CN101831229A - Hollow microsphere thermal insulation coating and production method thereof - Google Patents
Hollow microsphere thermal insulation coating and production method thereof Download PDFInfo
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Abstract
The invention relates to a hollow microsphere thermal insulation coating which is prepared by mixing the following raw materials in parts by weight: 140-160 parts of water, 0.5-1.5 parts of sterilizing agent, 1-2 parts of mildew preventive, 5-7 parts of dispersing agent, 2-6 parts of antifoaming agent, 1-2 parts of pH regulating agent, 18-22 parts of ethylene glycol, 1-2 parts of wetting agent, 18-22 parts of film-forming auxiliary, 45-55 parts of mica powder, 90-110 parts of pigment, 190-210 parts of hollow glass cenosphere, 45-55 parts of covering polymer, 390-410 parts of base stock and 6-10 parts of thickening agent. The production method comprises the steps of: preparing materials, premixing, dispersing at high speed, dispersing hollow microsphere and mixing coating. The produced coating has the advantages of difficult ageing, difficult shedding, fireproof and seepage-proofing properties and integration of thermal insulation, fire prevention, corrosion resistance and water prevention, and is especially suitable for coating roof, floor and equipment surface needing thermal insulation in buildings and external wall bodies.
Description
Technical field
The present invention relates to a kind of inner, external wall coating for building, be specially insulating mold coating and production method thereof with stopping property high porosity.
Background technology
People live or the active indoor environment, the same requirements that the cold of winter-warm syndrome summer is all arranged, border on the river, the homestead of adjacent mountain, sylvan life is selected, the building of thatched cottage, one of purpose wherein also is for realizing the demand of winter-warm syndrome summer cold, inconvenient for selecting house site, how to work hard in transformation materials for wall and architectural design, more be to adopt air-conditioning to realize the cold of winter-warm syndrome summer, and rarely seen the innovation from coating addresses the report of cool environmental problem of winter-warm syndrome summer within doors.CN200910085967.3 discloses the patented technology of " reflective heat-insulation paint and preparation method thereof ", has made good trial, gives society with useful contribution.
Summary of the invention
The approach that solves cool demand of indoor winter-warm syndrome summer is a lot, but what have has many difficulties and unfavorable, as the restriction of selecting homestead ploughed by country of origin and control, the trouble that the lid thatched cottage is subjected to raw material and leakproof and overhauls, wall reconstruction and architectural design need have high-tech to support, the very big power consumption of air-conditioning meeting, at these realistic problems, the technical problem to be solved in the present invention provides a kind of hollow microsphere thermal insulation coating and production method thereof, the coating of producing with present method to the application of inner, external wall body after, can improve the environment of indoor winter-warm syndrome summer cold.
The technical scheme that solves the problems of the technologies described above is: this coating is mixed by following raw material and weight part thereof and forms: 140-160 part process water, 0.5-1.5 part K20 sterilant 1-2 part DF19 mould inhibitor 5-7 part is as the 112D modified polypropene acid ammonium salt of dispersion agent, 1-3 part NXZ mineral oil antifoam agent, 1-2 part is a 2-amino-2-methyl propyl alcohol as the AMP-95 of pH regulator agent, 18-22 part is as the ethylene glycol of frostproofer, 1-2 part is as the PE-100 nonionic surface active agent of wetting agent, 18-22 part is as the Yi Shiman lauryl alcohol ester of film coalescence aid, 45-55 part is as 1250 order sericites in powder of filler, 90-110 part is as the R-969 titanium dioxide of pigment, 190-210 part is as the hollow glass microbead of filler, 45-55 part OP-62B opacity polymer, 390-410 part is as the pure acrylic resin emulsion of base-material, 1-3 part 681F mineral oil antifoam agent, 3-5 part associative thickener and 3-5 part polyurethane thickener.
