CN112028352A - Preparation method of negative oxygen ion small-particle-size cluster water - Google Patents
Preparation method of negative oxygen ion small-particle-size cluster water Download PDFInfo
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 168
- 229910052760 oxygen Inorganic materials 0.000 title claims abstract description 27
- 239000001301 oxygen Substances 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 235000020682 bottled natural mineral water Nutrition 0.000 claims abstract description 48
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 46
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 46
- 241001330002 Bambuseae Species 0.000 claims abstract description 46
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 46
- 239000011425 bamboo Substances 0.000 claims abstract description 46
- 239000000919 ceramic Substances 0.000 claims abstract description 36
- 239000000419 plant extract Substances 0.000 claims abstract description 28
- -1 oxygen ion Chemical class 0.000 claims abstract description 26
- 238000001914 filtration Methods 0.000 claims abstract description 25
- 239000000463 material Substances 0.000 claims abstract description 23
- 238000000034 method Methods 0.000 claims abstract description 19
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000003610 charcoal Substances 0.000 claims abstract description 16
- 239000002689 soil Substances 0.000 claims abstract description 14
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 11
- 239000011707 mineral Substances 0.000 claims abstract description 11
- 239000011032 tourmaline Substances 0.000 claims abstract description 11
- 229910052613 tourmaline Inorganic materials 0.000 claims abstract description 11
- 229940070527 tourmaline Drugs 0.000 claims abstract description 11
- 238000007789 sealing Methods 0.000 claims abstract description 10
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910052749 magnesium Inorganic materials 0.000 claims abstract description 9
- 239000011777 magnesium Substances 0.000 claims abstract description 9
- 239000000203 mixture Substances 0.000 claims abstract description 8
- 239000000284 extract Substances 0.000 claims description 35
- 238000011282 treatment Methods 0.000 claims description 25
- 239000000843 powder Substances 0.000 claims description 24
- 235000005206 Hibiscus Nutrition 0.000 claims description 18
- 235000007185 Hibiscus lunariifolius Nutrition 0.000 claims description 18
- 244000284380 Hibiscus rosa sinensis Species 0.000 claims description 18
- 235000007164 Oryza sativa Nutrition 0.000 claims description 16
- 239000002245 particle Substances 0.000 claims description 16
- 235000009566 rice Nutrition 0.000 claims description 16
- 238000002156 mixing Methods 0.000 claims description 15
- 235000008282 Sanguisorba officinalis Nutrition 0.000 claims description 11
- 150000001450 anions Chemical class 0.000 claims description 11
- 235000008291 Poterium sanguisorba Nutrition 0.000 claims description 9
- 239000010977 jade Substances 0.000 claims description 8
- 238000009210 therapy by ultrasound Methods 0.000 claims description 6
- 244000048199 Hibiscus mutabilis Species 0.000 claims description 5
- 235000003973 Hibiscus mutabilis Nutrition 0.000 claims description 5
- 239000010017 yuan zhi Substances 0.000 claims description 3
- 244000058281 Ulmus pumila Species 0.000 claims description 2
- 235000001547 Ulmus pumila Nutrition 0.000 claims description 2
- 240000007594 Oryza sativa Species 0.000 claims 2
- 240000004064 Poterium sanguisorba Species 0.000 claims 1
- 230000007613 environmental effect Effects 0.000 claims 1
- 150000002500 ions Chemical class 0.000 abstract description 21
- 230000000052 comparative effect Effects 0.000 description 15
- 241000758794 Asarum Species 0.000 description 14
- 241000209094 Oryza Species 0.000 description 14
- 229910000838 Al alloy Inorganic materials 0.000 description 12
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 12
- 229930006000 Sucrose Natural products 0.000 description 12
- 229960004793 sucrose Drugs 0.000 description 12
- 244000173853 Sanguisorba officinalis Species 0.000 description 10
- 244000025254 Cannabis sativa Species 0.000 description 8
- 241001080798 Polygala tenuifolia Species 0.000 description 8
- 230000003203 everyday effect Effects 0.000 description 7
- 239000005720 sucrose Substances 0.000 description 7
- 230000000844 anti-bacterial effect Effects 0.000 description 6
- 238000004659 sterilization and disinfection Methods 0.000 description 6
- 239000010404 Scutellaria baicalensis extract Substances 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 235000012907 honey Nutrition 0.000 description 5
- 230000001954 sterilising effect Effects 0.000 description 5
- 241000196324 Embryophyta Species 0.000 description 4
- RQMIWLMVTCKXAQ-UHFFFAOYSA-N [AlH3].[C] Chemical compound [AlH3].[C] RQMIWLMVTCKXAQ-UHFFFAOYSA-N 0.000 description 4
- 238000001514 detection method Methods 0.000 description 4
- 238000001035 drying Methods 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 4
- 241000605447 Anemarrhena Species 0.000 description 3
- 241000208966 Polygala Species 0.000 description 3
