step (1), stirring at the rotating speed of 500r/min for 20min, then reducing the temperature to room temperature, and adding the rest raw material components to obtain the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent.
Example 2
Embodiment 2 provides a hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent, which comprises the following raw materials in parts by weight: the component A comprises: 1.2 parts of purified water, 0.2 part of sodium silicate, 0.09 part of catalyst, 1.5 parts of pure acrylic emulsion, 5 parts of dispersant, 2 parts of defoaming agent, 3 parts of pigment and filler, 1 part of hydroxyethyl cellulose, 15 parts of hydroxyl-terminated polysiloxane and 1 part of fluorine-containing polyether polyol; the component B comprises: 8 parts of inorganic thixotropic thickener, 2 parts of surfactant, 5 parts of mildew preventive, 3 parts of film-forming additive, 10 parts of plasticizer, 0.1 part of ammonia water, 10 parts of kaolin, 20 parts of heavy calcium powder and 5 parts of titanium dioxide.
The preparation method of the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent of the embodiment 2 comprises the following steps:
(1) mixing and stirring the raw materials of the component A, heating to 60 ℃, stirring for 30min at the rotating speed of 500r/min, filtering by using a filter screen with the aperture of 1nm, and collecting filtrate.
(2) And (2) mixing and adding the inorganic thixotropic thickener, the surfactant, the mildew preventive, the film forming aid and the plasticizer in the component B into the product obtained in the step (1), stirring at the rotating speed of 3000r/min for 10min, then reducing the temperature to room temperature, and adding the rest raw material components to obtain the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent.
Example 3
Embodiment 3 provides a hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent, which comprises the following raw materials in parts by weight: 1 part of purified water, 0.25 part of sodium silicate, 0.085 part of catalyst, 4 parts of pure acrylic emulsion, 2.5 parts of dispersing agent, 3 parts of defoaming agent, 1.75 parts of pigment and filler, 4 parts of hydroxyethyl cellulose, 9 parts of hydroxyl-terminated polysiloxane and 5 parts of fluorine-containing polyether polyol; the component B comprises: 4 parts of inorganic thixotropic thickener, 6 parts of surfactant, 2.5 parts of mildew preventive, 5 parts of film-forming additive, 5 parts of plasticizer, 0.5 part of ammonia water, 7.5 parts of kaolin, 25 parts of heavy calcium powder and 3.5 parts of titanium dioxide.
The preparation method of the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent of the embodiment 3 comprises the following steps:
(1) mixing and stirring the raw materials of the component A, heating to 50 ℃, stirring at the rotation speed of 1800r/min for 22min, filtering by using a filter screen with the aperture of 50nm, and collecting filtrate.
(2) And (2) mixing and adding the inorganic thixotropic thickener, the surfactant, the mildew preventive, the film forming aid and the plasticizer in the component B into the product obtained in the step (1), stirring at the rotating speed of 2200r/min for 15min, then reducing the temperature to room temperature, and adding the rest raw material components to obtain the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent.
In conclusion, the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent has high adhesive force, can generate hydrophobic chemical bonds and generate esterification reaction to enable emulsion to be crosslinked into a film, greatly improves the waterproof and hot water-proof performances of the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent, is stable in components, convenient to store, excellent in heat insulation and light reflection performance, environment-friendly and safe, flexible in coating, difficult to crack, strong in adhesive force and covering power, low in cost, long in service life and wide in application prospect.
In the description herein, references to the description of the term "one embodiment," "some embodiments," "an example," "a specific example," or "some examples," etc., mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the invention. In this specification, the schematic representations of the terms used above are not necessarily intended to refer to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples. Furthermore, various embodiments or examples and features of different embodiments or examples described in this specification can be combined and combined by one skilled in the art without contradiction.
Although embodiments of the present invention have been shown and described above, it is understood that the above embodiments are exemplary and should not be construed as limiting the present invention, and that variations, modifications, substitutions and alterations can be made to the above embodiments by those of ordinary skill in the art within the scope of the present invention.