The production method of this hollow microsphere thermal insulation coating is through following steps:
(1) following raw materials according is prepared enough in calculating by weight: 140-160 part process water, buy 0.5-1.5 part K20 sterilant and 1-2 part DF19 mould inhibitor to German Shu Mei company, buy 5-7 part 112D modified polypropene acid ammonium salt to U.S. Rhom and Hass, buy NXZ mineral oil antifoam agent 1-3 part to Japanese Nuo Puke company, buy AMP-95pH conditioning agent 1-2 part to U.S. Anguds company and buy antifreeze glycol 18-22 part to the industrial and commercial shop of domestication, buy 1-2 part PE-100 nonionic surface active agent to U.S. Kening Co.,Ltd, buy 18-22 part lauryl alcohol ester to U.S. Yi Shi Man, buy 45-55 part 1250 purpose sericites in powder to the industrial and commercial shop of domestication, buy 90-110 part R-969 titanium dioxide to Jiangsu town titanium titanium white company, buy 1250 orders-2500 purpose hollow glass microbead 190-210 part to the industrial and commercial shop of domestication and buy 45-55 part OP-62B opacity polymer to U.S. Rhom and Hass, buy 390-410 part BLJ-961 type pure acrylic resin emulsion to Shanghai Bao Lijia chemical industry company limited, buy 681F mineral oil antifoam agent 1-3 part to French Rhodia, buy 3-5 part associative thickener and 3-5 part polyurethane thickener to Shenzhen Hai Chuan chemical industry company limited;
(2) pre-mixing: earlier 140-160 part water, 5-7 part 112D modified polypropene acid ammonium salt 1-3 part NXZ mineral oil antifoam agent, 90-110 part R-969 titanium dioxide, 45-55 part sericite in powder, 3-5 part 3351 type associative thickeners are added successively premix in the dispersion cylinder of dispersion machine, stir 5-10min by (300-400) r/min rotating speed;
(3) high speed dispersion: regulate rotating speed to (1200-1500) r/min, under high-speed stirring, disperse 20-30min, pigment and filler grain are dispersed into simple particle under the high shear rate effect, add 2-3 part 3256 type polyurethane thickening materials, be adjusted to rotating speed and disperse 5-8min for the middling speed of (900-1100) r/min;
(4) hollow beads is disperseed: when pigment and filler reach the requirement fineness, add 390-410 part cinnamic acid resin emulsion 3/5 amount, add 190-210 part hollow glass microbead at a slow speed, continue the rotating speed of (900-1100) r/min, disperse 10-15min;
(5) paint: add remaining 2/5 cinnamic acid resin emulsion, 1-3 part 681F mineral oil antifoam agent, 1-2 part AMP-95pH conditioning agent, 1-2 part 3256 type polyurethane thickening materials, 0.5-1.5 part K20 sterilant, 1-2 part DF19 mould inhibitor, 18-22 part ethylene glycol, 1-2 part PE-100 wetting agent, 18-22 part lauryl alcohol ester, 45-55 part OP-62B opacity polymer, this process meets to be coated with the heavy viscosity of (300-400) r/min stirring at low speed 5-10min in the paint cylinder ends 4 glasss of 70-85 seconds, check, discharging, barreled.
The invention has the beneficial effects as follows the wall heat insulation material that adopts many Inorganic Chemicals and select specific function for use, make the coating of stopping property high porosity, overcome organic polyphenyl class lagging material easily aging, inflammable, come off and deficiency such as infiltration, integrate heat insulation, insulation, fire prevention, anticorrosion and water-fast.
Embodiment
The present invention does further commentary below in conjunction with embodiment: earlier each raw material and weight part thereof are listed as follows by eight embodiment:
In the last table there be material name with being called for short (down with), and wherein to be 112D modified propylene acid ammonium salt, NXZ defoamer be that NXZ mineral oil antifoam agent PE-100 wetting agent is that PE-100 nonionic surface active agent, OP-62B covering agent are OP-62B and hide that resin, pure propyl group material are the pure acrylic resin emulsion, the 681F defoamer is the 681F mineral oil antifoam agent to the 112D dispersion agent.
Embodiment 1 (in the contrast table in embodiment 1 corresponding raw material and weight part proportioning value): earlier 150 parts of water, 6 parts of 112D dispersion agents, 2 parts of NXZ defoamers, 100 parts of R-969 titanium dioxides, 50 parts of sericites in powder, 4 parts of associative thickeners are joined successively in the dispersion cylinder of dispersion machine and stir pre-mixing 5-10min by (300-400) r/min rotating speed; Heighten rotating speed again to (1200-1500) r/min high speed dispersion 20-30min, pigment is become simple particle with fillers dispersed, 2.5 parts of polyurethane thickeners during elder generation adds 4 parts, speed governing to (900-1100) r/min middling speed is disperseed 5-8min again; About 240 parts of pure propyl group material in adding 400 parts earlier then add 200 parts of hollow glass microbeads more at a slow speed, continue (900-1100) r/min rotating speed and disperse 10-15min; Carry out paint at last, add remaining i.e. 160 parts of pure propyl group material, 2 parts of 681F defoamers, 1.5 parts of AMP-95, remaining i.e. 1.5 parts of polyurethane thickeners, 1 part of sterilant, 1.5 parts of mould inhibitors, 20 parts of ethylene glycol, 1.5 parts of PE-100 wetting agents, 20 parts of lauryl alcohol esters, 50 parts of OP-62B covering agents, this process is carried out in the paint cylinder, reach to be coated with to viscosity with (300-400) r/min stirring at low speed 5-10min and end four glasss of 70-85 seconds, check, discharging, barreled.