- 240000004534 Scutellaria baicalensis Species 0.000 description 3
- 235000017089 Scutellaria baicalensis Nutrition 0.000 description 3
- 229930191283 anemarrhena Natural products 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 230000000087 stabilizing effect Effects 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 241000894006 Bacteria Species 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 241000207929 Scutellaria Species 0.000 description 2
- 241001106462 Ulmus Species 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 229910001385 heavy metal Inorganic materials 0.000 description 2
- 230000010355 oscillation Effects 0.000 description 2
- 238000000527 sonication Methods 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000002023 wood Substances 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 238000005481 NMR spectroscopy Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000003385 bacteriostatic effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 235000020188 drinking water Nutrition 0.000 description 1
- 239000003651 drinking water Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 230000003116 impacting effect Effects 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F9/00—Multistage treatment of water, waste water or sewage
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/001—Processes for the treatment of water whereby the filtration technique is of importance
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/283—Treatment of water, waste water, or sewage by sorption using coal, charred products, or inorganic mixtures containing them
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/34—Treatment of water, waste water, or sewage with mechanical oscillations
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/34—Treatment of water, waste water, or sewage with mechanical oscillations
- C02F1/36—Treatment of water, waste water, or sewage with mechanical oscillations ultrasonic vibrations
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/68—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
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- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to the technical field of water preparation, in particular to a preparation method of negative oxygen ion small-particle-size cluster water. The method comprises the following steps: vibrating natural mineral water in a fall mode, and standing in a bamboo charcoal soil ceramic jar; sequentially filtering the mixture by activated carbon, mineral magnesium material and tourmaline filter material; treating for 25-35 days by sound waves with the frequency of 200-800 Hz and the corresponding sound intensity of 60-70 dB, adding the plant extract, sealing and standing for 1 year; the small-particle-size water obtained by the invention has the diameter less than 0.5 nanometer, has negative ions, can keep the stability of the small-particle-size water for a long time, is sterile and has a long quality guarantee period.
Description
Technical Field
The invention relates to the technical field of water preparation, in particular to a preparation method of negative oxygen ion small-particle-size cluster water.
Background
The water molecules in the water exist in the form of molecular chain groups, the water molecules are associated together by hydrogen bonds, and the small molecular group water is different from the large molecular group water and is formed by associating 5-6 water molecules. The detection means of the size of the molecular group of water is nuclear magnetic resonance. The detection value is that the water is small molecular group water within 100 Hz, and the water is large molecular group water above 100 Hz. The small molecular group water with the diameter less than 0.5 nanometer can directly pass through the hydrophilic channel of the cell and can be directly absorbed by the cell. The large molecular group water is absorbed through the intestinal wall membrane.
At present, all the generated anion water in the market is formed by converting charges through electronic instruments, and is partially formed by diluting oxygen anion powder or adding anion additives. Although containing negative oxygen ions, the water molecules are not easy to be absorbed by human bodies; there may be side effects such as dependence of other substances on human body.
Patent No. CN201910912381.3 discloses a method for preparing small molecular group water, which prepares large molecular clusters in water into small molecular clusters by means of ultrasonic high-frequency oscillation, but the prepared water does not contain negative ions, and the stability of natural mineral water is impaired by means of sterilization by means of boiling and ultrasonic wave.
Disclosure of Invention
Technical problem to be solved
In view of the above disadvantages and shortcomings of the prior art, the present invention provides a method for preparing negative oxygen ion small-particle-size water, which is easy to be absorbed by human body, from natural mineral water by physical methods such as filtration and sound wave.