Claims (8)
1. The multifunctional waterproof agent is characterized by comprising the following raw materials in parts by weight:
the component A comprises: 0.8 to 1.2 portions of purified water, 0.2 to 0.3 portion of sodium silicate, 0.08 to 0.09 portion of catalyst, 1.5 to 6.8 portions of pure acrylic emulsion, 1 to 5 portions of dispersant, 2 to 4 portions of defoaming agent, 0.5 to 3 portions of pigment and filler, 1 to 8 portions of hydroxyethyl cellulose, 4 to 15 portions of hydroxyl-terminated polysiloxane and 1 to 10 portions of fluorine-containing polyether polyol;
the component B comprises: 1 to 8 portions of inorganic thixotropic thickener, 2 to 10 portions of surfactant, 1 to 5 portions of mildew inhibitor, 3 to 7 portions of film-forming assistant, 1 to 10 portions of plasticizer, 0.1 to 1 portion of ammonia water, 5 to 10 portions of kaolin, 20 to 30 portions of heavy calcium powder and 2 to 5 portions of titanium pigment.
2. The hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent of claim 1, which is characterized by comprising the following raw materials in parts by weight:
the component A comprises: 0.8 part of purified water, 0.3 part of sodium silicate, 0.08 part of catalyst, 6.8 parts of pure acrylic emulsion, 1 part of dispersant, 4 parts of defoaming agent, 0.5 part of pigment and filler, 8 parts of hydroxyethyl cellulose, 4 parts of hydroxyl-terminated polysiloxane and 10 parts of fluorine-containing polyether polyol;
the component B comprises: 1 part of inorganic thixotropic thickener, 10 parts of surfactant, 1 part of mildew inhibitor, 7 parts of film-forming assistant, 1 part of plasticizer, 1 part of ammonia water, 5 parts of kaolin, 30 parts of heavy calcium powder and 2 parts of titanium dioxide.
3. The hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent of claim 1, which is characterized by comprising the following raw materials in parts by weight:
the component A comprises: 1.2 parts of purified water, 0.2 part of sodium silicate, 0.09 part of catalyst, 1.5 parts of pure acrylic emulsion, 5 parts of dispersant, 2 parts of defoaming agent, 3 parts of pigment and filler, 1 part of hydroxyethyl cellulose, 15 parts of hydroxyl-terminated polysiloxane and 1 part of fluorine-containing polyether polyol;
the component B comprises: 8 parts of inorganic thixotropic thickener, 2 parts of surfactant, 5 parts of mildew preventive, 3 parts of film-forming additive, 10 parts of plasticizer, 0.1 part of ammonia water, 10 parts of kaolin, 20 parts of heavy calcium powder and 5 parts of titanium dioxide.
4. The hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent of claim 1, which is characterized by comprising the following raw materials in parts by weight:
the component A comprises: 1 part of purified water, 0.25 part of sodium silicate, 0.085 part of catalyst, 4 parts of pure acrylic emulsion, 2.5 parts of dispersing agent, 3 parts of defoaming agent, 1.75 parts of pigment and filler, 4 parts of hydroxyethyl cellulose, 9 parts of hydroxyl-terminated polysiloxane and 5 parts of fluorine-containing polyether polyol;
the component B comprises: 4 parts of inorganic thixotropic thickener, 6 parts of surfactant, 2.5 parts of mildew preventive, 5 parts of film-forming additive, 5 parts of plasticizer, 0.5 part of ammonia water, 7.5 parts of kaolin, 25 parts of heavy calcium powder and 3.5 parts of titanium dioxide.
5. The preparation method of the hexagonal matrix self-repairing permeable crystalline multifunctional waterproof agent as claimed in any one of claims 1 to 4, characterized by comprising the following steps:
s101: mixing and stirring the raw materials of the component A, heating to 40-60 ℃, stirring for 15-30 min, filtering and collecting filtrate;
s102: and mixing the inorganic thixotropic thickener, the surfactant, the mildew preventive, the film forming aid and the plasticizer in the component B, adding the mixture into the product obtained in the step S101, stirring for 10-20 min, then reducing the temperature to room temperature, and adding the rest raw material components to obtain the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent.
6. The preparation method of the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent as claimed in claim 5, wherein the rotation speed during stirring is 500r/min to 3000 r/min.
7. The preparation method of the hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent as claimed in claim 5, wherein the aperture of a filter screen adopted during filtering is 1 nm-100 nm.
8. The application of the hexagonal matrix self-repairing permeable crystalline multifunctional waterproof agent disclosed by any one of claims 1 to 7 in the field of construction.
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| CN201910589880.3A CN112159199A (en) | 2019-07-02 | 2019-07-02 | Hexagonal matrix self-repairing permeable crystallization multifunctional waterproof agent and preparation method thereof |
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