Raw material and weight part proportioning value thereof and embodiment 1 are with legal system cost coating in the equal synopsis of all the other embodiment 2-8.Preferred among eight embodiment with embodiment 1.
This hollow microsphere thermal insulation coating is a kind of speciality coating that contains hollow glass microbead, integrates heat insulation, insulation, fire prevention, anticorrosion, water-fast function.Disadvantages such as organic polyphenyl class heat-insulation system is easily aging, inflammable, the infiltration that comes off, comes off have been overcome.
The alternative metope polyphenyl of this coating heat insulation system carries out application to building inside and outside metope, can effectively prevent phenomenons such as " heat bridge " and " dewfall, hang frost, " workability difference, and it is little to take up room, and is widely used in the owned building metope.Heat insulating on roofing, ground and the equipment surface uses.
Now the insulation mechanism with coating is described below: in this coating in the high porosity airtight air vent low heat conductivity of still air reach the purpose of insulation.After metope is coated certain thickness hollow beads thermal insulation coatings, wall heat resistance is significantly improved, thereby play the heat-insulation and heat-preservation effect.Because the diameter of hollow beads is little of the micron number magnitude, make the air molecule in the pore convection current can not carry out pedesis again, in fact such pore is equivalent to vacuum state, can make thus to be coated with membrane molecule convection heat transfer coefficient and to level off to zero.And such micropore can make material internal that considerable reflecting interface is arranged, and the radiative transfer effect is gone to zero, and this thermal conductivity of filming is just near zero in theory.
This coating has following premium properties:
(1) fire-retardant, possess high-quality fire protecting performance.
Because the product that most of filler of adopting of this product all is inorganic material, hollow glass microbead and auxiliary agent etc. mixes crosslinked rear generation high heat stabilities, by incombustible material (A level) standard testing among the GB8624-1997 " Classification on burning behaviour for building materials ", when fire takes place, not only do not have naked light but also do not produce thick smoke, do not cause harm, be the first-selected quality material of Building Fire Protection.
(2) superpower chemical stability.
Acid-alkali-corrosive-resisting, ultraviolet-resistant aging not only is suitable for various facing mortars, water paint, and can spray various solvent-borne type facings paint, emulsion paint, stone similar paint, fluorine carbon lacquer etc., also direct wall tile, all extra construction processing.
(3) environment protection health, green product, interior wall face, roofing, all can be equally suitable.
This product does not contain volatile organic matter and other hazardous compound, all can environment can not worked the mischief to workmen's health in production and the construction, and be Green Product.
(4) have the energy saving space of potentiality, coating layer thickness only needs 3mm.
The heat insulation effect test: 20 ℃ of indoor environment temperatures, the outer coating thickness 3mm of iron sheet test tank, the test tank heating-up temperature is 80 ℃ of constant temperature water baths, water temperature inside is all the time low more than 10 ℃ than the external world. Coating is more thick, and heat insulating effect is more good.
(5) construction is simple, only needs spray mo(u)lding to get final product.
(6) durable for a long time, than long 5 times of polyphenyl class heat-insulation system life-span.
(7) insulation is disconnected hot, heat insulation, energy-conservation, cost performance is excellent.
(8) sound insulation is every dry, and hollow beads has the good sound absorption ability.
(9) unit weight is light, low-consuming, and density＜0.9kg/L is bigger than the spray area that waits heavy common coating.
Claims (2)
1. hollow microsphere thermal insulation coating, it is characterized in that being mixed by following raw material and weight part thereof forms: 140-160 part process water, 0.5-1.5 part K20 sterilant, 1-2 part DF19 mould inhibitor, 5-7 part is as the 112D modified polypropene acid ammonium salt of dispersion agent, 1-3 part NXZ mineral oil antifoam agent, 1-2 part is a 2-amino-2-methyl propyl alcohol as the AMP-95 of pH regulator agent, 18-22 part is as the ethylene glycol of frostproofer, 1-2 part is as the PE-100 nonionic surface active agent of wetting agent, 18-22 part is as the Yi Shiman lauryl alcohol ester of film coalescence aid, 45-55 part is as 1250 order sericites in powder of filler, 90-110 part is as the R-969 titanium dioxide of pigment, 190-210 part is as the hollow glass microbead of filler, 45-55 part OP-62B opacity polymer, 390-410 part is as the pure acrylic resin emulsion of base-material, 1-3 part 681F mineral oil antifoam agent, 3-5 part associative thickener and 3-5 part polyurethane thickener.