(II) technical scheme
In order to achieve the purpose, the invention adopts the main technical scheme that:
the embodiment of the invention provides a preparation method of negative oxygen ion small-particle-size cluster water, which comprises the following steps of:
s1, vibrating natural mineral water by a fall of more than 10 meters, and standing in a bamboo charcoal soil ceramic jar for 2-5 days;
s2 filtering: sequentially filtering natural mineral water through activated carbon, mineral magnesium material and tourmaline filter material;
s3 acoustic wave treatment: placing the filtered natural mineral water in a completely sound-proof ceramic container, and treating for 25-35 days by using sound waves with the frequency of 200-800 Hz and the corresponding sound intensity of 60-70 dB;
s4 plant extract treatment: adding plant extract which accounts for 2 to 15 percent of the weight of the natural mineral water after ultrasonic treatment into the natural mineral water, and sealing and standing the mixture for 1 year; the plant extract comprises one or more of herba asari extract, rhizoma anemarrhenae extract, Scutellariae radix extract, and cortex et radix Polygalae extract.
Optionally, it includes step S5, natural mineral water is treated in an atomizer or a negative ion oscillator.
Optionally, the natural mineral water is obtained from mountain stream over 10 m above sea level and at an ambient temperature of 16-24 ℃.
Optionally, the following step in step S1: introducing natural mineral water from water source with altitude of more than 10 m into bamboo charcoal ceramic jar in sea level line through bamboo chips.
Optionally, the length of the bamboo chips is 400-500 m, and the bamboo chips are formed by connecting 25-30 sections of small bamboo chips.
Alternatively, the method for preparing negative oxygen ion small-sized cluster water as claimed in claim 1, wherein the natural mineral water after ultrasonic treatment is further processed by the following steps before being added to the plant extract in step S4: adding Hibiscus Mutabilis Jade powder, Ulmus pumila and new rice into natural mineral water treated by ultrasonic treatment, and mixing to obtain water-like product.
Optionally, the ratio of the natural mineral water to the hibiscus jade powder to the garden burnet herb to the new rice is 5-8: 1 by weight.
(III) advantageous effects
The invention has the beneficial effects that:
according to the preparation method of the negative oxygen ion small-particle-size cluster water, due to the adoption of fall shock, filtration, sound wave physics, a bamboo charcoal ceramic container and the manner of adding the plant extracting solution for treatment, compared with the prior art, the obtained small-particle-size cluster water has the diameter of less than 0.5 nanometer, has negative ions, can keep the stability of the small-particle-size cluster water for a long time, is sterile and has a long quality guarantee period.
The main reason for adopting fall oscillation is that the natural mineral water is made into small-particle-size water in a gravity impact mode at the vibration frequency of the feed water, so that the structure of the small-particle-size water is easily stabilized by the plant extracting solution;
the test shows that: the asarum extract, the rhizoma anemarrhenae extract, the scutellaria baicalensis extract or/and the polygala tenuifolia extract can form a stable chain with small-particle-size cluster water, and the plant extract is quickly separated from other small-particle-size cluster water, so that the stability of the small-particle-size cluster water is improved, the fine feeling of the obtained negative oxygen ion small-particle-size cluster water is increased, and the quality guarantee period of the small-particle-size cluster water can be prolonged;
wherein, the stability of the small-particle-size cluster water is further improved by adopting a bamboo charcoal soil ceramic cylinder;
wherein, degerming is carried out in a plurality of filtering non-thermal modes, and the filtered bacteria are sequentially treated by sound waves and plant extract, so that the sterilization is further carried out on the premise of improving the water quality.
Detailed Description
For a better understanding of the present invention, reference will now be made in detail to the present invention by way of specific embodiments thereof.
According to the preparation method of the negative oxygen ion small-particle-size water, disclosed by the embodiment of the invention, natural mineral water is subjected to micromolecule reduction through the following steps which are sequentially carried out, and has negative ions, the stability of the small-particle-size water can be kept for a long time through the negative ions with the diameter less than 0.5 nanometer, and the small-particle-size water is sterile and has a long quality guarantee period.
S1, vibrating natural mineral water by a fall of more than 10 meters, and standing in a bamboo charcoal soil ceramic jar for 2-5 days;
s2 filtering: sequentially filtering natural mineral water through activated carbon, mineral magnesium material and tourmaline filter material;
s3 acoustic wave treatment: placing the filtered natural mineral water in a completely sound-proof ceramic container, and treating for 25-35 days by using sound waves with the frequency of 200-800 Hz and the corresponding sound intensity of 60-70 dB;
s4 plant extract treatment: adding plant extract which accounts for 2 to 15 percent of the weight of the natural mineral water after ultrasonic treatment into the natural mineral water, and sealing and standing the mixture for 1 year; the plant extract comprises one or more of herba asari extract, rhizoma anemarrhenae extract, Scutellariae radix extract, and cortex et radix Polygalae extract.
The key points of the invention are as follows: vibrating by a fall of more than 10 meters, processing by bamboo charcoal soil ceramic cylinder, filtering for sterilization and sound wave, and more importantly adding plant extract.
In this embodiment, the method further includes step S5, wherein the natural mineral water is treated in an atomizer or a negative ion oscillator. During the use process, more uniform negative ion small particle cluster water can be generated. Can be easily absorbed by human body, and has effects of resisting oxidation, resisting aging, and eliminating free radicals.
1. Water source
The natural mineral water is required to vibrate in a fall of more than 10 meters, and only when the natural mineral water vibrates in a fall of more than 10 meters, the natural mineral water can be dispersed into small molecular groups under the action of gravity impact, and the structures among the small molecular groups are rearranged in the falling process;
optionally, the natural mineral water is mountain stream over 10 m above sea level and at an ambient temperature of 16-24 ℃, and the natural mineral water obtained in the environment is mountain stream rich in minerals such as calcium, manganese, iron and the like. In the later water-nourishing process, the ceramic jar made of mineral water and bamboo charcoal soil can generate good water quality stabilizing effect.
Furthermore, a sectional fall mode can be adopted, namely, the vibration frequency is increased to prepare water molecules with smaller particle size; on the other hand, it simulates the process of natural mineral water flowing down a mountain and impacting under natural environment.
Specifically, natural mineral water is introduced into the bamboo charcoal soil ceramic jar of the sea level line from a water source with an altitude of more than 10 m through bamboo chips. The purpose of standing for 2-4 days is to stabilize the structure between water molecular groups.
Furthermore, the length of the bamboo chips is 400-500 m, and the bamboo chips are formed by connecting 25-30 sections of small bamboo chips.
The purpose of adopting multiple bamboo chips is to increase the vibration frequency, and each bamboo chip is 1.5-2 m. The vertical fall of each section of drainage bamboo chip is 15-18 cm, so that the natural mineral water has 25-30 times of fall vibration in the falling process; furthermore, the bamboo chips are arranged in the shade. The bamboo chips are selected instead of other materials to maintain the connection structure between water molecules, and the bamboo chips are selected instead of bamboo tubes or bamboo pipes to ensure that water can fully absorb anions of mountain plants and bacteria are not easy to generate.
The bamboo charcoal soil ceramic cylinder is used for stably collecting natural mineral water, stabilizing the structure and negative ions of small molecular groups, and further stabilizing the structure of the small molecular group water by having antibacterial and bactericidal effects after filtration and sterilization.
2. Filtration sterilization
Experiments show that the clean direct drinking water can be obtained by multilayer filtration of activated carbon, mineral magnesium material and tourmaline filter material;
specifically, get 50L's active carbon, 30L's mineral magnesium material and 5L's tuo lin filter material and arrange in proper order in the aluminum alloy container of the mutual intercommunication of corresponding size, and be equipped with the water inlet in active carbon aluminum alloy container department, adorn the filter sponge in water inlet department, be equipped with the delivery port in tuo lin aluminum alloy container department of filter material, the delivery port passes through the pipeline and extends to in the ceramic container.
3. Sonication
The filtered water is respectively placed in the ceramic containers with the sound-absorbing cotton at the water inlets. And (3) treating for 25-35 days by using sound waves with the frequency of 200-800 Hz and the corresponding sound intensity of 60-70 dB. Wherein, the continuous and uniform sound wave treatment is still critical to the treatment of the natural mineral water, and the sound wave treatment process cannot be interrupted, and if the interruption is needed, the treatment is restarted. Experiments show that the frequency of the sound waves can adjust the structure between water molecules into small molecular groups at a slow speed, so that the particle size of the small molecular groups is smaller and smaller, and the water quality is softer and softer. Specifically, in 100L of water, the water is placed for 30 days, and the Chinese zither music played in the ceramic container continuously and circularly by using the 'high mountain and running water' every day so as to emit sound waves with corresponding frequency and sound intensity, and tests show that: the sound wave generated by the 'mountain and river water' koto is adopted, and compared with the small molecular group water obtained without sound wave treatment, the small molecular group water has smaller diameter and softer taste. The sonicated water was designated as sonicated water.