2. the production method of hollow microsphere thermal insulation coating as claimed in claim 1 is characterized in that through following steps:
(1) following raw materials according is prepared enough in calculating by weight: 140-160 part process water, buy 0.5-1.5 part K20 sterilant and 1-2 part DF19 mould inhibitor to German Shu Mei company, buy 5-7 part 112D modified polypropene acid ammonium salt to U.S. Rhom and Hass, buy NXZ mineral oil antifoam agent 1-3 part to Japanese Nuo Puke company, buy AMP-95pH conditioning agent 1-2 part to U.S. Anguds company, buy antifreeze glycol 18-22 part to the industrial and commercial shop of domestication, buy 1-2 part PE-100 nonionic surface active agent to U.S. Kening Co.,Ltd, buy 18-22 part lauryl alcohol ester to U.S. Yi Shi Man, buy 45-55 part 1250 purpose sericites in powder to the industrial and commercial shop of domestication, buy 90-110 part R-969 titanium dioxide to Jiangsu town titanium titanium white company, buy 1250-2500 purpose hollow glass microbead 190-210 part to the industrial and commercial shop of domestication, buy 45-55 part OP-62B opacity polymer to U.S. Rhom and Hass, buy 390-410 part BLJ-961 type pure acrylic resin emulsion to Shanghai Bao Lijia chemical industry company limited, buy 681F mineral oil antifoam agent 1-3 part to French Rhodia, buy 3-5 part associative thickener and 3-5 part polyurethane thickener to Shenzhen Hai Chuan chemical industry company limited;
(2) pre-mixing: earlier 140-160 part water, 5-7 part 112D modified polypropene acid ammonium salt, 1-3 part NXZ mineral oil antifoam agent, 90-110 part R-969 titanium dioxide, 45-55 part sericite in powder, 3-5 part 3351 type associative thickeners are added successively premix in the dispersion cylinder of dispersion machine, stir 5-10min by (300-400) r/min rotating speed;
(3) high speed dispersion: regulate rotating speed to (1200-1500) r/min, under high-speed stirring, disperse 20-30min, pigment and filler grain are dispersed into simple particle under the high shear rate effect, add 2-3 part 3256 type polyurethane thickening materials, be adjusted to rotating speed and disperse 5-8min for the middling speed of (900-1100) r/min;
(4) hollow beads is disperseed: when pigment and filler reach the requirement fineness, add 390-410 part cinnamic acid resin emulsion 3/5 amount, add 190-210 part hollow glass microbead at a slow speed, continue the rotating speed of (900-1100) r/min, disperse 10-15min;
(5) paint: add remaining 2/5 cinnamic acid resin emulsion, 1-3 part 681F mineral oil antifoam agent, 1-2 part AMP-95 conditioning agent, 1-2 part 3256 type polyurethane thickening materials, 0.5-1.5 part K20 sterilant, 1-2 part DF19 mould inhibitor, 18-22 part ethylene glycol, 1-2 part PE-100 wetting agent, 18-22 part lauryl alcohol ester, 45-55 part OP-62B opacity polymer, this process meets to be coated with the heavy viscosity of (300-400) r/min stirring at low speed 5-10min in the paint cylinder ends 4 glasss of 70-85 seconds, check, discharging, barreled.