4. Bacteriostatic treatment
Marking natural mineral water which is treated by ultrasonic waves as sound wave water, adding the hibiscus powder, the elm grass and the new rice into the sound wave water, mixing the hibiscus powder, the elm grass and the new rice in a high-speed stirrer until the hibiscus powder is in a water quality state, improving the bacteriostasis of the small-particle-size water, and enabling the prepared negative oxygen ion small-particle-size water to have a shelf life of more than two years under the synergistic action of negative ion water.
Furthermore, the ratio of the natural mineral water to the hibiscus jade powder to the garden burnet herb to the new rice is 5-8: 1 by weight. Wherein the powder of Hibiscus Mutabilis Jade is 1250 mesh.
5. Plant extract
Wherein, the plant extract aims to form a stable chain with the small molecular group water, and is quickly separated from other small molecular group water by the components of the plant extract. Experiments show that not all plant extracts have the above effects, and the plant extracts include, but are not limited to, asarum extract, rhizoma anemarrhenae extract, scutellaria extract or/and polygala extract.
The preparation method of the asarum extracting solution comprises the following steps: taking 5 cm of raw asarum root and root system part, cleaning and drying in the sun. Cut into 1-2 cm with scissors. Taking 10 kg of the trimmed asarum, adding 35 kg of sonic water and 5kg of honey, placing the mixture in a ceramic jar with the volume of 100 kg, mixing the mixture for 30 minutes by a stirrer every day, and tightly covering the jar. Sealing after 15 days, fermenting for 1 year in a shady and shady place, and filtering.
The preparation method of the rhizoma anemarrhenae extracting solution comprises the following steps: cleaning raw rhizoma anemarrhenae root, and cutting into large and small pieces with a slicer. Taking 10 kg of sliced rhizoma anemarrhenae, adding 37 kg of sonic water and 3kg of honey, placing the rhizoma anemarrhenae in a ceramic jar with the volume of 100 kg, mixing the rhizoma anemarrhenae and the honey by a stirrer for 30 minutes every day, and tightly covering the ceramic jar. Sealing after 15 days, fermenting for 1 year in a shady and shady place, and filtering.
The preparation method of the scutellaria baicalensis extracting solution comprises the following steps: cleaning root of radix Scutellariae, and sun drying. The sheet was cut into pieces of various sizes with a slicer. Taking 10 kg of sliced scutellaria baicalensis, adding 35 kg of sonic water and 5kg of honey, placing the mixture in a ceramic jar with the volume of 100 kg, mixing the mixture for 30 minutes by a stirrer every day, and tightly covering the ceramic jar. Sealing after 15 days, fermenting for 1 year in a shady and shady place, and filtering.
The preparation method of the polygala tenuifolia extract comprises the following steps: removing residual stem, fibrous root and soil from picked cortex et radix Polygalae, slightly drying in the sun, selecting thick part, horizontally placing on plate, back and forth rubbing until skin and flesh are separated from wood core, removing wood core, slicing, and drying in the sun. Taking 15kg of sliced polygala tenuifolia, adding 28 kg of sonic water and 7 kg of honey, placing the polygala tenuifolia and the sonic water in a ceramic jar with the volume of 100 kg, mixing the polygala tenuifolia and the sonic water in a stirrer for 30 minutes every day, and tightly covering the polygala tenuifolia. Sealing after 15 days, fermenting for 1 year in a shady and shady place, and filtering.
The plant extract is extracted by a plant extractor to obtain an extracting solution, and then the extracting solution is placed in a ceramic container to be stirred and processed for 3 days, specifically: stirring with a common electric stirrer for 5 min every day, and stirring again at an interval of 10 min for 5 times. The proportion of the plant extract and the natural mineral water is very important, and the excessive plant extract can cause the small molecular group water to be condensed again to become the large molecular group water.
Specifically, the natural mineral water sonicated by the plant extract and the step S3 is recorded as: sonic water; respectively mixing the sound wave water with the asarum extract, the rhizoma anemarrhenae extract, the scutellaria baicalensis extract or/and the polygala tenuifolia extract to prepare negative oxygen ion small-particle-size cluster water according to the following weight ratio:
example 1
15kg of asarum extracting solution, 1.5kg of cane sugar and 34.5kg of sonic water.
In this example, the sonic water was mixed with the asarum herb extract and sucrose after the following treatment.
Firstly, mixing the sonic water, the hibiscus jalapa powder, the garden burnet grass and the new rice in a high-speed stirrer according to the weight ratio of 5-8: 1 until the hibiscus jalapa powder is in a water quality state.
Example 2
11kg of rhizoma anemarrhenae extracting solution, 2kg of cane sugar and 31kg of sonic water.
In this example, the sound wave water was mixed with the rhizoma anemarrhenae extract and sucrose after the following treatment.
Firstly, mixing the sonic water, the hibiscus jalapa powder, the garden burnet grass and the new rice in a high-speed stirrer according to the weight ratio of 5-8: 1 until the hibiscus jalapa powder is in a water quality state.
Example 3
16kg of scutellaria baicalensis extracting solution, 2kg of cane sugar and 32kg of sonic water.
Example 4
13kg of polygala root extracting solution, 1kg of cane sugar and 36kg of sonic water.
Example 5
Taking 4kg of asarum extract, 3kg of rhizoma anemarrhenae extract, 4kg of scutellaria baicalensis extract, 3kg of polygala tenuifolia extract, 2kg of sucrose and 36kg of sonic water.
In this embodiment, the sonic water is first mixed with the asarum herb extract, the anemarrhena rhizome extract, the scutellaria root extract, the polygala root extract and the sucrose.
Firstly, mixing the sonic water, the hibiscus jalapa powder, the garden burnet grass and the new rice in a high-speed stirrer according to the weight ratio of 5-8: 1 until the hibiscus jalapa powder is in a water quality state.
Example 6
Taking 5kg of asarum extract, 4kg of rhizoma anemarrhenae extract, 4kg of scutellaria baicalensis extract, 2kg of sucrose and 30kg of sonic water.
In this example, the sonic water is first mixed with the asarum herb extract, the anemarrhena rhizome extract, the scutellaria baicalensis extract and the sucrose after the following treatments.
Firstly, mixing the sonic water, the hibiscus jalapa powder, the garden burnet grass and the new rice in a high-speed stirrer according to the weight ratio of 5-8: 1 until the hibiscus jalapa powder is in a water quality state.
Example 7
Taking 6kg of asarum extracting solution, 8kg of rhizoma anemarrhenae extracting solution, 1.5kg of cane sugar and 34.5kg of sonic water.
In this example, the sonic water was mixed with the asarum herb extract, the anemarrhena rhizome extract, and sucrose after the following treatments.
Firstly, mixing the sonic water, the hibiscus jalapa powder, the garden burnet grass and the new rice in a high-speed stirrer according to the weight ratio of 5-8: 1 until the hibiscus jalapa powder is in a water quality state.
Specific examples of the preparation of the negative oxygen ion small-particle cluster water are as follows:
example 8
Preparing negative oxygen ion small-particle-size cluster water:
introducing 450-meter-long bamboo chips consisting of 30 segments of small bamboo chips from a mountain stream water source with the altitude of 200 meters and the ambient temperature of 20 ℃ into a bamboo charcoal soil ceramic cylinder with the altitude of 100 meters, sealing and standing for 3 days, and filtering by a filtering device; 100L of the filtered water is placed in a 120L ceramic container which is completely soundproof, sonic water is obtained after the koto music of 'mountain and river water' is continuously and circularly played in the ceramic container for 30 days every day, negative ion small-particle-size cluster water is obtained after blending according to the mode of the embodiment 5, and when the water is used, the water is placed in an atomizer or a negative ion oscillator to be treated and sprayed with water.
Wherein, the preparation of the filtering device is as follows: 50L of activated carbon, 30L of mineral magnesium material and 5L of tourmaline filter material are sequentially placed in aluminum alloy containers which are communicated with each other and have corresponding sizes, a water inlet is arranged at the position of the activated carbon aluminum alloy container, a filter sponge is arranged at the position of the water inlet, a water outlet is arranged at the position of the aluminum alloy container of the tourmaline filter material, and the water outlet extends into the ceramic container through a pipeline.