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Cited By (13)
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| CN101967339A (en) * | 2010-09-30 | 2011-02-09 | 苏州新海宜通信科技股份有限公司 | Anti-solar radiation spraying coating used for surface of outdoor communication equipment |
| CN102249708A (en) * | 2011-05-16 | 2011-11-23 | 西南科技大学 | Preparation method for anti-corrosion and flameproof integrated coating for thick-type steel structure |
| CN102329545A (en) * | 2011-10-17 | 2012-01-25 | 青岛爱尔家佳新材料有限公司 | Waterborne external thermal insulation coating and preparation method thereof |
| CN102690559A (en) * | 2012-05-24 | 2012-09-26 | 北京国泰瑞华精藻硅特种材料有限公司 | Aqueous heat-insulating anticorrosive paint |
| CN103173079A (en) * | 2013-02-26 | 2013-06-26 | 安徽真信涂料有限公司 | Exterior wall coating material of high-stability paint film and preparation method of exterior wall coating material |
| CN104073113A (en) * | 2013-03-29 | 2014-10-01 | 关西涂料株式会社 | Heat insulation delustering paint composition and heat insulation delustering coating forming method |
| CN105062167A (en) * | 2015-08-06 | 2015-11-18 | 天长市巨龙车船涂料有限公司 | Thermal-insulation scrub-resistant emulsion paint containing plant component and preparation method thereof |
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| CN106010017A (en) * | 2016-08-01 | 2016-10-12 | 安庆瑞泰化工有限公司 | Thermal insulation water-based coating and preparation method thereof |
| CN106752631A (en) * | 2016-12-19 | 2017-05-31 | 英德科迪颜料技术有限公司 | A kind of aqueous self-clean type Graphene modified nano heat-insulating reflective coating |
| CN109415580A (en) * | 2016-07-08 | 2019-03-01 | 阿克佐诺贝尔国际涂料股份有限公司 | Composition of insulating mold coating applies the method for this coating composition and the component suit comprising this coating composition |
| CN110218491A (en) * | 2019-05-17 | 2019-09-10 | 重庆多仑建材有限公司 | A kind of water nano hollow glass microbead insulating mold coating and preparation method thereof |
| CN111548695A (en) * | 2020-05-30 | 2020-08-18 | 湖北美利佳涂料有限公司 | Exterior wall latex paint |
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Cited By (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101967339B (en) * | 2010-09-30 | 2012-08-29 | 苏州新海宜通信科技股份有限公司 | Anti-solar radiation spraying coating used for surface of outdoor communication equipment |
| CN101967339A (en) * | 2010-09-30 | 2011-02-09 | 苏州新海宜通信科技股份有限公司 | Anti-solar radiation spraying coating used for surface of outdoor communication equipment |
| CN102249708A (en) * | 2011-05-16 | 2011-11-23 | 西南科技大学 | Preparation method for anti-corrosion and flameproof integrated coating for thick-type steel structure |
| CN102249708B (en) * | 2011-05-16 | 2013-05-15 | 西南科技大学 | Preparation method for anti-corrosion and flameproof integrated coating for thick-type steel structure |
| CN102329545A (en) * | 2011-10-17 | 2012-01-25 | 青岛爱尔家佳新材料有限公司 | Waterborne external thermal insulation coating and preparation method thereof |
| CN102690559A (en) * | 2012-05-24 | 2012-09-26 | 北京国泰瑞华精藻硅特种材料有限公司 | Aqueous heat-insulating anticorrosive paint |
| CN103173079A (en) * | 2013-02-26 | 2013-06-26 | 安徽真信涂料有限公司 | Exterior wall coating material of high-stability paint film and preparation method of exterior wall coating material |
| CN104073113B (en) * | 2013-03-29 | 2017-01-11 | 关西涂料株式会社 | Heat insulation delustering paint composition and heat insulation delustering coating forming method |
| CN104073113A (en) * | 2013-03-29 | 2014-10-01 | 关西涂料株式会社 | Heat insulation delustering paint composition and heat insulation delustering coating forming method |
| CN105062167A (en) * | 2015-08-06 | 2015-11-18 | 天长市巨龙车船涂料有限公司 | Thermal-insulation scrub-resistant emulsion paint containing plant component and preparation method thereof |
| CN105062265A (en) * | 2015-08-06 | 2015-11-18 | 天长市巨龙车船涂料有限公司 | High-quality health-care emulsion paint added with specially-produced plant pulp and preparation method thereof |
| CN109415580A (en) * | 2016-07-08 | 2019-03-01 | 阿克佐诺贝尔国际涂料股份有限公司 | Composition of insulating mold coating applies the method for this coating composition and the component suit comprising this coating composition |
| CN106010017A (en) * | 2016-08-01 | 2016-10-12 | 安庆瑞泰化工有限公司 | Thermal insulation water-based coating and preparation method thereof |
| CN106752631A (en) * | 2016-12-19 | 2017-05-31 | 英德科迪颜料技术有限公司 | A kind of aqueous self-clean type Graphene modified nano heat-insulating reflective coating |
| CN110218491A (en) * | 2019-05-17 | 2019-09-10 | 重庆多仑建材有限公司 | A kind of water nano hollow glass microbead insulating mold coating and preparation method thereof |
| CN111548695A (en) * | 2020-05-30 | 2020-08-18 | 湖北美利佳涂料有限公司 | Exterior wall latex paint |
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Open date: 20100915 |