Example 9
Preparing negative oxygen ion small-particle-size cluster water:
leading a 500-meter-long bamboo chip consisting of 25 segments of small bamboo chips from a mountain stream water source with the altitude of 10 meters and the ambient temperature of 24 ℃ to a bamboo charcoal soil ceramic cylinder on the horizon, standing the bamboo chip in a closed manner for 2 to 5 days, filtering the bamboo chip by a filter, placing 100L of the filtered water in a 120L ceramic container which is completely sound-proof, treating the water for 25 days by using sound waves with the frequency of 200Hz and the corresponding sound intensity of 70 dB to obtain sound wave water, preparing the sound wave water according to the method of the embodiment 6 to obtain negative ion small-particle-size cluster water, and placing the water in an atomizer or a negative ion oscillator to treat and spray water when in use.
Wherein, the preparation of the filtering device is as follows: 50L of activated carbon, 30L of mineral magnesium material and 5L of tourmaline filter material are sequentially placed in aluminum alloy containers which are communicated with each other and have corresponding sizes, a water inlet is arranged at the position of the activated carbon aluminum alloy container, a filter sponge is arranged at the position of the water inlet, a water outlet is arranged at the position of the aluminum alloy container of the tourmaline filter material, and the water outlet extends into the ceramic container through a pipeline.
Example 10
Preparing negative oxygen ion small-particle-size cluster water:
leading a 400-meter-long bamboo chip consisting of 30 segments of small bamboo chips from a mountain stream water source with an altitude of 50 meters and an ambient temperature of 16 ℃ to a bamboo charcoal soil ceramic cylinder on the horizon, sealing and standing for 5 days, filtering by a filter, placing 100L of the filtered water in a 120L ceramic container completely insulated from sound, treating for 25 days by using a sound wave with a frequency of 200Hz and a corresponding sound intensity of 70 dB to obtain sound wave water, blending according to the method of the embodiment 7 to obtain negative ion small-particle-size cluster water, and placing the negative ion small-particle-size cluster water in an atomizer or a negative ion oscillator to treat and spray water when in use.
Wherein, the preparation of the filtering device is as follows: 50L of activated carbon, 30L of mineral magnesium material and 5L of tourmaline filter material are sequentially placed in aluminum alloy containers which are communicated with each other and have corresponding sizes, a water inlet is arranged at the position of the activated carbon aluminum alloy container, a filter sponge is arranged at the position of the water inlet, a water outlet is arranged at the position of the aluminum alloy container of the tourmaline filter material, and the water outlet extends into the ceramic container through a pipeline.
The test shows that: the horizontal average particle size of the negative ion small particle size clusters obtained in example 8 was the smallest.
Comparative example 1
The other example was conducted in the same manner as example 8 except that the sonication was not conducted.
Comparative example 2
The other example was conducted in the same manner as example 8 except that the treatment with the plant extract was not conducted.
Comparative example 3
The other example was conducted in the same manner as example 8 except that no treatment with Hibiscus mutabilis powder, Sanguisorbae officinalis and fresh rice was conducted.
Comparative example 4
The other example is the same as example 8, except that the water source was directly loaded through the bamboo charcoal soil ceramic jar without being guided to the horizon through the small bamboo chips, and the ultrasonic vibration treatment was performed for 20 min.
1. Through the detection of harmful substances, the contents of the heavy metals in the negative oxygen ion small-particle-size cluster water obtained in the examples 8 to 10 are shown in the following table 1:
TABLE 1
As can be seen from the data in Table 1, the harmful heavy metal contents of the small-particle size anion cluster water obtained in examples 8-10 are far less than the standard values. Is still suitable for people with susceptible constitution.
2. The negative oxygen ion small-particle-size cluster water obtained in example 8 and comparative example 3 was subjected to the detection method in disinfection technical Specification to obtain the following analysis results in Table 2:
TABLE 2
As can be seen from the data in table 2, example 8 has a better antibacterial effect than comparative example 3. The antibacterial rate of the example 8 is more than 99%. The antibacterial rate of the anion small-particle-size cluster water can be improved by treating the hibiscus jade powder, the garden burnet grass and the new rice.
3. The negative ion release amounts of the small-particle size anion cluster waters obtained in examples 8 to 10 were measured and shown in Table 3, respectively:
TABLE 3
| Sample (I) | Negative ion release amount (per cm)3) |
| Example 8 | 6.02×103 |
| Example 9 | 5.02×103 |
| Example 10 | 5.59×103 |
| Comparative example 1 | 2.19×103 |
| Comparative example 2 | 3.64×103 |
| Comparative example 3 | 5.36×103 |
From the data in table 3: the anion small cluster water of the embodiments 8 to 10 of the present invention can obtain high content of anions. Sonic waves, plant extracts, and treatments of hibiscus jade powder, sanguisorba officinalis and new rice all have varying degrees of influence on the production of negative ions.
4. The sizes of the negative oxygen ion small particle diameter cluster water obtained in inventive examples 8 to 10 and comparative examples 1 to 3 are shown in Table 4:
TABLE 4
| Sample (I) | Size of negative oxygen ion small particle size cluster (Hertz HZ) |
| Example 8 | 45.21 |
| Example 9 | 50.49 |
| Example 10 | 61.57 |
| Comparative example 1 | 96.78 |
| Comparative example 2 | 122.12 |
| Comparative example 3 | 76.31 |
| Comparative example 4 | 92.36 |
As can be seen from the data in Table 4, the small cluster water obtained in examples 8, 9 and 10 has a small particle size, and can maintain the particle size equivalent to that of natural mineral water, resulting in a softer mouthfeel.
The sound wave treatment, the plant extract treatment and the vibration treatment of the small bamboo chips introduced to the horizon have obvious influence on the particle size of the small molecular group water.
And experiments show that: the shelf life of the small cluster water of comparative examples 2 and 3 was significantly less than examples 8-10. This is because the treatment of the plant extract and the powder of hibiscus mutabilis, sanguisorba officinalis and new rice has a significant effect on the antibacterial action and the maintenance of the size of the particle size of the small molecular particle size cluster water.
Finally, it should be noted that: the above embodiments are only used to illustrate the technical solution of the present invention, and not to limit the same; while the invention has been described in detail and with reference to the foregoing embodiments, it will be understood by those skilled in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some or all of the technical features may be equivalently replaced; and the modifications or the substitutions do not make the essence of the corresponding technical solutions depart from the scope of the technical solutions of the embodiments of the present invention.
Claims (7)
1. The preparation method of the negative oxygen ion small-particle-size cluster water is characterized by comprising the following steps of:
s1, vibrating natural mineral water by a fall of more than 10 meters, and standing in a bamboo charcoal soil ceramic jar for 2-5 days;
s2 filtering: sequentially filtering natural mineral water through activated carbon, mineral magnesium material and tourmaline filter material;
s3 acoustic wave treatment: placing the filtered natural mineral water in a completely sound-proof ceramic container, and treating for 25-35 days by using sound waves with the frequency of 200-800 Hz and the corresponding sound intensity of 60-70 dB;
s4 plant extract treatment: adding plant extract which accounts for 2 to 15 percent of the weight of the natural mineral water after ultrasonic treatment into the natural mineral water, and sealing and standing the mixture for 1 year; the plant extract comprises one or more of herba asari extract, rhizoma anemarrhenae extract, Scutellariae radix extract, and cortex et radix Polygalae extract.
2. The method for preparing small-sized anion oxide cluster water of claim 1, which comprises a step S5 of treating natural mineral water in an atomizer or an anion shaker.
3. The method for preparing the small-particle cluster water containing negative oxygen ions according to claim 1, wherein: the natural mineral water is obtained from mountain stream with the altitude of more than 10 meters and the environmental temperature of 16-24 ℃.
4. The method for preparing small-size cluster water of negative oxygen ions according to claim 1, wherein the step S1 comprises the steps of: introducing natural mineral water from water source with altitude of more than 10 m into bamboo charcoal ceramic jar in sea level line through bamboo chips.
5. The method for preparing small-size cluster water of negative oxygen ions according to claim 4, wherein: the length of the bamboo chips is 400-500 meters, and the bamboo chips are formed by connecting 25-30 sections of small bamboo chips.
6. The method for preparing small-sized anion oxide cluster water as claimed in claim 1, wherein the natural mineral water treated with ultrasonic wave is further treated by the following steps before being added to the plant extract in step S4: adding Hibiscus Mutabilis Jade powder, Ulmus pumila and new rice into natural mineral water treated by ultrasonic treatment, and mixing to obtain water-like product.
7. The method for preparing small-size cluster water of negative oxygen ions according to claim 6, wherein: the ratio of the natural mineral water to the hibiscus jade powder to the garden burnet herb to the new rice is 5-8: 1 by weight.
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